#------------------------------------------------------------------------------
#$Date: 2011-11-08 16:24:06 +0200 (Tue, 08 Nov 2011) $
#$Revision: 29951 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/82/2018255.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2018255_Fobs
loop_
_publ_author_name
'Friese, K.'
'Halasyamani, P. S.'
'Tolkiehn, M.'
'Grzechnik, A.'
_publ_section_title
;
 A high-pressure single-crystal synchrotron diffraction study of
 NH~4~RbTe~4~O~9~·2H~2~O: stability of three different
 TeO~<i>x~</i> coordination polyhedra
;
_journal_coeditor_code           LG3063
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              i45
_journal_page_last               i49
_journal_volume                  67
_journal_year                    2011
_space_group_IT_number           15
_symmetry_space_group_name_Hall  '-I 2ya'
_symmetry_space_group_name_H-M   'I 1 2/a 1'
_cell_angle_alpha                90
_cell_angle_beta                 101.41(10)
_cell_angle_gamma                90
_cell_length_a                   18.501(3)
_cell_length_b                   6.5420(10)
_cell_length_c                   20.045(7)
_exptl_crystal_F_000             2720
_reflns_d_resolution_high        0.5278
_[local]_cod_data_source_file    lg3063I_3.45GPasup5.hkl
_[local]_cod_data_source_block   I_3.45GPa
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     '   '
_shelx_refln_list_code           4
_shelx_f_calc_maximum            840.20
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y, -z'
'-x, -y, -z'
'x+1/2, -y, z'
'x+1/2, y+1/2, z+1/2'
'-x, y+1/2, -z+1/2'
'-x+1/2, -y+1/2, -z+1/2'
'x, -y+1/2, z+1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
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0 3 1 14835.70 12686.90 1606.51 o
0 3 3 233072.00 263507.00 4141.60 o
0 3 5 37208.70 40963.10 2577.82 o
0 4 0 322929.00 314782.00 5523.08 o
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0 5 3 35697.90 35576.80 2347.10 o
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0 5 7 77163.10 65701.60 4010.57 o
0 5 9 9762.67 20773.50 4674.25 o
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