#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/83/2018327.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018327_Fobs loop_ _publ_author_name 'Buron-Le Cointe, Marylise' 'Cormary, Beno\?\^it' 'Toupet, Lo\"ic' 'Malfant, Isabelle' _publ_section_title ; The three-dimensional intermolecular network formed via water molecules in trans-bis(nitrito-\kN)tetrakis(pyridine-\kN)ruthenium(II) dihydrate ; _journal_coeditor_code MX3053 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m375 _journal_page_last m377 _journal_volume 67 _journal_year 2011 _space_group_IT_number 142 _symmetry_space_group_name_Hall '-I 4bd 2c' _symmetry_space_group_name_H-M 'I 41/a c d :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.3418 _cell_length_b 16.3418 _cell_length_c 16.6448 _exptl_crystal_F_000 2224.00 _reflns_d_resolution_high 0.7830 _[local]_cod_data_source_file mx3053Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' test structure: runo22py4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 447.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z' 'x, -y, -z+1/2' '-x+1/2, y, -z' '-y+1/4, -x+1/4, -z+1/4' 'y+3/4, x+1/4, -z+1/4' 'y+1/4, -x+1/4, z+3/4' '-y+1/4, x+3/4, z+1/4' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1, z+1/2' 'x+1/2, -y+1/2, -z+1' '-x+1, y+1/2, -z+1/2' '-y+3/4, -x+3/4, -z+3/4' 'y+5/4, x+3/4, -z+3/4' 'y+3/4, -x+3/4, z+5/4' '-y+3/4, x+5/4, z+3/4' '-x, -y, -z' 'x, y-1/2, -z' '-x, y, z-1/2' 'x-1/2, -y, z' 'y-1/4, x-1/4, z-1/4' '-y-3/4, -x-1/4, z-1/4' '-y-1/4, x-1/4, -z-3/4' 'y-1/4, -x-3/4, -z-1/4' '-x+1/2, -y+1/2, -z+1/2' 'x+1/2, y, -z+1/2' '-x+1/2, y+1/2, z' 'x, -y+1/2, z+1/2' 'y+1/4, x+1/4, z+1/4' '-y-1/4, -x+1/4, z+1/4' '-y+1/4, x+1/4, -z-1/4' 'y+1/4, -x-1/4, -z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 2 0 183376.41 190152.36 1283.31 o 0 4 0 26045.55 27539.61 522.40 o 2 4 0 51687.95 50935.65 266.84 o 4 4 0 57884.94 59076.59 445.64 o 0 6 0 68877.07 72717.25 402.54 o 2 6 0 53887.54 53085.53 257.83 o 4 6 0 77353.88 73651.59 363.27 o 6 6 0 6480.27 6094.29 151.04 o 0 8 0 7758.48 6317.24 129.93 o 2 8 0 26998.05 24558.52 159.69 o 4 8 0 89417.85 88032.27 475.33 o 6 8 0 64214.02 62848.36 358.67 o 8 8 0 41727.56 40742.44 382.12 o 0 10 0 269.38 114.43 83.81 o 2 10 0 50655.71 48436.44 300.30 o 4 10 0 55890.55 55638.86 264.72 o 6 10 0 47686.01 48125.91 269.13 o 8 10 0 84435.80 85360.73 419.24 o 10 10 0 76393.27 78588.86 641.69 o 0 12 0 126084.63 127519.25 827.92 o 2 12 0 51612.90 52680.34 309.32 o 4 12 0 13972.93 13255.33 153.80 o 6 12 0 13410.76 13590.48 184.90 o 8 12 0 35316.82 36018.03 329.65 o 10 12 0 9137.38 8748.72 195.58 o 12 12 0 17087.37 16981.87 337.77 o 0 14 0 53360.86 55366.50 520.30 o 2 14 0 27082.65 27451.50 273.04 o 4 14 0 19434.65 20287.31 256.76 o 6 14 0 13851.72 13786.07 197.87 o 8 14 0 1818.33 1895.38 126.24 o 10 14 0 9857.28 10102.10 227.69 o 12 14 0 27736.78 26900.83 382.41 o 14 14 0 10343.52 9495.59 434.97 o 0 16 0 20583.00 20562.76 391.40 o 2 16 0 11700.88 11686.06 222.62 o 4 16 0 11649.59 12068.20 239.13 o 6 16 0 31971.70 32770.59 364.47 o 8 16 0 6174.07 6134.28 220.35 o 10 16 0 8325.73 8227.80 266.30 o 12 16 0 12973.22 12951.62 329.56 o 0 18 0 15517.52 15484.87 394.42 o 2 18 0 21143.06 22205.24 308.65 o 4 18 0 22643.92 24268.57 392.32 o 6 18 0 8852.10 8439.51 247.33 o 8 18 0 12722.94 12776.80 294.29 o 10 18 0 5587.88 5458.53 294.04 o 0 20 0 10007.40 11017.21 438.00 o 2 20 0 18395.35 18473.39 379.56 o 4 20 0 20926.28 21325.01 418.90 o 1 2 1 421.15 432.96 17.83 o 2 3 1 8630.40 8403.25 72.85 o 1 4 1 2335.06 2723.79 79.21 o 3 4 1 3795.66 4384.00 53.34 o 2 5 1 12183.86 12051.99 74.35 o 4 5 1 23830.75 24627.92 104.13 o 1 6 1 2419.50 2449.61 42.19 o 3 6 1 5390.71 5934.13 59.56 o 5 6 1 2959.80 2978.07 53.90 o 2 7 1 609.92 550.76 34.27 o 4 7 1 8.72 -24.70 49.10 o 6 7 1 881.08 851.93 43.01 o 1 8 1 1518.61 1852.24 49.13 o 3 8 1 4990.14 5340.10 53.80 o 5 8 1 7225.19 7271.91 83.18 o 7 8 1 64.01 110.71 29.46 o 2 9 1 256.63 230.69 37.90 o 4 9 1 35.88 22.02 33.47 o 6 9 1 720.15 736.02 53.43 o 8 9 1 2018.49 1930.87 70.13 o 1 10 1 5877.88 5874.18 74.05 o 3 10 1 1064.33 1070.57 40.37 o 5 10 1 104.68 147.73 38.38 o 7 10 1 213.57 273.86 51.58 o 9 10 1 1539.96 1518.89 78.09 o 2 11 1 3.75 12.66 42.31 o 4 11 1 3368.47 3379.56 58.26 o 6 11 1 32.03 43.45 51.48 o 8 11 1 146.15 139.95 65.12 o 10 11 1 824.25 798.88 79.14 o 1 12 1 101.37 122.83 51.76 o 3 12 1 1105.79 1094.87 47.88 o 5 12 1 1364.99 1303.48 59.69 o 7 12 1 329.08 358.22 72.83 o 9 12 1 1448.81 1466.59 86.35 o 11 12 1 1276.83 1211.03 93.32 o 2 13 1 1514.49 1526.75 61.43 o 4 13 1 2940.83 2789.19 77.52 o 6 13 1 2431.02 2355.41 76.93 o 8 13 1 2288.51 2131.48 91.99 o 10 13 1 6317.27 5945.81 132.83 o 12 13 1 115.48 92.76 105.25 o 1 14 1 3234.56 3075.95 87.64 o 3 14 1 2358.51 2167.69 79.28 o 5 14 1 1832.82 1897.19 88.22 o 7 14 1 89.75 94.56 67.96 o 9 14 1 53.35 -42.15 91.03 o 11 14 1 4165.05 3793.03 130.64 o 13 14 1 159.74 165.27 126.66 o 2 15 1 298.12 335.96 73.49 o 4 15 1 424.38 393.14 79.05 o 6 15 1 48.38 6.92 76.25 o 8 15 1 2237.00 2325.06 105.64 o 10 15 1 283.16 208.70 104.07 o 12 15 1 1163.67 1205.95 129.10 o 14 15 1 210.16 98.80 147.92 o 1 16 1 44.07 115.40 79.77 o 3 16 1 564.77 471.75 82.40 o 5 16 1 1089.68 989.42 99.20 o 7 16 1 1002.53 1045.94 99.92 o 9 16 1 1027.41 1170.26 118.15 o 11 16 1 70.85 109.96 123.69 o 13 16 1 502.57 277.03 143.64 o 2 17 1 77.42 99.84 91.19 o 4 17 1 747.31 688.75 113.53 o 6 17 1 335.25 227.51 99.32 o 8 17 1 915.21 966.02 113.32 o 10 17 1 1327.56 1264.08 139.87 o 12 17 1 575.91 839.65 171.91 o 1 18 1 801.83 671.35 99.25 o 3 18 1 1881.65 1586.21 119.54 o 5 18 1 808.34 812.73 123.34 o 7 18 1 530.16 557.99 118.42 o 9 18 1 57.90 24.33 126.92 o 2 19 1 21.28 56.26 105.68 o 4 19 1 92.22 68.05 120.66 o 6 19 1 34.32 36.14 133.35 o 8 19 1 224.16 333.11 135.49 o 1 20 1 297.45 385.19 132.58 o 3 20 1 131.91 283.47 130.55 o 5 20 1 230.40 247.48 129.57 o 1 1 2 181647.14 189364.83 833.06 o 0 2 2 5043.03 4761.17 72.31 o 1 3 2 109322.65 110980.54 595.73 o 3 3 2 46011.97 45000.28 191.96 o 0 4 2 11729.37 13328.18 68.85 o 2 4 2 10220.31 9830.04 70.75 o 1 5 2 25418.58 25145.01 80.80 o 3 5 2 148186.30 148181.89 346.56 o 5 5 2 107000.89 106415.55 456.97 o 0 6 2 55323.41 56123.89 437.08 o 2 6 2 100.36 176.58 32.78 o 4 6 2 1554.99 1632.02 38.08 o 1 7 2 12730.58 11743.53 65.78 o 3 7 2 123748.30 122118.16 293.29 o 5 7 2 42453.21 41228.60 162.10 o 7 7 2 33856.24 31673.04 248.52 o 0 8 2 2117.47 2128.76 81.64 o 2 8 2 1702.09 1665.37 45.77 o 4 8 2 26.29 89.55 33.30 o 6 8 2 5272.90 5351.78 65.40 o 1 9 2 25811.55 24205.61 111.72 o 3 9 2 34679.58 32738.36 135.69 o 5 9 2 40868.21 39533.09 189.39 o 7 9 2 71197.63 70419.59 228.85 o 9 9 2 55991.55 55910.32 467.93 o 0 10 2 2249.19 2702.80 84.88 o 2 10 2 675.86 741.37 44.38 o 4 10 2 1157.08 1093.99 40.18 o 6 10 2 371.33 397.99 55.86 o 8 10 2 788.22 764.03 67.30 o 1 11 2 58940.93 58897.66 258.34 o 3 11 2 19126.03 18685.96 119.44 o 5 11 2 29877.47 29717.11 150.72 o 7 11 2 27797.62 27828.26 179.41 o 9 11 2 11275.75 11395.32 132.39 o 11 11 2 23908.96 23405.20 292.03 o 0 12 2 3171.88 3225.62 98.97 o 2 12 2 1546.02 1551.96 58.44 o 4 12 2 1780.38 1808.83 60.10 o 6 12 2 554.42 573.26 54.46 o 8 12 2 111.42 87.12 71.75 o 10 12 2 1215.61 1212.20 91.57 o 1 13 2 53944.46 54557.99 217.83 o 3 13 2 15436.06 15533.18 130.94 o 5 13 2 18108.01 17998.45 141.09 o 7 13 2 21049.29 21067.59 173.52 o 9 13 2 12414.48 12442.89 159.10 o 11 13 2 26020.65 25364.97 234.89 o 13 13 2 28468.91 28969.82 385.40 o 0 14 2 0.09 50.32 82.17 o 2 14 2 242.80 190.73 65.69 o 4 14 2 188.87 184.53 66.09 o 6 14 2 10.58 36.49 71.19 o 8 14 2 21.68 90.38 82.80 o 10 14 2 1245.66 1118.56 110.81 o 12 14 2 1828.94 1798.30 121.85 o 1 15 2 25448.25 25937.90 190.05 o 3 15 2 18088.11 18483.27 168.12 o 5 15 2 23819.94 24361.92 241.93 o 7 15 2 28782.17 29843.83 221.22 o 9 15 2 16445.80 16494.41 184.19 o 11 15 2 8955.32 8481.48 175.66 o 13 15 2 11344.88 11598.53 241.40 o 0 16 2 661.84 396.86 123.48 o 2 16 2 1200.82 1284.65 84.91 o 4 16 2 290.76 225.55 80.64 o 6 16 2 150.32 144.22 92.10 o 8 16 2 383.36 407.69 95.40 o 10 16 2 20.54 118.44 112.86 o 12 16 2 246.49 350.04 129.65 o 1 17 2 16589.37 17428.61 193.92 o 3 17 2 25863.41 26431.60 242.57 o 5 17 2 22799.11 23584.59 258.53 o 7 17 2 9253.24 9632.47 168.21 o 9 17 2 6334.28 5928.23 170.74 o 11 17 2 8803.08 8502.65 217.27 o 0 18 2 477.33 520.85 162.85 o 2 18 2 622.59 626.64 109.93 o 4 18 2 17.06 -8.71 116.08 o 6 18 2 404.40 356.73 109.07 o 8 18 2 20.17 100.43 137.27 o 10 18 2 1390.85 1472.13 149.50 o 1 19 2 11347.79 12123.24 209.54 o 3 19 2 15551.44 15741.88 229.40 o 5 19 2 11358.45 11840.61 212.13 o 7 19 2 6163.09 5834.72 186.00 o 0 20 2 22.54 -54.80 176.99 o 2 20 2 114.78 63.31 127.30 o 4 20 2 57.91 116.40 142.48 o 1 2 3 39012.33 42321.98 151.36 o 2 3 3 124484.91 125697.14 361.38 o 1 4 3 3397.21 3544.45 38.39 o 3 4 3 21422.25 23264.36 99.28 o 2 5 3 39.77 81.24 29.95 o 4 5 3 2284.58 2296.74 42.02 o 1 6 3 391.26 282.12 29.40 o 3 6 3 717.59 788.80 31.13 o 5 6 3 2991.12 3168.16 45.71 o 2 7 3 1309.40 1404.96 38.89 o 4 7 3 444.96 399.89 36.45 o 6 7 3 1718.60 1780.10 42.28 o 1 8 3 2235.57 2661.53 47.01 o 3 8 3 23236.94 25135.00 104.13 o 5 8 3 8.15 -8.27 35.86 o 7 8 3 163.86 110.60 29.15 o 2 9 3 4107.44 3897.71 59.80 o 4 9 3 3184.76 3515.59 55.73 o 6 9 3 836.35 865.37 50.75 o 8 9 3 38.51 21.19 46.07 o 1 10 3 920.29 970.96 43.80 o 3 10 3 2646.15 2553.83 44.54 o 5 10 3 1279.32 1227.00 42.13 o 7 10 3 188.11 152.28 53.63 o 9 10 3 80.14 70.56 62.75 o 2 11 3 1392.77 1315.41 44.78 o 4 11 3 55.66 93.35 36.99 o 6 11 3 10.29 21.34 45.70 o 8 11 3 323.33 264.42 64.24 o 10 11 3 449.66 423.73 83.48 o 1 12 3 11.76 -35.70 49.72 o 3 12 3 253.48 254.30 45.66 o 5 12 3 300.12 314.95 49.75 o 7 12 3 2413.43 2373.56 78.32 o 9 12 3 1071.99 1195.20 85.43 o 11 12 3 2854.45 2842.70 111.96 o 2 13 3 11.54 21.24 53.54 o 4 13 3 12031.75 12029.01 120.30 o 6 13 3 77.94 136.20 72.33 o 8 13 3 5278.85 5182.00 116.91 o 10 13 3 935.61 1093.99 104.92 o 12 13 3 111.73 175.36 100.74 o 1 14 3 204.61 242.32 61.11 o 3 14 3 5976.59 6193.49 99.56 o 5 14 3 232.95 180.37 72.33 o 7 14 3 110.17 109.66 75.09 o 9 14 3 521.28 443.62 99.07 o 11 14 3 160.75 257.56 105.89 o 13 14 3 9.69 -1.23 124.58 o 2 15 3 1420.44 1562.58 81.78 o 4 15 3 258.85 180.18 76.49 o 6 15 3 22.23 59.84 78.04 o 8 15 3 53.39 141.30 89.87 o 10 15 3 287.03 247.55 106.60 o 12 15 3 21.13 -16.68 119.94 o 14 15 3 219.47 416.83 140.73 o 1 16 3 7.50 68.41 81.04 o 3 16 3 48.17 -35.82 81.66 o 5 16 3 327.26 292.37 92.33 o 7 16 3 76.23 87.52 88.14 o 9 16 3 1883.42 1697.93 117.03 o 11 16 3 1.89 60.52 120.66 o 13 16 3 3528.66 3661.92 179.22 o 2 17 3 264.66 361.37 91.78 o 4 17 3 1253.48 1173.83 97.89 o 6 17 3 4.33 55.59 103.35 o 8 17 3 109.77 17.03 124.75 o 10 17 3 366.91 364.61 132.60 o 1 18 3 438.36 453.39 107.43 o 3 18 3 246.94 278.49 108.16 o 5 18 3 2081.95 2003.72 128.93 o 7 18 3 728.99 709.69 122.25 o 9 18 3 180.57 206.44 136.57 o 2 19 3 315.33 224.77 121.86 o 4 19 3 47.43 104.24 127.31 o 6 19 3 47.89 31.00 134.51 o 8 19 3 3.24 -34.00 150.14 o 1 20 3 28.38 -20.98 131.35 o 3 20 3 470.02 462.21 128.59 o 5 20 3 114.99 112.46 149.86 o 0 0 4 33126.81 34965.36 294.54 o 0 2 4 93395.83 92393.46 338.01 o 2 2 4 7684.76 7002.38 66.77 o 1 3 4 23883.68 24908.37 93.12 o 0 4 4 41789.48 41292.54 197.45 o 2 4 4 41120.63 40021.41 211.44 o 4 4 4 150253.53 148442.31 575.69 o 1 5 4 878.43 888.37 28.18 o 3 5 4 3189.99 3339.68 45.41 o 0 6 4 83125.59 83842.23 262.23 o 2 6 4 158974.00 159082.02 406.92 o 4 6 4 84883.00 85966.30 310.04 o 6 6 4 56145.60 55047.84 294.59 o 1 7 4 5431.81 5671.36 51.79 o 3 7 4 371.47 401.75 33.19 o 5 7 4 717.15 827.93 40.97 o 0 8 4 14187.92 13642.41 91.59 o 2 8 4 74649.18 72851.28 234.85 o 4 8 4 70939.34 69134.69 208.68 o 6 8 4 14673.70 13679.87 95.21 o 8 8 4 38278.90 37144.49 250.13 o 1 9 4 180.15 219.88 32.07 o 3 9 4 55.13 55.41 30.00 o 5 9 4 1663.48 1640.76 38.39 o 7 9 4 672.21 743.07 49.17 o 0 10 4 39234.56 38823.66 275.89 o 2 10 4 24065.85 22788.49 119.08 o 4 10 4 36108.16 34512.14 136.62 o 6 10 4 14916.73 14346.25 97.89 o 8 10 4 18658.66 18643.11 141.52 o 10 10 4 25068.70 25313.28 271.48 o 1 11 4 539.72 580.95 44.72 o 3 11 4 81.99 96.47 43.57 o 5 11 4 1906.01 2003.76 58.89 o 7 11 4 2651.81 2734.66 86.56 o 9 11 4 1.10 25.78 73.15 o 0 12 4 46378.92 46979.14 291.68 o 2 12 4 48247.59 48769.86 236.10 o 4 12 4 22228.33 22282.21 138.07 o 6 12 4 11559.34 11448.50 122.11 o 8 12 4 5715.55 5862.33 115.58 o 10 12 4 32949.37 33487.70 250.30 o 12 12 4 25931.56 25130.15 324.56 o 1 13 4 130.91 142.98 51.75 o 3 13 4 60.45 63.69 56.74 o 5 13 4 18.29 27.94 59.48 o 7 13 4 5.80 4.68 77.06 o 9 13 4 167.02 219.22 90.78 o 11 13 4 0.49 -1.08 99.02 o 0 14 4 28231.79 29198.76 244.54 o 2 14 4 17257.12 17915.02 148.33 o 4 14 4 19787.80 20401.23 155.51 o 6 14 4 45914.03 46555.80 249.59 o 8 14 4 29738.52 29931.26 232.72 o 10 14 4 13051.56 12965.27 192.64 o 12 14 4 14637.45 14792.43 214.83 o 14 14 4 9220.24 9213.49 300.13 o 1 15 4 164.88 156.97 68.61 o 3 15 4 7.36 25.33 75.94 o 5 15 4 357.84 352.99 80.34 o 7 15 4 1037.68 875.10 95.21 o 9 15 4 2.96 31.07 100.30 o 11 15 4 432.54 383.74 118.17 o 13 15 4 92.03 41.16 124.95 o 0 16 4 6666.23 6798.86 183.83 o 2 16 4 9003.56 9269.20 158.84 o 4 16 4 28423.51 29989.56 225.47 o 6 16 4 33401.89 33413.78 249.69 o 8 16 4 32134.47 31726.30 266.73 o 10 16 4 13206.12 12858.45 216.25 o 12 16 4 11568.63 11435.94 206.52 o 1 17 4 160.72 188.41 101.28 o 3 17 4 230.88 307.63 93.76 o 5 17 4 26.22 58.08 89.36 o 7 17 4 180.27 178.83 99.72 o 9 17 4 138.66 113.12 113.60 o 11 17 4 4.35 107.54 142.15 o 0 18 4 20428.91 20473.08 356.23 o 2 18 4 13254.45 13713.82 216.33 o 4 18 4 7655.01 7736.40 164.26 o 6 18 4 16405.92 16831.90 241.68 o 8 18 4 10312.08 9996.89 199.38 o 1 19 4 807.09 694.12 125.69 o 3 19 4 19.08 41.29 119.42 o 5 19 4 10.39 118.47 136.42 o 7 19 4 80.50 -39.58 144.14 o 0 20 4 11197.51 10778.20 323.36 o 2 20 4 10879.75 11578.83 225.66 o 4 20 4 7684.58 8014.78 237.31 o 1 2 5 506.43 602.42 32.25 o 2 3 5 51297.50 51438.89 131.52 o 1 4 5 20032.66 19808.14 84.20 o 3 4 5 3921.27 4289.89 39.79 o 2 5 5 235.89 326.84 40.38 o 4 5 5 1968.57 2306.28 36.45 o 1 6 5 8425.03 9119.16 59.10 o 3 6 5 679.53 728.58 39.54 o 5 6 5 215.30 185.23 32.36 o 2 7 5 1940.02 2099.64 36.79 o 4 7 5 372.75 483.76 46.29 o 6 7 5 4305.84 4319.82 80.51 o 1 8 5 11239.58 11519.53 69.49 o 3 8 5 253.82 210.27 29.82 o 5 8 5 2660.43 2581.41 47.02 o 7 8 5 153.33 149.96 41.93 o 2 9 5 5751.43 5794.40 63.33 o 4 9 5 219.26 191.98 35.47 o 6 9 5 0.00 -5.95 36.85 o 8 9 5 2187.55 2064.85 63.02 o 1 10 5 8093.35 8181.34 78.61 o 3 10 5 5759.81 5696.20 69.09 o 5 10 5 1229.84 1173.95 52.81 o 7 10 5 5169.05 5141.77 87.54 o 9 10 5 52.26 25.57 76.93 o 2 11 5 2409.17 2442.99 61.16 o 4 11 5 5226.77 5230.07 73.77 o 6 11 5 498.19 497.66 59.91 o 8 11 5 3421.10 3268.40 95.18 o 10 11 5 4358.10 4410.47 115.53 o 1 12 5 260.63 296.72 54.14 o 3 12 5 492.18 508.36 49.64 o 5 12 5 1929.18 1982.68 70.70 o 7 12 5 1652.07 1610.11 81.49 o 9 12 5 460.08 444.23 88.20 o 11 12 5 508.95 583.02 93.02 o 2 13 5 2786.18 2814.54 73.89 o 4 13 5 3.87 -20.93 65.21 o 6 13 5 365.50 363.30 67.78 o 8 13 5 149.09 186.04 89.46 o 10 13 5 404.24 437.91 91.46 o 12 13 5 58.41 119.81 106.97 o 1 14 5 1032.10 978.61 74.09 o 3 14 5 1525.32 1401.20 77.72 o 5 14 5 2772.49 2692.19 90.73 o 7 14 5 31.16 -3.83 91.60 o 9 14 5 567.19 635.28 102.50 o 11 14 5 92.27 74.98 102.57 o 13 14 5 333.28 307.91 120.68 o 2 15 5 1292.42 1390.19 80.87 o 4 15 5 809.30 743.74 81.34 o 6 15 5 1174.73 1231.74 89.47 o 8 15 5 74.62 126.45 99.60 o 10 15 5 56.75 79.09 107.82 o 12 15 5 135.38 63.31 117.30 o 1 16 5 1074.88 1060.33 87.44 o 3 16 5 853.92 847.27 87.58 o 5 16 5 151.90 145.19 87.49 o 7 16 5 350.08 398.67 103.88 o 9 16 5 302.93 394.46 104.51 o 11 16 5 0.05 2.47 126.83 o 2 17 5 102.99 110.38 94.41 o 4 17 5 498.33 469.77 92.73 o 6 17 5 11.57 108.57 98.93 o 8 17 5 337.03 361.36 109.51 o 10 17 5 52.30 31.91 113.28 o 1 18 5 1012.62 1023.47 113.64 o 3 18 5 835.99 708.90 115.01 o 5 18 5 100.53 99.31 108.59 o 7 18 5 129.68 61.80 118.47 o 9 18 5 919.88 1020.20 127.73 o 2 19 5 80.48 47.49 125.04 o 4 19 5 32.75 206.41 139.22 o 6 19 5 1836.19 1704.00 158.78 o 1 20 5 4.85 -36.79 139.49 o 3 20 5 167.11 212.76 144.85 o 1 1 6 102169.20 99269.38 283.44 o 0 2 6 6394.42 6886.41 89.47 o 1 3 6 32466.40 30366.65 99.62 o 3 3 6 56602.10 55666.13 203.96 o 0 4 6 5.59 22.95 50.22 o 2 4 6 135.73 189.42 42.22 o 1 5 6 68734.95 68862.05 211.29 o 3 5 6 50088.83 48022.09 165.86 o 5 5 6 14616.43 11840.03 91.10 o 0 6 6 49227.36 50369.25 168.44 o 2 6 6 363.37 444.09 43.91 o 4 6 6 2776.78 3158.82 48.47 o 1 7 6 79976.84 78512.73 246.92 o 3 7 6 58078.95 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143.51 o