#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/83/2018323.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018323_Fobs loop_ _publ_author_name 'Garc\'ia-Rubi\~no, M. Eugenia' 'Choquesillo-Lazarte, Duane' 'N\'u\~nez, M. C.' 'Campos, Joaqu\'in M.' _publ_section_title ; Two tautomeric polymorphs of 2,6-dichloropurine ; _journal_coeditor_code GG3264 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o484 _journal_page_last o486 _journal_volume 67 _journal_year 2011 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.5716 _cell_length_b 9.5820 _cell_length_c 13.1594 _exptl_crystal_F_000 376.00 _reflns_d_resolution_high 0.8418 _[local]_cod_data_source_file gg3264IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title II _shelx_refln_list_code 4 _shelx_f_calc_maximum 162.09 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 444.24 468.43 10.13 o 4 0 0 0.67 -0.65 4.33 o 6 0 0 0.32 -5.66 5.66 o 1 1 0 206.25 198.63 3.97 o 2 1 0 489.31 469.52 8.92 o 3 1 0 184.47 141.62 5.71 o 4 1 0 938.31 912.83 19.84 o 5 1 0 75.99 80.27 6.44 o 6 1 0 319.01 323.26 15.04 o 0 2 0 17.96 27.82 3.41 o 1 2 0 4884.17 5399.85 41.45 o 2 2 0 83.52 79.55 3.72 o 3 2 0 408.58 379.06 9.77 o 4 2 0 10.95 10.05 3.22 o 5 2 0 180.44 176.08 13.73 o 6 2 0 4.83 8.20 4.77 o 1 3 0 2570.01 2696.47 23.62 o 2 3 0 1642.40 1715.14 20.01 o 3 3 0 14.50 11.28 2.92 o 4 3 0 677.32 671.44 23.95 o 5 3 0 165.71 170.09 10.18 o 6 3 0 36.46 28.77 6.25 o 0 4 0 2122.38 2238.48 44.35 o 1 4 0 1786.66 2013.36 22.20 o 2 4 0 362.28 366.51 9.80 o 3 4 0 4.49 4.42 2.87 o 4 4 0 374.57 357.64 13.28 o 5 4 0 1.32 2.17 8.47 o 6 4 0 109.21 121.60 9.85 o 1 5 0 5.62 7.07 2.95 o 2 5 0 785.63 789.81 15.63 o 3 5 0 1388.45 1416.11 25.49 o 4 5 0 726.47 733.59 21.89 o 5 5 0 109.71 100.97 11.76 o 0 6 0 229.25 253.49 10.94 o 1 6 0 141.04 126.95 6.51 o 2 6 0 180.39 161.69 7.36 o 3 6 0 319.49 296.66 13.50 o 4 6 0 51.82 53.15 7.21 o 5 6 0 2.64 3.80 6.19 o 1 7 0 1524.88 1642.33 25.31 o 2 7 0 379.31 399.60 12.38 o 3 7 0 79.43 72.10 7.69 o 4 7 0 591.14 565.77 20.45 o 5 7 0 13.38 20.79 5.90 o 0 8 0 404.48 416.80 23.41 o 1 8 0 31.18 29.86 4.50 o 2 8 0 3.36 3.17 3.75 o 3 8 0 146.17 145.58 10.16 o 4 8 0 135.48 125.61 9.51 o 1 9 0 19.06 13.72 6.19 o 2 9 0 134.05 118.13 9.49 o 3 9 0 124.10 137.14 10.07 o 4 9 0 58.31 62.90 7.35 o 0 10 0 10.70 -1.02 25.21 o 1 10 0 42.49 54.77 7.02 o 2 10 0 304.30 323.14 15.80 o 3 10 0 90.94 105.32 11.76 o 1 11 0 250.12 238.06 25.06 o 1 0 1 27.49 27.99 2.32 o 2 0 1 5811.16 6032.89 38.02 o 3 0 1 260.72 261.56 7.76 o 4 0 1 17.77 22.66 4.13 o 5 0 1 18.04 12.63 3.86 o 6 0 1 38.92 37.46 6.83 o -6 1 1 260.02 289.63 13.95 o -5 1 1 428.20 407.43 15.40 o -4 1 1 86.58 81.58 7.40 o -3 1 1 688.33 653.00 13.18 o -2 1 1 2101.08 2091.77 21.30 o -1 1 1 860.20 859.63 12.95 o 0 1 1 973.51 1009.10 7.62 o 1 1 1 878.35 876.45 8.49 o 2 1 1 2106.53 2060.44 17.16 o 3 1 1 684.30 648.20 9.49 o 4 1 1 86.79 77.01 5.68 o 5 1 1 426.35 428.02 13.81 o 6 1 1 263.59 294.44 13.88 o -6 2 1 50.82 60.94 7.71 o -5 2 1 186.00 203.45 10.96 o -4 2 1 574.67 596.34 15.89 o -3 2 1 83.33 85.72 4.82 o -2 2 1 21.55 24.22 2.95 o -1 2 1 4065.34 4345.28 27.95 o 0 2 1 0.95 -1.49 1.49 o 1 2 1 4027.83 4178.08 25.34 o 2 2 1 20.81 18.23 2.48 o 3 2 1 91.44 91.28 4.23 o 4 2 1 568.14 566.24 15.44 o 5 2 1 186.30 156.04 12.24 o 6 2 1 53.69 45.89 7.08 o -6 3 1 355.24 385.50 19.01 o -5 3 1 170.45 171.08 12.11 o -4 3 1 376.65 359.86 20.22 o -3 3 1 1357.43 1346.67 19.46 o -2 3 1 922.19 918.45 12.23 o -1 3 1 497.62 545.16 9.67 o 0 3 1 25.11 26.76 2.82 o 1 3 1 496.98 535.06 10.14 o 2 3 1 903.62 886.31 14.43 o 3 3 1 1365.14 1343.47 17.44 o 4 3 1 378.44 359.48 12.61 o 5 3 1 176.11 174.42 11.10 o 6 3 1 364.62 413.98 16.86 o -6 4 1 38.37 44.46 7.41 o -5 4 1 208.86 193.06 15.63 o -4 4 1 24.12 25.89 5.43 o -3 4 1 301.69 302.42 11.14 o -2 4 1 3085.00 3327.53 31.13 o -1 4 1 500.27 512.38 10.60 o 0 4 1 121.66 121.78 4.66 o 1 4 1 508.57 511.09 10.96 o 2 4 1 3102.18 3276.42 31.90 o 3 4 1 296.41 280.69 9.17 o 4 4 1 24.47 19.16 4.08 o 5 4 1 204.51 199.36 11.22 o 6 4 1 37.84 52.63 10.54 o -5 5 1 129.92 128.14 11.28 o -4 5 1 171.83 154.73 9.69 o -3 5 1 294.73 271.06 10.52 o -2 5 1 342.62 329.61 9.78 o -1 5 1 1008.58 1092.00 16.24 o 0 5 1 603.52 595.37 11.03 o 1 5 1 994.75 1054.37 18.73 o 2 5 1 321.79 338.86 10.31 o 3 5 1 292.88 276.23 10.96 o 4 5 1 178.11 157.41 8.69 o 5 5 1 140.70 129.29 10.69 o -5 6 1 72.40 78.87 8.99 o -4 6 1 450.66 422.24 17.80 o -3 6 1 39.26 42.81 6.77 o -2 6 1 58.14 64.47 5.22 o -1 6 1 780.39 750.18 15.67 o 0 6 1 756.54 779.10 13.80 o 1 6 1 785.24 740.28 16.92 o 2 6 1 59.98 61.43 5.55 o 3 6 1 37.68 40.88 4.98 o 4 6 1 477.07 465.37 18.02 o 5 6 1 74.79 84.92 9.49 o -5 7 1 87.41 122.46 9.73 o -4 7 1 135.35 149.35 9.91 o -3 7 1 250.51 234.70 12.23 o -2 7 1 620.25 631.77 16.30 o -1 7 1 266.87 267.93 9.86 o 0 7 1 869.17 886.60 19.89 o 1 7 1 269.35 247.28 9.43 o 2 7 1 630.04 598.74 16.65 o 3 7 1 244.37 217.06 11.85 o 4 7 1 132.93 103.06 9.10 o 5 7 1 85.83 113.24 9.28 o -4 8 1 81.11 88.47 9.39 o -3 8 1 314.25 308.52 14.50 o -2 8 1 817.00 776.05 20.51 o -1 8 1 482.79 479.61 17.30 o 0 8 1 55.38 55.60 6.42 o 1 8 1 476.10 470.21 15.29 o 2 8 1 814.19 803.35 22.72 o 3 8 1 329.01 321.98 16.75 o 4 8 1 78.43 84.84 9.57 o -4 9 1 30.01 28.66 6.10 o -3 9 1 74.21 65.07 8.02 o -2 9 1 317.30 326.28 15.74 o -1 9 1 15.78 10.84 4.63 o 0 9 1 766.07 788.77 23.06 o 1 9 1 12.67 14.39 4.06 o 2 9 1 317.00 304.46 14.30 o 3 9 1 75.09 71.42 9.40 o 4 9 1 31.36 41.27 8.08 o -3 10 1 48.32 32.71 13.10 o -2 10 1 31.88 32.66 6.92 o -1 10 1 168.26 177.36 10.46 o 0 10 1 158.56 130.42 9.84 o 1 10 1 163.33 168.81 13.96 o 2 10 1 31.95 24.06 6.30 o 3 10 1 48.36 39.39 10.03 o -1 11 1 252.22 269.40 15.50 o 0 11 1 199.95 193.20 14.44 o 1 11 1 253.46 265.00 25.79 o 0 0 2 129.69 129.67 3.77 o 1 0 2 11.21 12.83 1.98 o 2 0 2 497.25 479.38 9.34 o 3 0 2 1520.07 1530.25 20.14 o 4 0 2 168.57 148.53 7.90 o 5 0 2 42.28 46.75 5.80 o 6 0 2 0.30 1.80 6.30 o -6 1 2 222.90 225.10 15.90 o -5 1 2 120.48 120.57 9.68 o -4 1 2 716.92 681.21 23.50 o -3 1 2 623.54 609.60 12.67 o -2 1 2 966.42 960.92 15.41 o -1 1 2 3379.83 3475.12 29.24 o 0 1 2 2115.99 2276.15 16.02 o 1 1 2 3378.32 3553.54 19.71 o 2 1 2 964.06 936.59 10.29 o 3 1 2 632.44 596.45 9.74 o 4 1 2 721.02 700.32 16.27 o 5 1 2 119.58 100.00 6.64 o 6 1 2 217.07 219.87 12.62 o -6 2 2 60.94 76.22 8.14 o -5 2 2 150.12 146.07 12.87 o -4 2 2 179.34 173.90 8.49 o -3 2 2 1371.80 1371.91 19.30 o -2 2 2 677.10 598.69 11.72 o -1 2 2 30.41 19.38 2.67 o 0 2 2 209.32 195.37 4.49 o 1 2 2 32.13 29.84 2.47 o 2 2 2 687.13 604.09 9.46 o 3 2 2 1363.84 1407.11 20.24 o 4 2 2 175.15 159.27 7.26 o 5 2 2 156.19 148.03 9.98 o 6 2 2 60.20 73.69 7.51 o -6 3 2 150.64 156.20 11.59 o -5 3 2 934.97 958.91 30.28 o -4 3 2 548.49 541.06 23.60 o -3 3 2 522.86 509.94 11.63 o -2 3 2 434.09 456.41 9.47 o -1 3 2 750.54 759.51 15.01 o 0 3 2 166.63 145.09 4.46 o 1 3 2 739.74 747.19 11.42 o 2 3 2 429.39 441.79 9.18 o 3 3 2 524.01 522.73 10.92 o 4 3 2 550.75 554.14 15.82 o 5 3 2 937.05 986.61 27.12 o 6 3 2 144.16 142.05 9.83 o -6 4 2 23.14 14.54 5.99 o -5 4 2 99.67 107.77 9.47 o -4 4 2 563.06 567.42 21.10 o -3 4 2 759.46 792.75 17.33 o -2 4 2 335.72 337.34 8.95 o -1 4 2 2228.44 2444.71 22.62 o 0 4 2 4972.88 5707.78 43.58 o 1 4 2 2209.09 2418.15 23.62 o 2 4 2 352.42 344.58 8.28 o 3 4 2 763.69 763.15 15.89 o 4 4 2 567.78 580.71 16.95 o 5 4 2 97.84 108.02 8.12 o 6 4 2 22.30 22.89 6.01 o -5 5 2 56.77 56.89 10.47 o -4 5 2 415.59 408.65 16.09 o -3 5 2 59.92 67.74 7.06 o -2 5 2 395.58 378.22 10.09 o -1 5 2 217.86 236.42 7.38 o 0 5 2 1403.35 1477.85 18.00 o 1 5 2 215.07 238.53 7.48 o 2 5 2 416.23 393.34 11.25 o 3 5 2 51.68 57.39 4.88 o 4 5 2 398.71 394.65 14.19 o 5 5 2 56.57 59.57 7.45 o -5 6 2 287.78 275.07 15.38 o -4 6 2 12.22 19.35 4.89 o -3 6 2 210.64 208.77 11.70 o -2 6 2 464.42 448.22 12.93 o -1 6 2 469.06 442.54 10.84 o 0 6 2 177.49 176.96 6.42 o 1 6 2 460.69 443.30 13.03 o 2 6 2 466.04 461.34 13.92 o 3 6 2 200.98 205.10 8.85 o 4 6 2 11.43 18.53 4.20 o 5 6 2 281.06 264.05 15.55 o -5 7 2 110.48 121.49 15.75 o -4 7 2 85.62 85.08 7.75 o -3 7 2 40.06 26.34 5.53 o -2 7 2 85.20 93.32 6.33 o -1 7 2 1420.52 1437.08 26.05 o 0 7 2 60.53 61.37 5.85 o 1 7 2 1435.83 1513.34 24.33 o 2 7 2 80.47 72.37 6.42 o 3 7 2 40.29 31.95 5.03 o 4 7 2 90.49 69.33 7.26 o 5 7 2 108.23 131.38 11.03 o -4 8 2 188.18 183.02 11.15 o -3 8 2 63.09 63.06 7.14 o -2 8 2 362.37 358.24 12.73 o -1 8 2 726.18 683.83 18.39 o 0 8 2 2137.18 2143.99 37.74 o 1 8 2 729.46 742.66 19.36 o 2 8 2 350.46 344.90 14.91 o 3 8 2 62.66 58.66 8.75 o 4 8 2 179.57 190.55 11.19 o -3 9 2 98.73 120.15 10.57 o -2 9 2 205.74 222.19 11.07 o -1 9 2 130.39 137.28 9.95 o 0 9 2 229.06 217.08 11.43 o 1 9 2 133.67 133.09 8.96 o 2 9 2 193.54 197.47 11.89 o 3 9 2 99.94 93.24 10.53 o -3 10 2 308.27 332.32 17.78 o -2 10 2 223.14 248.66 17.98 o -1 10 2 135.65 120.59 12.05 o 0 10 2 0.26 4.24 5.10 o 1 10 2 135.57 135.86 13.03 o 2 10 2 224.70 219.60 18.48 o 3 10 2 306.12 315.66 31.39 o -1 11 2 338.31 379.94 18.70 o 0 11 2 426.91 475.15 36.83 o 1 11 2 339.49 335.18 32.57 o 1 0 3 26271.72 29417.42 162.75 o 2 0 3 609.09 634.58 11.51 o 3 0 3 0.08 -2.05 2.87 o 4 0 3 674.70 707.51 17.78 o 5 0 3 0.69 4.75 3.65 o 6 0 3 53.91 63.61 8.49 o -6 1 3 5.89 -1.92 6.14 o -5 1 3 47.49 36.52 5.93 o -4 1 3 235.17 228.41 16.15 o -3 1 3 1106.46 1092.88 19.23 o -2 1 3 703.88 660.53 12.03 o -1 1 3 278.49 276.72 6.38 o 0 1 3 4934.24 5186.04 66.55 o 1 1 3 289.45 299.27 5.65 o 2 1 3 689.30 625.81 9.25 o 3 1 3 1091.21 1080.49 14.01 o 4 1 3 244.46 236.27 8.44 o 5 1 3 43.66 44.63 6.14 o 6 1 3 6.03 0.10 6.78 o -6 2 3 68.78 76.17 8.46 o -5 2 3 161.62 138.14 19.23 o -4 2 3 21.77 25.25 5.29 o -3 2 3 94.99 86.42 5.75 o -2 2 3 97.26 99.25 3.87 o -1 2 3 493.03 485.47 8.31 o 0 2 3 6193.94 6993.57 53.87 o 1 2 3 488.89 465.94 8.42 o 2 2 3 94.01 87.24 4.19 o 3 2 3 99.31 84.62 4.51 o 4 2 3 24.81 25.92 4.23 o 5 2 3 167.53 142.35 9.62 o 6 2 3 63.61 54.35 6.90 o -6 3 3 6.52 11.04 5.98 o -5 3 3 220.75 241.76 14.76 o -4 3 3 219.92 210.13 12.47 o -3 3 3 1635.17 1629.15 24.08 o -2 3 3 504.20 503.78 11.54 o -1 3 3 504.98 518.74 9.65 o 0 3 3 30.87 24.52 2.49 o 1 3 3 493.88 501.43 9.38 o 2 3 3 514.24 528.43 9.57 o 3 3 3 1637.80 1615.19 19.24 o 4 3 3 212.88 189.67 9.43 o 5 3 3 214.84 217.63 11.80 o 6 3 3 6.42 15.45 5.36 o -6 4 3 17.55 30.12 8.87 o -5 4 3 167.65 160.58 11.39 o -4 4 3 212.74 213.34 12.83 o -3 4 3 494.56 476.05 15.71 o -2 4 3 567.94 557.98 13.32 o -1 4 3 309.81 279.96 8.46 o 0 4 3 1551.07 1672.81 19.84 o 1 4 3 305.39 259.15 7.07 o 2 4 3 565.64 549.86 11.24 o 3 4 3 493.55 485.55 12.88 o 4 4 3 213.18 198.90 9.60 o 5 4 3 166.42 149.19 10.00 o 6 4 3 17.88 26.31 5.88 o -5 5 3 37.53 31.35 6.62 o -4 5 3 567.45 564.63 21.89 o -3 5 3 199.82 196.79 10.84 o -2 5 3 934.23 962.50 17.99 o -1 5 3 780.26 851.68 15.78 o 0 5 3 273.22 244.52 7.02 o 1 5 3 787.96 836.87 12.79 o 2 5 3 933.48 942.37 19.31 o 3 5 3 202.23 192.66 8.55 o 4 5 3 560.35 557.53 17.41 o 5 5 3 36.96 31.43 6.03 o -5 6 3 169.43 178.20 12.40 o -4 6 3 128.45 145.97 9.29 o -3 6 3 350.88 346.15 14.30 o -2 6 3 178.83 176.73 8.24 o -1 6 3 607.07 614.82 14.33 o 0 6 3 276.18 267.61 7.99 o 1 6 3 609.38 628.09 15.68 o 2 6 3 182.80 170.72 8.76 o 3 6 3 343.47 329.62 11.61 o 4 6 3 128.88 128.09 8.49 o 5 6 3 161.68 160.54 15.89 o -5 7 3 103.38 109.98 12.25 o -4 7 3 23.59 21.08 6.98 o -3 7 3 983.55 986.46 24.41 o -2 7 3 196.51 188.25 9.19 o -1 7 3 332.28 319.76 11.00 o 0 7 3 118.56 112.86 7.98 o 1 7 3 336.72 325.95 11.78 o 2 7 3 199.87 173.19 9.15 o 3 7 3 985.18 949.65 25.57 o 4 7 3 25.23 21.63 4.74 o 5 7 3 101.46 102.34 9.94 o -4 8 3 92.73 109.32 8.59 o -3 8 3 81.52 74.20 6.59 o -2 8 3 107.80 109.56 7.02 o -1 8 3 427.42 422.75 14.45 o 0 8 3 20.94 15.96 4.56 o 1 8 3 431.66 429.55 14.48 o 2 8 3 112.51 118.65 7.92 o 3 8 3 83.69 75.38 7.76 o 4 8 3 90.84 77.64 9.24 o -3 9 3 3.76 6.42 5.53 o -2 9 3 37.94 41.90 7.91 o -1 9 3 98.88 100.91 9.66 o 0 9 3 52.70 66.62 8.18 o 1 9 3 95.82 92.15 9.07 o 2 9 3 38.13 46.50 8.02 o 3 9 3 3.44 3.78 6.84 o -2 10 3 187.99 169.44 15.80 o -1 10 3 289.46 317.67 17.05 o 0 10 3 20.25 5.53 5.23 o 1 10 3 292.42 308.26 16.37 o 2 10 3 192.51 190.41 27.68 o -1 11 3 68.39 94.99 9.50 o 0 11 3 0.01 23.05 16.14 o 1 11 3 66.49 59.10 9.00 o 0 0 4 0.08 -1.52 1.82 o 1 0 4 11060.13 12432.15 57.32 o 2 0 4 72.92 57.47 3.62 o 3 0 4 463.94 422.36 10.09 o 4 0 4 27.04 24.08 3.51 o 5 0 4 46.83 49.45 6.39 o 6 0 4 130.11 134.92 11.60 o -6 1 4 118.40 138.11 11.56 o -5 1 4 451.93 465.04 19.43 o -4 1 4 28.26 34.22 5.49 o -3 1 4 175.21 170.85 6.83 o -2 1 4 437.41 419.51 9.97 o -1 1 4 3607.94 3835.22 30.26 o 0 1 4 8.74 7.24 1.80 o 1 1 4 3582.94 3836.76 26.78 o 2 1 4 408.95 397.65 6.43 o 3 1 4 174.97 154.24 5.38 o 4 1 4 26.53 24.80 4.14 o 5 1 4 457.61 457.38 15.50 o 6 1 4 119.47 147.94 11.24 o -6 2 4 120.74 133.41 9.86 o -5 2 4 559.74 572.05 22.81 o -4 2 4 219.76 211.37 11.67 o -3 2 4 28.01 28.42 3.60 o -2 2 4 857.28 826.57 15.66 o -1 2 4 18.24 24.30 2.66 o 0 2 4 673.22 619.74 10.12 o 1 2 4 20.30 24.52 2.75 o 2 2 4 872.74 844.35 12.31 o 3 2 4 23.62 21.26 2.55 o 4 2 4 220.46 221.66 8.35 o 5 2 4 561.44 611.91 20.78 o 6 2 4 120.26 140.21 11.30 o -6 3 4 44.47 38.62 7.07 o -5 3 4 144.19 139.50 11.77 o -4 3 4 38.52 36.51 5.75 o -3 3 4 80.06 73.11 8.93 o -2 3 4 1947.89 2056.68 23.50 o -1 3 4 1633.81 1744.34 18.60 o 0 3 4 834.94 870.63 13.14 o 1 3 4 1639.02 1737.88 19.23 o 2 3 4 1967.05 2044.72 22.97 o 3 3 4 75.00 72.00 4.40 o 4 3 4 37.24 36.28 4.92 o 5 3 4 153.63 161.27 10.12 o 6 3 4 44.62 59.40 6.84 o -5 4 4 16.84 8.27 4.63 o -4 4 4 156.91 153.33 16.67 o -3 4 4 315.80 312.59 12.88 o -2 4 4 623.93 618.75 13.39 o -1 4 4 1232.03 1293.00 17.11 o 0 4 4 219.34 224.36 9.86 o 1 4 4 1221.85 1264.63 17.10 o 2 4 4 606.54 584.47 11.16 o 3 4 4 318.39 304.19 10.41 o 4 4 4 147.94 138.17 8.31 o 5 4 4 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