#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/80/2018019.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018019_Fobs loop_ _publ_author_name 'Naicker, Tricia' 'Govender, Thavendran' 'Kruger, Hendrik G.' 'Maguire, Glenn E. M.' _publ_section_title ; Optically active diaryl tetrahydroisoquinoline derivatives ; _journal_coeditor_code SF3143 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o100 _journal_page_last o103 _journal_volume 67 _journal_year 2011 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.287 _cell_angle_gamma 90.000 _cell_length_a 11.0446 _cell_length_b 17.0083 _cell_length_c 18.4891 _exptl_crystal_F_000 1312.00 _reflns_d_resolution_high 0.7341 _[local]_cod_data_source_file sf3143IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' tricia4 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 189.97 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 5 -21 0 13.69 -50.11 51.49 o 6 -21 0 6.51 -34.21 45.61 o 4 -20 0 96.74 155.17 62.55 o 5 -20 0 141.98 122.17 36.52 o 6 -20 0 29.17 30.29 34.85 o 7 -20 0 5.02 34.56 49.42 o 1 -19 0 73.74 141.78 96.07 o 2 -19 0 84.97 70.81 49.25 o 3 -19 0 32.55 63.86 37.16 o 4 -19 0 51.45 85.40 32.60 o 5 -19 0 18.36 -20.74 33.29 o 6 -19 0 52.65 32.59 54.43 o 7 -19 0 8.48 27.62 35.94 o 8 -19 0 60.75 53.91 50.80 o 0 -18 0 14.34 -30.06 30.06 o 1 -18 0 14.85 46.28 26.37 o 2 -18 0 84.49 105.84 24.41 o 3 -18 0 192.11 212.02 24.37 o 4 -18 0 175.07 195.02 24.35 o 5 -18 0 101.29 158.34 28.18 o 6 -18 0 14.31 44.14 25.64 o 7 -18 0 23.28 68.06 35.13 o 8 -18 0 23.36 20.27 58.23 o 9 -18 0 18.30 74.64 52.53 o 1 -17 0 8.19 15.95 24.43 o 2 -17 0 57.30 73.27 22.64 o 3 -17 0 72.44 73.33 19.49 o 4 -17 0 57.59 45.41 19.82 o 5 -17 0 71.23 78.65 21.71 o 6 -17 0 57.23 65.80 26.00 o 7 -17 0 64.44 58.48 26.45 o 8 -17 0 29.91 -12.63 33.16 o 9 -17 0 26.48 88.61 60.99 o 0 -16 0 199.54 183.87 42.51 o 1 -16 0 3.13 -21.62 21.62 o 2 -16 0 446.60 410.67 26.75 o 3 -16 0 203.89 223.99 25.54 o 4 -16 0 147.36 175.64 27.51 o 5 -16 0 41.53 16.44 18.97 o 6 -16 0 369.82 424.97 29.66 o 7 -16 0 11.57 -22.62 22.62 o 8 -16 0 179.18 168.61 29.08 o 9 -16 0 53.80 88.34 38.77 o 10 -16 0 0.06 -44.58 44.58 o 1 -15 0 587.79 767.57 64.31 o 2 -15 0 310.41 297.27 28.79 o 3 -15 0 1070.29 1089.47 61.16 o 4 -15 0 985.07 1001.24 39.21 o 5 -15 0 70.20 59.93 19.00 o 6 -15 0 17.94 36.21 19.66 o 7 -15 0 22.83 50.19 24.27 o 8 -15 0 177.15 194.48 29.79 o 9 -15 0 10.95 11.26 25.95 o 10 -15 0 72.03 49.89 36.25 o 0 -14 0 68.81 68.43 31.79 o 1 -14 0 164.61 190.71 25.90 o 2 -14 0 882.99 889.56 61.30 o 3 -14 0 89.39 71.92 17.29 o 4 -14 0 563.28 554.02 28.22 o 5 -14 0 2.03 20.90 17.70 o 6 -14 0 104.69 115.06 23.49 o 7 -14 0 121.54 126.36 22.32 o 8 -14 0 58.01 59.03 25.03 o 9 -14 0 199.02 178.08 30.33 o 10 -14 0 3.34 27.47 26.79 o 11 -14 0 101.08 42.21 64.11 o 1 -13 0 1199.51 1079.85 43.83 o 2 -13 0 71.70 95.17 19.17 o 3 -13 0 321.62 340.38 22.27 o 4 -13 0 235.58 252.26 21.30 o 5 -13 0 96.01 117.14 18.98 o 6 -13 0 81.86 97.14 22.05 o 7 -13 0 327.98 388.25 27.12 o 8 -13 0 51.87 53.32 20.49 o 9 -13 0 0.62 11.99 23.69 o 10 -13 0 36.26 66.69 27.30 o 11 -13 0 10.03 5.99 26.58 o 0 -12 0 1131.04 1221.08 76.12 o 1 -12 0 1099.21 1087.03 42.25 o 2 -12 0 243.56 254.08 21.61 o 3 -12 0 2950.10 2822.93 96.42 o 4 -12 0 216.91 271.17 20.68 o 5 -12 0 131.97 127.45 18.19 o 6 -12 0 488.64 482.60 27.18 o 7 -12 0 16.20 1.38 17.54 o 8 -12 0 88.12 83.60 20.40 o 9 -12 0 42.26 28.87 23.87 o 10 -12 0 99.65 109.11 28.06 o 11 -12 0 136.00 86.79 29.19 o 12 -12 0 12.20 -5.01 37.14 o 1 -11 0 3958.18 3984.19 110.95 o 2 -11 0 1743.47 1714.61 55.98 o 3 -11 0 468.28 475.69 23.03 o 4 -11 0 196.22 186.88 17.31 o 5 -11 0 62.09 82.01 18.19 o 6 -11 0 1169.63 1191.84 50.81 o 7 -11 0 50.78 50.04 17.67 o 8 -11 0 184.91 159.32 27.99 o 9 -11 0 101.23 79.59 23.21 o 10 -11 0 53.39 36.71 24.81 o 11 -11 0 13.85 21.15 25.81 o 12 -11 0 1.96 -21.47 25.84 o 0 -10 0 1852.59 1838.19 95.27 o 1 -10 0 738.59 830.18 34.21 o 2 -10 0 619.62 566.32 43.40 o 3 -10 0 382.32 374.99 19.99 o 4 -10 0 1230.76 1241.11 44.55 o 5 -10 0 679.55 757.59 29.96 o 6 -10 0 273.18 275.91 25.17 o 7 -10 0 11.40 -14.38 15.87 o 8 -10 0 69.99 63.91 18.55 o 9 -10 0 13.73 9.35 19.09 o 10 -10 0 66.83 46.31 29.57 o 11 -10 0 5.48 -10.34 23.80 o 12 -10 0 18.70 39.37 27.50 o 13 -10 0 22.62 34.56 51.84 o 1 -9 0 4264.92 4532.87 121.76 o 2 -9 0 57.16 78.69 13.94 o 3 -9 0 339.25 371.59 22.74 o 4 -9 0 58.88 52.83 12.92 o 5 -9 0 623.35 578.11 31.97 o 6 -9 0 20.52 1.69 13.59 o 7 -9 0 955.87 935.98 35.51 o 8 -9 0 102.29 74.80 18.48 o 9 -9 0 29.02 28.95 18.41 o 10 -9 0 25.22 32.14 23.97 o 11 -9 0 72.06 68.70 26.03 o 12 -9 0 55.67 84.16 35.64 o 13 -9 0 18.91 0.85 26.89 o 0 -8 0 1939.51 2186.46 132.78 o 1 -8 0 1136.86 1050.46 36.70 o 2 -8 0 1625.97 1786.59 46.95 o 3 -8 0 475.28 471.51 20.19 o 4 -8 0 154.67 177.63 14.88 o 5 -8 0 1235.75 1191.51 37.69 o 6 -8 0 99.11 85.49 15.24 o 7 -8 0 15.69 4.42 14.72 o 8 -8 0 433.10 448.76 25.67 o 9 -8 0 140.02 133.03 20.27 o 10 -8 0 331.54 326.62 48.89 o 11 -8 0 16.32 4.96 23.53 o 12 -8 0 58.84 111.29 29.32 o 13 -8 0 13.10 21.08 26.44 o 1 -7 0 1125.12 1170.52 38.42 o 2 -7 0 665.73 628.62 22.91 o 3 -7 0 547.11 562.24 21.55 o 4 -7 0 1452.20 1517.27 41.95 o 5 -7 0 992.52 886.03 30.18 o 6 -7 0 482.25 445.07 22.51 o 7 -7 0 367.57 365.90 22.02 o 8 -7 0 533.52 531.09 27.45 o 9 -7 0 8.04 -14.36 14.83 o 10 -7 0 104.24 58.16 19.92 o 11 -7 0 16.52 38.47 24.66 o 12 -7 0 119.01 123.00 29.08 o 13 -7 0 73.44 67.85 30.19 o 0 -6 0 531.06 568.14 29.63 o 1 -6 0 1610.28 1557.14 46.25 o 2 -6 0 469.82 503.43 19.38 o 3 -6 0 568.85 649.91 33.08 o 4 -6 0 2488.97 2444.98 60.92 o 5 -6 0 371.25 382.57 24.75 o 6 -6 0 755.95 748.64 28.87 o 7 -6 0 523.63 502.94 24.42 o 8 -6 0 203.23 190.05 18.99 o 9 -6 0 171.86 143.09 19.12 o 10 -6 0 415.63 422.84 26.95 o 11 -6 0 36.70 25.60 23.79 o 12 -6 0 34.13 31.95 25.75 o 13 -6 0 2.00 -16.99 26.23 o 1 -5 0 829.77 850.96 30.99 o 2 -5 0 1742.82 1675.07 41.82 o 3 -5 0 1321.05 1296.51 35.12 o 4 -5 0 412.25 479.88 32.14 o 5 -5 0 898.13 814.84 27.79 o 6 -5 0 337.90 291.96 17.98 o 7 -5 0 826.68 815.13 30.64 o 8 -5 0 190.67 220.13 29.37 o 9 -5 0 163.01 182.69 20.17 o 10 -5 0 426.15 366.56 26.16 o 11 -5 0 17.00 34.03 27.90 o 12 -5 0 59.20 26.91 25.61 o 13 -5 0 44.93 50.26 22.82 o 14 -5 0 14.45 3.33 24.83 o 0 -4 0 36080.11 36917.75 1917.58 o 1 -4 0 8021.83 7647.67 206.80 o 2 -4 0 3623.07 3611.99 81.81 o 3 -4 0 1515.71 1452.40 37.66 o 4 -4 0 641.57 691.16 23.98 o 5 -4 0 1705.38 1881.24 96.16 o 6 -4 0 109.31 100.89 19.85 o 7 -4 0 333.32 311.15 19.18 o 8 -4 0 171.89 202.75 17.99 o 9 -4 0 1581.15 1620.68 50.32 o 10 -4 0 300.71 303.62 24.30 o 11 -4 0 17.77 29.18 18.87 o 12 -4 0 66.77 86.58 26.43 o 13 -4 0 16.99 -9.70 21.29 o 14 -4 0 10.57 73.31 24.18 o 1 -3 0 5994.18 5734.32 145.06 o 2 -3 0 3966.73 3651.72 82.19 o 3 -3 0 116.60 92.91 9.84 o 4 -3 0 1928.39 1839.39 46.47 o 5 -3 0 699.93 722.49 25.46 o 6 -3 0 285.46 260.01 16.33 o 7 -3 0 348.97 381.10 20.31 o 8 -3 0 202.94 176.13 32.53 o 9 -3 0 1235.48 1196.59 43.64 o 10 -3 0 64.24 58.91 21.10 o 11 -3 0 135.31 130.10 20.98 o 12 -3 0 74.09 75.67 20.84 o 13 -3 0 5.96 19.26 21.18 o 14 -3 0 1.29 -3.34 28.21 o 0 -2 0 743.02 854.88 38.37 o 1 -2 0 8713.45 8612.04 185.83 o 2 -2 0 9203.60 8879.65 191.40 o 3 -2 0 3071.75 3032.07 69.76 o 4 -2 0 108.20 86.01 10.74 o 5 -2 0 2569.42 2712.18 65.66 o 6 -2 0 161.47 157.86 14.20 o 7 -2 0 850.41 874.88 30.98 o 8 -2 0 1017.33 1120.11 48.78 o 9 -2 0 1079.97 1002.98 36.97 o 10 -2 0 138.99 151.36 19.93 o 11 -2 0 6.35 16.36 16.71 o 12 -2 0 76.94 114.74 22.54 o 13 -2 0 17.58 2.82 21.06 o 14 -2 0 2.07 -24.98 24.98 o 1 -1 0 4648.99 4258.20 92.77 o 2 -1 0 8908.98 8601.81 185.75 o 3 -1 0 1391.72 1285.46 33.06 o 4 -1 0 5751.93 5303.59 118.76 o 5 -1 0 983.99 1107.83 37.32 o 6 -1 0 79.93 69.10 11.62 o 7 -1 0 13.89 4.81 11.39 o 8 -1 0 795.81 791.93 30.48 o 9 -1 0 10.56 15.33 14.74 o 10 -1 0 59.77 67.52 15.70 o 11 -1 0 140.70 133.58 18.13 o 12 -1 0 22.88 31.45 20.50 o 13 -1 0 114.97 115.58 28.98 o 14 -1 0 62.52 69.96 32.63 o 1 0 0 4713.51 4301.83 108.14 o 2 0 0 16351.98 16172.99 346.81 o 3 0 0 214.08 207.13 15.98 o 4 0 0 12.08 25.01 8.83 o 5 0 0 990.35 970.79 34.16 o 6 0 0 7.77 20.46 10.50 o 7 0 0 123.55 130.36 14.62 o 8 0 0 23.94 23.54 12.51 o 9 0 0 43.11 46.54 14.16 o 10 0 0 142.27 149.19 17.56 o 11 0 0 48.69 82.81 30.78 o 12 0 0 2.06 -3.49 22.07 o 13 0 0 37.67 52.47 27.40 o 14 0 0 266.35 393.80 60.66 o 1 1 0 4651.31 4113.19 122.22 o 2 1 0 8860.70 8351.18 175.22 o 3 1 0 1404.64 1341.09 33.25 o 4 1 0 5764.98 5268.18 104.53 o 5 1 0 1005.22 1104.59 52.11 o 6 1 0 80.48 74.67 10.72 o 7 1 0 13.87 -1.48 9.84 o 8 1 0 790.09 774.77 26.35 o 9 1 0 10.36 -10.56 14.63 o 10 1 0 59.45 48.41 17.68 o 11 1 0 140.64 134.23 27.29 o 12 1 0 23.43 50.77 24.65 o 13 1 0 113.39 187.12 91.06 o 14 1 0 62.65 30.19 33.86 o 0 2 0 743.65 785.53 38.89 o 1 2 0 8739.68 8740.25 257.02 o 2 2 0 9220.01 8861.39 261.79 o 3 2 0 3106.04 2924.96 75.59 o 4 2 0 101.40 75.41 10.96 o 5 2 0 2561.16 2822.10 92.14 o 6 2 0 158.48 162.54 17.31 o 7 2 0 840.60 764.34 28.40 o 8 2 0 1020.13 1041.02 53.15 o 9 2 0 1077.42 1008.00 36.83 o 10 2 0 138.83 109.41 19.16 o 11 2 0 6.16 3.01 18.00 o 12 2 0 76.71 108.38 32.62 o 13 2 0 17.46 3.32 30.06 o 14 2 0 2.11 5.92 60.30 o 1 3 0 5992.02 5511.65 164.40 o 2 3 0 3920.41 3453.57 106.32 o 3 3 0 119.97 75.38 15.55 o 4 3 0 1931.86 1911.96 75.96 o 5 3 0 683.86 637.89 26.14 o 6 3 0 285.10 227.62 21.30 o 7 3 0 351.13 366.37 19.91 o 8 3 0 199.66 198.83 19.23 o 9 3 0 1239.57 1181.83 41.34 o 10 3 0 64.76 23.02 19.36 o 11 3 0 135.18 140.86 24.13 o 12 3 0 73.07 108.32 32.46 o 13 3 0 5.63 61.38 33.21 o 14 3 0 1.35 3.48 33.63 o 0 4 0 36087.57 37139.86 1530.56 o 1 4 0 8003.80 7462.54 222.18 o 2 4 0 3620.60 3770.42 177.26 o 3 4 0 1544.87 1496.17 52.46 o 4 4 0 624.66 606.60 29.70 o 5 4 0 1703.51 1725.70 62.96 o 6 4 0 106.47 122.00 18.57 o 7 4 0 326.89 342.79 26.89 o 8 4 0 169.80 183.54 20.06 o 9 4 0 1576.43 1598.81 57.26 o 10 4 0 299.70 272.15 26.79 o 11 4 0 18.09 23.77 20.88 o 12 4 0 66.41 128.70 33.77 o 13 4 0 16.73 23.70 32.96 o 14 4 0 10.70 15.72 42.33 o 1 5 0 810.57 832.28 33.91 o 2 5 0 1756.81 1586.85 62.39 o 3 5 0 1314.64 1287.31 48.38 o 4 5 0 418.72 401.26 23.35 o 5 5 0 900.30 795.58 36.82 o 6 5 0 335.06 306.36 24.20 o 7 5 0 828.11 771.15 40.97 o 8 5 0 188.12 212.27 24.94 o 9 5 0 164.22 160.96 21.96 o 10 5 0 423.73 448.84 31.76 o 11 5 0 16.70 9.00 21.10 o 12 5 0 58.86 69.82 48.55 o 13 5 0 45.22 14.73 32.20 o 14 5 0 14.50 -5.18 42.16 o 0 6 0 514.39 452.52 32.87 o 1 6 0 1615.10 1633.67 57.01 o 2 6 0 474.44 442.73 24.09 o 3 6 0 585.32 644.93 24.59 o 4 6 0 2476.16 2387.19 81.43 o 5 6 0 368.71 395.33 45.12 o 6 6 0 748.19 780.58 39.74 o 7 6 0 520.32 505.14 31.77 o 8 6 0 204.15 241.19 45.97 o 9 6 0 172.18 166.89 26.06 o 10 6 0 416.87 350.40 32.72 o 11 6 0 36.02 24.30 21.79 o 12 6 0 34.21 9.75 30.71 o 13 6 0 1.93 -16.66 31.00 o 1 7 0 1135.89 1148.71 44.32 o 2 7 0 654.86 606.76 30.44 o 3 7 0 547.82 510.01 62.26 o 4 7 0 1459.12 1524.84 45.75 o 5 7 0 987.91 812.92 44.12 o 6 7 0 488.76 446.04 28.73 o 7 7 0 364.84 373.58 42.69 o 8 7 0 535.80 556.76 36.79 o 9 7 0 8.35 4.49 21.37 o 10 7 0 102.94 111.97 23.35 o 11 7 0 16.86 15.22 41.13 o 12 7 0 119.71 96.72 33.07 o 13 7 0 73.32 38.77 34.92 o 0 8 0 1925.92 2149.45 105.39 o 1 8 0 1145.89 1074.44 44.18 o 2 8 0 1617.16 1822.85 65.28 o 3 8 0 470.27 460.79 27.75 o 4 8 0 152.39 144.42 19.55 o 5 8 0 1236.05 1285.98 41.68 o 6 8 0 102.29 75.03 19.86 o 7 8 0 16.64 26.09 19.04 o 8 8 0 429.42 446.53 38.55 o 9 8 0 140.88 107.76 26.03 o 10 8 0 330.36 300.49 37.26 o 11 8 0 16.03 -10.93 21.45 o 12 8 0 58.58 61.76 33.75 o 13 8 0 13.19 -7.78 33.39 o 1 9 0 4278.07 4237.98 175.79 o 2 9 0 62.76 89.08 22.46 o 3 9 0 333.68 355.91 24.89 o 4 9 0 57.28 43.59 16.71 o 5 9 0 631.32 661.95 56.71 o 6 9 0 19.34 9.10 17.71 o 7 9 0 954.74 968.65 76.96 o 8 9 0 104.27 108.06 36.81 o 9 9 0 28.69 17.33 22.44 o 10 9 0 24.56 12.80 23.46 o 11 9 0 71.78 135.84 41.12 o 12 9 0 56.28 62.06 34.13 o 13 9 0 18.74 45.42 35.59 o 0 10 0 1854.07 1812.55 95.96 o 1 10 0 728.67 828.26 40.23 o 2 10 0 623.19 554.39 31.91 o 3 10 0 384.36 366.00 26.40 o 4 10 0 1243.17 1240.94 52.94 o 5 10 0 684.04 712.93 43.57 o 6 10 0 270.10 263.20 27.50 o 7 10 0 10.79 11.81 20.88 o 8 10 0 70.22 49.06 27.65 o 9 10 0 14.28 -7.69 33.17 o 10 10 0 67.33 87.01 28.96 o 11 10 0 5.68 -21.22 29.13 o 12 10 0 18.16 20.22 53.22 o 1 11 0 3962.82 3951.30 130.26 o 2 11 0 1750.25 1900.06 71.62 o 3 11 0 467.47 462.33 30.89 o 4 11 0 191.79 172.82 41.13 o 5 11 0 59.00 71.50 25.57 o 6 11 0 1164.36 1088.10 53.67 o 7 11 0 49.04 22.03 22.11 o 8 11 0 183.00 156.20 27.60 o 9 11 0 102.17 159.90 34.56 o 10 11 0 51.90 55.77 27.64 o 11 11 0 14.29 52.87 40.78 o 12 11 0 2.11 39.96 35.61 o 0 12 0 1135.12 1171.60 73.01 o 1 12 0 1109.54 977.82 47.71 o 2 12 0 240.31 253.21 50.12 o 3 12 0 2955.83 2873.52 131.90 o 4 12 0 211.86 213.11 25.65 o 5 12 0 133.64 114.41 24.71 o 6 12 0 485.10 482.80 35.80 o 7 12 0 15.61 5.01 22.24 o 8 12 0 89.93 47.45 23.09 o 9 12 0 41.70 88.30 48.55 o 10 12 0 99.69 155.86 42.85 o 11 12 0 135.97 221.87 52.88 o 12 12 0 12.11 33.34 35.23 o 1 13 0 1205.42 1080.49 70.93 o 2 13 0 67.35 58.38 20.76 o 3 13 0 323.64 263.12 27.37 o 4 13 0 239.67 245.85 31.97 o 5 13 0 93.30 104.02 24.31 o 6 13 0 81.70 98.71 44.06 o 7 13 0 328.39 328.37 35.78 o 8 13 0 50.56 68.78 26.12 o 9 13 0 0.57 -18.74 23.33 o 10 13 0 35.32 23.15 39.74 o 11 13 0 10.37 0.00 40.09 o 0 14 0 64.75 91.93 34.21 o 1 14 0 161.28 209.45 28.10 o 2 14 0 884.42 902.30 54.13 o 3 14 0 90.79 114.74 25.03 o 4 14 0 571.28 561.37 39.44 o 5 14 0 1.76 13.63 23.45 o 6 14 0 107.56 140.45 27.73 o 7 14 0 121.16 144.64 55.64 o 8 14 0 59.15 51.40 27.25 o 9 14 0 199.88 149.31 45.62 o 10 14 0 3.25 -22.12 39.05 o 11 14 0 101.38 149.29 51.49 o 1 15 0 589.94 660.83 43.27 o 2 15 0 312.06 373.07 49.43 o 3 15 0 1066.71 1026.45 55.40 o 4 15 0 988.12 1004.25 53.88 o 5 15 0 67.91 75.17 26.02 o 6 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