#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/82/2018293.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018293_Fobs loop_ _publ_author_name 'Chaplin, Adrian B.' 'Weller, Andrew S.' _publ_section_title ; A rhodium(III) complex of the linear diborazine H~3~B·NMe~2~BH~2~·NMe~2~H: an intermediate in the dehydrocoupling of H~3~B·NMe~2~H ; _journal_coeditor_code OV3008 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m355 _journal_page_last m358 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 73.018 _cell_angle_beta 76.413 _cell_angle_gamma 86.688 _cell_length_a 12.8309 _cell_length_b 14.0813 _cell_length_c 19.1638 _exptl_crystal_F_000 1436.00 _reflns_d_resolution_high 0.7705 _[local]_cod_data_source_file ov3008XVsup2.hkl _[local]_cod_data_source_block XV #BEGIN Tags that were not found in dictionaries: _shelx_title ' 118abc09 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 205.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 187.01 9.96 4.27 o 3 0 0 67.42 38.69 2.16 o 4 0 0 2605.06 2613.73 69.39 o 5 0 0 1.19 7.31 1.66 o 6 0 0 1032.77 873.94 20.32 o 7 0 0 2187.34 1741.93 48.73 o 8 0 0 3284.44 3387.57 93.43 o 9 0 0 1053.08 891.13 46.24 o 10 0 0 637.53 606.43 24.19 o 11 0 0 173.50 162.24 8.30 o 12 0 0 4.91 14.72 10.04 o 13 0 0 150.63 138.22 14.41 o 14 0 0 488.50 430.59 27.76 o 15 0 0 14.46 9.48 18.02 o 16 0 0 281.99 277.90 36.99 o -16 1 0 51.11 73.03 24.66 o -15 1 0 111.60 96.74 23.24 o -14 1 0 658.02 619.57 37.30 o -13 1 0 316.64 297.72 41.50 o -12 1 0 147.64 161.10 15.27 o -11 1 0 1009.07 1252.99 53.47 o -10 1 0 1222.48 1259.53 46.59 o -9 1 0 1220.70 1357.97 47.01 o -8 1 0 181.24 224.27 10.91 o -7 1 0 714.91 740.22 14.47 o -6 1 0 813.61 708.72 16.24 o -5 1 0 283.26 230.98 7.62 o -4 1 0 676.26 699.48 22.36 o -3 1 0 3550.78 3296.12 79.23 o 3 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2315.08 48.29 o 9 3 0 125.24 106.23 7.59 o 10 3 0 1539.95 1577.14 50.86 o 11 3 0 391.79 330.28 13.97 o 12 3 0 1952.48 2083.53 72.87 o 13 3 0 349.51 351.96 26.56 o 14 3 0 115.28 137.87 21.81 o 15 3 0 250.25 221.94 35.57 o -15 4 0 37.54 35.31 12.21 o -14 4 0 863.85 1018.29 56.67 o -13 4 0 371.25 398.83 24.23 o -12 4 0 3.32 5.40 13.52 o -11 4 0 301.73 305.51 17.07 o -10 4 0 387.09 426.58 13.77 o -9 4 0 485.71 507.27 16.14 o -8 4 0 38.34 60.20 5.79 o -7 4 0 4104.23 4360.14 129.94 o -6 4 0 6775.75 6399.35 187.32 o -5 4 0 765.18 959.38 28.45 o -4 4 0 398.15 454.04 12.30 o -3 4 0 1082.13 1264.83 36.21 o -2 4 0 4.75 31.28 8.30 o -1 4 0 4810.33 4583.00 108.95 o 0 4 0 1676.82 1558.80 39.61 o 1 4 0 11762.94 10656.91 243.62 o 2 4 0 19.15 65.36 4.27 o 3 4 0 17120.37 16339.65 340.18 o 4 4 0 263.32 406.04 13.99 o 5 4 0 313.37 376.61 12.57 o 6 4 0 87.37 58.34 9.48 o 7 4 0 4843.74 5106.73 112.82 o 8 4 0 312.11 314.35 9.04 o 9 4 0 240.02 237.09 7.83 o 10 4 0 2037.79 2315.57 77.70 o 11 4 0 2534.44 2714.62 103.84 o 12 4 0 217.24 161.67 33.91 o 13 4 0 15.05 10.02 10.91 o 14 4 0 243.51 222.26 19.04 o 15 4 0 18.28 22.29 32.25 o -15 5 0 197.26 171.67 19.92 o -14 5 0 242.73 217.67 19.44 o -13 5 0 83.43 67.34 13.75 o -12 5 0 34.11 34.62 4.74 o -11 5 0 1147.04 1118.25 52.17 o -10 5 0 1050.29 1106.39 39.84 o -9 5 0 0.35 2.37 5.22 o -8 5 0 752.29 744.55 22.76 o -7 5 0 1960.28 1867.55 36.99 o -6 5 0 2335.13 2517.72 66.87 o -5 5 0 6.74 -4.27 5.69 o -4 5 0 5676.38 5537.64 138.06 o -3 5 0 8346.27 7423.57 199.97 o -2 5 0 4049.39 4514.94 107.34 o -1 5 0 2.64 -3.18 4.09 o 0 5 0 5200.16 5096.90 131.37 o 1 5 0 6117.87 6193.34 130.65 o 2 5 0 5014.73 4520.91 97.79 o 3 5 0 618.40 622.07 12.86 o 4 5 0 1464.13 1734.59 35.09 o 5 5 0 225.65 212.70 7.06 o 6 5 0 1374.56 1491.08 33.59 o 7 5 0 2276.14 2407.20 70.42 o 8 5 0 1537.51 1557.14 33.45 o 9 5 0 260.85 221.30 8.20 o 10 5 0 537.84 532.37 15.49 o 11 5 0 46.55 16.58 11.86 o 12 5 0 3.89 -2.02 10.67 o 13 5 0 697.61 674.96 42.52 o 14 5 0 361.72 396.96 28.59 o 15 5 0 199.17 193.01 31.30 o -15 6 0 14.10 -1.90 23.24 o -14 6 0 79.93 73.51 18.02 o -13 6 0 404.35 346.19 23.24 o -12 6 0 632.10 673.42 27.51 o -11 6 0 340.71 383.18 17.55 o -10 6 0 311.51 354.73 12.80 o -9 6 0 29.23 59.28 6.64 o -8 6 0 870.13 856.00 17.55 o -7 6 0 559.55 501.74 14.70 o -6 6 0 59.60 54.06 6.17 o -5 6 0 1297.23 1573.99 44.58 o -4 6 0 8508.36 8327.94 217.59 o -3 6 0 3158.03 2787.90 61.82 o -2 6 0 1444.46 1245.66 32.11 o -1 6 0 10.38 39.84 4.38 o 0 6 0 1982.79 1892.16 40.73 o 1 6 0 1495.38 1929.86 39.40 o 2 6 0 51.37 78.98 4.78 o 3 6 0 243.25 138.55 8.30 o 4 6 0 625.65 817.18 17.62 o 5 6 0 889.14 863.95 18.79 o 6 6 0 5327.06 5237.07 110.13 o 7 6 0 1254.13 1310.04 50.51 o 8 6 0 36.97 26.96 4.51 o 9 6 0 274.04 294.22 9.66 o 10 6 0 232.36 245.94 9.22 o 11 6 0 1.31 17.91 21.58 o 12 6 0 217.97 246.23 18.17 o 13 6 0 997.27 1113.33 64.94 o 14 6 0 129.77 138.24 21.73 o 15 6 0 2.86 -23.71 23.71 o -14 7 0 106.96 128.99 19.44 o -13 7 0 158.89 143.22 16.12 o -12 7 0 9.65 3.32 5.69 o -11 7 0 66.10 93.42 8.06 o -10 7 0 282.96 315.37 12.80 o -9 7 0 66.95 90.58 3.79 o -8 7 0 287.41 291.18 9.01 o -7 7 0 309.18 349.04 13.28 o -6 7 0 412.50 408.79 13.75 o -5 7 0 2342.54 2078.85 49.69 o -4 7 0 3999.67 4319.03 114.39 o -3 7 0 177.64 125.17 7.20 o -2 7 0 14283.81 13634.28 317.36 o -1 7 0 2487.01 2205.79 49.01 o 0 7 0 2279.42 2446.75 55.46 o 1 7 0 98.38 219.52 6.82 o 2 7 0 2144.35 2037.59 42.59 o 3 7 0 3284.36 3208.85 79.95 o 4 7 0 3003.97 2922.26 65.60 o 5 7 0 400.88 335.28 10.38 o 6 7 0 2442.18 2500.61 56.29 o 7 7 0 260.49 300.52 8.55 o 8 7 0 1540.95 1516.89 34.27 o 9 7 0 1020.90 1096.85 33.43 o 10 7 0 9.11 2.25 5.93 o 11 7 0 720.83 715.80 27.88 o 12 7 0 1089.34 1106.80 56.32 o 13 7 0 55.39 71.53 24.42 o 14 7 0 26.95 35.96 11.83 o -14 8 0 86.46 73.03 27.03 o -13 8 0 0.26 -12.33 13.75 o -12 8 0 334.86 352.36 22.76 o -11 8 0 101.88 79.67 9.01 o -10 8 0 837.57 888.25 28.45 o -9 8 0 1101.49 1198.40 29.88 o -8 8 0 1.10 4.74 4.74 o -7 8 0 156.80 135.16 8.06 o -6 8 0 535.11 563.39 18.50 o -5 8 0 492.52 547.10 17.86 o -4 8 0 614.62 636.47 20.17 o -3 8 0 2325.29 2529.94 61.24 o -2 8 0 10666.78 10866.83 264.43 o -1 8 0 3541.80 3659.29 81.41 o 0 8 0 246.67 158.48 7.35 o 1 8 0 743.98 816.65 18.00 o 2 8 0 55.44 64.31 14.94 o 3 8 0 7.39 -9.81 18.73 o 4 8 0 239.03 373.81 12.39 o 5 8 0 270.29 304.42 10.04 o 6 8 0 1117.32 1151.91 30.67 o 7 8 0 117.79 127.47 7.29 o 8 8 0 62.03 36.65 5.69 o 9 8 0 264.02 215.30 22.05 o 10 8 0 406.85 453.82 15.33 o 11 8 0 272.26 275.46 15.70 o 12 8 0 31.11 7.36 9.43 o 13 8 0 22.45 30.69 11.59 o 14 8 0 93.74 124.11 19.92 o -13 9 0 296.52 224.79 30.35 o -12 9 0 250.76 274.58 19.44 o -11 9 0 158.13 122.83 10.43 o -10 9 0 113.86 112.39 5.69 o -9 9 0 32.52 14.23 4.27 o -8 9 0 862.07 931.40 27.51 o -7 9 0 892.19 962.23 31.77 o -6 9 0 269.35 257.51 9.96 o -5 9 0 3.06 4.28 6.48 o -4 9 0 502.27 560.18 17.89 o -3 9 0 1422.75 1444.38 34.73 o -2 9 0 823.39 849.33 21.77 o -1 9 0 646.07 724.10 24.90 o 0 9 0 3225.08 3194.95 62.87 o 1 9 0 1012.53 988.51 21.67 o 2 9 0 933.17 917.27 21.28 o 3 9 0 576.01 658.66 19.26 o 4 9 0 884.53 841.74 23.55 o 5 9 0 2366.68 2452.99 68.47 o 6 9 0 76.22 89.84 8.77 o 7 9 0 160.15 140.39 7.86 o 8 9 0 731.16 763.74 26.78 o 9 9 0 7.25 13.76 12.80 o 10 9 0 1.68 8.54 6.64 o 11 9 0 258.24 203.92 18.50 o 12 9 0 33.31 39.84 12.80 o 13 9 0 16.71 19.92 21.34 o -13 10 0 162.10 145.59 24.66 o -12 10 0 36.20 34.15 25.61 o -11 10 0 483.76 484.20 21.34 o -10 10 0 467.34 469.97 17.55 o -9 10 0 804.60 917.17 26.56 o -8 10 0 676.14 685.27 21.34 o -7 10 0 100.79 59.75 8.06 o -6 10 0 577.60 623.15 23.24 o -5 10 0 457.90 471.39 23.24 o -4 10 0 374.16 345.71 22.29 o -3 10 0 642.35 692.18 18.16 o -2 10 0 360.98 416.55 12.83 o -1 10 0 4965.08 5337.84 119.38 o 0 10 0 2863.76 2882.39 65.08 o 1 10 0 577.72 610.36 14.51 o 2 10 0 69.15 46.56 5.17 o 3 10 0 8491.87 8586.68 222.64 o 4 10 0 235.23 194.53 9.79 o 5 10 0 71.31 44.23 7.63 o 6 10 0 123.82 121.61 9.22 o 7 10 0 326.68 403.10 14.18 o 8 10 0 725.68 629.38 24.44 o 9 10 0 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12 0 163.05 157.92 11.38 o -5 12 0 21.39 15.65 10.43 o -4 12 0 24.53 37.89 9.33 o -3 12 0 684.13 610.77 26.32 o -2 12 0 534.02 532.59 18.73 o -1 12 0 527.59 520.68 17.75 o 0 12 0 171.84 181.27 8.17 o 1 12 0 325.76 340.47 14.94 o 2 12 0 659.61 557.04 41.97 o 3 12 0 251.39 231.77 14.46 o 4 12 0 992.45 1139.06 43.36 o 5 12 0 868.16 814.67 33.14 o 6 12 0 372.70 369.18 18.77 o 7 12 0 41.43 29.04 7.62 o 8 12 0 272.81 331.40 19.11 o 9 12 0 410.05 393.31 18.77 o 10 12 0 155.74 99.59 17.07 o 11 12 0 0.64 4.27 11.86 o -10 13 0 48.48 40.78 16.60 o -9 13 0 499.42 442.46 28.93 o -8 13 0 720.55 754.04 31.77 o -7 13 0 122.09 91.53 9.48 o -6 13 0 273.24 346.67 18.97 o -5 13 0 1174.47 1248.19 74.46 o -4 13 0 323.57 377.02 22.29 o -3 13 0 0.61 -1.39 8.03 o -2 13 0 49.27 44.02 6.83 o -1 13 0 113.45 118.25 8.09 o 0 13 0 887.95 875.46 49.08 o 1 13 0 75.07 64.54 7.29 o 2 13 0 231.79 186.93 10.37 o 3 13 0 7.93 -13.18 19.68 o 4 13 0 424.36 393.82 19.65 o 5 13 0 96.00 94.97 9.04 o 6 13 0 225.19 237.89 19.92 o 7 13 0 280.60 279.01 18.70 o 8 13 0 382.76 372.66 19.90 o 9 13 0 24.23 41.45 14.18 o 10 13 0 35.43 17.55 22.76 o -9 14 0 58.62 51.22 17.07 o -8 14 0 170.21 173.57 22.76 o -7 14 0 458.82 441.04 18.97 o -6 14 0 1423.71 1456.86 64.50 o -5 14 0 199.53 177.36 13.75 o -4 14 0 106.70 98.64 9.96 o -3 14 0 121.47 83.70 12.80 o -2 14 0 121.03 99.23 10.43 o -1 14 0 16.86 4.43 6.14 o 0 14 0 4.42 -0.36 6.48 o 1 14 0 181.37 178.14 9.79 o 2 14 0 85.56 72.17 9.32 o 3 14 0 136.87 146.09 13.99 o 4 14 0 22.32 2.09 8.66 o 5 14 0 18.32 9.48 8.54 o 6 14 0 88.54 78.04 11.93 o 7 14 0 172.02 169.33 26.08 o 8 14 0 26.73 31.57 14.85 o 9 14 0 44.95 73.98 23.24 o -8 15 0 43.62 35.09 26.56 o -7 15 0 267.98 268.42 22.76 o -6 15 0 1.49 10.43 9.96 o -5 15 0 27.99 16.12 11.38 o -4 15 0 318.68 366.59 21.34 o -3 15 0 793.78 903.93 75.40 o -2 15 0 163.72 170.55 14.11 o -1 15 0 61.49 50.28 10.43 o 0 15 0 39.99 66.24 12.33 o 1 15 0 77.71 96.29 9.39 o 2 15 0 79.24 102.70 12.75 o 3 15 0 11.93 13.64 14.94 o 4 15 0 37.58 52.74 44.34 o 5 15 0 191.49 158.82 27.51 o 6 15 0 83.91 82.72 15.72 o 7 15 0 94.40 75.05 21.65 o 8 15 0 1.20 45.05 33.67 o -6 16 0 27.66 25.61 14.70 o -5 16 0 252.11 253.24 22.29 o -4 16 0 409.60 331.49 25.13 o -3 16 0 123.03 146.31 24.66 o -2 16 0 51.78 60.94 9.57 o -1 16 0 533.61 475.97 23.48 o 0 16 0 192.83 167.42 12.17 o 1 16 0 51.23 71.49 10.18 o 2 16 0 15.49 17.18 16.36 o 3 16 0 148.89 133.36 14.88 o 4 16 0 44.73 33.90 23.47 o 5 16 0 74.09 54.41 16.86 o -3 17 0 5.77 0.95 15.18 o -2 17 0 410.62 393.14 27.98 o -1 17 0 265.01 231.90 22.76 o 0 17 0 27.70 0.95 16.12 o 1 17 0 52.33 33.20 12.80 o 2 17 0 271.88 253.24 41.26 o -1 -17 1 97.65 96.27 27.98 o 0 -17 1 129.85 158.40 39.84 o 1 -17 1 26.70 7.59 23.71 o 2 -17 1 81.49 57.86 22.29 o 3 -17 1 344.67 268.42 40.31 o -5 -16 1 60.10 89.63 24.66 o -4 -16 1 27.27 16.60 23.24 o -3 -16 1 27.84 26.09 26.79 o -2 -16 1 123.13 149.68 27.27 o -1 -16 1 178.30 145.23 18.36 o 0 -16 1 33.22 6.24 11.56 o 1 -16 1 159.41 158.34 20.16 o 2 -16 1 160.67 190.82 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57.39 15.18 o 2 10 23 75.30 75.91 20.04 o 3 10 23 410.34 410.34 31.47 o 4 10 23 188.36 196.96 15.61 o 5 10 23 275.94 297.42 26.13 o 6 10 23 216.74 198.17 20.62 o 7 10 23 4.38 21.81 19.44 o 2 11 23 173.16 153.04 25.48 o 3 11 23 337.65 358.52 49.32 o 4 11 23 28.25 30.35 22.76 o 5 11 23 27.89 -3.95 13.30 o 6 11 23 57.11 54.54 24.66 o 3 1 24 15.91 46.95 24.19 o 4 1 24 62.86 24.19 22.29 o 5 1 24 3.78 38.41 21.34 o 1 2 24 35.22 18.50 20.87 o 2 2 24 46.12 1.42 18.97 o 3 2 24 56.89 82.99 29.40 o 4 2 24 68.62 48.85 26.56 o 5 2 24 170.35 207.72 35.57 o 6 2 24 100.69 122.83 25.13 o 1 3 24 11.15 -15.65 17.07 o 2 3 24 69.58 55.49 16.12 o 3 3 24 431.38 461.91 32.25 o 4 3 24 19.55 18.50 16.12 o 5 3 24 81.81 75.40 21.34 o 6 3 24 9.91 -18.50 27.98 o 7 3 24 33.61 61.65 27.03 o 0 4 24 56.35 39.19 11.90 o 1 4 24 122.74 162.57 16.52 o 2 4 24 113.11 73.63 13.06 o 3 4 24 79.79 72.73 14.10 o 4 4 24 148.00 146.54 18.02 o 5 4 24 109.40 91.05 32.72 o 6 4 24 100.50 97.22 21.81 o 7 4 24 271.06 274.11 36.99 o 0 5 24 84.06 87.92 11.95 o 1 5 24 103.19 74.93 13.57 o 2 5 24 87.74 74.87 13.10 o 3 5 24 0.08 -1.22 9.25 o 4 5 24 93.39 70.66 15.90 o 5 5 24 233.93 220.52 38.89 o 6 5 24 17.38 29.40 21.81 o 7 5 24 0.20 24.19 21.81 o 0 6 24 370.99 312.31 26.73 o 1 6 24 134.46 121.40 20.87 o 2 6 24 12.46 14.59 11.73 o 3 6 24 204.68 201.38 32.72 o 4 6 24 54.70 66.96 16.81 o 5 6 24 164.53 145.82 15.34 o 7 6 24 385.29 358.05 42.21 o 0 7 24 4.00 17.07 14.75 o 1 7 24 43.54 29.84 12.54 o 2 7 24 157.86 200.18 72.80 o 3 7 24 309.61 316.71 20.76 o 4 7 24 167.82 153.32 16.14 o 5 7 24 3.83 -6.72 19.44 o 6 7 24 19.57 17.55 20.39 o 7 7 24 290.39 279.33 36.04 o 1 8 24 4.77 5.85 18.89 o 2 8 24 342.51 225.63 19.48 o 3 8 24 87.77 61.14 12.65 o 4 8 24 56.92 64.07 17.01 o 5 8 24 176.50 152.07 21.39 o 6 8 24 197.45 141.24 23.24 o 7 8 24 8.59 34.62 32.72 o 2 9 24 88.92 53.19 18.50 o 3 9 24 6.35 -8.54 27.51 o 4 9 24 370.49 337.27 25.04 o 5 9 24 134.14 145.49 21.18 o