#------------------------------------------------------------------------------ #$Date: 2011-10-07 16:37:56 +0300 (Fri, 07 Oct 2011) $ #$Revision: 27934 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/82/2018232.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018232_Fobs loop_ _publ_author_name 'Lennartson, Anders' 'McKenzie, Christine J.' _publ_section_title ; 1,2-Bis[(pyridin-2-ylmethyl)sulfanyl]ethane and its dimorphic hydrochloride salt ; _journal_coeditor_code SU3068 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o354 _journal_page_last o358 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.297 _cell_angle_gamma 90.000 _cell_length_a 7.8247 _cell_length_b 7.8382 _cell_length_c 14.1408 _exptl_crystal_F_000 364.00 _reflns_d_resolution_high 0.8076 _[local]_cod_data_source_file su3068IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' CM10130 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 110.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1152.09 1330.74 14.07 o 4 0 0 65.11 49.37 3.54 o 6 0 0 1139.81 1134.98 20.03 o 8 0 0 1588.17 1556.03 43.30 o 1 1 0 4375.72 4458.45 33.62 o 2 1 0 303.46 304.53 3.13 o 3 1 0 1453.84 1484.05 12.72 o 4 1 0 39.36 39.32 1.91 o 5 1 0 10.72 9.95 1.44 o 6 1 0 635.73 625.43 8.64 o 7 1 0 538.38 532.91 12.48 o 8 1 0 18.75 7.39 3.75 o 9 1 0 162.85 189.44 9.43 o 0 2 0 431.62 463.64 5.51 o 1 2 0 176.71 167.77 2.23 o 2 2 0 1789.35 1778.17 13.27 o 3 2 0 1805.58 1889.31 16.14 o 4 2 0 1.48 4.65 1.11 o 5 2 0 145.08 137.65 3.82 o 6 2 0 224.15 238.79 5.63 o 7 2 0 31.21 27.62 3.90 o 8 2 0 935.57 938.05 20.92 o 9 2 0 259.33 276.41 11.26 o 1 3 0 860.50 867.58 7.33 o 2 3 0 0.53 -0.85 0.85 o 3 3 0 562.25 519.92 6.83 o 4 3 0 101.42 92.25 2.58 o 5 3 0 12.16 10.14 1.58 o 6 3 0 11.99 14.53 2.67 o 7 3 0 137.46 143.43 6.36 o 8 3 0 5.53 1.65 3.71 o 9 3 0 0.07 5.17 4.95 o 0 4 0 522.92 515.48 7.02 o 1 4 0 4562.82 4625.31 36.42 o 2 4 0 0.16 -0.08 1.10 o 3 4 0 130.54 106.46 2.73 o 4 4 0 463.34 447.69 7.21 o 5 4 0 426.45 451.29 7.43 o 6 4 0 490.96 499.09 11.13 o 7 4 0 819.96 818.88 22.84 o 8 4 0 31.84 41.96 5.48 o 1 5 0 439.30 473.39 6.08 o 2 5 0 369.73 366.93 5.80 o 3 5 0 399.04 404.13 5.81 o 4 5 0 70.04 73.84 3.57 o 5 5 0 264.58 260.90 7.33 o 6 5 0 20.68 16.71 3.37 o 7 5 0 708.31 700.85 19.12 o 8 5 0 7.18 8.54 5.47 o 0 6 0 275.62 282.25 7.67 o 1 6 0 555.13 554.70 7.63 o 2 6 0 409.28 409.16 6.57 o 3 6 0 70.45 78.41 3.60 o 4 6 0 2521.94 2446.22 34.16 o 5 6 0 176.34 178.88 7.43 o 6 6 0 160.64 181.67 7.63 o 7 6 0 48.36 59.05 9.68 o 1 7 0 33.00 34.75 3.77 o 2 7 0 36.86 34.33 3.96 o 3 7 0 460.99 449.38 12.20 o 4 7 0 0.09 -0.61 3.32 o 5 7 0 89.30 93.77 7.48 o 6 7 0 7.69 12.34 6.49 o 0 8 0 39.52 31.04 6.27 o 1 8 0 6.83 0.78 3.24 o 2 8 0 5.60 11.36 4.17 o 3 8 0 41.34 43.43 5.99 o 4 8 0 673.22 710.91 21.73 o 5 8 0 73.68 64.60 9.28 o 1 9 0 36.72 48.14 7.27 o 2 9 0 25.09 17.07 6.39 o 3 9 0 81.43 89.77 9.85 o -9 0 1 255.48 255.05 14.61 o -7 0 1 1890.03 1791.49 39.07 o -5 0 1 726.93 674.26 11.42 o -3 0 1 133.06 111.00 4.84 o 3 0 1 658.73 742.27 9.46 o 5 0 1 52.26 49.53 3.93 o 7 0 1 378.28 361.14 13.17 o 9 0 1 1124.26 1171.76 48.16 o -9 1 1 24.42 31.57 4.53 o -8 1 1 2.60 0.81 3.00 o -7 1 1 0.41 2.46 2.56 o -6 1 1 864.20 855.29 11.93 o -5 1 1 0.29 -0.75 1.25 o -4 1 1 2952.68 2825.17 26.98 o -3 1 1 1096.53 1132.12 10.85 o -2 1 1 9990.98 10413.01 89.92 o -1 1 1 1170.16 1110.16 16.73 o 1 1 1 36.46 53.31 0.97 o 2 1 1 437.93 452.58 4.00 o 3 1 1 296.05 298.74 4.52 o 4 1 1 999.53 1010.99 10.00 o 5 1 1 261.56 279.60 4.59 o 6 1 1 1982.26 1995.36 26.43 o 7 1 1 282.30 277.17 8.08 o 8 1 1 118.32 126.51 6.90 o 9 1 1 0.09 6.70 4.35 o -9 2 1 142.33 146.22 8.30 o -8 2 1 6.67 6.10 3.42 o -7 2 1 1.05 -0.41 2.47 o -6 2 1 581.40 580.52 8.92 o -5 2 1 365.65 351.66 5.63 o -4 2 1 78.87 92.72 2.55 o -3 2 1 49.06 38.94 1.54 o -2 2 1 326.34 349.22 3.69 o -1 2 1 9997.28 10168.52 73.22 o 0 2 1 12195.13 12180.92 89.25 o 1 2 1 2078.40 2172.14 14.96 o 2 2 1 21.62 26.53 1.13 o 3 2 1 405.35 413.76 4.37 o 4 2 1 34.45 20.37 1.41 o 5 2 1 136.53 146.63 3.61 o 6 2 1 957.25 962.32 13.72 o 7 2 1 1493.05 1485.84 24.40 o 8 2 1 248.23 230.32 9.40 o 9 2 1 197.21 195.24 9.89 o -9 3 1 192.80 207.90 11.08 o -8 3 1 316.90 313.52 11.92 o -7 3 1 340.29 344.11 10.52 o -6 3 1 206.56 212.18 6.01 o -5 3 1 713.25 719.76 10.88 o -4 3 1 1756.78 1735.69 15.74 o -3 3 1 1488.86 1445.07 12.81 o -2 3 1 1769.60 1723.11 14.68 o -1 3 1 126.68 102.26 2.07 o 0 3 1 359.40 373.02 3.94 o 1 3 1 529.25 538.73 4.70 o 2 3 1 532.32 532.26 5.05 o 3 3 1 149.04 130.73 2.51 o 4 3 1 27.06 22.31 1.69 o 5 3 1 206.85 208.02 4.48 o 6 3 1 2029.71 1978.33 28.01 o 7 3 1 45.03 50.18 4.57 o 8 3 1 1.81 2.84 3.59 o -8 4 1 18.28 11.62 4.26 o -7 4 1 33.81 24.47 4.66 o -6 4 1 323.70 321.55 9.05 o -5 4 1 388.97 364.95 6.24 o -4 4 1 146.26 157.74 3.60 o -3 4 1 172.28 186.23 3.42 o -2 4 1 713.63 735.57 8.28 o -1 4 1 2814.38 2874.58 24.92 o 0 4 1 790.17 903.50 7.65 o 1 4 1 252.21 260.90 3.25 o 2 4 1 937.60 944.13 9.58 o 3 4 1 1433.43 1426.95 13.87 o 4 4 1 437.39 459.54 7.14 o 5 4 1 75.69 73.17 3.70 o 6 4 1 26.42 23.84 3.07 o 7 4 1 427.10 417.54 11.55 o 8 4 1 404.66 445.33 13.92 o -8 5 1 432.00 459.39 15.35 o -7 5 1 490.29 488.19 15.17 o -6 5 1 113.85 116.38 6.85 o -5 5 1 403.14 404.25 9.10 o -4 5 1 0.25 0.98 1.60 o -3 5 1 816.42 795.38 9.93 o -2 5 1 41.96 48.64 2.20 o -1 5 1 1022.84 1027.80 10.69 o 0 5 1 2222.12 2240.47 20.32 o 1 5 1 615.22 603.77 7.15 o 2 5 1 1751.66 1724.87 17.17 o 3 5 1 649.61 670.72 8.27 o 4 5 1 0.92 0.78 2.03 o 5 5 1 396.56 381.21 8.81 o 6 5 1 20.01 18.28 3.72 o 7 5 1 266.67 273.96 12.26 o -7 6 1 150.47 150.17 11.05 o -6 6 1 18.64 21.82 4.67 o -5 6 1 468.88 470.04 10.53 o -4 6 1 29.56 33.22 3.17 o -3 6 1 307.38 323.87 6.48 o -2 6 1 84.40 86.58 3.17 o -1 6 1 28.58 25.03 1.95 o 0 6 1 298.24 297.15 5.64 o 1 6 1 72.37 79.60 3.03 o 2 6 1 2.24 3.84 1.52 o 3 6 1 315.94 306.10 7.56 o 4 6 1 11.49 10.26 2.97 o 5 6 1 505.74 495.52 13.33 o 6 6 1 7.61 7.59 3.77 o 7 6 1 46.02 39.15 8.10 o -6 7 1 568.54 576.04 20.01 o -5 7 1 23.57 24.05 4.74 o -4 7 1 12.96 9.92 3.24 o -3 7 1 295.16 300.61 8.83 o -2 7 1 125.85 127.67 5.70 o -1 7 1 42.63 33.39 4.55 o 0 7 1 186.01 191.36 7.54 o 1 7 1 0.08 1.19 2.77 o 2 7 1 1138.94 1113.51 20.50 o 3 7 1 5.95 8.03 3.18 o 4 7 1 45.55 42.03 5.49 o 5 7 1 100.54 107.89 7.65 o 6 7 1 225.25 213.42 15.38 o -5 8 1 473.66 464.24 20.70 o -4 8 1 131.67 121.03 19.61 o -3 8 1 49.72 46.74 6.05 o -2 8 1 3.07 4.26 5.25 o -1 8 1 24.56 30.23 5.08 o 0 8 1 4.19 3.05 3.36 o 1 8 1 0.97 1.62 3.44 o 2 8 1 23.21 27.51 7.53 o 3 8 1 1189.97 1165.29 28.63 o 4 8 1 228.50 214.76 12.58 o 5 8 1 318.59 371.10 21.62 o -3 9 1 0.07 -4.42 4.94 o -2 9 1 0.95 6.65 5.41 o -1 9 1 194.95 179.94 13.12 o 0 9 1 372.55 365.39 13.04 o 1 9 1 252.15 255.02 16.26 o 2 9 1 870.17 911.80 36.82 o 3 9 1 45.89 36.37 7.52 o -8 0 2 572.18 584.74 17.44 o -6 0 2 180.52 171.14 9.42 o -4 0 2 3721.00 3930.43 54.89 o -2 0 2 779.33 758.19 15.09 o 2 0 2 8657.89 9020.07 88.00 o 4 0 2 3364.85 3553.42 43.00 o 6 0 2 490.81 480.39 17.64 o 8 0 2 45.69 48.64 6.13 o -9 1 2 139.78 137.99 7.72 o -8 1 2 123.94 117.31 5.72 o -7 1 2 35.16 37.77 5.90 o -6 1 2 290.06 284.40 5.35 o -5 1 2 794.74 748.09 8.92 o -4 1 2 1.37 5.91 1.23 o -3 1 2 4787.80 4729.32 45.30 o -2 1 2 513.49 520.07 7.01 o -1 1 2 423.65 381.31 6.48 o 0 1 2 26.85 21.47 0.68 o 1 1 2 16.12 12.70 0.74 o 2 1 2 377.80 369.15 3.58 o 3 1 2 623.06 624.71 5.65 o 4 1 2 380.19 396.95 4.78 o 5 1 2 3558.12 3591.07 31.74 o 6 1 2 14.31 13.72 1.88 o 7 1 2 342.88 349.63 9.95 o 8 1 2 186.82 185.33 8.39 o 9 1 2 0.02 1.28 3.54 o -9 2 2 163.05 159.83 8.21 o -8 2 2 557.80 551.12 12.90 o -7 2 2 868.16 858.75 14.62 o -6 2 2 3373.24 3287.54 36.03 o -5 2 2 675.65 657.37 8.63 o -4 2 2 66.15 66.51 2.34 o -3 2 2 11.31 15.17 1.38 o -2 2 2 555.57 559.64 6.55 o -1 2 2 4574.65 4544.83 49.52 o 0 2 2 4426.42 4504.43 31.60 o 1 2 2 1954.81 2044.50 14.21 o 2 2 2 357.57 344.22 3.33 o 3 2 2 34.01 53.34 1.73 o 4 2 2 992.95 988.24 9.66 o 5 2 2 58.66 64.93 2.77 o 6 2 2 260.39 271.45 6.17 o 7 2 2 160.55 140.64 6.97 o 8 2 2 212.58 227.82 9.16 o 9 2 2 33.36 57.01 12.61 o -9 3 2 268.25 266.34 11.68 o -8 3 2 83.66 74.61 6.02 o -7 3 2 19.57 25.41 3.68 o -6 3 2 194.81 204.62 5.99 o -5 3 2 1076.67 1048.27 12.29 o -4 3 2 1537.21 1585.24 15.75 o -3 3 2 626.92 614.55 6.34 o -2 3 2 439.49 409.32 4.71 o -1 3 2 126.54 146.10 2.35 o 0 3 2 6958.66 7037.69 51.90 o 1 3 2 102.89 100.51 1.93 o 2 3 2 1196.80 1209.40 9.57 o 3 3 2 176.20 171.72 3.02 o 4 3 2 1221.24 1252.78 12.64 o 5 3 2 1341.62 1344.24 19.03 o 6 3 2 1421.05 1402.52 21.39 o 7 3 2 23.61 21.99 4.12 o 8 3 2 253.27 255.64 9.81 o -8 4 2 65.25 61.94 5.98 o -7 4 2 9.46 10.54 3.51 o -6 4 2 296.84 304.68 11.44 o -5 4 2 691.52 694.33 9.69 o -4 4 2 39.62 40.27 1.81 o -3 4 2 711.43 726.50 7.72 o -2 4 2 1441.42 1439.52 13.11 o -1 4 2 43.31 43.53 1.73 o 0 4 2 0.03 -0.88 0.88 o 1 4 2 9.59 4.70 0.92 o 2 4 2 654.10 647.85 6.51 o 3 4 2 1401.43 1427.54 13.14 o 4 4 2 143.34 143.67 3.56 o 5 4 2 119.80 114.85 4.77 o 6 4 2 6.45 8.48 2.77 o 7 4 2 22.36 22.67 3.40 o 8 4 2 101.02 124.05 10.72 o -8 5 2 6.88 2.72 4.32 o -7 5 2 54.06 64.48 6.31 o -6 5 2 9.98 12.87 3.62 o -5 5 2 146.36 150.34 6.01 o -4 5 2 470.65 470.51 7.16 o -3 5 2 328.64 343.33 5.70 o -2 5 2 197.87 190.93 3.95 o -1 5 2 39.18 37.17 1.90 o 0 5 2 26.17 29.49 1.69 o 1 5 2 726.09 709.27 7.62 o 2 5 2 80.17 78.73 2.73 o 3 5 2 1.74 1.10 1.41 o 4 5 2 433.29 397.77 7.78 o 5 5 2 325.34 324.32 8.69 o 6 5 2 187.51 178.44 7.62 o 7 5 2 48.97 44.77 5.10 o -7 6 2 222.04 219.53 15.08 o -6 6 2 0.95 8.62 4.31 o -5 6 2 278.37 273.87 7.94 o -4 6 2 22.88 24.06 3.00 o -3 6 2 22.44 22.52 2.37 o -2 6 2 990.16 1014.22 12.83 o -1 6 2 39.39 43.73 2.32 o 0 6 2 1325.75 1312.03 13.07 o 1 6 2 113.61 116.13 3.54 o 2 6 2 289.79 296.88 6.40 o 3 6 2 187.67 178.28 5.93 o 4 6 2 136.13 133.27 6.17 o 5 6 2 13.17 10.01 5.31 o 6 6 2 476.67 473.66 22.00 o 7 6 2 28.97 35.60 7.60 o -6 7 2 2.43 -0.87 5.42 o -5 7 2 29.33 20.75 3.95 o -4 7 2 66.79 59.26 5.54 o -3 7 2 0.03 -1.12 2.58 o -2 7 2 2.39 -1.09 2.54 o -1 7 2 1584.89 1583.78 21.90 o 0 7 2 34.64 30.12 3.77 o 1 7 2 2522.01 2425.34 38.52 o 2 7 2 0.38 -2.82 2.82 o 3 7 2 198.40 193.26 8.12 o 4 7 2 102.83 95.37 6.76 o 5 7 2 31.97 30.46 8.79 o 6 7 2 0.13 1.39 5.20 o -5 8 2 0.81 3.20 5.28 o -4 8 2 512.69 476.43 16.12 o -3 8 2 318.16 304.76 12.19 o -2 8 2 859.18 834.89 30.41 o -1 8 2 1.80 4.20 3.70 o 0 8 2 305.17 316.70 10.16 o 1 8 2 0.39 3.18 3.37 o 2 8 2 37.59 35.36 4.81 o 3 8 2 0.05 5.41 3.88 o 4 8 2 0.99 5.16 5.10 o 5 8 2 26.73 41.44 12.48 o -3 9 2 5.89 9.83 6.99 o -2 9 2 24.53 24.32 11.56 o -1 9 2 95.76 108.60 10.65 o 0 9 2 7.06 3.04 5.31 o 1 9 2 730.81 737.84 26.86 o 2 9 2 128.45 144.27 23.55 o 3 9 2 1.60 1.67 8.19 o -9 0 3 392.13 358.75 15.32 o -7 0 3 2912.41 2789.78 56.20 o -5 0 3 1142.12 1104.95 24.43 o -3 0 3 1109.98 1184.23 19.63 o -1 0 3 3221.05 3209.75 116.22 o 1 0 3 8491.63 9151.76 88.65 o 3 0 3 1372.85 1204.34 14.05 o 5 0 3 3.31 3.19 1.75 o 7 0 3 76.72 81.79 7.03 o 9 0 3 20.20 13.22 5.24 o -9 1 3 5.13 11.83 3.58 o -8 1 3 261.44 270.23 7.81 o -7 1 3 133.83 142.13 5.45 o -6 1 3 131.21 117.28 3.50 o -5 1 3 104.41 111.19 3.11 o -4 1 3 208.87 227.47 4.11 o -3 1 3 225.63 237.05 4.48 o -2 1 3 1562.37 1434.73 22.51 o -1 1 3 1.59 2.34 1.15 o 0 1 3 866.60 903.67 7.75 o 1 1 3 305.72 304.69 2.79 o 2 1 3 42.72 49.46 1.39 o 3 1 3 21.85 28.88 1.33 o 4 1 3 1886.53 1913.35 17.24 o 5 1 3 8.10 10.32 1.59 o 6 1 3 37.76 37.91 2.63 o 7 1 3 37.19 42.65 3.52 o 8 1 3 14.56 19.39 3.78 o -9 2 3 129.37 139.70 9.81 o -8 2 3 55.07 51.51 4.82 o -7 2 3 533.10 529.94 10.93 o -6 2 3 77.88 71.34 3.04 o -5 2 3 296.43 309.16 5.61 o -4 2 3 1375.40 1455.13 15.69 o -3 2 3 25.73 23.60 1.50 o -2 2 3 1752.53 1753.09 20.29 o -1 2 3 399.51 399.82 4.49 o 0 2 3 0.23 0.33 0.69 o 1 2 3 2465.94 2423.49 16.70 o 2 2 3 4354.46 4519.17 31.15 o 3 2 3 5668.88 5942.52 43.00 o 4 2 3 963.75 976.95 10.18 o 5 2 3 15.76 13.14 1.66 o 6 2 3 200.82 195.09 6.50 o 7 2 3 1.97 -0.67 2.59 o 8 2 3 165.75 164.24 7.52 o -9 3 3 100.48 110.01 7.96 o -8 3 3 396.83 387.49 11.50 o -7 3 3 775.62 774.11 14.57 o -6 3 3 14.80 12.10 2.24 o -5 3 3 69.17 83.03 2.67 o -4 3 3 793.14 794.32 9.94 o -3 3 3 1007.78 1075.36 13.19 o -2 3 3 591.83 629.71 6.85 o -1 3 3 1295.90 1343.50 11.52 o 0 3 3 1499.29 1440.43 12.21 o 1 3 3 1135.96 1138.36 8.91 o 2 3 3 113.48 121.29 2.25 o 3 3 3 1.98 0.48 0.99 o 4 3 3 809.32 815.01 8.86 o 5 3 3 0.28 0.36 1.54 o 6 3 3 101.56 101.30 5.02 o 7 3 3 26.49 30.18 3.63 o 8 3 3 349.32 347.35 12.81 o -8 4 3 223.02 226.16 9.32 o -7 4 3 356.71 353.92 14.49 o -6 4 3 1775.20 1780.88 27.27 o -5 4 3 17.87 16.22 1.97 o -4 4 3 0.32 2.76 1.36 o -3 4 3 458.75 447.26 5.38 o -2 4 3 1118.32 1118.60 11.49 o -1 4 3 752.54 741.02 7.35 o 0 4 3 2446.70 2517.31 21.13 o 1 4 3 502.08 492.87 5.52 o 2 4 3 666.22 629.72 6.56 o 3 4 3 648.87 642.09 7.66 o 4 4 3 455.06 447.35 6.53 o 5 4 3 432.79 429.19 8.37 o 6 4 3 269.47 263.90 7.93 o 7 4 3 543.15 527.91 20.41 o 8 4 3 111.73 130.18 9.72 o -8 5 3 19.43 23.84 5.10 o -7 5 3 1.48 0.70 3.40 o -6 5 3 163.42 161.22 7.88 o -5 5 3 12.40 17.95 3.10 o -4 5 3 268.41 264.46 5.29 o -3 5 3 189.12 202.14 4.14 o -2 5 3 114.71 126.62 3.17 o -1 5 3 107.69 124.78 3.13 o 0 5 3 3157.80 3188.71 29.60 o 1 5 3 0.09 -1.45 1.45 o 2 5 3 43.57 41.09 2.26 o 3 5 3 68.70 64.24 3.42 o 4 5 3 517.79 482.55 9.32 o 5 5 3 29.73 25.75 3.52 o 6 5 3 107.13 99.29 6.63 o 7 5 3 95.02 96.29 8.69 o -7 6 3 113.09 110.96 10.38 o -6 6 3 11.94 10.95 3.97 o -5 6 3 208.08 216.83 10.45 o -4 6 3 82.18 86.53 4.34 o -3 6 3 2244.11 2282.30 29.18 o -2 6 3 121.99 139.48 4.42 o -1 6 3 355.30 345.88 5.28 o 0 6 3 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