#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:18:59 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/79/2017977.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017977_Fobs loop_ _publ_author_name 'Smeets, Stef' 'Lutz, Martin' _publ_section_title ; Hexakis(urea-\kO)zinc(II) dinitrate at 110 and 250K: uniaxial negative thermal expansion ; _journal_coeditor_code FN3074 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m50 _journal_page_last m55 _journal_volume 67 _journal_year 2011 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.651 _cell_angle_gamma 90.000 _cell_length_a 17.0337 _cell_length_b 18.0092 _cell_length_c 7.3550 _exptl_crystal_F_000 1136.00 _reflns_d_resolution_high 0.6196 _cod_data_source_file fn3074Iasup2.hkl _cod_data_source_block Ia #BEGIN Tags that were not found in dictionaries: _shelx_title ' m072c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 289.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 28919.24 28308.89 253.56 o 4 0 0 2778.07 2739.74 22.76 o 6 0 0 11563.33 11317.47 89.79 o 8 0 0 26464.01 27147.12 195.83 o 10 0 0 3308.83 3170.24 29.42 o 12 0 0 2112.81 1929.68 19.43 o 14 0 0 611.29 579.44 10.61 o 16 0 0 1080.04 1031.27 30.27 o 18 0 0 7443.61 7121.66 235.68 o 20 0 0 274.84 296.04 22.13 o 22 0 0 79.94 82.03 22.08 o 24 0 0 581.28 663.46 37.28 o 1 1 0 2109.44 2057.27 11.36 o 3 1 0 5129.41 5716.26 26.92 o 5 1 0 381.73 356.25 3.71 o 7 1 0 3728.86 4198.17 23.99 o 9 1 0 3671.56 3627.46 24.17 o 11 1 0 923.80 928.67 10.09 o 13 1 0 133.24 122.42 4.14 o 15 1 0 284.95 284.32 5.60 o 17 1 0 664.80 695.04 14.88 o 19 1 0 76.94 91.98 10.77 o 21 1 0 785.03 799.53 26.42 o 23 1 0 3.24 -7.37 14.16 o 25 1 0 116.08 139.07 19.01 o 0 2 0 648.04 575.47 6.11 o 2 2 0 21512.46 22187.68 105.12 o 4 2 0 7441.34 7137.60 38.92 o 6 2 0 8188.62 8834.33 48.85 o 8 2 0 10086.23 10390.80 56.36 o 10 2 0 46.66 85.96 3.97 o 12 2 0 400.85 419.75 7.63 o 14 2 0 1101.53 1127.02 14.76 o 16 2 0 7654.74 7849.04 57.93 o 18 2 0 127.81 121.52 10.98 o 20 2 0 27.80 44.53 16.56 o 22 2 0 42.51 57.33 15.13 o 24 2 0 310.59 357.66 23.30 o 1 3 0 20086.24 21079.53 100.47 o 3 3 0 8185.83 8257.37 45.58 o 5 3 0 19062.86 18554.95 103.22 o 7 3 0 6430.05 6539.89 44.69 o 9 3 0 12084.07 12341.40 71.44 o 11 3 0 2658.41 2659.27 21.93 o 13 3 0 13856.77 14047.09 82.77 o 15 3 0 311.08 328.89 13.62 o 17 3 0 1297.56 1250.83 22.37 o 19 3 0 1550.94 1497.16 26.43 o 21 3 0 734.84 801.62 26.71 o 23 3 0 1807.05 1869.81 40.88 o 25 3 0 1316.98 1362.54 36.79 o 0 4 0 2139.61 1849.62 19.24 o 2 4 0 1.87 4.46 1.12 o 4 4 0 6062.19 5653.88 38.07 o 6 4 0 14377.57 15507.89 87.93 o 8 4 0 85.41 58.74 4.46 o 10 4 0 1962.03 2180.42 18.92 o 12 4 0 617.51 600.73 9.01 o 14 4 0 20.17 18.83 6.98 o 16 4 0 1013.31 1004.33 18.69 o 18 4 0 95.23 80.91 10.15 o 20 4 0 267.11 257.15 15.44 o 22 4 0 2.85 7.55 14.65 o 24 4 0 235.77 211.24 20.37 o 1 5 0 5160.83 4980.49 30.67 o 3 5 0 502.52 327.23 4.81 o 5 5 0 431.29 359.42 5.99 o 7 5 0 25906.79 26895.22 160.00 o 9 5 0 5145.25 5140.95 37.53 o 11 5 0 2697.46 2716.61 25.35 o 13 5 0 854.99 889.61 12.49 o 15 5 0 3607.10 3478.47 34.54 o 17 5 0 3029.36 2924.16 47.43 o 19 5 0 564.80 590.76 25.69 o 21 5 0 355.20 348.66 33.60 o 23 5 0 20.19 14.04 15.42 o 25 5 0 988.10 1001.61 32.25 o 0 6 0 56162.97 55860.99 442.17 o 2 6 0 432.47 572.47 5.91 o 4 6 0 1102.44 1342.52 11.89 o 6 6 0 1311.08 1686.27 15.59 o 8 6 0 19770.98 20097.53 123.17 o 10 6 0 7902.41 8052.07 55.56 o 12 6 0 2332.06 2302.67 23.51 o 14 6 0 7866.93 7708.95 53.98 o 16 6 0 4180.83 4330.25 38.27 o 18 6 0 5653.40 5632.02 65.01 o 20 6 0 1762.65 1792.42 35.12 o 22 6 0 957.31 1026.14 42.35 o 24 6 0 182.25 246.72 29.12 o 1 7 0 11808.46 12637.05 78.93 o 3 7 0 239.32 274.87 4.39 o 5 7 0 4582.99 4938.99 35.30 o 7 7 0 187.04 218.01 6.08 o 9 7 0 4585.71 5017.82 36.55 o 11 7 0 2.65 13.02 5.40 o 13 7 0 964.70 929.60 14.70 o 15 7 0 159.30 121.99 9.83 o 17 7 0 602.87 615.01 13.00 o 19 7 0 21.84 17.70 11.86 o 21 7 0 0.48 6.15 14.38 o 23 7 0 0.21 -5.61 15.17 o 25 7 0 28.62 41.28 17.99 o 0 8 0 135.67 102.06 3.88 o 2 8 0 4307.51 4000.14 27.89 o 4 8 0 409.67 522.52 7.12 o 6 8 0 2646.10 2406.36 20.98 o 8 8 0 9374.64 9386.88 54.60 o 10 8 0 1798.55 1819.14 18.52 o 12 8 0 855.89 878.71 18.20 o 14 8 0 4887.98 4896.07 53.89 o 16 8 0 9643.69 9516.53 76.29 o 18 8 0 2157.23 2206.46 30.01 o 20 8 0 2398.75 2570.40 45.51 o 22 8 0 473.47 479.80 23.06 o 24 8 0 381.79 390.22 23.65 o 1 9 0 6252.92 6246.59 45.06 o 3 9 0 2633.59 2639.70 21.88 o 5 9 0 8834.65 9083.90 58.25 o 7 9 0 2274.07 2274.08 21.90 o 9 9 0 6064.60 6316.04 44.77 o 11 9 0 1876.27 2004.21 20.07 o 13 9 0 6256.82 6003.80 52.01 o 15 9 0 220.05 210.66 8.65 o 17 9 0 13.70 30.38 7.57 o 19 9 0 179.41 159.92 13.99 o 21 9 0 1167.08 1268.40 35.97 o 23 9 0 582.20 521.26 30.07 o 0 10 0 19077.68 19950.63 167.98 o 2 10 0 691.30 490.41 7.68 o 4 10 0 4339.28 4473.65 34.10 o 6 10 0 240.13 256.69 6.95 o 8 10 0 137.50 168.49 6.34 o 10 10 0 1122.28 1034.80 13.78 o 12 10 0 481.88 397.23 11.30 o 14 10 0 37.02 35.18 8.19 o 16 10 0 102.64 87.91 8.21 o 18 10 0 568.92 532.68 14.58 o 20 10 0 176.14 163.97 14.95 o 22 10 0 14.84 9.65 15.23 o 24 10 0 97.34 162.98 25.44 o 1 11 0 13327.39 14016.55 85.25 o 3 11 0 12967.76 13485.36 86.51 o 5 11 0 4940.10 5053.67 38.40 o 7 11 0 15051.93 15602.94 95.95 o 9 11 0 6311.79 6025.41 43.19 o 11 11 0 662.36 614.21 11.47 o 13 11 0 188.70 200.72 10.35 o 15 11 0 1140.56 1214.71 22.43 o 17 11 0 35.29 32.58 11.15 o 19 11 0 184.42 198.35 15.05 o 21 11 0 499.12 488.53 29.13 o 23 11 0 49.87 38.04 17.13 o 0 12 0 21517.23 23377.59 208.04 o 2 12 0 5142.86 4939.40 35.54 o 4 12 0 1386.10 1334.86 15.12 o 6 12 0 12.43 17.14 5.14 o 8 12 0 2385.63 2298.44 23.42 o 10 12 0 1730.21 1730.32 17.46 o 12 12 0 251.28 254.06 11.71 o 14 12 0 98.15 101.95 13.82 o 16 12 0 55.70 67.77 9.25 o 18 12 0 364.62 339.91 21.57 o 20 12 0 569.81 564.09 21.87 o 22 12 0 762.14 822.91 34.97 o 1 13 0 2472.15 2548.98 20.52 o 3 13 0 271.13 287.90 7.19 o 5 13 0 4.71 6.28 3.89 o 7 13 0 2171.06 2106.21 23.95 o 9 13 0 1176.40 1217.10 19.92 o 11 13 0 1073.60 1014.95 18.92 o 13 13 0 77.21 68.67 11.17 o 15 13 0 459.48 450.48 16.00 o 17 13 0 519.02 502.91 16.86 o 19 13 0 136.97 130.74 12.72 o 21 13 0 8.81 69.47 19.47 o 23 13 0 614.17 645.68 31.94 o 0 14 0 13343.53 13639.40 174.72 o 2 14 0 6162.65 6079.18 43.52 o 4 14 0 4094.80 3785.34 32.76 o 6 14 0 16653.04 16923.86 117.91 o 8 14 0 1744.05 1824.79 24.96 o 10 14 0 263.36 233.85 9.89 o 12 14 0 1093.55 1047.95 38.35 o 14 14 0 2014.47 2073.93 30.26 o 16 14 0 1605.51 1606.89 27.67 o 18 14 0 1043.98 969.59 20.60 o 20 14 0 216.37 179.12 19.51 o 22 14 0 15.28 20.14 20.33 o 1 15 0 61.27 71.10 4.71 o 3 15 0 6738.01 6727.05 48.90 o 5 15 0 1801.12 1877.40 20.95 o 7 15 0 12.06 19.20 10.52 o 9 15 0 1046.71 1028.07 28.00 o 11 15 0 162.36 142.97 10.32 o 13 15 0 445.99 397.36 13.88 o 15 15 0 298.37 314.60 13.15 o 17 15 0 125.14 126.26 13.88 o 19 15 0 159.57 161.20 17.17 o 21 15 0 863.21 826.30 34.30 o 0 16 0 3457.82 3456.73 45.56 o 2 16 0 5052.54 4994.44 48.89 o 4 16 0 555.46 566.96 14.63 o 6 16 0 527.72 573.46 13.66 o 8 16 0 1078.43 1088.98 28.29 o 10 16 0 1153.50 1201.86 22.54 o 12 16 0 287.77 304.83 13.37 o 14 16 0 491.55 467.54 16.44 o 16 16 0 395.71 343.38 17.20 o 18 16 0 32.45 17.59 11.39 o 20 16 0 373.73 348.77 23.05 o 1 17 0 284.61 289.69 9.44 o 3 17 0 443.53 425.55 14.39 o 5 17 0 4860.20 4949.86 52.86 o 7 17 0 7209.58 7329.18 75.83 o 9 17 0 44.10 35.20 9.46 o 11 17 0 2652.30 2611.82 39.50 o 13 17 0 5362.45 5334.39 68.06 o 15 17 0 1645.24 1631.59 32.23 o 17 17 0 1819.50 1825.92 35.21 o 19 17 0 1676.91 1713.53 35.54 o 21 17 0 75.02 83.67 23.56 o 0 18 0 197.18 179.99 24.78 o 2 18 0 8.53 6.59 9.47 o 4 18 0 26.52 2.35 9.13 o 6 18 0 62.27 66.85 9.36 o 8 18 0 166.20 150.17 15.85 o 10 18 0 331.41 333.92 15.77 o 12 18 0 221.20 198.49 13.53 o 14 18 0 254.09 240.48 16.38 o 16 18 0 801.04 798.68 24.80 o 18 18 0 73.47 64.72 15.91 o 20 18 0 38.98 38.68 21.78 o 1 19 0 1759.83 1776.97 32.30 o 3 19 0 16.68 31.77 8.83 o 5 19 0 145.13 138.05 11.66 o 7 19 0 2184.66 2084.34 30.05 o 9 19 0 2861.30 2857.31 42.41 o 11 19 0 2508.67 2603.99 41.02 o 13 19 0 490.14 426.80 20.92 o 15 19 0 637.09 607.66 22.18 o 17 19 0 369.73 369.04 20.33 o 19 19 0 713.95 686.00 28.35 o 0 20 0 3455.47 3454.46 58.96 o 2 20 0 1117.26 1178.04 27.24 o 4 20 0 501.55 479.34 17.61 o 6 20 0 2210.78 2221.94 35.61 o 8 20 0 909.78 936.39 22.88 o 10 20 0 511.53 543.77 19.61 o 12 20 0 1479.34 1513.10 28.34 o 14 20 0 1458.69 1544.74 32.45 o 16 20 0 749.50 758.88 28.91 o 18 20 0 1373.77 1440.20 45.03 o 1 21 0 3.18 5.69 8.34 o 3 21 0 94.68 109.65 10.80 o 5 21 0 136.55 115.30 11.92 o 7 21 0 138.12 137.15 10.73 o 9 21 0 58.71 51.19 12.15 o 11 21 0 1295.11 1358.38 59.98 o 13 21 0 108.80 112.23 14.70 o 15 21 0 303.79 262.49 18.85 o 17 21 0 26.01 18.54 19.51 o 0 22 0 1157.58 1146.69 41.41 o 2 22 0 2103.91 2139.35 40.77 o 4 22 0 1023.15 930.35 26.73 o 6 22 0 1728.41 1676.87 29.33 o 8 22 0 302.10 289.29 17.48 o 10 22 0 94.45 107.26 14.77 o 12 22 0 766.45 824.27 23.21 o 14 22 0 1244.10 1285.95 36.52 o 16 22 0 843.61 846.50 42.48 o 1 23 0 603.73 627.43 23.63 o 3 23 0 887.40 831.32 26.47 o 5 23 0 2313.87 2321.46 38.74 o 7 23 0 1556.80 1619.03 38.07 o 9 23 0 297.12 250.45 20.81 o 11 23 0 122.22 142.16 23.17 o 13 23 0 602.27 585.91 23.60 o 15 23 0 307.75 311.53 20.52 o 0 24 0 32.59 20.42 32.96 o 2 24 0 218.85 254.74 16.37 o 4 24 0 8.32 19.80 13.75 o 6 24 0 58.25 39.69 17.15 o 8 24 0 11.24 -10.06 17.49 o 10 24 0 6.70 23.31 17.60 o 12 24 0 60.54 45.40 16.39 o 14 24 0 927.05 942.60 33.37 o 1 25 0 2118.30 2091.63 38.62 o 3 25 0 2087.30 2185.24 39.20 o 5 25 0 457.19 464.79 32.89 o 7 25 0 2219.46 2290.38 41.73 o 9 25 0 1910.16 2104.71 45.74 o 11 25 0 346.34 337.58 24.46 o 13 25 0 22.88 26.94 21.62 o 0 26 0 1311.54 1407.03 42.69 o 2 26 0 638.42 600.40 20.86 o 4 26 0 932.92 895.52 25.85 o 6 26 0 890.55 881.48 27.21 o 8 26 0 105.57 111.18 19.85 o 10 26 0 5.69 -3.29 20.39 o 1 27 0 464.93 473.08 21.10 o 3 27 0 60.61 62.40 14.94 o 5 27 0 426.70 488.95 23.33 o 7 27 0 561.09 554.32 28.44 o 9 27 0 168.90 159.42 21.84 o 0 28 0 327.64 327.07 27.60 o 2 28 0 1003.19 1014.22 26.89 o 4 28 0 310.14 321.65 22.63 o 6 28 0 330.07 298.98 24.61 o 1 29 0 8.44 -15.75 15.75 o -25 1 1 1219.38 1308.68 34.68 o -23 1 1 310.31 337.62 19.98 o -21 1 1 139.05 137.34 14.12 o -19 1 1 340.70 332.25 13.49 o -17 1 1 3722.54 3506.02 28.51 o -15 1 1 2535.25 2537.95 18.06 o -13 1 1 3903.42 3933.84 24.95 o -11 1 1 5641.69 5561.33 32.42 o -9 1 1 20882.19 21714.99 126.12 o -7 1 1 45753.09 47967.17 243.37 o -5 1 1 37014.59 38302.14 164.97 o -3 1 1 25010.12 24883.62 96.91 o -1 1 1 19856.93 20352.16 78.26 o 1 1 1 26217.17 26909.90 113.77 o 3 1 1 3051.20 3249.71 20.45 o 5 1 1 705.50 885.65 8.02 o 7 1 1 861.61 641.93 8.83 o 9 1 1 2160.14 2062.78 15.21 o 11 1 1 807.90 775.06 9.04 o 13 1 1 2124.70 2111.66 20.57 o 15 1 1 3816.36 3876.60 37.00 o 17 1 1 1898.95 1848.43 37.40 o 19 1 1 609.75 563.73 17.97 o 21 1 1 1340.41 1367.93 35.46 o 23 1 1 984.91 972.45 31.58 o 25 1 1 927.23 1022.49 34.40 o -26 2 1 1324.30 1323.26 57.62 o -24 2 1 483.30 535.13 22.73 o -22 2 1 198.90 188.50 16.31 o -20 2 1 246.21 289.75 15.93 o -18 2 1 63.10 74.25 7.15 o -16 2 1 874.42 910.11 17.05 o -14 2 1 10129.02 10476.85 61.99 o -12 2 1 2394.36 2290.54 16.60 o -10 2 1 1396.36 1553.12 11.88 o -8 2 1 27856.28 29010.62 141.30 o -6 2 1 3067.93 3051.03 17.06 o -4 2 1 10658.58 10756.57 44.48 o -2 2 1 8590.70 9191.38 38.25 o 0 2 1 9138.53 9471.52 42.56 o 2 2 1 6701.04 6449.03 35.35 o 4 2 1 48844.80 48420.41 249.62 o 6 2 1 2019.39 2072.24 16.30 o 8 2 1 2342.68 2072.65 18.66 o 10 2 1 8751.07 8751.96 56.02 o 12 2 1 23.56 30.84 4.75 o 14 2 1 668.04 635.20 14.59 o 16 2 1 1997.48 1983.51 33.34 o 18 2 1 754.62 725.07 22.16 o 20 2 1 403.41 388.11 16.77 o 22 2 1 1899.97 2092.34 60.02 o 24 2 1 156.30 184.23 25.70 o -25 3 1 74.42 91.46 16.52 o -23 3 1 24.90 14.91 13.87 o -21 3 1 63.62 60.44 20.45 o -19 3 1 362.55 354.38 12.08 o -17 3 1 221.03 203.94 8.54 o -15 3 1 169.33 155.57 6.81 o -13 3 1 6.15 7.35 3.41 o -11 3 1 1165.48 1244.64 12.54 o -9 3 1 1289.41 1231.50 11.68 o -7 3 1 4317.40 4487.09 25.30 o -5 3 1 896.98 1040.88 6.88 o -3 3 1 3775.44 3631.45 17.33 o -1 3 1 1365.33 1449.32 7.61 o 1 3 1 6883.68 6750.27 36.55 o 3 3 1 3685.11 3563.27 21.83 o 5 3 1 1580.15 1362.73 11.42 o 7 3 1 307.52 302.47 6.41 o 9 3 1 1013.15 1081.76 14.46 o 11 3 1 4205.05 4257.54 31.90 o 13 3 1 362.84 323.92 8.97 o 15 3 1 18.67 12.58 8.14 o 17 3 1 1.33 14.28 9.56 o 19 3 1 21.94 17.95 11.06 o 21 3 1 35.83 50.68 14.10 o 23 3 1 113.42 104.84 18.18 o -26 4 1 500.63 491.34 30.30 o -24 4 1 1836.32 1887.49 40.55 o -22 4 1 546.67 541.25 34.31 o -20 4 1 304.76 341.80 17.92 o -18 4 1 3740.50 3674.68 43.78 o -16 4 1 7381.99 7331.85 80.55 o -14 4 1 1331.67 1376.70 15.89 o -12 4 1 4127.27 4231.88 30.89 o -10 4 1 2770.46 2646.31 23.45 o -8 4 1 5129.20 5364.88 34.65 o -6 4 1 19349.48 19354.42 95.65 o -4 4 1 234.86 145.91 2.88 o -2 4 1 30927.54 31711.66 151.46 o 0 4 1 32773.00 33818.84 175.61 o 2 4 1 67763.20 65367.62 577.07 o 4 4 1 6227.45 6161.09 37.40 o 6 4 1 4809.90 4670.93 30.97 o 8 4 1 18812.28 19779.28 117.17 o 10 4 1 4016.16 4078.11 33.16 o 12 4 1 6805.34 6713.68 47.94 o 14 4 1 4543.04 4451.99 36.99 o 16 4 1 105.17 107.87 10.35 o 18 4 1 778.73 757.38 22.68 o 20 4 1 2183.77 2252.21 48.62 o 22 4 1 1400.47 1471.80 50.09 o 24 4 1 179.03 168.51 20.76 o -25 5 1 811.78 913.81 29.63 o -23 5 1 11.24 -1.58 13.06 o -21 5 1 1765.18 1783.07 36.19 o -19 5 1 2468.19 2511.08 34.06 o -17 5 1 2400.06 2290.73 27.46 o -15 5 1 128.76 144.41 6.27 o -13 5 1 1189.39 1123.63 13.05 o -11 5 1 131.47 152.58 5.13 o -9 5 1 9867.74 10550.96 64.02 o -7 5 1 3118.66 2902.98 19.98 o -5 5 1 7928.22 8674.02 44.59 o -3 5 1 2907.80 2672.61 15.26 o -1 5 1 12805.23 12744.87 68.42 o 1 5 1 9925.97 10188.85 57.76 o 3 5 1 1427.24 1531.88 13.19 o 5 5 1 6858.13 6636.99 40.79 o 7 5 1 373.18 303.34 7.35 o 9 5 1 13525.93 13642.72 84.95 o 11 5 1 2522.76 2816.79 29.11 o 13 5 1 1398.52 1367.19 23.80 o 15 5 1 2180.09 2073.07 31.91 o 17 5 1 1005.48 977.63 21.32 o 19 5 1 61.25 40.37 11.56 o 21 5 1 144.51 174.98 16.74 o 23 5 1 467.74 519.99 28.29 o -26 6 1 62.53 64.92 22.55 o -24 6 1 638.58 652.44 31.80 o -22 6 1 360.27 402.28 20.96 o -20 6 1 83.35 63.68 12.95 o -18 6 1 483.50 470.02 12.23 o -16 6 1 2024.86 1943.49 42.27 o -14 6 1 2452.78 2693.02 28.39 o -12 6 1 1728.12 1769.71 16.89 o -10 6 1 368.69 265.13 7.70 o -8 6 1 440.39 384.10 5.87 o -6 6 1 4828.90 5277.00 33.10 o -4 6 1 664.72 730.39 6.30 o -2 6 1 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