#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/80/2018072.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018072_Fobs loop_ _publ_author_name '\'Slepokura, Katarzyna' 'Mitaszewska, Irmina' _publ_section_title ; Acidic and anionic forms of 1,3-cyclic dihydroxyacetone phosphate (cDHAP) dimethyl acetal ; _journal_coeditor_code MX3045 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o161 _journal_page_last o165 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 89.130 _cell_angle_beta 76.000 _cell_angle_gamma 81.180 _cell_length_a 6.8590 _cell_length_b 7.1140 _cell_length_c 8.9390 _exptl_crystal_F_000 208.00 _reflns_d_resolution_high 0.7107 _[local]_cod_data_source_file mx30455ksup4.hkl _[local]_cod_data_source_block 5k #BEGIN Tags that were not found in dictionaries: _shelx_title ' mita3 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 75.65 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 304.75 317.47 2.46 o 2 0 0 323.49 296.97 1.37 o 3 0 0 352.17 346.38 3.16 o 4 0 0 185.09 206.01 1.31 o 5 0 0 147.50 141.19 3.19 o 6 0 0 19.24 19.76 0.48 o 7 0 0 64.02 57.03 1.23 o -8 1 0 3.84 3.52 1.08 o -7 1 0 26.99 24.72 0.71 o -6 1 0 0.47 0.10 0.39 o -5 1 0 27.39 21.97 0.54 o -4 1 0 13.16 10.53 0.42 o -3 1 0 1286.50 1316.79 5.56 o -2 1 0 1883.35 2001.59 11.89 o -1 1 0 3321.65 3537.78 45.56 o 0 1 0 0.62 1.17 0.39 o 1 1 0 5.40 4.98 0.39 o 2 1 0 381.44 375.28 3.28 o 3 1 0 258.51 267.02 1.23 o 4 1 0 4.87 5.70 0.41 o 5 1 0 212.53 217.72 2.31 o 6 1 0 272.88 265.43 2.36 o 7 1 0 36.43 40.29 1.32 o 8 1 0 9.54 9.19 1.68 o -8 2 0 13.23 13.79 0.82 o -7 2 0 14.41 16.53 0.71 o -6 2 0 28.42 25.65 0.64 o -5 2 0 89.17 82.74 2.29 o -4 2 0 389.76 381.82 2.65 o -3 2 0 1324.61 1385.60 10.14 o -2 2 0 59.85 69.26 1.00 o -1 2 0 12.26 15.68 0.74 o 0 2 0 290.99 265.59 1.21 o 1 2 0 68.35 54.83 2.11 o 2 2 0 0.76 2.32 0.48 o 3 2 0 48.59 51.43 0.79 o 4 2 0 112.44 106.01 2.83 o 5 2 0 228.16 236.76 4.96 o 6 2 0 19.44 17.97 2.65 o 7 2 0 2.01 2.18 0.99 o 8 2 0 5.67 5.25 1.68 o -8 3 0 93.81 102.49 1.75 o -7 3 0 35.80 39.83 1.04 o -6 3 0 78.85 91.77 1.26 o -5 3 0 56.96 51.35 1.38 o -4 3 0 140.89 136.39 1.57 o -3 3 0 27.98 32.95 0.92 o -2 3 0 1.70 1.50 0.54 o -1 3 0 60.37 64.58 1.01 o 0 3 0 77.12 60.99 0.56 o 1 3 0 229.35 206.29 2.78 o 2 3 0 1574.03 1776.32 27.10 o 3 3 0 3.32 11.79 0.74 o 4 3 0 104.73 106.85 1.66 o 5 3 0 56.47 56.17 1.50 o 6 3 0 238.28 231.29 4.91 o 7 3 0 17.35 15.97 1.83 o 8 3 0 11.54 12.71 1.93 o -7 4 0 0.14 0.55 0.76 o -6 4 0 61.77 61.53 1.33 o -5 4 0 56.08 58.07 1.31 o -4 4 0 186.52 169.30 2.21 o -3 4 0 229.75 217.98 2.62 o -2 4 0 88.35 95.91 0.87 o -1 4 0 3.97 5.61 0.45 o 0 4 0 24.48 29.11 0.48 o 1 4 0 4.08 2.50 0.30 o 2 4 0 278.64 259.58 2.39 o 3 4 0 362.45 384.42 2.88 o 4 4 0 79.63 81.30 2.40 o 5 4 0 526.82 522.85 10.21 o 6 4 0 11.81 11.18 2.94 o 7 4 0 15.52 10.12 1.88 o 8 4 0 42.28 41.46 2.66 o -7 5 0 24.79 26.39 1.24 o -6 5 0 43.14 43.15 1.16 o -5 5 0 5.26 3.71 0.67 o -4 5 0 247.00 242.35 1.95 o -3 5 0 1.51 1.60 0.45 o -2 5 0 10.09 11.05 0.53 o -1 5 0 6.80 6.31 0.51 o 0 5 0 30.59 32.53 0.65 o 1 5 0 643.17 692.71 4.51 o 2 5 0 242.89 248.39 1.45 o 3 5 0 672.87 698.60 2.65 o 4 5 0 36.42 34.80 1.30 o 5 5 0 283.29 271.38 3.11 o 6 5 0 16.76 13.41 1.27 o 7 5 0 49.76 53.12 2.63 o -6 6 0 101.46 106.70 1.88 o -5 6 0 22.27 21.36 1.07 o -4 6 0 50.63 46.62 1.09 o -3 6 0 4.61 4.10 0.55 o -2 6 0 409.63 414.66 2.30 o -1 6 0 1.81 1.91 0.52 o 0 6 0 335.87 346.13 2.50 o 1 6 0 146.52 147.74 1.51 o 2 6 0 172.26 173.31 3.22 o 3 6 0 148.26 145.95 1.30 o 4 6 0 131.80 126.44 2.16 o 5 6 0 54.76 54.36 1.74 o 6 6 0 137.12 143.67 2.67 o 7 6 0 14.12 10.31 2.07 o -5 7 0 25.44 24.55 1.66 o -4 7 0 16.12 15.49 1.13 o -3 7 0 89.99 91.67 1.37 o -2 7 0 47.24 43.88 1.00 o -1 7 0 194.34 184.08 1.92 o 0 7 0 0.01 0.15 0.66 o 1 7 0 54.58 52.17 1.71 o 2 7 0 76.48 74.42 2.59 o 3 7 0 11.08 10.73 1.27 o 4 7 0 6.16 5.97 1.16 o 5 7 0 139.08 144.56 2.64 o 6 7 0 2.59 2.03 0.93 o -4 8 0 30.00 30.04 1.81 o -3 8 0 5.22 4.38 0.90 o -2 8 0 69.22 68.39 1.46 o -1 8 0 1.58 1.81 0.76 o 0 8 0 12.33 13.16 0.99 o 1 8 0 7.39 4.34 0.78 o 2 8 0 24.37 27.53 1.74 o 3 8 0 30.50 31.61 1.73 o 4 8 0 70.14 76.05 2.94 o 5 8 0 87.75 86.78 2.50 o -2 9 0 33.09 36.34 1.81 o -1 9 0 68.78 70.89 1.74 o 0 9 0 8.54 7.43 0.92 o 1 9 0 19.68 19.00 1.02 o 2 9 0 0.89 1.67 1.30 o 3 9 0 20.04 21.57 2.44 o 4 9 0 2.27 3.26 1.99 o -4 -9 1 39.63 34.94 2.78 o -3 -9 1 8.04 8.22 1.42 o -2 -9 1 1.12 2.26 0.83 o -1 -9 1 14.23 14.69 1.03 o 0 -9 1 0.22 0.81 0.86 o 1 -9 1 0.49 0.00 1.00 o 2 -9 1 51.21 51.07 2.05 o -5 -8 1 6.05 7.79 1.96 o -4 -8 1 11.87 10.23 1.42 o -3 -8 1 27.37 27.97 1.73 o -2 -8 1 4.05 3.68 0.77 o -1 -8 1 25.39 25.99 1.03 o 0 -8 1 12.49 11.70 0.90 o 1 -8 1 0.15 1.32 0.78 o 2 -8 1 84.76 83.79 1.58 o 3 -8 1 0.80 0.39 1.08 o 4 -8 1 22.85 22.88 1.69 o -6 -7 1 0.09 0.32 1.58 o -5 -7 1 0.15 0.30 0.84 o -4 -7 1 108.10 111.57 2.26 o -3 -7 1 9.70 8.34 0.75 o -2 -7 1 18.79 21.73 1.11 o -1 -7 1 109.50 111.37 3.15 o 0 -7 1 86.05 77.03 2.16 o 1 -7 1 236.04 245.70 2.45 o 2 -7 1 34.53 31.39 0.90 o 3 -7 1 48.06 47.60 0.90 o 4 -7 1 6.28 5.91 0.78 o 5 -7 1 16.45 15.53 1.78 o -7 -6 1 17.33 17.92 2.29 o -6 -6 1 40.91 38.26 2.29 o -5 -6 1 34.88 37.11 1.53 o -4 -6 1 0.04 0.00 0.91 o -3 -6 1 17.78 15.05 0.65 o -2 -6 1 1573.63 1632.54 5.95 o -1 -6 1 28.31 27.53 0.87 o 0 -6 1 28.57 29.57 0.87 o 1 -6 1 58.29 56.23 1.43 o 2 -6 1 14.87 15.58 0.66 o 3 -6 1 9.18 9.32 0.60 o 4 -6 1 18.99 16.08 0.79 o 5 -6 1 12.33 11.26 0.88 o 6 -6 1 61.48 63.69 1.54 o -7 -5 1 23.49 21.65 2.09 o -6 -5 1 21.27 19.69 1.95 o -5 -5 1 169.97 164.46 2.48 o -4 -5 1 549.50 550.60 14.10 o -3 -5 1 1020.75 1037.96 12.79 o -2 -5 1 10.50 10.75 0.72 o -1 -5 1 201.59 201.12 1.80 o 0 -5 1 143.77 136.31 1.51 o 1 -5 1 25.09 24.74 0.53 o 2 -5 1 58.95 54.56 0.79 o 3 -5 1 22.42 21.78 0.62 o 4 -5 1 293.44 281.56 6.15 o 5 -5 1 23.65 25.76 0.90 o 6 -5 1 0.44 0.53 0.75 o 7 -5 1 192.42 201.24 2.40 o -8 -4 1 16.95 16.21 2.23 o -7 -4 1 41.44 40.10 2.43 o -6 -4 1 306.82 305.82 4.81 o -5 -4 1 733.00 694.29 11.88 o -4 -4 1 106.62 105.98 3.90 o -3 -4 1 74.19 65.79 1.70 o -2 -4 1 202.63 192.19 2.13 o -1 -4 1 545.83 557.84 4.47 o 0 -4 1 12.03 11.08 0.41 o 1 -4 1 25.43 24.31 0.59 o 2 -4 1 238.63 237.70 1.65 o 3 -4 1 205.58 199.26 2.28 o 4 -4 1 213.03 220.33 3.82 o 5 -4 1 37.46 33.25 1.10 o 6 -4 1 65.54 65.66 1.18 o 7 -4 1 77.60 82.64 1.41 o 8 -4 1 0.24 0.00 0.90 o -8 -3 1 91.84 95.91 3.53 o -7 -3 1 4.19 3.21 1.66 o -6 -3 1 3.74 1.71 1.45 o -5 -3 1 61.21 57.18 1.81 o -4 -3 1 31.57 45.48 2.63 o -3 -3 1 5.44 7.07 0.66 o -2 -3 1 7.24 7.21 0.34 o -1 -3 1 223.25 235.86 1.29 o 0 -3 1 773.22 839.70 6.46 o 1 -3 1 21.38 28.50 0.52 o 2 -3 1 7.42 8.00 0.59 o 3 -3 1 27.69 20.93 0.88 o 4 -3 1 0.24 0.32 0.41 o 5 -3 1 32.03 29.24 1.35 o 6 -3 1 18.09 15.64 1.01 o 7 -3 1 0.28 0.57 0.64 o 8 -3 1 7.31 7.91 0.90 o -8 -2 1 56.44 59.56 2.74 o -7 -2 1 1.32 1.82 0.95 o -6 -2 1 2.45 1.62 0.52 o -5 -2 1 70.30 65.59 0.87 o -4 -2 1 0.60 0.16 0.51 o -3 -2 1 2.88 3.99 0.44 o -2 -2 1 6.00 5.23 0.53 o -1 -2 1 1942.81 2161.72 12.08 o 0 -2 1 117.20 89.28 0.68 o 1 -2 1 163.54 163.56 1.50 o 2 -2 1 188.69 176.41 1.42 o 3 -2 1 470.26 476.51 2.62 o 4 -2 1 122.04 113.03 0.90 o 5 -2 1 32.42 35.15 0.75 o 6 -2 1 18.14 25.35 0.68 o 7 -2 1 5.27 7.05 0.59 o 8 -2 1 36.03 37.62 1.20 o -8 -1 1 45.90 47.10 1.92 o -7 -1 1 28.09 25.61 0.87 o -6 -1 1 332.29 339.31 3.91 o -5 -1 1 111.45 115.46 0.96 o -4 -1 1 75.71 71.32 0.85 o -3 -1 1 96.61 97.04 1.60 o -2 -1 1 17.10 17.06 0.47 o -1 -1 1 1764.48 1955.56 10.47 o 0 -1 1 886.23 948.75 11.97 o 1 -1 1 3852.01 4138.74 71.19 o 2 -1 1 335.43 322.69 3.31 o 3 -1 1 2463.30 2793.46 4.12 o 4 -1 1 216.02 240.05 1.42 o 5 -1 1 224.62 238.34 3.37 o 6 -1 1 16.77 17.03 0.52 o 7 -1 1 11.75 12.80 0.78 o 8 -1 1 11.72 10.04 0.97 o -7 0 1 29.10 34.50 1.10 o -6 0 1 73.97 70.80 1.52 o -5 0 1 1.78 1.10 0.34 o -4 0 1 138.97 137.94 0.92 o -3 0 1 13.31 11.93 0.43 o -2 0 1 616.95 651.83 2.12 o -1 0 1 40.60 38.56 1.45 o 1 0 1 869.42 950.70 10.09 o 2 0 1 3218.39 3509.10 15.60 o 3 0 1 321.99 324.28 1.35 o 4 0 1 227.93 224.73 2.70 o 5 0 1 61.95 60.58 0.61 o 6 0 1 70.81 69.77 1.13 o 7 0 1 0.73 0.89 0.60 o 8 0 1 16.02 15.89 1.31 o -8 1 1 52.27 53.28 1.77 o -7 1 1 9.14 8.37 0.77 o -6 1 1 129.12 130.79 1.63 o -5 1 1 286.46 284.28 4.71 o -4 1 1 48.23 55.41 1.18 o -3 1 1 1055.51 1078.35 4.56 o -2 1 1 310.48 331.26 2.05 o -1 1 1 39.59 49.32 1.47 o 0 1 1 5723.53 5883.97 20.73 o 1 1 1 508.85 511.68 2.16 o 2 1 1 446.93 402.14 5.12 o 3 1 1 484.47 449.58 4.58 o 4 1 1 0.08 0.32 0.35 o 5 1 1 610.50 601.22 3.03 o 6 1 1 55.63 51.96 0.83 o 7 1 1 5.79 5.31 1.08 o 8 1 1 166.46 178.26 3.19 o -8 2 1 7.48 6.48 0.77 o -7 2 1 101.62 106.28 1.27 o -6 2 1 128.32 137.62 2.39 o -5 2 1 21.41 15.41 0.75 o -4 2 1 347.10 360.30 1.63 o -3 2 1 345.40 343.98 4.02 o -2 2 1 2.52 3.26 0.29 o -1 2 1 43.42 39.09 1.03 o 0 2 1 275.76 272.57 1.32 o 1 2 1 736.69 752.71 5.50 o 2 2 1 1542.79 1631.60 4.34 o 3 2 1 1026.35 1143.15 6.02 o 4 2 1 96.60 85.04 2.62 o 5 2 1 553.41 554.48 10.55 o 6 2 1 210.70 206.48 2.61 o 7 2 1 74.37 85.33 1.99 o 8 2 1 2.50 3.53 1.12 o 9 2 1 6.49 6.52 1.73 o -8 3 1 2.89 2.47 0.89 o -7 3 1 76.66 84.13 1.37 o -6 3 1 10.26 12.21 0.66 o -5 3 1 3.86 2.62 0.53 o -4 3 1 169.67 172.55 2.31 o -3 3 1 128.76 132.30 1.25 o -2 3 1 42.14 48.98 0.83 o -1 3 1 1.16 0.63 0.49 o 0 3 1 90.22 86.76 1.48 o 1 3 1 12.90 18.80 0.37 o 2 3 1 490.26 578.49 5.12 o 3 3 1 126.35 132.37 1.64 o 4 3 1 439.86 435.86 9.36 o 5 3 1 40.69 39.36 3.87 o 6 3 1 3.92 4.03 0.97 o 7 3 1 78.20 80.32 2.83 o 8 3 1 23.11 21.01 1.92 o -7 4 1 2.11 2.44 1.07 o -6 4 1 10.28 11.02 0.70 o -5 4 1 52.43 50.47 1.42 o -4 4 1 162.91 148.94 1.43 o -3 4 1 121.35 121.52 1.38 o -2 4 1 13.17 14.45 0.53 o -1 4 1 11.88 8.45 0.44 o 0 4 1 23.17 28.42 0.70 o 1 4 1 12.87 9.42 0.37 o 2 4 1 1185.62 1333.39 15.66 o 3 4 1 9.59 14.19 0.74 o 4 4 1 83.35 88.05 1.71 o 5 4 1 22.48 24.07 1.21 o 6 4 1 404.82 396.49 3.80 o 7 4 1 2.18 2.17 1.12 o 8 4 1 2.02 2.35 1.85 o -7 5 1 10.65 11.09 1.26 o -6 5 1 124.88 128.25 2.32 o -5 5 1 8.89 7.30 0.67 o -4 5 1 7.64 4.75 0.62 o -3 5 1 393.24 386.53 2.59 o -2 5 1 25.66 23.46 1.18 o -1 5 1 161.69 158.80 2.07 o 0 5 1 13.29 11.84 0.50 o 1 5 1 11.03 12.01 0.57 o 2 5 1 311.83 319.57 2.80 o 3 5 1 192.81 192.99 2.97 o 4 5 1 63.40 76.73 1.40 o 5 5 1 563.82 527.31 12.81 o 6 5 1 0.06 0.00 1.05 o 7 5 1 47.73 44.52 3.78 o 8 5 1 8.84 6.31 1.98 o -6 6 1 5.67 4.62 1.37 o -5 6 1 0.10 0.36 0.78 o -4 6 1 162.77 158.15 1.86 o -3 6 1 4.55 3.61 0.64 o -2 6 1 40.47 37.74 0.98 o -1 6 1 114.56 111.41 1.73 o 0 6 1 77.44 85.03 1.21 o 1 6 1 97.04 101.91 1.76 o 2 6 1 399.77 375.65 2.23 o 3 6 1 95.16 101.58 1.54 o 4 6 1 84.40 79.35 1.51 o 5 6 1 2.12 2.11 0.86 o 6 6 1 56.69 53.27 1.48 o 7 6 1 28.61 27.41 1.61 o -5 7 1 6.05 6.66 1.35 o -4 7 1 2.34 1.73 0.73 o -3 7 1 32.63 34.18 1.09 o -2 7 1 311.79 313.65 2.71 o -1 7 1 9.36 8.36 1.21 o 0 7 1 38.81 38.76 1.03 o 1 7 1 302.90 298.60 4.55 o 2 7 1 105.06 99.64 2.25 o 3 7 1 18.86 19.12 1.63 o 4 7 1 58.56 53.01 4.69 o 5 7 1 28.54 28.50 1.25 o 6 7 1 29.10 24.02 1.72 o 7 7 1 0.74 0.19 0.96 o -4 8 1 52.24 52.15 2.07 o -3 8 1 29.62 27.71 1.15 o -2 8 1 82.92 83.86 1.65 o -1 8 1 223.04 218.68 2.27 o 0 8 1 46.22 50.67 2.17 o 1 8 1 1.35 2.10 0.70 o 2 8 1 1.19 0.95 1.26 o 3 8 1 2.45 2.27 1.25 o 4 8 1 29.48 28.15 2.85 o 5 8 1 35.73 35.72 1.91 o 6 8 1 0.00 0.00 1.78 o -2 9 1 45.70 44.73 1.95 o -1 9 1 0.07 0.00 1.10 o 0 9 1 10.24 10.32 0.94 o 1 9 1 2.66 4.06 1.41 o 2 9 1 34.40 34.58 1.94 o 3 9 1 0.75 0.83 1.33 o -3 -9 2 0.26 1.78 1.69 o -2 -9 2 66.29 70.89 3.65 o -1 -9 2 1.68 1.64 0.87 o 0 -9 2 27.99 30.71 1.39 o 1 -9 2 60.04 63.27 2.15 o 2 -9 2 41.66 39.61 1.91 o -4 -8 2 23.26 25.56 2.27 o -3 -8 2 117.59 121.47 1.77 o -2 -8 2 18.34 16.82 0.95 o -1 -8 2 19.47 20.96 1.01 o 0 -8 2 11.50 11.43 0.91 o 1 -8 2 24.44 23.57 1.05 o 2 -8 2 41.38 40.93 1.52 o 3 -8 2 0.02 0.00 1.05 o 4 -8 2 8.36 6.77 0.97 o -6 -7 2 10.21 8.67 1.87 o -5 -7 2 13.21 14.42 1.81 o -4 -7 2 46.89 44.92 1.48 o -3 -7 2 26.84 26.25 0.97 o -2 -7 2 1.20 1.21 0.69 o -1 -7 2 180.61 183.94 1.90 o 0 -7 2 9.17 7.28 0.76 o 1 -7 2 128.98 119.48 1.63 o 2 -7 2 30.52 29.62 0.73 o 3 -7 2 17.16 18.05 0.81 o 4 -7 2 15.92 16.13 0.87 o 5 -7 2 0.02 0.44 0.90 o -6 -6 2 0.14 0.00 1.57 o -5 -6 2 53.73 55.29 2.42 o -4 -6 2 157.16 156.60 3.39 o -3 -6 2 18.05 17.14 0.77 o -2 -6 2 250.17 267.75 2.35 o -1 -6 2 125.88 127.29 1.47 o 0 -6 2 257.36 241.11 1.95 o 1 -6 2 366.16 364.29 2.14 o 2 -6 2 50.53 50.33 1.06 o 3 -6 2 44.57 43.47 0.94 o 4 -6 2 4.47 4.76 0.68 o 5 -6 2 7.34 7.56 0.79 o 6 -6 2 13.28 11.95 1.03 o -7 -5 2 62.43 64.01 3.05 o -6 -5 2 24.62 21.73 2.14 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1.21 o 7 -1 9 1.26 0.67 0.79 o -4 0 9 101.67 106.67 3.35 o -3 0 9 139.44 150.56 3.31 o -2 0 9 0.00 0.24 0.82 o -1 0 9 209.28 217.36 3.41 o 0 0 9 10.83 8.81 0.81 o 1 0 9 236.45 239.01 4.56 o 2 0 9 14.96 14.69 0.92 o 3 0 9 33.04 33.18 1.01 o 4 0 9 127.84 127.31 2.10 o 5 0 9 276.34 265.11 2.62 o 6 0 9 251.05 249.37 2.18 o 7 0 9 20.96 21.89 1.12 o 8 0 9 13.20 10.28 1.55 o -4 1 9 352.87 365.04 4.36 o -3 1 9 52.19 51.23 1.96 o -2 1 9 43.07 43.98 1.06 o -1 1 9 2.18 3.05 0.63 o 0 1 9 29.04 27.99 0.78 o 1 1 9 1.24 1.69 0.56 o 2 1 9 4.46 4.50 0.60 o 3 1 9 418.48 427.71 5.24 o 4 1 9 140.30 143.54 1.51 o 5 1 9 115.60 120.71 1.63 o 6 1 9 67.11 67.01 1.46 o 7 1 9 57.06 56.18 2.68 o 8 1 9 31.75 33.60 1.91 o -4 2 9 32.72 35.41 1.91 o -3 2 9 3.16 3.90 0.97 o -2 2 9 1.01 0.85 0.63 o -1 2 9 16.26 14.00 0.59 o 0 2 9 53.14 50.25 1.09 o 1 2 9 4.10 3.41 0.62 o 2 2 9 227.37 210.90 2.25 o 3 2 9 9.07 7.32 0.65 o 4 2 9 30.52 30.18 0.83 o 5 2 9 186.48 188.01 4.78 o 6 2 9 0.71 0.55 0.95 o 7 2 9 1.61 1.32 1.07 o 8 2 9 3.63 3.95 1.42 o -3 3 9 35.66 36.86 3.34 o -2 3 9 30.20 28.73 1.32 o -1 3 9 78.86 77.51 1.50 o 0 3 9 20.30 22.92 1.13 o 1 3 9 20.43 18.68 1.03 o 2 3 9 56.86 59.04 1.04 o 3 3 9 3.56 3.08 0.73 o 4 3 9 8.82 7.94 0.92 o 5 3 9 7.66 7.19 0.72 o 6 3 9 5.13 4.87 0.80 o 7 3 9 35.06 36.71 1.50 o -3 4 9 0.01 0.00 0.89 o -2 4 9 114.73 113.80 2.10 o -1 4 9 94.46 101.44 1.61 o 0 4 9 3.86 2.80 0.66 o 1 4 9 122.32 115.26 3.00 o 2 4 9 67.68 71.11 1.48 o 3 4 9 0.07 0.00 0.73 o 4 4 9 33.45 32.29 1.20 o 5 4 9 3.98 4.87 0.94 o 6 4 9 35.19 35.35 1.14 o 7 4 9 8.09 8.63 1.51 o -2 5 9 22.36 21.57 1.65 o -1 5 9 6.05 5.68 1.13 o 0 5 9 34.03 36.10 1.17 o 1 5 9 184.01 181.24 5.18 o 2 5 9 21.63 22.18 1.67 o 3 5 9 5.23 4.30 0.96 o 4 5 9 4.44 4.70 0.99 o 5 5 9 2.35 2.17 0.82 o 6 5 9 78.22 81.62 1.56 o 0 6 9 1.13 1.22 1.01 o 1 6 9 0.96 0.88 1.03 o 2 6 9 32.12 33.37 1.38 o 3 6 9 3.41 2.94 1.05 o 4 6 9 41.70 44.85 2.55 o 5 6 9 30.09 29.43 1.68 o 6 6 9 16.51 18.31 2.95 o 2 7 9 11.69 12.15 1.25 o 3 7 9 19.51 18.55 1.28 o 0 -5 10 0.73 0.60 1.05 o 1 -5 10 131.10 138.70 2.41 o 2 -5 10 25.02 27.54 1.34 o -1 -4 10 11.66 7.50 1.82 o 0 -4 10 312.07 341.80 4.12 o 1 -4 10 8.23 8.73 0.96 o 2 -4 10 3.92 3.42 0.82 o 3 -4 10 291.75 311.58 3.95 o 4 -4 10 17.40 18.51 2.06 o -2 -3 10 0.22 0.40 1.61 o -1 -3 10 32.92 32.21 1.69 o 0 -3 10 51.91 52.90 1.94 o 1 -3 10 18.73 17.41 1.55 o 2 -3 10 61.51 60.93 2.04 o 3 -3 10 2.23 1.44 1.27 o 4 -3 10 0.44 0.00 1.14 o 5 -3 10 22.85 22.02 1.21 o 6 -3 10 0.01 0.00 1.22 o -2 -2 10 3.94 3.57 1.30 o -1 -2 10 66.29 64.27 2.07 o 0 -2 10 14.97 14.85 1.41 o 1 -2 10 5.74 6.47 1.29 o 2 -2 10 2.74 2.19 1.23 o 3 -2 10 0.02 0.00 1.29 o 4 -2 10 28.65 27.25 1.10 o 5 -2 10 1.35 0.96 0.80 o 6 -2 10 0.05 0.36 1.16 o -3 -1 10 27.64 23.80 2.28 o -2 -1 10 51.95 50.44 1.96 o -1 -1 10 99.54 101.09 2.45 o 0 -1 10 36.57 37.10 1.35 o 1 -1 10 0.60 0.44 0.67 o 2 -1 10 0.78 0.37 1.18 o 3 -1 10 38.70 38.77 1.11 o 4 -1 10 47.40 45.74 1.22 o 5 -1 10 123.61 126.25 1.83 o 6 -1 10 76.49 78.28 1.60 o 7 -1 10 0.11 0.00 1.33 o -3 0 10 191.94 193.70 4.32 o -2 0 10 26.96 23.81 2.05 o -1 0 10 16.36 18.03 1.01 o 0 0 10 94.28 96.50 1.56 o 1 0 10 7.51 7.37 0.80 o 2 0 10 75.69 70.79 1.99 o 3 0 10 79.62 85.76 1.69 o 4 0 10 110.66 110.01 2.07 o 5 0 10 131.94 132.80 1.84 o 6 0 10 20.88 19.73 1.28 o 7 0 10 0.12 0.94 1.35 o -2 1 10 6.54 7.42 1.16 o -1 1 10 120.43 125.88 3.09 o 0 1 10 0.13 0.52 0.77 o 1 1 10 116.29 113.12 1.32 o 2 1 10 5.71 5.33 0.64 o 3 1 10 42.30 41.83 1.00 o 4 1 10 37.98 35.55 0.90 o 5 1 10 101.24 103.50 1.68 o 6 1 10 113.63 118.74 2.15 o 7 1 10 5.84 5.92 1.45 o -3 2 10 91.50 99.78 2.50 o -2 2 10 72.37 73.36 1.56 o -1 2 10 0.06 0.00 1.01 o 0 2 10 85.44 80.29 2.03 o 1 2 10 117.88 127.98 1.92 o 2 2 10 17.90 14.65 0.76 o 3 2 10 52.27 54.73 1.05 o 4 2 10 37.54 35.47 0.94 o 5 2 10 72.98 72.76 2.01 o 6 2 10 9.93 9.46 1.17 o 7 2 10 1.47 0.32 1.43 o -2 3 10 21.91 21.86 1.73 o -1 3 10 43.82 40.11 1.19 o 0 3 10 92.20 98.15 1.53 o 1 3 10 67.59 66.96 1.30 o 2 3 10 47.04 47.05 1.04 o 3 3 10 2.45 1.90 0.67 o 4 3 10 28.18 26.80 1.02 o 5 3 10 23.12 23.93 1.01 o 6 3 10 0.67 0.92 0.93 o 7 3 10 6.00 8.15 1.49 o -1 4 10 15.20 15.58 1.12 o 0 4 10 60.76 60.72 1.35 o 1 4 10 4.01 3.47 0.83 o 2 4 10 13.71 14.90 1.39 o 3 4 10 12.22 11.11 1.47 o 4 4 10 21.64 21.19 1.29 o 5 4 10 16.23 13.72 0.99 o 6 4 10 7.61 7.16 1.07 o 0 5 10 5.83 5.54 1.07 o 1 5 10 23.29 24.77 1.35 o 2 5 10 75.89 76.46 1.71 o 3 5 10 24.03 25.35 1.30 o 4 5 10 43.88 45.31 1.59 o 5 5 10 36.05 37.12 1.41 o 2 6 10 130.44 134.31 3.96 o 3 6 10 21.06 21.98 1.99 o 4 6 10 0.09 0.18 1.09 o 1 -4 11 39.98 40.40 1.88 o 0 -2 11 30.45 26.51 1.72 o 1 -2 11 5.23 4.70 1.33 o 2 -2 11 0.04 0.00 1.37 o 3 -2 11 0.65 1.11 1.31 o 5 -2 11 91.10 94.30 2.35 o -1 -1 11 29.89 25.17 2.47 o 0 -1 11 57.00 52.94 2.44 o 1 -1 11 0.88 0.61 1.25 o 2 -1 11 53.74 55.69 2.03 o 3 -1 11 31.55 32.85 1.82 o 4 -1 11 46.49 43.22 1.28 o 5 -1 11 19.56 16.33 1.44 o 6 -1 11 0.55 0.19 1.28 o -1 0 11 142.25 139.64 3.98 o 0 0 11 166.40 171.46 3.46 o 1 0 11 1.75 1.61 0.80 o 2 0 11 41.09 39.31 1.17 o 3 0 11 0.23 0.00 0.82 o 4 0 11 16.83 17.22 1.03 o 5 0 11 12.20 11.05 1.10 o 6 0 11 63.50 61.40 2.18 o -1 1 11 100.59 102.27 2.58 o 0 1 11 59.69 63.23 2.66 o 1 1 11 4.80 4.33 0.88 o 2 1 11 72.67 77.80 1.68 o 3 1 11 54.59 55.98 1.35 o 4 1 11 0.05 0.16 0.86 o 5 1 11 235.07 234.19 2.87 o 6 1 11 1.24 1.01 1.30 o -1 2 11 68.29 71.55 2.33 o 0 2 11 0.05 0.00 1.06 o 1 2 11 26.73 24.11 1.17 o 2 2 11 215.58 226.56 2.31 o 3 2 11 0.32 0.00 0.71 o 4 2 11 73.77 75.49 1.49 o 5 2 11 4.32 4.70 1.37 o 6 2 11 29.48 29.21 1.83 o -1 3 11 0.26 0.60 1.35 o 0 3 11 15.14 15.28 1.08 o 1 3 11 273.00 276.36 3.19 o 2 3 11 55.82 55.79 1.49 o 3 3 11 1.24 0.42 0.82 o 4 3 11 3.30 3.03 0.84 o 5 3 11 1.26 1.81 0.98 o 6 3 11 0.46 1.57 0.96 o 0 4 11 30.22 32.85 1.39 o 1 4 11 3.47 2.55 1.00 o 2 4 11 12.65 12.82 1.41 o 3 4 11 22.72 21.21 1.24 o 4 4 11 0.03 0.35 1.01 o 5 4 11 16.78 15.43 1.18 o 0 0 12 1.41 0.00 1.27 o 1 0 12 46.61 46.83 1.83 o 3 0 12 10.03 9.37 1.27 o 4 0 12 82.27 90.42 2.36 o 0 1 12 124.98 124.04 2.82 o 1 1 12 37.99 37.09 1.78 o 2 1 12 0.04 0.10 0.82 o 3 1 12 66.17 69.24 1.49 o 4 1 12 60.48 59.45 2.11 o 5 1 12 8.65 8.46 1.43 o 1 2 12 4.85 4.71 0.94 o 2 2 12 203.13 217.59 2.45 o 3 2 12 0.16 0.00 0.90 o 4 2 12 23.38 23.45 1.16 o 2 3 12 56.38 58.40 1.57 o 3 3 12 0.45 0.76 1.02 o