Crystallography Open Database

Information card for entry 2018025

2018024 << 2018025 >> 2018026

Preview

Coordinates	2018025.cif
Structure factors	2018025.hkl
Original IUCr paper	HTML

Structure parameters

Chemical name	(Aqua-2κ<i>O</i>)bis(2,2'-bipyridine-1κ^2^<i>N</i>,<i>N</i>'){μ-<i>N</i>- [3-(dimethylamino)propyl]-<i>N</i>'-(2-oxidophenyl)oxamidato(3-)- 1:2κ^2^<i>O</i>,<i>O</i>':κ^4^<i>O</i>'',<i>N</i>,<i>N</i>',<i>N</i>''} copper(II)nickel(II) perchlorate
Formula	C33 H34 Cl Cu N7 Ni O8
Calculated formula	C33 H34 Cl Cu N7 Ni O8
Title of publication	(Aqua-2κ<i>O</i>)bis(2,2'-bipyridine-1κ^2^<i>N</i>,<i>N</i>'){μ-<i>N</i>-[3-(dimethylamino)propyl]-<i>N</i>'-(2-oxidophenyl)oxamidato(3{-})-1:2κ^2^<i>O</i>,<i>O</i>':κ^4^<i>O</i>'',<i>N</i>,<i>N</i>',<i>N</i>''}copper(II)nickel(II) perchlorate
Authors of publication	Yue, Xi-Teng; Nie, Jin-Ju; Li, Yan-Tuan; Wu, Zhi-Yong; Yan, Cui-Wei
Journal of publication	Acta Crystallographica Section C
Year of publication	2011
Journal volume	67
Journal issue	4
Pages of publication	m115 - m118
a	11.4692 ± 0.0005 Å
b	11.8976 ± 0.0005 Å
c	15.1818 ± 0.0007 Å
α	92.261 ± 0.003°
β	109.043 ± 0.003°
γ	112.911 ± 0.003°
Cell volume	1770.51 ± 0.15 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0992
Residual factor for significantly intense reflections	0.0491
Weighted residual factors for significantly intense reflections	0.1104
Weighted residual factors for all reflections included in the refinement	0.131
Goodness-of-fit parameter for all reflections included in the refinement	0.958
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

Version history

Revision	Date	Message	Files
180849 (current)	2016-04-02	cif/2/01/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/01/80.	2018025.cif 2018025.hkl
176760	2016-02-20	cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/01.	2018025.cif 2018025.hkl
125873	2014-10-25	cod/ (saulius@koala.ibt.lt) Adding DOIs to 1887 Acta Cryst. CIFs, their DOIs fetched using ACCE codes.	2018025.cif 2018025.hkl
88064	2013-08-29	Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet.	2018025.cif 2018025.hkl
26848	2011-09-28	cif/2/, hkl/2/, html/ Reorganising CIFs of the range 2* into the "prefix-directory" tree.	2018025.cif 2018025.hkl
19531	2011-05-17	hkl/2/ Adding Fobs data for the latest IUCr deposition.	2018025.cif 2018025.hkl
19030	2011-05-06	../uploads/cif-deposit/cod/cif Adding structures of 2018025 via cif-deposit CGI script.	2018025.cif