#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:19:31 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180849 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/80/2018097.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018097_Fobs loop_ _publ_author_name 'Nalla, Sowjanya' 'Bond, Marcus R.' _publ_section_title ; [CuCl~3~(H~2~O)]^{-^} complexes aggregated to form hydrate columns in methyl-substituted pyridinium or piperidinium salts ; _journal_coeditor_code BM3105 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m185 _journal_page_last m194 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.927 _cell_angle_gamma 90.000 _cell_length_a 10.1958 _cell_length_b 7.6080 _cell_length_c 16.3281 _exptl_crystal_F_000 620.00 _reflns_d_resolution_high 0.7398 _cod_data_source_file bm3105IV100Ksup8.hkl _cod_data_source_block IV100K #BEGIN Tags that were not found in dictionaries: _shelx_title ' bond114 in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 214.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10210.13 9908.08 199.04 o 3 0 0 442.38 486.01 14.87 o 4 0 0 360.19 346.00 10.50 o 5 0 0 4476.73 4413.64 89.45 o 6 0 0 9896.10 9940.63 191.27 o 7 0 0 2564.21 2691.15 75.48 o 8 0 0 24.67 18.14 6.60 o 9 0 0 299.49 311.04 13.56 o 10 0 0 2130.77 2254.38 65.26 o 11 0 0 618.17 596.76 27.88 o 12 0 0 301.25 278.01 24.90 o 13 0 0 331.43 233.46 68.51 o 2 1 0 11410.66 10849.82 153.63 o 3 1 0 1173.22 1115.66 20.04 o 4 1 0 7543.21 7444.91 101.89 o 5 1 0 3815.55 3669.13 54.54 o 6 1 0 3.40 -2.04 4.73 o 7 1 0 135.97 152.01 7.31 o 8 1 0 1783.20 1935.88 47.59 o 9 1 0 1977.88 2064.75 39.28 o 10 1 0 164.77 159.13 24.33 o 11 1 0 1240.99 1296.56 52.46 o 12 1 0 135.41 168.80 26.12 o 13 1 0 11.53 22.10 20.74 o 0 2 0 508.46 643.68 15.99 o 1 2 0 327.50 268.26 6.20 o 2 2 0 1280.40 1198.34 26.64 o 3 2 0 1629.63 1484.38 24.91 o 4 2 0 741.63 629.24 12.57 o 5 2 0 3202.72 3451.48 53.62 o 6 2 0 1616.16 1620.50 28.61 o 7 2 0 6616.11 7005.08 103.52 o 8 2 0 60.45 72.42 17.73 o 9 2 0 1741.57 1818.66 36.59 o 10 2 0 167.24 143.33 10.73 o 11 2 0 160.03 119.85 13.71 o 12 2 0 215.94 195.13 28.04 o 13 2 0 850.86 700.85 46.23 o 1 3 0 1473.03 1468.16 48.94 o 2 3 0 2792.24 2663.63 40.72 o 3 3 0 24.75 33.50 13.19 o 4 3 0 982.18 949.60 19.68 o 5 3 0 31.64 39.19 5.16 o 6 3 0 1399.78 1406.11 25.06 o 7 3 0 27.21 22.33 17.32 o 8 3 0 1410.48 1435.35 25.88 o 9 3 0 143.33 151.39 35.47 o 10 3 0 497.96 480.84 18.30 o 11 3 0 34.49 39.14 14.63 o 12 3 0 0.71 34.46 26.39 o 0 4 0 6261.43 5833.18 150.89 o 1 4 0 977.49 929.09 32.26 o 2 4 0 103.44 158.96 143.52 o 3 4 0 3238.11 3193.17 50.79 o 4 4 0 2559.16 2626.39 49.78 o 5 4 0 603.16 586.07 14.04 o 6 4 0 65.22 77.71 19.79 o 7 4 0 143.06 124.50 9.90 o 8 4 0 48.95 43.40 16.49 o 9 4 0 422.07 364.88 17.74 o 10 4 0 48.13 44.63 13.61 o 11 4 0 37.79 9.29 15.13 o 12 4 0 60.09 67.68 20.21 o 1 5 0 566.36 527.69 12.53 o 2 5 0 1817.72 1780.60 47.43 o 3 5 0 874.02 827.64 23.08 o 4 5 0 1916.22 1913.82 49.98 o 5 5 0 822.65 834.22 19.18 o 6 5 0 1480.26 1507.31 35.88 o 7 5 0 124.68 151.95 29.28 o 8 5 0 2396.80 2417.04 48.54 o 9 5 0 384.78 347.41 19.19 o 10 5 0 463.17 382.96 21.55 o 11 5 0 109.81 89.54 17.45 o 0 6 0 3429.07 3395.95 76.42 o 1 6 0 1482.08 1467.67 24.76 o 2 6 0 14.54 38.80 47.41 o 3 6 0 551.03 534.65 17.39 o 4 6 0 144.34 131.32 37.12 o 5 6 0 320.28 308.76 42.08 o 6 6 0 566.91 558.56 23.13 o 7 6 0 345.94 333.94 10.37 o 8 6 0 35.70 54.18 14.80 o 9 6 0 245.83 211.87 26.02 o 10 6 0 325.13 283.83 27.19 o 1 7 0 3793.18 3984.73 91.75 o 2 7 0 1020.48 1105.36 35.50 o 3 7 0 25.17 68.69 47.83 o 4 7 0 114.34 140.85 14.85 o 5 7 0 629.17 654.55 28.79 o 6 7 0 406.87 480.13 25.72 o 7 7 0 308.03 274.51 46.61 o 8 7 0 5.45 66.68 20.80 o 9 7 0 1216.89 1176.71 61.44 o 0 8 0 788.33 893.08 72.66 o 1 8 0 5.56 -11.02 11.54 o 2 8 0 1155.73 1176.60 131.77 o 3 8 0 1703.10 1835.19 87.23 o 4 8 0 1381.15 1474.10 53.71 o 5 8 0 7.79 38.91 17.08 o 6 8 0 820.35 759.85 37.75 o 7 8 0 3.78 2.47 37.52 o 8 8 0 12.85 56.99 51.54 o 1 9 0 3.82 4.95 31.33 o 2 9 0 480.39 521.94 37.55 o 3 9 0 84.50 59.51 49.48 o 4 9 0 290.33 247.53 33.82 o 5 9 0 663.69 649.18 42.56 o 6 9 0 856.24 855.12 89.99 o 0 10 0 20.09 93.18 54.43 o 1 10 0 505.87 435.68 54.63 o 2 10 0 342.72 294.51 46.29 o 3 10 0 179.61 205.64 30.07 o -13 1 1 582.29 501.78 42.50 o -12 1 1 753.50 685.33 35.23 o -11 1 1 546.99 549.55 30.12 o -10 1 1 229.65 207.74 18.56 o -9 1 1 789.96 829.13 18.20 o -8 1 1 1472.98 1524.61 28.98 o -7 1 1 3347.38 3583.69 61.74 o -6 1 1 2271.88 2172.07 34.42 o -5 1 1 3458.52 3288.82 50.01 o -4 1 1 687.24 684.49 13.40 o -3 1 1 241.62 253.19 8.64 o -2 1 1 4137.54 4340.66 62.05 o 0 1 1 3.76 -1.65 1.65 o 1 1 1 9543.79 9189.08 265.04 o 2 1 1 2007.34 1953.17 32.71 o 3 1 1 25345.84 26621.44 529.76 o 4 1 1 11.81 36.67 11.13 o 5 1 1 3423.02 3488.76 51.37 o 6 1 1 1825.57 1888.49 34.69 o 7 1 1 1645.80 1705.79 28.10 o 8 1 1 2913.86 3045.02 52.22 o 9 1 1 279.06 277.54 11.08 o 10 1 1 1315.66 1282.69 29.57 o 11 1 1 35.03 43.10 17.32 o 12 1 1 223.84 196.31 38.77 o 13 1 1 69.02 39.53 23.09 o -13 2 1 18.05 4.33 36.28 o -12 2 1 420.75 415.35 28.47 o -11 2 1 37.43 45.52 19.79 o -10 2 1 1477.64 1525.21 119.86 o -9 2 1 175.17 173.03 13.61 o -8 2 1 428.79 443.42 44.15 o -7 2 1 3290.89 3441.90 58.98 o -6 2 1 1905.09 1803.29 34.92 o -5 2 1 643.67 594.90 12.81 o -4 2 1 2550.48 2422.78 69.46 o -3 2 1 289.77 303.50 7.89 o -2 2 1 344.07 325.16 10.32 o -1 2 1 3424.25 3023.58 74.81 o 0 2 1 6553.31 6060.62 89.92 o 1 2 1 0.31 3.30 4.08 o 2 2 1 56.66 40.21 6.60 o 3 2 1 553.99 512.49 11.32 o 4 2 1 5295.23 5405.60 85.62 o 5 2 1 2370.71 2350.07 40.81 o 6 2 1 4258.37 4403.90 67.94 o 7 2 1 3.25 7.70 6.64 o 8 2 1 55.74 62.73 20.62 o 9 2 1 1159.45 1243.39 27.35 o 10 2 1 377.77 397.30 34.65 o 11 2 1 187.49 189.77 13.95 o 12 2 1 78.88 54.62 27.47 o 13 2 1 33.56 49.48 39.58 o -12 3 1 2587.77 2744.75 91.70 o -11 3 1 161.34 198.75 41.24 o -10 3 1 12.08 -12.97 12.97 o -9 3 1 93.24 128.74 10.54 o -8 3 1 572.58 559.16 42.93 o -7 3 1 315.15 342.37 11.13 o -6 3 1 1045.72 1063.89 20.52 o -5 3 1 2521.27 2639.61 46.11 o -4 3 1 2167.37 1993.75 51.45 o -3 3 1 3785.40 3655.54 77.65 o -2 3 1 18715.88 18261.95 273.99 o -1 3 1 3442.68 3264.02 50.53 o 0 3 1 93.11 125.50 4.54 o 1 3 1 4699.04 4396.15 91.78 o 2 3 1 1220.99 1123.48 25.67 o 3 3 1 16545.02 17060.18 381.28 o 4 3 1 8097.01 7658.41 248.41 o 5 3 1 560.27 516.74 12.51 o 6 3 1 796.23 825.63 30.98 o 7 3 1 83.84 100.84 7.55 o 8 3 1 499.15 530.48 14.37 o 9 3 1 0.47 5.11 21.03 o 10 3 1 262.95 234.68 48.26 o 11 3 1 445.10 414.14 20.91 o 12 3 1 320.66 225.76 58.16 o -12 4 1 60.81 4.03 22.72 o -11 4 1 618.27 655.33 32.29 o -10 4 1 171.96 201.88 28.46 o -9 4 1 277.05 267.43 14.09 o -8 4 1 308.49 311.42 18.98 o -7 4 1 1395.81 1409.69 35.14 o -6 4 1 6.94 25.40 5.94 o -5 4 1 295.80 309.72 9.74 o -4 4 1 1812.51 1721.55 33.26 o -3 4 1 12469.29 12454.22 192.52 o -2 4 1 306.20 277.53 10.73 o -1 4 1 5487.83 5242.06 105.63 o 0 4 1 7556.08 7696.93 145.12 o 1 4 1 772.15 720.76 24.14 o 2 4 1 9360.80 8910.23 166.56 o 3 4 1 4792.93 4739.84 97.24 o 4 4 1 849.63 841.38 33.05 o 5 4 1 1496.55 1500.65 45.92 o 6 4 1 1907.36 1950.92 36.92 o 7 4 1 1431.36 1398.63 29.32 o 8 4 1 372.10 357.87 32.18 o 9 4 1 263.58 225.03 10.32 o 10 4 1 138.23 139.77 14.49 o 11 4 1 137.62 150.04 18.98 o 12 4 1 1672.46 1775.28 97.50 o -11 5 1 23.47 45.72 16.23 o -10 5 1 213.17 238.13 21.79 o -9 5 1 1707.76 1761.39 70.69 o -8 5 1 2062.02 2176.40 43.91 o -7 5 1 86.48 87.59 21.03 o -6 5 1 1638.71 1703.46 36.61 o -5 5 1 1619.58 1735.34 31.28 o -4 5 1 29.53 38.17 14.02 o -3 5 1 1558.45 1541.57 35.92 o -2 5 1 954.71 913.31 22.57 o -1 5 1 26.94 21.23 4.73 o 0 5 1 3017.97 2972.23 49.45 o 1 5 1 4956.29 4881.67 139.39 o 2 5 1 3353.68 3290.94 72.39 o 3 5 1 331.22 293.32 22.69 o 4 5 1 1104.42 1158.18 36.48 o 5 5 1 168.12 155.66 5.46 o 6 5 1 889.28 842.73 19.41 o 7 5 1 2337.57 2594.33 94.39 o 8 5 1 1668.65 1685.62 48.78 o 9 5 1 42.27 54.43 15.63 o 10 5 1 542.23 515.49 29.97 o 11 5 1 364.92 334.44 24.40 o -11 6 1 1.74 -7.69 40.82 o -10 6 1 532.81 474.51 24.68 o -9 6 1 0.42 28.94 22.54 o -8 6 1 491.17 496.34 23.51 o -7 6 1 1424.95 1523.65 48.77 o -6 6 1 3254.87 3311.83 68.96 o -5 6 1 2134.74 2078.19 56.71 o -4 6 1 1475.81 1472.94 46.67 o -3 6 1 3106.59 3116.68 82.41 o -2 6 1 146.02 131.11 6.34 o -1 6 1 1129.28 1147.22 25.21 o 0 6 1 1129.02 1175.61 33.89 o 1 6 1 32.23 5.21 23.09 o 2 6 1 80.75 77.17 8.80 o 3 6 1 189.43 183.23 18.15 o 4 6 1 655.18 692.54 24.52 o 5 6 1 313.32 286.18 42.49 o 6 6 1 2007.52 2096.80 64.16 o 7 6 1 0.62 -4.76 12.88 o 8 6 1 304.35 262.99 14.56 o 9 6 1 648.16 605.59 54.06 o 10 6 1 127.14 102.30 18.97 o -9 7 1 10.44 -10.83 19.80 o -8 7 1 14.58 -22.81 22.81 o -7 7 1 2.84 59.41 19.49 o -6 7 1 31.31 22.54 22.68 o -5 7 1 207.88 165.82 17.87 o -4 7 1 66.18 76.39 51.54 o -3 7 1 14.37 6.23 17.73 o -2 7 1 407.48 383.78 15.38 o -1 7 1 651.78 687.48 54.08 o 0 7 1 5.39 16.35 15.25 o 1 7 1 264.97 246.52 32.17 o 2 7 1 49.01 33.68 10.72 o 3 7 1 47.62 68.18 20.62 o 4 7 1 1239.89 1318.13 45.40 o 5 7 1 566.34 541.06 26.61 o 6 7 1 13.78 23.26 15.06 o 7 7 1 42.42 27.90 16.73 o 8 7 1 15.48 6.88 42.47 o 9 7 1 54.92 116.61 26.85 o -8 8 1 182.01 157.81 29.60 o -7 8 1 205.65 226.12 28.71 o -6 8 1 170.86 130.35 20.88 o -5 8 1 244.89 184.17 29.70 o -4 8 1 76.76 106.53 17.05 o -3 8 1 466.16 419.59 17.96 o -2 8 1 119.60 135.12 19.79 o -1 8 1 159.27 160.10 10.43 o 0 8 1 96.96 71.32 10.31 o 1 8 1 149.43 138.22 18.56 o 2 8 1 493.27 458.73 35.07 o 3 8 1 18.08 11.29 28.86 o 4 8 1 1102.36 1126.11 42.53 o 5 8 1 26.91 33.20 50.71 o 6 8 1 320.59 297.83 76.72 o 7 8 1 276.79 235.55 28.16 o 8 8 1 131.81 119.72 43.71 o -6 9 1 296.97 314.09 61.87 o -5 9 1 701.98 437.46 50.54 o -4 9 1 206.17 191.67 42.48 o -3 9 1 159.22 167.11 22.03 o -2 9 1 86.10 64.84 16.74 o -1 9 1 479.09 503.98 70.14 o 0 9 1 34.10 17.79 12.95 o 1 9 1 4.26 14.31 53.19 o 2 9 1 130.67 144.71 46.19 o 3 9 1 0.14 -18.25 46.59 o 4 9 1 548.43 548.99 37.28 o 5 9 1 1195.41 1198.95 59.04 o 6 9 1 6.04 29.15 29.50 o -3 10 1 1266.98 1115.94 117.82 o -2 10 1 54.82 75.04 37.94 o -1 10 1 312.43 306.05 49.59 o 0 10 1 153.79 188.04 40.46 o 1 10 1 77.97 97.31 38.77 o 2 10 1 676.03 595.08 58.90 o -13 0 2 227.93 225.18 41.30 o -12 0 2 198.03 215.28 27.30 o -11 0 2 1016.79 970.47 37.61 o -10 0 2 17.57 2.47 16.49 o -9 0 2 9514.87 10354.76 196.55 o -8 0 2 178.32 175.70 11.68 o -7 0 2 2063.46 2138.87 45.16 o -6 0 2 11967.19 12544.39 260.49 o -5 0 2 175.20 150.16 9.20 o -4 0 2 422.63 359.32 12.11 o -3 0 2 176.38 173.33 7.63 o -2 0 2 10238.92 9936.42 226.08 o 1 0 2 327.54 479.68 26.08 o 2 0 2 11979.79 11947.13 242.74 o 3 0 2 2408.12 2311.08 46.21 o 4 0 2 202.66 184.02 7.65 o 5 0 2 6366.85 6212.35 130.81 o 6 0 2 926.73 952.19 25.03 o 7 0 2 1037.66 1052.97 33.13 o 8 0 2 127.24 127.02 12.44 o 9 0 2 4299.15 4516.57 114.03 o 10 0 2 1058.96 1061.46 46.66 o 11 0 2 319.74 384.45 47.18 o 12 0 2 299.12 263.16 27.35 o 13 0 2 411.56 328.37 74.33 o -13 1 2 481.80 456.83 27.32 o -12 1 2 412.78 406.77 19.75 o -11 1 2 1.14 -2.70 9.50 o -10 1 2 517.37 533.55 18.45 o -9 1 2 769.60 823.27 19.21 o -8 1 2 764.21 808.20 18.77 o -7 1 2 172.73 177.74 8.78 o -6 1 2 6210.99 6382.27 92.38 o -5 1 2 934.65 805.61 15.96 o -4 1 2 953.98 975.78 29.38 o -3 1 2 1509.83 1441.23 25.34 o -2 1 2 12239.61 12131.23 158.38 o -1 1 2 7.30 24.93 9.07 o 1 1 2 4066.63 3814.04 50.93 o 2 1 2 391.02 413.28 7.85 o 3 1 2 3054.82 2730.03 45.95 o 4 1 2 5581.22 5268.22 73.36 o 5 1 2 719.43 765.46 15.24 o 6 1 2 2757.33 2850.53 47.02 o 7 1 2 1484.87 1582.97 26.97 o 8 1 2 69.16 63.24 7.83 o 9 1 2 32.05 41.18 8.09 o 10 1 2 979.68 937.90 27.40 o 11 1 2 329.57 301.45 25.42 o 12 1 2 12.74 39.48 54.42 o 13 1 2 261.68 275.51 56.16 o -13 2 2 104.13 123.45 27.36 o -12 2 2 45.11 33.98 32.99 o -11 2 2 692.21 672.67 56.96 o -10 2 2 2190.42 2273.81 173.81 o -9 2 2 1409.29 1474.65 31.42 o -8 2 2 2258.53 2469.33 43.85 o -7 2 2 869.87 892.93 26.03 o -6 2 2 184.70 175.85 7.25 o -5 2 2 2325.08 2298.71 36.72 o -4 2 2 15727.21 16432.25 372.08 o -3 2 2 1208.57 1220.76 20.15 o -2 2 2 20083.57 19849.12 290.11 o -1 2 2 92.84 51.64 8.25 o 0 2 2 705.17 656.19 12.00 o 1 2 2 14263.07 14347.48 200.07 o 2 2 2 656.81 642.99 13.23 o 3 2 2 1298.74 1313.56 23.77 o 4 2 2 6424.94 6729.95 100.26 o 5 2 2 6253.03 6311.94 83.25 o 6 2 2 11233.07 11852.34 172.56 o 7 2 2 1125.77 1247.69 27.28 o 8 2 2 1571.26 1686.55 38.42 o 9 2 2 118.86 98.26 10.80 o 10 2 2 592.99 603.19 24.35 o 11 2 2 836.85 850.24 36.12 o 12 2 2 594.23 536.39 33.60 o -13 3 2 137.80 281.57 55.67 o -12 3 2 34.98 52.93 44.94 o -11 3 2 15.89 15.50 21.03 o -10 3 2 151.47 149.63 21.03 o -9 3 2 602.77 614.48 78.01 o -8 3 2 1252.25 1342.43 26.59 o -7 3 2 853.32 925.10 48.74 o -6 3 2 447.04 434.20 14.34 o -5 3 2 2.45 -7.01 7.01 o -4 3 2 330.06 334.82 9.07 o -3 3 2 4089.67 3841.66 106.55 o -2 3 2 4.99 -0.41 4.54 o -1 3 2 149.22 140.44 12.38 o 0 3 2 3387.15 3381.31 81.88 o 1 3 2 562.00 550.88 16.53 o 2 3 2 1043.85 1069.50 28.07 o 3 3 2 290.51 270.51 7.40 o 4 3 2 1306.47 1392.60 25.39 o 5 3 2 978.45 978.18 19.66 o 6 3 2 13.63 22.25 14.84 o 7 3 2 2012.35 2153.62 32.92 o 8 3 2 163.97 142.82 9.49 o 9 3 2 459.02 407.57 23.93 o 10 3 2 1.04 27.38 11.28 o 11 3 2 60.15 92.89 20.48 o 12 3 2 8.12 1.92 19.72 o -12 4 2 78.51 40.64 28.86 o -11 4 2 51.94 36.67 24.74 o -10 4 2 699.57 725.32 32.19 o -9 4 2 1315.96 1430.67 37.43 o -8 4 2 29.83 -2.07 9.90 o -7 4 2 137.48 134.87 13.61 o -6 4 2 1770.92 1830.65 57.11 o -5 4 2 1312.16 1302.90 85.19 o -4 4 2 397.00 423.76 31.37 o -3 4 2 53.83 52.26 6.18 o -2 4 2 14.97 31.43 10.31 o -1 4 2 1095.89 1022.01 28.54 o 0 4 2 358.56 412.45 24.76 o 1 4 2 978.12 959.03 24.46 o 2 4 2 4.67 12.81 9.07 o 3 4 2 218.12 175.44 25.16 o 4 4 2 393.39 385.39 10.32 o 5 4 2 0.45 -4.12 9.07 o 6 4 2 1484.76 1514.21 28.35 o 7 4 2 312.75 285.82 13.20 o 8 4 2 69.26 73.69 7.29 o 9 4 2 89.72 63.05 8.76 o 10 4 2 358.35 354.73 25.16 o 11 4 2 144.75 132.12 30.52 o 12 4 2 33.50 65.97 44.53 o -11 5 2 66.70 51.33 25.48 o -10 5 2 197.87 170.21 28.04 o -9 5 2 1186.77 1205.15 34.06 o -8 5 2 718.05 738.47 21.00 o -7 5 2 1132.30 1168.06 27.27 o -6 5 2 481.48 471.12 31.78 o -5 5 2 314.33 293.69 28.47 o -4 5 2 33.94 28.57 10.31 o -3 5 2 2233.57 2256.45 46.06 o -2 5 2 198.87 185.83 7.01 o -1 5 2 688.01 696.60 20.40 o 0 5 2 1909.85 1902.53 32.73 o 1 5 2 219.17 236.94 15.26 o 2 5 2 312.34 301.38 13.27 o 3 5 2 422.07 417.73 16.09 o 4 5 2 83.64 94.62 18.56 o 5 5 2 2076.33 2106.61 50.50 o 6 5 2 1.99 0.87 5.34 o 7 5 2 2914.88 3147.65 82.88 o 8 5 2 66.91 69.09 16.08 o 9 5 2 496.74 538.82 26.24 o 10 5 2 2.19 -23.50 23.50 o 11 5 2 1.26 2.66 19.31 o -11 6 2 124.57 111.50 18.78 o -10 6 2 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