#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:20:17 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180851 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/82/2018220.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018220_Fobs loop_ _publ_author_name 'Collas, Alain' 'Blockhuys, Frank' _publ_section_title ; (E)-4-[2-(3,4,5-Trimethoxyphenyl)ethenyl]nitrobenzene and its `bridge-flipped' analogues ; _journal_coeditor_code FA3256 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o364 _journal_page_last o369 _journal_volume 67 _journal_year 2011 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.2150 _cell_length_b 14.4290 _cell_length_c 14.5950 _exptl_crystal_F_000 664.00 _reflns_d_resolution_high 0.8311 _cod_data_source_file fa3256IIIsup4.hkl _cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' 345mcn4n in P -1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 242.37 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 58743.33 67527.91 813.86 o 4 0 0 596.55 624.68 8.94 o 6 0 0 9.75 10.28 1.71 o 8 0 0 0.43 -4.14 4.45 o 1 1 0 350.33 286.00 5.21 o 2 1 0 20413.79 19901.41 25.62 o 3 1 0 42.30 43.43 0.88 o 4 1 0 1192.92 1165.31 12.20 o 5 1 0 3.04 2.38 1.44 o 6 1 0 96.29 100.06 3.05 o 7 1 0 0.00 -0.73 3.83 o 8 1 0 10.54 11.91 2.39 o 0 2 0 334.63 495.71 16.86 o 1 2 0 8246.14 10202.41 1003.07 o 2 2 0 3142.89 2937.64 97.18 o 3 2 0 396.33 359.95 4.29 o 4 2 0 228.20 211.72 5.55 o 5 2 0 48.73 41.63 1.81 o 6 2 0 0.81 -0.59 3.54 o 7 2 0 3.35 0.51 2.00 o 8 2 0 0.16 -1.50 4.65 o 1 3 0 623.72 758.84 34.51 o 2 3 0 1508.04 1572.34 31.63 o 3 3 0 117.13 116.69 2.35 o 4 3 0 9.22 10.98 1.24 o 5 3 0 89.68 86.53 2.52 o 6 3 0 7.21 8.36 1.76 o 7 3 0 60.81 54.30 2.67 o 8 3 0 5.42 3.99 2.36 o 0 4 0 11787.96 16791.30 217.85 o 1 4 0 453.77 554.75 15.54 o 2 4 0 0.62 2.69 3.13 o 3 4 0 216.11 233.95 5.28 o 4 4 0 868.30 788.46 10.84 o 5 4 0 480.09 483.38 9.78 o 6 4 0 88.13 81.75 2.63 o 7 4 0 121.23 129.34 3.99 o 8 4 0 6.33 0.62 4.68 o 1 5 0 285.65 320.63 17.14 o 2 5 0 1831.70 2060.93 257.27 o 3 5 0 182.00 212.12 5.38 o 4 5 0 12.09 11.24 1.40 o 5 5 0 170.99 154.58 4.94 o 6 5 0 71.79 60.91 2.52 o 7 5 0 4.62 4.17 1.92 o 8 5 0 15.08 13.97 2.58 o 0 6 0 1352.12 1728.75 8.63 o 1 6 0 148.47 159.55 9.09 o 2 6 0 124.78 144.29 16.17 o 3 6 0 251.21 284.09 6.50 o 4 6 0 20.53 20.14 1.51 o 5 6 0 3.99 2.63 1.55 o 6 6 0 29.92 27.11 2.12 o 7 6 0 2.25 0.00 4.03 o 8 6 0 0.98 1.99 2.42 o 1 7 0 20.06 29.28 0.82 o 2 7 0 77.50 114.35 4.94 o 3 7 0 9.44 8.43 1.20 o 4 7 0 208.10 191.96 5.57 o 5 7 0 9.29 7.52 1.63 o 6 7 0 4.54 1.69 1.89 o 7 7 0 11.15 10.56 2.14 o 0 8 0 35.06 36.89 0.97 o 1 8 0 48.42 57.47 3.05 o 2 8 0 58.64 53.51 1.19 o 3 8 0 35.44 39.81 1.69 o 4 8 0 100.02 117.02 3.71 o 5 8 0 12.70 12.23 1.86 o 6 8 0 24.64 21.19 2.23 o 7 8 0 10.54 8.82 2.27 o 1 9 0 274.72 314.67 7.85 o 2 9 0 496.00 645.37 27.99 o 3 9 0 246.90 299.64 7.56 o 4 9 0 51.63 55.45 2.18 o 5 9 0 48.16 47.34 2.30 o 6 9 0 10.10 8.10 2.19 o 7 9 0 2.09 -1.50 4.43 o 0 10 0 1182.42 1397.23 13.71 o 1 10 0 129.72 167.46 3.98 o 2 10 0 187.15 250.61 7.27 o 3 10 0 12.80 15.72 1.53 o 4 10 0 55.77 53.88 2.43 o 5 10 0 12.25 8.03 1.98 o 6 10 0 40.40 30.50 2.51 o 7 10 0 20.46 19.65 2.73 o 1 11 0 14.61 18.47 1.13 o 2 11 0 7.03 8.02 1.15 o 3 11 0 87.42 94.46 2.61 o 4 11 0 31.93 38.71 2.25 o 5 11 0 1.77 3.89 1.97 o 6 11 0 0.68 -1.17 4.42 o 0 12 0 112.80 133.63 4.50 o 1 12 0 181.68 193.89 14.39 o 2 12 0 83.08 100.05 8.79 o 3 12 0 326.99 358.29 9.87 o 4 12 0 0.86 0.84 1.98 o 5 12 0 132.22 125.28 4.00 o 6 12 0 8.34 6.06 2.38 o 1 13 0 26.43 27.75 1.60 o 2 13 0 715.21 840.20 54.23 o 3 13 0 121.37 112.49 3.24 o 4 13 0 373.37 431.02 11.94 o 5 13 0 151.98 142.59 4.12 o 0 14 0 176.55 198.34 4.18 o 1 14 0 1.94 -1.69 1.69 o 2 14 0 0.13 1.90 1.88 o 3 14 0 3.12 3.53 1.92 o 4 14 0 219.49 240.82 6.81 o 5 14 0 8.06 2.47 2.43 o 1 15 0 0.19 2.06 2.63 o 2 15 0 8.06 7.27 1.48 o 3 15 0 10.59 13.95 2.14 o 4 15 0 66.89 73.19 3.33 o 0 16 0 48.43 50.70 1.88 o 1 16 0 33.36 35.93 1.69 o 2 16 0 25.23 28.57 1.69 o 3 16 0 13.35 10.44 2.12 o 1 17 0 4.62 4.45 1.51 o 1 0 1 1285.44 1133.73 27.57 o 2 0 1 19.79 23.32 1.02 o 3 0 1 2189.26 1993.37 10.72 o 4 0 1 84.76 90.16 2.13 o 5 0 1 384.48 348.84 9.82 o 6 0 1 69.07 66.42 2.78 o 7 0 1 0.94 0.49 3.29 o 8 0 1 8.04 9.13 1.65 o 0 1 1 709.90 663.97 34.19 o 1 1 1 1520.33 1315.49 35.11 o 2 1 1 9875.39 9158.62 37.96 o 3 1 1 872.60 786.53 7.41 o 4 1 1 1274.81 1132.37 8.48 o 5 1 1 243.85 217.27 4.12 o 6 1 1 23.30 19.50 1.35 o 7 1 1 32.83 30.70 2.30 o 8 1 1 0.56 -0.75 3.18 o 0 2 1 462.91 462.79 9.69 o 1 2 1 154.63 192.09 14.77 o 2 2 1 1190.05 1134.95 21.93 o 3 2 1 493.53 441.29 3.33 o 4 2 1 828.36 739.70 14.60 o 5 2 1 246.91 237.22 4.89 o 6 2 1 53.84 45.53 1.56 o 7 2 1 26.60 23.60 1.67 o 8 2 1 0.97 3.91 4.96 o 0 3 1 508.55 570.41 12.25 o 1 3 1 427.67 535.38 34.70 o 2 3 1 3843.70 3772.53 79.76 o 3 3 1 121.25 115.87 1.69 o 4 3 1 662.67 615.22 15.59 o 5 3 1 162.11 158.78 3.38 o 6 3 1 101.82 99.86 2.03 o 7 3 1 32.82 31.52 1.73 o 8 3 1 11.20 12.56 1.69 o 0 4 1 1268.91 1577.79 24.71 o 1 4 1 39.47 52.25 3.78 o 2 4 1 210.01 215.95 14.23 o 3 4 1 122.94 114.13 2.35 o 4 4 1 6.51 6.41 0.86 o 5 4 1 22.60 23.40 1.18 o 6 4 1 23.88 23.42 1.42 o 7 4 1 15.70 15.08 1.56 o 8 4 1 9.05 6.55 3.44 o 0 5 1 921.82 1286.57 18.58 o 1 5 1 322.31 418.65 10.86 o 2 5 1 177.10 207.79 12.93 o 3 5 1 382.32 429.35 26.18 o 4 5 1 41.40 36.88 2.84 o 5 5 1 37.09 36.35 1.32 o 6 5 1 23.56 24.97 4.27 o 7 5 1 9.45 7.92 1.48 o 8 5 1 1.50 -1.87 3.34 o 0 6 1 366.45 459.14 11.27 o 1 6 1 197.10 281.56 4.52 o 2 6 1 611.85 736.52 30.14 o 3 6 1 525.02 609.34 47.91 o 4 6 1 259.81 236.17 5.29 o 5 6 1 35.41 33.14 1.36 o 6 6 1 1.04 -2.58 4.03 o 7 6 1 0.90 1.23 1.45 o 8 6 1 4.00 -1.16 6.95 o 0 7 1 219.00 278.57 2.86 o 1 7 1 255.23 314.82 8.31 o 2 7 1 112.13 150.50 6.61 o 3 7 1 50.62 60.28 3.46 o 4 7 1 29.40 31.50 1.34 o 5 7 1 23.72 22.58 1.30 o 6 7 1 6.50 7.95 1.33 o 7 7 1 0.04 -0.57 3.02 o 0 8 1 533.99 598.48 6.37 o 1 8 1 43.29 44.44 0.98 o 2 8 1 78.46 84.28 4.23 o 3 8 1 45.50 53.69 4.83 o 4 8 1 58.87 64.83 2.42 o 5 8 1 150.36 138.75 2.89 o 6 8 1 6.92 6.70 1.67 o 7 8 1 29.52 22.21 3.32 o 0 9 1 312.41 380.56 4.74 o 1 9 1 196.25 229.60 6.03 o 2 9 1 415.38 520.00 16.00 o 3 9 1 31.60 38.13 1.24 o 4 9 1 7.13 8.71 1.47 o 5 9 1 22.24 24.65 1.46 o 6 9 1 6.31 5.42 1.50 o 7 9 1 47.28 44.92 2.07 o 0 10 1 43.01 42.26 0.98 o 1 10 1 185.67 202.74 6.55 o 2 10 1 158.41 183.28 4.13 o 3 10 1 6.69 7.26 1.74 o 4 10 1 73.17 83.13 2.74 o 5 10 1 45.74 44.15 1.69 o 6 10 1 23.49 21.90 1.88 o 7 10 1 14.33 9.89 1.84 o 0 11 1 171.83 176.93 2.69 o 1 11 1 36.30 40.59 0.94 o 2 11 1 112.98 135.91 2.72 o 3 11 1 30.20 31.01 1.45 o 4 11 1 16.73 19.52 1.68 o 5 11 1 5.38 4.40 1.37 o 6 11 1 0.02 -2.41 3.01 o 0 12 1 2106.86 2232.02 28.98 o 1 12 1 555.57 568.89 5.59 o 2 12 1 400.19 456.92 17.98 o 3 12 1 108.12 124.40 2.57 o 4 12 1 24.53 25.05 1.60 o 5 12 1 3.52 4.53 2.87 o 6 12 1 5.79 1.08 3.48 o 0 13 1 1031.07 1065.73 9.88 o 1 13 1 226.24 247.30 5.70 o 2 13 1 932.35 1065.87 36.02 o 3 13 1 50.33 56.15 1.81 o 4 13 1 156.30 178.57 11.03 o 5 13 1 8.07 -2.45 3.62 o 0 14 1 276.42 252.36 3.83 o 1 14 1 123.28 126.44 3.22 o 2 14 1 326.13 348.01 4.93 o 3 14 1 27.54 26.08 1.63 o 4 14 1 121.93 126.93 6.88 o 5 14 1 10.70 10.14 6.74 o 0 15 1 5.81 -2.15 2.23 o 1 15 1 35.00 32.02 1.12 o 2 15 1 24.02 25.00 1.19 o 3 15 1 34.46 33.80 1.67 o 4 15 1 32.20 34.75 2.00 o 0 16 1 36.62 43.00 1.26 o 1 16 1 28.11 27.32 1.18 o 2 16 1 3.71 2.21 1.33 o 3 16 1 1.38 1.97 1.83 o 0 17 1 5.88 4.56 1.20 o 1 17 1 7.43 9.07 1.98 o 0 0 2 504.47 444.39 4.38 o 1 0 2 2267.33 1909.98 42.84 o 2 0 2 2843.10 2446.09 34.79 o 3 0 2 2368.08 2125.29 10.28 o 4 0 2 328.68 276.13 4.81 o 5 0 2 31.38 33.96 1.25 o 6 0 2 2.23 3.31 1.54 o 7 0 2 2.34 4.17 3.15 o 8 0 2 0.04 -0.76 1.95 o 0 1 2 6485.95 5761.81 97.13 o 1 1 2 5058.99 4315.94 102.84 o 2 1 2 6480.04 5944.87 46.20 o 3 1 2 61.46 64.11 1.02 o 4 1 2 2441.24 2203.81 93.94 o 5 1 2 85.55 73.62 1.59 o 6 1 2 73.56 66.59 1.72 o 7 1 2 25.61 23.04 1.62 o 8 1 2 1.32 3.12 1.52 o 0 2 2 7830.65 7534.75 343.76 o 1 2 2 878.87 939.94 63.60 o 2 2 2 2192.72 2091.73 44.16 o 3 2 2 206.10 188.37 2.33 o 4 2 2 1396.04 1276.45 9.24 o 5 2 2 10.47 11.32 1.09 o 6 2 2 536.28 496.26 13.64 o 7 2 2 9.94 12.06 3.24 o 8 2 2 45.89 44.90 4.85 o 0 3 2 927.53 923.73 11.94 o 1 3 2 238.55 282.01 24.29 o 2 3 2 170.25 165.79 6.91 o 3 3 2 132.20 129.61 1.79 o 4 3 2 130.27 127.73 2.77 o 5 3 2 54.68 47.68 1.36 o 6 3 2 171.73 161.27 3.52 o 7 3 2 4.31 6.36 2.97 o 8 3 2 64.55 58.34 5.41 o 0 4 2 2686.06 2600.21 65.51 o 1 4 2 220.03 267.97 26.04 o 2 4 2 416.11 423.21 29.54 o 3 4 2 31.97 29.26 0.81 o 4 4 2 134.63 129.15 3.13 o 5 4 2 131.24 120.50 2.89 o 6 4 2 39.68 41.40 2.36 o 7 4 2 33.33 30.13 1.73 o 8 4 2 4.43 6.12 1.72 o 0 5 2 15.47 15.78 0.46 o 1 5 2 1208.34 1544.81 100.79 o 2 5 2 225.21 254.11 16.16 o 3 5 2 469.84 505.41 40.10 o 4 5 2 286.18 277.87 18.54 o 5 5 2 128.47 129.90 2.72 o 6 5 2 3.83 3.98 1.21 o 7 5 2 17.96 15.55 1.60 o 8 5 2 0.02 0.75 7.46 o 0 6 2 754.31 807.33 33.27 o 1 6 2 1394.44 1877.96 102.26 o 2 6 2 139.82 160.25 15.71 o 3 6 2 362.32 410.22 55.13 o 4 6 2 148.39 137.06 6.91 o 5 6 2 46.96 48.62 1.99 o 6 6 2 11.44 11.31 1.30 o 7 6 2 2.61 -0.93 4.78 o 8 6 2 0.63 -4.13 6.68 o 0 7 2 108.06 179.07 4.97 o 1 7 2 1563.73 2158.73 89.81 o 2 7 2 356.52 410.27 34.37 o 3 7 2 413.51 473.38 49.36 o 4 7 2 13.04 12.29 1.07 o 5 7 2 12.95 13.01 1.23 o 6 7 2 54.82 55.21 1.84 o 7 7 2 7.40 5.57 3.09 o 0 8 2 861.17 1032.94 17.50 o 1 8 2 41.25 51.51 1.83 o 2 8 2 116.37 129.29 10.13 o 3 8 2 108.35 132.22 19.88 o 4 8 2 18.44 19.26 1.20 o 5 8 2 159.32 147.65 11.59 o 6 8 2 11.65 14.43 1.49 o 7 8 2 6.96 6.37 2.65 o 0 9 2 23.86 40.40 1.26 o 1 9 2 71.26 70.99 2.57 o 2 9 2 30.65 33.35 1.52 o 3 9 2 62.55 76.28 5.53 o 4 9 2 14.22 15.88 3.56 o 5 9 2 72.37 71.04 1.89 o 6 9 2 16.18 16.00 1.60 o 7 9 2 20.23 19.33 1.84 o 0 10 2 7.04 7.35 0.67 o 1 10 2 494.91 541.88 13.21 o 2 10 2 16.76 18.82 1.44 o 3 10 2 168.41 181.37 9.11 o 4 10 2 128.72 127.70 23.31 o 5 10 2 83.55 81.53 7.83 o 6 10 2 55.83 51.47 2.01 o 7 10 2 5.87 3.65 3.42 o 0 11 2 69.00 73.19 1.38 o 1 11 2 173.40 194.76 3.43 o 2 11 2 758.11 851.70 37.00 o 3 11 2 230.51 250.83 5.14 o 4 11 2 390.19 434.46 64.49 o 5 11 2 18.24 17.57 1.61 o 6 11 2 44.58 38.19 1.95 o 0 12 2 2890.44 3072.24 65.98 o 1 12 2 416.94 430.80 17.95 o 2 12 2 1161.17 1340.53 39.68 o 3 12 2 32.25 35.08 1.54 o 4 12 2 133.01 138.32 22.48 o 5 12 2 12.93 12.49 1.56 o 6 12 2 6.74 8.50 1.65 o 0 13 2 62.46 48.70 1.56 o 1 13 2 5.03 6.62 0.88 o 2 13 2 51.43 51.30 1.97 o 3 13 2 47.85 52.31 2.34 o 4 13 2 16.68 19.10 2.82 o 5 13 2 24.46 27.49 1.76 o 0 14 2 26.46 23.16 1.05 o 1 14 2 23.42 20.42 1.04 o 2 14 2 51.20 51.52 1.36 o 3 14 2 8.60 11.85 1.40 o 4 14 2 114.89 125.11 5.10 o 5 14 2 23.41 23.23 3.81 o 0 15 2 1.88 2.02 1.17 o 1 15 2 7.02 9.20 1.52 o 2 15 2 77.97 86.91 1.85 o 3 15 2 42.55 45.38 1.77 o 4 15 2 40.91 50.25 2.41 o 0 16 2 14.15 12.78 1.06 o 1 16 2 6.64 5.79 2.38 o 2 16 2 9.81 11.73 1.09 o 3 16 2 3.77 7.56 3.05 o 0 17 2 16.69 15.79 1.14 o 1 17 2 0.28 -0.46 1.61 o 1 0 3 63.09 48.12 1.75 o 2 0 3 855.83 728.64 12.03 o 3 0 3 40.08 40.18 0.63 o 4 0 3 5.23 4.76 0.83 o 5 0 3 87.95 90.61 4.41 o 6 0 3 2.31 0.69 2.53 o 7 0 3 1.47 1.46 1.99 o 8 0 3 0.30 -0.16 2.00 o 0 1 3 25.19 25.10 0.50 o 1 1 3 3805.85 3144.68 72.56 o 2 1 3 3958.71 3545.09 39.26 o 3 1 3 240.47 227.54 4.32 o 4 1 3 1411.62 1313.59 26.11 o 5 1 3 70.19 68.99 2.63 o 6 1 3 44.65 44.39 1.57 o 7 1 3 11.06 11.45 1.50 o 8 1 3 0.42 -1.85 2.02 o 0 2 3 595.01 515.62 13.71 o 1 2 3 2792.15 2569.62 74.84 o 2 2 3 1378.83 1309.95 16.64 o 3 2 3 233.59 225.31 3.84 o 4 2 3 955.71 866.54 23.53 o 5 2 3 66.84 74.18 1.99 o 6 2 3 313.04 302.52 9.73 o 7 2 3 7.49 -0.73 3.09 o 8 2 3 3.91 3.84 4.65 o 0 3 3 3268.48 2975.81 118.78 o 1 3 3 1770.99 1881.83 169.75 o 2 3 3 303.68 272.05 8.86 o 3 3 3 965.55 925.59 14.83 o 4 3 3 30.17 30.84 1.08 o 5 3 3 119.19 114.18 2.46 o 6 3 3 179.23 176.62 4.04 o 7 3 3 39.21 41.21 1.82 o 8 3 3 56.63 57.69 2.21 o 0 4 3 386.19 386.88 4.56 o 1 4 3 211.22 240.72 28.10 o 2 4 3 463.66 455.82 33.37 o 3 4 3 61.93 62.42 5.93 o 4 4 3 20.27 19.30 1.23 o 5 4 3 12.84 15.99 2.22 o 6 4 3 12.31 10.03 1.35 o 7 4 3 8.40 8.62 2.32 o 8 4 3 7.78 7.18 1.76 o 0 5 3 595.48 552.02 7.55 o 1 5 3 307.78 382.90 38.95 o 2 5 3 639.06 699.42 63.09 o 3 5 3 297.84 298.08 25.73 o 4 5 3 22.07 17.21 2.76 o 5 5 3 14.32 15.89 1.15 o 6 5 3 42.17 41.17 1.64 o 7 5 3 4.09 6.37 1.45 o 8 5 3 3.54 4.48 1.79 o 0 6 3 1022.73 1051.99 21.50 o 1 6 3 2922.46 3946.92 338.70 o 2 6 3 1158.29 1326.45 131.06 o 3 6 3 103.65 111.65 16.51 o 4 6 3 565.31 548.19 31.64 o 5 6 3 10.93 8.29 2.18 o 6 6 3 29.60 28.01 2.28 o 7 6 3 0.46 -1.63 3.00 o 8 6 3 1.12 -3.67 3.67 o 0 7 3 947.43 1008.54 33.04 o 1 7 3 1837.58 2253.60 163.57 o 2 7 3 82.96 109.72 11.90 o 3 7 3 769.85 920.91 140.41 o 4 7 3 39.15 40.11 5.46 o 5 7 3 70.66 68.28 5.24 o 6 7 3 24.93 23.11 1.60 o 7 7 3 7.86 8.95 1.53 o 0 8 3 155.40 151.01 5.48 o 1 8 3 237.24 260.68 17.75 o 2 8 3 128.51 145.01 13.90 o 3 8 3 210.93 248.67 33.46 o 4 8 3 29.34 28.00 1.31 o 5 8 3 42.96 45.09 3.17 o 6 8 3 20.20 19.51 2.62 o 7 8 3 7.61 6.82 1.58 o 0 9 3 5.98 6.68 0.61 o 1 9 3 137.42 159.31 7.31 o 2 9 3 28.61 37.58 2.79 o 3 9 3 159.50 169.43 25.11 o 4 9 3 3.06 0.41 5.17 o 5 9 3 91.85 83.35 7.65 o 6 9 3 55.73 58.58 3.87 o 7 9 3 11.82 10.42 1.74 o 0 10 3 1.82 0.32 1.14 o 1 10 3 77.29 82.85 6.57 o 2 10 3 65.11 64.92 4.17 o 3 10 3 167.47 187.68 18.31 o 4 10 3 99.20 114.08 23.63 o 5 10 3 51.43 50.64 6.22 o 6 10 3 34.63 31.28 1.88 o 0 11 3 51.05 48.68 1.83 o 1 11 3 250.12 254.27 6.59 o 2 11 3 181.91 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1.18 o 2 10 13 4.64 6.25 1.03 o 3 10 13 5.11 6.33 1.42 o 0 11 13 4.16 0.89 2.51 o 1 11 13 5.56 6.15 2.67 o 0 0 14 162.69 141.45 3.73 o 1 0 14 11.13 11.62 0.88 o 2 0 14 64.38 61.71 1.59 o 3 0 14 0.38 0.29 1.13 o 4 0 14 8.43 11.46 2.36 o 5 0 14 5.54 1.55 3.39 o 0 1 14 23.54 22.93 0.96 o 1 1 14 3.32 2.11 1.62 o 2 1 14 9.02 8.90 1.06 o 3 1 14 74.43 79.71 2.06 o 4 1 14 1.67 2.86 1.74 o 5 1 14 20.90 23.42 1.80 o 0 2 14 176.17 152.38 3.96 o 1 2 14 91.51 97.68 1.50 o 2 2 14 56.44 63.14 1.82 o 3 2 14 37.38 38.79 1.20 o 4 2 14 29.60 31.11 1.75 o 5 2 14 4.35 -0.93 7.25 o 0 3 14 59.00 51.87 1.19 o 1 3 14 206.50 192.95 2.81 o 2 3 14 118.96 125.65 2.49 o 3 3 14 6.14 6.87 1.10 o 4 3 14 59.27 68.29 2.13 o 5 3 14 31.46 36.35 1.93 o 0 4 14 3.80 1.55 1.53 o 1 4 14 22.74 25.72 1.03 o 2 4 14 1.45 1.12 1.31 o 3 4 14 28.38 26.46 2.41 o 4 4 14 14.38 15.59 4.52 o 0 5 14 1.02 1.21 1.56 o 1 5 14 4.13 5.40 1.20 o 2 5 14 9.41 10.36 0.95 o 3 5 14 0.47 -0.93 2.57 o 4 5 14 15.55 18.95 2.00 o 0 6 14 5.85 7.05 0.86 o 1 6 14 20.38 23.48 1.05 o 2 6 14 7.65 9.48 0.95 o 3 6 14 4.84 5.39 1.34 o 4 6 14 1.52 -3.34 4.47 o 0 7 14 1.63 -1.88 1.88 o 1 7 14 21.80 22.06 1.08 o 2 7 14 1.47 0.47 1.80 o 3 7 14 10.00 13.62 2.50 o 0 8 14 0.04 -1.46 1.77 o 1 8 14 9.27 8.29 0.97 o 2 8 14 2.53 4.78 3.40 o 3 8 14 1.58 -2.86 3.13 o 0 9 14 28.44 28.63 1.15 o 1 9 14 4.09 4.02 1.13 o 2 9 14 13.20 13.98 1.13 o 0 10 14 8.55 7.71 1.99 o 1 10 14 1.30 3.68 1.27 o 1 0 15 18.86 22.59 1.00 o 2 0 15 2.12 -1.44 1.95 o 3 0 15 2.82 3.79 0.92 o 4 0 15 1.72 -0.13 1.82 o 0 1 15 43.16 37.15 1.41 o 1 1 15 15.05 14.81 0.98 o 2 1 15 44.82 41.81 1.25 o 3 1 15 15.97 21.22 1.11 o 4 1 15 14.17 14.05 1.63 o 0 2 15 0.00 0.80 0.87 o 1 2 15 18.25 19.84 1.18 o 2 2 15 5.29 6.41 1.27 o 3 2 15 3.96 3.91 1.07 o 4 2 15 3.98 6.42 1.49 o 0 3 15 18.89 15.81 1.00 o 1 3 15 44.60 42.40 1.43 o 2 3 15 37.94 38.53 1.30 o 3 3 15 12.02 11.77 1.03 o 4 3 15 16.84 17.87 2.99 o 0 4 15 4.14 2.04 1.34 o 1 4 15 12.71 10.83 1.46 o 2 4 15 28.86 29.87 1.18 o 3 4 15 17.98 21.54 1.32 o 4 4 15 15.83 19.00 1.71 o 0 5 15 2.15 3.27 0.88 o 1 5 15 4.80 4.38 1.28 o 2 5 15 5.42 6.37 1.29 o 3 5 15 7.13 9.57 1.49 o 0 6 15 0.07 0.88 1.18 o 1 6 15 17.08 20.48 1.07 o 2 6 15 1.37 2.05 1.04 o 3 6 15 5.52 8.12 1.51 o 0 7 15 0.85 1.86 1.14 o 1 7 15 1.54 2.53 1.06 o 2 7 15 2.87 3.07 1.57 o 0 8 15 20.79 20.35 1.21 o 1 8 15 38.53 50.21 1.36 o 2 8 15 7.74 7.10 1.10 o 0 9 15 3.00 -1.27 2.56 o 0 0 16 0.57 0.13 1.66 o 1 0 16 0.35 -0.47 1.35 o 2 0 16 0.04 -1.83 1.83 o 3 0 16 5.93 2.20 1.64 o 0 1 16 2.17 0.67 1.11 o 1 1 16 1.75 1.46 1.17 o 2 1 16 5.27 4.87 1.33 o 3 1 16 1.21 2.03 1.79 o 0 2 16 17.46 16.10 1.00 o 1 2 16 4.23 6.58 1.25 o 2 2 16 10.38 10.23 1.68 o 3 2 16 8.27 6.15 1.21 o 0 3 16 9.56 8.77 0.97 o 1 3 16 18.05 19.99 1.12 o 2 3 16 12.52 15.20 1.11 o 3 3 16 55.42 69.08 2.11 o 0 4 16 8.11 10.50 1.38 o 1 4 16 22.21 21.23 1.11 o 2 4 16 4.47 6.53 1.05 o 0 5 16 0.14 -0.01 1.48 o 1 5 16 3.88 3.61 1.06 o 2 5 16 3.52 3.53 2.11 o 0 6 16 0.30 -0.84 1.44 o 1 6 16 3.82 4.05 1.25 o 0 7 16 0.76 1.81 0.98 o 1 0 17 1.31 0.98 1.22 o 2 0 17 0.55 0.31 1.22 o 0 1 17 0.23 -0.11 1.46 o 1 1 17 3.38 5.22 1.63 o 2 1 17 5.67 8.48 1.02 o 0 2 17 0.02 -2.04 2.04 o 1 2 17 3.19 4.45 1.52 o 0 3 17 6.68 8.98 1.35 o 1 3 17 1.78 1.26 1.69 o 0 4 17 108.96 120.09 2.71 o