#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:20:17 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180851 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/82/2018268.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018268_Fobs loop_ _publ_author_name 'Lan, Shao-Min' 'Di, Wen-Jing' 'Shao, Zhi-Dong' 'Liang, Yun-Xiao' _publ_section_title ; Two new transition metal inorganic--organic hybrid borates: [tris(2-aminoethoxy)trihydroxyhexaborato]cobalt(II) and its nickel(II) analogue ; _journal_coeditor_code BM3109 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m338 _journal_page_last m341 _journal_volume 67 _journal_year 2011 _space_group_IT_number 205 _symmetry_space_group_name_Hall '-P 2ac 2ab 3' _symmetry_space_group_name_H-M 'P a -3' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.2217 _cell_length_b 15.2217 _cell_length_c 15.2217 _exptl_crystal_F_000 1920.00 _reflns_d_resolution_high 0.8405 _cod_data_source_file bm3109IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' mm in Pa-3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 301.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' 'z, x, y' 'z+1/2, -x+1/2, -y' '-z+1/2, -x, y+1/2' '-z, x+1/2, -y+1/2' 'y, z, x' '-y, z+1/2, -x+1/2' 'y+1/2, -z+1/2, -x' '-y+1/2, -z, x+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' '-z, -x, -y' '-z-1/2, x-1/2, y' 'z-1/2, x, -y-1/2' 'z, -x-1/2, y-1/2' '-y, -z, -x' 'y, -z-1/2, x-1/2' '-y-1/2, z-1/2, x' 'y-1/2, z, -x-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 2 70777.59 68102.80 439.00 o 1 1 2 4631.30 4037.58 16.90 o 0 2 2 1278.87 1269.85 13.16 o 1 2 2 5638.45 5283.99 21.14 o 2 2 2 27386.13 25053.61 205.97 o 1 1 3 11189.14 10547.88 48.41 o 2 1 3 1902.62 1945.41 14.21 o 0 2 3 13022.87 11812.26 77.16 o 1 2 3 51.57 68.64 6.44 o 2 2 3 10977.39 10483.14 47.94 o 1 3 3 2304.08 2255.34 16.36 o 2 3 3 26186.59 25531.08 116.71 o 3 3 3 2047.01 1996.86 33.54 o 0 0 4 91195.98 86108.28 1064.17 o 1 0 4 51.73 111.32 11.78 o 2 0 4 8075.03 7509.43 57.16 o 3 0 4 39046.99 38216.19 256.38 o 1 1 4 23160.41 22169.88 108.38 o 2 1 4 6844.26 6497.53 35.73 o 3 1 4 1548.19 1416.13 15.70 o 0 2 4 36515.37 35584.60 261.49 o 1 2 4 355.10 309.33 10.04 o 2 2 4 1720.97 1629.71 14.79 o 3 2 4 336.49 363.14 11.04 o 1 3 4 1427.60 1507.68 16.08 o 2 3 4 1121.32 954.13 12.70 o 3 3 4 7726.13 7827.08 44.52 o 0 4 4 4976.88 4972.54 50.11 o 1 4 4 3302.65 3202.86 23.56 o 2 4 4 570.53 573.22 9.12 o 3 4 4 4855.28 5051.03 30.01 o 4 4 4 2304.59 1867.58 34.61 o 1 1 5 1446.52 1367.75 19.24 o 2 1 5 14014.89 13008.60 67.47 o 3 1 5 1320.69 1313.55 13.71 o 4 1 5 3424.39 3368.06 24.63 o 0 2 5 7546.24 6491.76 61.38 o 1 2 5 441.61 487.64 13.02 o 2 2 5 143.53 189.68 10.07 o 3 2 5 2773.60 2765.85 22.29 o 4 2 5 4017.58 3451.40 30.77 o 1 3 5 21849.94 21449.63 111.65 o 2 3 5 11162.28 10070.25 55.06 o 3 3 5 950.77 888.93 15.07 o 4 3 5 2910.80 3022.87 26.28 o 0 4 5 1589.59 1682.25 20.29 o 1 4 5 11386.70 11870.46 66.19 o 2 4 5 448.45 497.55 11.74 o 3 4 5 46.88 64.47 5.20 o 4 4 5 468.74 349.07 9.72 o 1 5 5 59.86 80.55 7.93 o 2 5 5 13157.89 13340.63 75.26 o 3 5 5 83.06 73.02 8.80 o 4 5 5 521.18 511.71 11.98 o 5 5 5 2297.51 2281.40 52.32 o 0 0 6 5421.52 4919.81 82.38 o 1 0 6 53140.29 51830.58 430.76 o 2 0 6 4495.54 4341.47 48.20 o 3 0 6 44524.85 43563.51 357.58 o 4 0 6 15409.86 15683.29 117.45 o 5 0 6 41396.54 41641.54 334.49 o 1 1 6 13340.43 12743.06 76.00 o 2 1 6 45.66 25.10 8.83 o 3 1 6 1551.02 1272.22 16.18 o 4 1 6 34.26 41.62 6.17 o 5 1 6 22437.50 22364.61 120.08 o 0 2 6 14960.14 14516.76 118.97 o 1 2 6 222.35 201.76 11.42 o 2 2 6 525.55 487.12 13.96 o 3 2 6 132.41 175.04 10.31 o 4 2 6 3935.76 4160.76 30.57 o 5 2 6 2686.71 2804.73 22.05 o 1 3 6 788.75 637.88 13.64 o 2 3 6 7648.70 7331.66 44.49 o 3 3 6 586.10 770.02 11.78 o 4 3 6 58.04 55.53 11.76 o 5 3 6 18098.72 17979.05 104.60 o 0 4 6 6580.33 6543.07 65.62 o 1 4 6 13747.11 13188.45 83.20 o 2 4 6 12673.29 13109.69 82.24 o 3 4 6 8135.23 7875.71 43.41 o 4 4 6 6538.32 6896.37 44.67 o 5 4 6 8222.21 7797.05 49.21 o 1 5 6 1042.77 916.46 16.71 o 2 5 6 961.08 973.89 17.83 o 3 5 6 1890.51 1566.95 22.04 o 4 5 6 125.06 106.50 11.16 o 5 5 6 9713.05 9610.46 61.97 o 0 6 6 1947.21 2033.83 37.48 o 1 6 6 29.08 54.67 10.62 o 2 6 6 1651.44 1706.43 21.76 o 3 6 6 1173.93 1128.26 22.88 o 4 6 6 10.74 2.56 10.96 o 5 6 6 1.50 15.26 11.25 o 6 6 6 3.00 69.87 26.24 o 1 1 7 14650.40 14182.88 91.79 o 2 1 7 18408.82 18420.85 104.38 o 3 1 7 14581.69 14197.57 83.15 o 4 1 7 1875.10 2007.32 22.94 o 5 1 7 2653.98 2541.46 29.19 o 6 1 7 1784.80 1650.31 24.11 o 0 2 7 3160.12 3021.64 47.42 o 1 2 7 28995.88 28814.34 174.54 o 2 2 7 0.75 10.59 9.43 o 3 2 7 4524.57 4204.12 34.54 o 4 2 7 6261.10 6053.58 42.02 o 5 2 7 7005.80 6550.51 42.61 o 6 2 7 368.98 384.63 12.22 o 1 3 7 7623.26 7428.79 48.79 o 2 3 7 32253.74 33568.85 191.03 o 3 3 7 12024.64 12084.33 74.69 o 4 3 7 1036.44 1131.95 22.09 o 5 3 7 4687.34 4633.17 43.70 o 6 3 7 221.22 235.36 14.95 o 0 4 7 1306.02 1435.40 35.77 o 1 4 7 2369.97 2491.36 25.34 o 2 4 7 2567.93 2720.81 26.39 o 3 4 7 4639.39 4609.99 35.50 o 4 4 7 632.07 808.25 16.97 o 5 4 7 114.40 119.71 11.73 o 6 4 7 192.32 235.17 12.74 o 1 5 7 47.24 35.24 10.24 o 2 5 7 371.94 419.13 18.42 o 3 5 7 74.19 90.15 11.75 o 4 5 7 2849.88 2852.15 29.57 o 5 5 7 478.04 515.56 18.20 o 6 5 7 714.55 742.49 16.01 o 0 6 7 98.07 102.49 18.69 o 1 6 7 31350.61 31533.35 185.16 o 2 6 7 2793.97 2894.24 32.32 o 3 6 7 381.56 331.40 17.92 o 4 6 7 4735.69 4898.88 52.13 o 5 6 7 6611.25 6657.94 60.49 o 6 6 7 1257.69 1295.52 30.08 o 1 7 7 1973.27 1873.96 28.40 o 2 7 7 1815.93 1912.08 27.09 o 3 7 7 2539.12 2510.37 36.46 o 4 7 7 786.77 879.74 21.16 o 5 7 7 1342.78 1290.57 25.75 o 6 7 7 1357.05 1410.76 31.94 o 7 7 7 1811.86 1812.82 60.87 o 0 0 8 22079.76 21386.08 269.73 o 1 0 8 372.60 424.15 23.04 o 2 0 8 6690.51 6570.89 69.86 o 3 0 8 438.55 456.61 21.92 o 4 0 8 86.79 160.36 20.05 o 5 0 8 132.14 116.20 21.18 o 6 0 8 2132.63 2083.79 45.64 o 7 0 8 14891.19 16016.04 158.04 o 1 1 8 79.57 91.16 13.85 o 2 1 8 11977.40 11684.45 75.42 o 3 1 8 1012.36 1075.31 20.57 o 4 1 8 2084.74 2064.49 27.55 o 5 1 8 190.72 221.39 13.09 o 6 1 8 11316.96 11182.34 79.96 o 7 1 8 577.70 630.93 19.84 o 0 2 8 14017.91 14334.21 137.90 o 1 2 8 629.41 645.09 20.10 o 2 2 8 993.60 1167.40 23.99 o 3 2 8 2231.20 2342.04 28.02 o 4 2 8 1522.80 1511.32 21.95 o 5 2 8 152.54 206.18 15.29 o 6 2 8 38.91 36.01 13.68 o 7 2 8 49.36 35.10 14.21 o 1 3 8 2607.49 2796.52 31.23 o 2 3 8 6703.48 6923.61 52.72 o 3 3 8 1419.34 1491.24 22.17 o 4 3 8 3482.17 3657.83 30.78 o 5 3 8 632.35 763.51 21.23 o 6 3 8 4452.87 4131.60 47.93 o 7 3 8 4649.07 4614.97 54.93 o 0 4 8 14158.29 13564.10 128.33 o 1 4 8 1890.47 1930.33 25.25 o 2 4 8 156.36 214.91 14.45 o 3 4 8 87.27 86.00 10.74 o 4 4 8 20599.05 20257.93 136.48 o 5 4 8 177.01 138.67 13.98 o 6 4 8 299.69 343.71 15.46 o 7 4 8 2722.86 2835.00 40.98 o 1 5 8 2135.16 1933.80 31.98 o 2 5 8 11755.60 11618.51 81.08 o 3 5 8 1070.35 1067.09 21.17 o 4 5 8 1021.18 1040.73 19.93 o 5 5 8 1642.66 1663.33 22.15 o 6 5 8 17443.01 17590.23 110.66 o 7 5 8 1022.54 1055.36 21.04 o 0 6 8 3196.41 3323.50 58.38 o 1 6 8 2658.15 2739.87 33.86 o 2 6 8 4.87 20.34 11.99 o 3 6 8 4.48 4.71 13.25 o 4 6 8 474.69 523.63 25.91 o 5 6 8 1333.20 1415.16 25.46 o 6 6 8 485.81 497.43 18.36 o 7 6 8 411.25 434.94 24.94 o 1 7 8 0.84 -14.96 14.96 o 2 7 8 13161.40 13716.99 103.60 o 3 7 8 229.98 296.53 20.29 o 4 7 8 1718.14 1750.17 31.52 o 5 7 8 3401.46 3344.41 53.46 o 6 7 8 1711.64 1685.75 38.03 o 7 7 8 4518.26 4502.55 60.05 o 0 8 8 14958.56 15105.47 146.19 o 1 8 8 2219.09 2221.74 35.27 o 2 8 8 6.08 25.38 13.86 o 3 8 8 4121.71 4201.05 53.93 o 4 8 8 9437.06 9730.92 85.43 o 5 8 8 361.46 357.90 23.32 o 6 8 8 1505.44 1608.37 40.70 o 7 8 8 725.93 810.70 31.77 o 8 8 8 15973.83 17241.82 283.29 o 1 1 9 96.73 103.34 15.58 o 2 1 9 20754.50 20609.81 127.66 o 3 1 9 155.27 214.11 16.35 o 4 1 9 2145.24 2213.66 32.14 o 5 1 9 450.16 481.41 20.63 o 6 1 9 7718.17 7789.14 64.74 o 7 1 9 1246.27 1270.65 28.28 o 8 1 9 10.98 29.25 13.25 o 0 2 9 18328.93 17470.91 174.09 o 1 2 9 12.69 31.03 14.73 o 2 2 9 239.93 242.94 17.97 o 3 2 9 650.45 566.69 20.30 o 4 2 9 10409.72 10201.01 73.92 o 5 2 9 5073.43 4959.64 45.96 o 6 2 9 442.76 519.53 18.67 o 7 2 9 65.24 59.77 12.42 o 8 2 9 9164.99 9464.13 77.17 o 1 3 9 5316.39 5218.00 50.53 o 2 3 9 20653.69 21164.24 134.15 o 3 3 9 3.91 1.77 11.35 o 4 3 9 1165.96 1151.89 21.13 o 5 3 9 1037.91 1046.00 22.22 o 6 3 9 10730.35 11070.49 92.99 o 7 3 9 228.99 233.74 18.73 o 8 3 9 53.51 75.56 16.46 o 0 4 9 98.09 91.29 20.79 o 1 4 9 3073.86 3147.44 37.90 o 2 4 9 239.94 248.61 15.01 o 3 4 9 177.95 198.41 13.36 o 4 4 9 7.01 -2.18 12.54 o 5 4 9 485.35 594.67 22.87 o 6 4 9 676.42 754.76 17.56 o 7 4 9 1103.69 1136.39 29.90 o 8 4 9 38.56 31.63 17.16 o 1 5 9 1978.11 1950.31 26.10 o 2 5 9 656.98 651.52 21.08 o 3 5 9 4716.07 4947.69 46.57 o 4 5 9 1932.65 1874.92 34.97 o 5 5 9 3072.85 3088.81 39.99 o 6 5 9 254.49 279.99 15.68 o 7 5 9 1895.11 1972.51 27.60 o 8 5 9 4866.89 5081.92 59.90 o 0 6 9 15170.16 15057.31 159.50 o 1 6 9 3942.12 4173.87 45.78 o 2 6 9 1184.52 1196.61 26.49 o 3 6 9 6053.04 6209.17 51.59 o 4 6 9 9884.67 9938.17 78.18 o 5 6 9 6092.12 6134.60 71.87 o 6 6 9 1218.71 1239.12 29.24 o 7 6 9 127.68 147.71 18.36 o 8 6 9 6715.02 7119.72 88.19 o 1 7 9 459.90 525.32 21.83 o 2 7 9 5015.03 5025.39 54.39 o 3 7 9 1111.29 1131.07 19.91 o 4 7 9 456.39 525.45 25.83 o 5 7 9 358.01 350.55 24.28 o 6 7 9 2262.43 2344.82 45.22 o 7 7 9 1843.95 2002.53 43.62 o 8 7 9 2198.91 2137.74 45.60 o 0 8 9 2937.75 3001.30 61.65 o 1 8 9 196.72 236.34 19.08 o 2 8 9 711.76 732.34 20.26 o 3 8 9 21.47 16.33 16.67 o 4 8 9 5718.60 5838.83 54.59 o 5 8 9 140.65 255.99 26.30 o 6 8 9 453.86 376.43 24.34 o 7 8 9 3.46 -3.00 16.48 o 8 8 9 929.54 1033.75 37.15 o 1 9 9 167.02 182.17 19.72 o 2 9 9 1310.28 1307.59 29.35 o 3 9 9 699.47 743.49 26.83 o 4 9 9 2.65 5.30 15.04 o 5 9 9 1163.74 1220.84 38.61 o 6 9 9 1785.79 1992.13 52.40 o 7 9 9 40.97 57.03 24.00 o 8 9 9 587.06 637.73 32.97 o 9 9 9 84.88 33.65 36.34 o 0 0 10 9423.03 10028.51 162.44 o 1 0 10 5430.94 5326.74 77.30 o 2 0 10 397.37 435.79 27.68 o 3 0 10 3402.27 3167.09 55.18 o 4 0 10 799.03 907.67 32.23 o 5 0 10 13571.36 14191.68 144.53 o 6 0 10 7253.39 7240.81 99.92 o 7 0 10 110.88 147.67 26.80 o 8 0 10 9242.81 9027.16 117.96 o 9 0 10 4742.59 5090.65 82.89 o 1 1 10 3864.67 3662.54 44.88 o 2 1 10 194.89 187.28 17.59 o 3 1 10 3563.14 3349.27 42.18 o 4 1 10 2237.68 2214.15 33.20 o 5 1 10 2886.75 3064.35 37.01 o 6 1 10 1034.60 970.85 28.80 o 7 1 10 9136.17 9826.34 88.22 o 8 1 10 388.54 364.52 23.70 o 9 1 10 280.68 317.09 21.63 o 0 2 10 992.11 1053.68 44.32 o 1 2 10 2273.89 2316.33 37.71 o 2 2 10 794.89 868.52 24.97 o 3 2 10 2.21 -1.36 11.72 o 4 2 10 9.41 -10.48 14.71 o 5 2 10 1394.25 1568.71 31.80 o 6 2 10 2907.14 3057.32 41.29 o 7 2 10 109.55 102.51 13.99 o 8 2 10 210.47 183.75 24.77 o 9 2 10 372.90 415.68 29.13 o 1 3 10 2288.98 2178.17 36.15 o 2 3 10 11.76 42.38 15.55 o 3 3 10 3621.03 3773.77 42.21 o 4 3 10 269.97 260.47 16.87 o 5 3 10 58.69 68.35 14.20 o 6 3 10 1449.35 1531.23 34.30 o 7 3 10 212.27 165.22 19.70 o 8 3 10 628.81 639.60 30.90 o 9 3 10 843.80 892.83 36.23 o 0 4 10 52.24 39.08 19.06 o 1 4 10 2444.04 2516.45 36.99 o 2 4 10 672.05 786.42 25.18 o 3 4 10 6144.48 6233.27 56.44 o 4 4 10 3132.07 3246.74 36.79 o 5 4 10 5583.26 5724.82 62.07 o 6 4 10 141.32 162.18 14.90 o 7 4 10 450.23 502.49 23.84 o 8 4 10 1807.50 1972.34 37.75 o 9 4 10 576.73 643.98 27.01 o 1 5 10 14.17 13.11 15.69 o 2 5 10 5138.53 5303.61 50.78 o 3 5 10 158.01 124.95 14.82 o 4 5 10 0.80 30.01 14.48 o 5 5 10 2208.13 2433.17 39.70 o 6 5 10 1347.91 1357.57 30.96 o 7 5 10 3689.58 3785.80 48.05 o 8 5 10 449.92 395.08 23.52 o 9 5 10 385.33 443.80 25.87 o 0 6 10 90.24 170.25 27.50 o 1 6 10 150.23 197.24 15.58 o 2 6 10 71.91 43.99 17.76 o 3 6 10 548.33 504.51 23.56 o 4 6 10 4141.82 4200.87 49.58 o 5 6 10 714.64 774.63 35.47 o 6 6 10 401.84 419.04 24.73 o 7 6 10 1488.75 1478.08 31.28 o 8 6 10 97.60 109.31 25.34 o 9 6 10 56.19 30.72 22.15 o 1 7 10 2734.63 2888.57 41.88 o 2 7 10 1004.93 1121.00 27.32 o 3 7 10 5628.53 5859.34 53.64 o 4 7 10 165.16 215.77 23.21 o 5 7 10 2361.79 2313.75 45.90 o 6 7 10 625.99 715.65 30.69 o 7 7 10 333.75 340.15 27.69 o 8 7 10 466.58 415.64 24.40 o 9 7 10 196.28 165.97 29.51 o 0 8 10 2554.68 2559.35 60.16 o 1 8 10 2819.93 2837.09 44.21 o 2 8 10 208.12 232.47 22.02 o 3 8 10 115.85 148.38 17.04 o 4 8 10 60.52 68.24 21.01 o 5 8 10 1798.86 2005.88 53.47 o 6 8 10 1559.98 1544.22 42.10 o 7 8 10 85.99 109.46 27.31 o 8 8 10 1519.77 1506.68 58.67 o 9 8 10 2001.71 2345.82 66.41 o 1 9 10 1770.59 1999.39 39.62 o 2 9 10 852.54 859.05 28.70 o 3 9 10 2600.64 2805.37 42.02 o 4 9 10 537.27 529.84 25.44 o 5 9 10 7.76 34.29 24.48 o 6 9 10 34.95 52.14 19.39 o 7 9 10 215.79 256.85 32.05 o 8 9 10 101.79 58.59 29.88 o 9 9 10 1231.35 1162.20 130.27 o 0 10 10 1006.79 991.89 48.77 o 1 10 10 2744.78 2828.63 45.48 o 2 10 10 67.13 68.83 24.23 o 3 10 10 245.40 312.05 30.35 o 4 10 10 7.07 39.80 16.30 o 5 10 10 19.68 47.30 19.06 o 6 10 10 59.22 41.07 25.07 o 7 10 10 934.34 855.86 73.47 o 8 10 10 24.09 7.67 23.20 o 9 10 10 83.13 49.21 29.38 o 10 10 10 12.17 20.60 60.27 o 1 1 11 240.87 260.47 21.48 o 2 1 11 97.88 138.48 18.85 o 3 1 11 2652.83 2726.76 42.80 o 4 1 11 63.40 76.83 15.03 o 5 1 11 59.33 72.21 17.17 o 6 1 11 2.70 8.82 13.81 o 7 1 11 926.01 984.59 28.74 o 8 1 11 1.58 2.39 14.58 o 9 1 11 32.09 58.33 18.10 o 10 1 11 601.10 576.47 25.86 o 0 2 11 1737.67 1942.71 70.22 o 1 2 11 180.66 138.88 19.18 o 2 2 11 39.43 15.80 15.05 o 3 2 11 3538.48 3469.82 44.32 o 4 2 11 2096.36 2122.40 37.44 o 5 2 11 1919.57 2009.94 35.87 o 6 2 11 200.46 207.29 20.97 o 7 2 11 482.87 551.06 30.99 o 8 2 11 402.66 484.23 30.97 o 9 2 11 5662.61 6166.79 80.42 o 10 2 11 9.46 -21.23 21.23 o 1 3 11 3361.80 3320.66 47.82 o 2 3 11 1549.23 1694.95 34.14 o 3 3 11 6659.77 6808.66 62.41 o 4 3 11 38.91 20.84 12.96 o 5 3 11 4342.99 4438.96 45.71 o 6 3 11 37.63 38.68 14.67 o 7 3 11 1084.42 1144.99 36.38 o 8 3 11 205.15 224.47 25.80 o 9 3 11 2457.57 2783.31 56.23 o 10 3 11 976.35 916.71 43.76 o 0 4 11 1594.81 1564.37 49.08 o 1 4 11 1124.22 1205.71 30.86 o 2 4 11 927.06 1013.26 29.34 o 3 4 11 819.35 890.93 24.97 o 4 4 11 5.93 -10.59 14.63 o 5 4 11 72.60 96.20 17.41 o 6 4 11 147.15 156.21 18.00 o 7 4 11 1953.08 2008.97 41.78 o 8 4 11 255.75 295.50 23.29 o 9 4 11 253.17 271.00 24.06 o 10 4 11 439.02 396.83 33.43 o 1 5 11 4425.16 4420.29 50.54 o 2 5 11 73.55 87.11 16.61 o 3 5 11 917.42 972.79 30.61 o 4 5 11 1750.14 1667.88 34.36 o 5 5 11 2039.50 2016.44 39.62 o 6 5 11 2973.37 3029.24 42.75 o 7 5 11 1131.33 1203.91 33.59 o 8 5 11 48.64 70.51 16.60 o 9 5 11 755.07 761.30 33.48 o 10 5 11 221.71 156.94 30.19 o 0 6 11 5.46 12.26 22.93 o 1 6 11 4250.68 4360.27 49.30 o 2 6 11 283.18 247.06 20.57 o 3 6 11 11192.01 11648.60 98.81 o 4 6 11 410.47 396.02 23.29 o 5 6 11 8918.50 9503.52 88.14 o 6 6 11 1104.78 1135.20 39.96 o 7 6 11 6092.28 6241.46 71.34 o 8 6 11 39.94 36.49 16.11 o 9 6 11 3684.01 3811.20 71.88 o 10 6 11 460.36 343.23 49.99 o 1 7 11 22.27 44.22 18.76 o 2 7 11 78.77 90.39 17.75 o 3 7 11 254.87 300.88 19.09 o 4 7 11 100.49 89.64 23.14 o 5 7 11 712.00 670.71 35.72 o 6 7 11 1415.29 1612.74 44.33 o 7 7 11 2757.95 2734.76 45.46 o 8 7 11 698.84 592.62 46.42 o 9 7 11 34.10 60.17 25.42 o 10 7 11 458.55 294.31 41.62 o 0 8 11 121.68 176.30 34.13 o 1 8 11 824.67 911.41 32.41 o 2 8 11 373.65 434.56 24.67 o 3 8 11 4.51 2.60 14.60 o 4 8 11 665.37 791.68 35.52 o 5 8 11 1021.80 1071.61 39.69 o 6 8 11 241.12 225.84 24.35 o 7 8 11 41.00 51.51 23.35 o 8 8 11 438.39 405.56 41.15 o 9 8 11 116.51 100.68 33.18 o 10 8 11 104.22 77.97 31.77 o 1 9 11 2906.86 3003.78 54.83 o 2 9 11 776.00 733.45 29.55 o 3 9 11 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