#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/83/2018338.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018338_Fobs loop_ _publ_author_name 'Baca, Svetlana G.' 'Breukers, Stefanie' 'Ellern, Arkady' 'K\"ogerler, Paul' _publ_section_title ; An octanuclear iron(III) isobutyrate wheel ; _journal_coeditor_code YF3006 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m371 _journal_page_last m374 _journal_volume 67 _journal_year 2011 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 90.557 _cell_angle_beta 110.485 _cell_angle_gamma 108.261 _cell_length_a 13.2648 _cell_length_b 16.6182 _cell_length_c 17.6790 _exptl_crystal_F_000 1510.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file yf3006Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' S52S in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 290.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h 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16443.34 17125.69 244.19 o 4 1 0 19761.50 20011.20 287.01 o 5 1 0 9759.26 10093.26 158.19 o 6 1 0 516.43 620.41 35.14 o 7 1 0 153.81 180.05 21.02 o 8 1 0 427.72 448.53 27.49 o 9 1 0 1338.56 1341.35 56.71 o 10 1 0 544.57 494.17 33.13 o 11 1 0 410.52 439.34 35.09 o 12 1 0 916.86 751.67 83.24 o 13 1 0 2188.81 2294.92 144.39 o -14 2 0 21.75 23.78 46.71 o -13 2 0 1218.41 1202.67 102.77 o -12 2 0 27.75 5.30 21.80 o -11 2 0 325.16 371.31 31.97 o -10 2 0 19.88 54.61 18.67 o -9 2 0 1558.40 1556.62 50.47 o -8 2 0 7201.00 7586.92 133.84 o -7 2 0 4368.22 4504.84 98.08 o -6 2 0 2987.65 3219.23 65.86 o -5 2 0 717.43 950.61 29.71 o -4 2 0 5497.56 5255.71 86.79 o -3 2 0 3701.98 3576.15 92.58 o -2 2 0 45.64 27.95 14.63 o -1 2 0 676.55 879.82 16.58 o 0 2 0 22726.74 19573.88 1465.54 o 1 2 0 6275.91 6462.67 121.88 o 2 2 0 3031.44 3307.02 68.75 o 3 2 0 12636.07 12060.44 216.80 o 4 2 0 2984.56 2875.44 98.60 o 5 2 0 4189.60 4534.85 83.55 o 6 2 0 291.99 387.79 23.10 o 7 2 0 144.23 292.40 22.14 o 8 2 0 17.16 31.55 15.49 o 9 2 0 848.33 908.54 53.19 o 10 2 0 2524.54 2470.18 70.67 o 11 2 0 139.10 187.20 37.37 o 12 2 0 2914.16 2940.42 160.53 o 13 2 0 375.31 451.00 74.74 o -14 3 0 17.61 13.59 45.86 o -13 3 0 91.50 81.23 29.72 o -12 3 0 334.21 321.08 31.78 o -11 3 0 897.43 981.66 55.49 o -10 3 0 11.68 14.96 16.80 o -9 3 0 3545.72 3783.39 84.16 o -8 3 0 3275.07 3180.31 71.57 o -7 3 0 214.26 298.13 21.39 o -6 3 0 1592.22 1503.30 41.43 o -5 3 0 7661.03 7477.59 120.92 o -4 3 0 6960.81 6715.74 129.62 o -2 3 0 2493.54 2780.75 52.25 o -1 3 0 1321.96 1204.61 19.88 o 0 3 0 479.96 453.48 15.56 o 1 3 0 46401.02 42528.15 5928.82 o 2 3 0 18.82 23.90 14.59 o 3 3 0 1438.07 1391.73 43.13 o 4 3 0 208.12 313.00 35.25 o 5 3 0 6255.01 6795.21 116.58 o 6 3 0 144.63 155.26 17.20 o 7 3 0 2009.68 2194.39 57.93 o 8 3 0 2204.18 2116.52 81.87 o 9 3 0 5091.97 5360.22 112.02 o 10 3 0 491.12 558.65 36.92 o 11 3 0 971.75 958.86 62.98 o 12 3 0 219.92 313.41 65.40 o -14 4 0 7.71 -1.70 41.62 o -13 4 0 473.29 460.71 45.34 o -12 4 0 1524.06 1446.97 56.43 o -11 4 0 963.03 971.33 44.92 o -10 4 0 279.24 345.66 28.57 o -9 4 0 2129.34 2055.49 57.83 o -8 4 0 1470.30 1670.01 48.50 o -7 4 0 3731.97 3872.19 78.26 o -6 4 0 24.55 36.22 19.75 o -5 4 0 1390.56 1611.56 47.87 o -4 4 0 1294.07 992.61 41.18 o -3 4 0 115.54 104.03 10.67 o -2 4 0 25548.91 25156.48 352.11 o -1 4 0 2325.85 2611.22 46.47 o 0 4 0 10161.48 10497.81 154.45 o 1 4 0 2697.87 2752.76 62.75 o 2 4 0 131.09 95.02 11.42 o 3 4 0 3270.72 3160.76 62.73 o 4 4 0 2503.44 2682.22 101.92 o 5 4 0 755.28 847.66 38.46 o 6 4 0 1890.97 2016.51 53.86 o 7 4 0 21.03 -8.49 13.64 o 8 4 0 5447.91 5502.24 152.60 o 9 4 0 7.00 8.65 17.49 o 10 4 0 625.08 724.47 108.29 o 11 4 0 1120.38 1052.49 68.67 o -14 5 0 12.83 -24.63 39.92 o -13 5 0 1024.61 975.03 65.82 o -12 5 0 276.59 219.27 28.43 o -11 5 0 369.57 369.71 30.84 o -10 5 0 917.72 1029.85 43.78 o -9 5 0 528.75 564.68 31.33 o -8 5 0 128.38 87.17 20.15 o -7 5 0 2060.41 1910.42 50.17 o -6 5 0 2946.80 3543.93 85.23 o -5 5 0 95.45 85.42 15.50 o -4 5 0 12457.39 12761.08 190.17 o -3 5 0 2390.32 2452.91 47.30 o -2 5 0 863.61 955.77 23.37 o -1 5 0 1716.21 1600.53 34.82 o 0 5 0 1653.48 1630.25 59.57 o 2 5 0 8609.56 8360.67 421.27 o 3 5 0 2699.36 2864.23 61.08 o 4 5 0 6015.56 6821.98 118.12 o 5 5 0 4789.56 5025.39 116.62 o 6 5 0 189.03 204.13 24.66 o 7 5 0 1543.97 1446.68 54.79 o 8 5 0 520.40 436.31 31.22 o 9 5 0 32.51 1.87 18.24 o 10 5 0 446.99 346.77 42.94 o 11 5 0 499.71 446.75 67.95 o -14 6 0 5.18 0.76 32.70 o -13 6 0 9.18 -15.26 20.12 o -12 6 0 8.60 1.33 18.31 o -11 6 0 1.78 -3.19 17.46 o -10 6 0 5097.48 4999.82 105.31 o -9 6 0 255.41 211.11 22.32 o -8 6 0 400.78 476.64 27.15 o -7 6 0 973.12 1157.30 69.65 o -6 6 0 136.78 157.78 15.99 o -5 6 0 0.06 11.15 10.56 o -4 6 0 15.00 -2.83 8.26 o -3 6 0 2892.21 2946.53 54.79 o -2 6 0 14.77 28.88 6.23 o -1 6 0 35.68 21.34 8.43 o 0 6 0 14469.51 13982.68 207.71 o 1 6 0 7909.55 7436.64 147.56 o 2 6 0 5997.80 6510.71 114.99 o 3 6 0 11750.54 11520.37 182.13 o 4 6 0 1154.92 1185.88 39.92 o 5 6 0 2673.73 2444.04 77.45 o 6 6 0 73.51 60.72 30.93 o 7 6 0 49.96 36.10 16.58 o 8 6 0 525.02 591.35 37.09 o 9 6 0 312.98 322.26 40.83 o 10 6 0 1.57 -10.19 38.22 o -14 7 0 258.37 256.63 40.54 o -13 7 0 18.11 -1.14 21.39 o -12 7 0 29.05 19.51 19.77 o -11 7 0 60.62 78.17 40.43 o -10 7 0 54.11 40.89 18.74 o -9 7 0 1286.78 1258.21 44.74 o -8 7 0 404.38 403.12 30.40 o -7 7 0 1557.49 1616.34 46.24 o -6 7 0 1677.41 1724.21 45.31 o -5 7 0 2004.40 2201.37 49.73 o -4 7 0 2196.46 2240.05 47.39 o -3 7 0 8429.98 8878.31 138.60 o -2 7 0 3479.35 3763.06 67.26 o -1 7 0 8268.89 8850.57 139.95 o 0 7 0 4447.74 4380.43 80.53 o 1 7 0 9045.54 9581.15 186.03 o 2 7 0 5855.48 5704.35 122.68 o 3 7 0 1029.15 839.99 52.66 o 4 7 0 3438.10 3594.11 78.36 o 5 7 0 1447.54 1317.20 45.35 o 6 7 0 1028.09 1163.11 45.26 o 7 7 0 322.83 327.75 33.06 o 8 7 0 96.81 93.15 21.36 o 9 7 0 166.91 140.99 49.26 o 10 7 0 301.10 254.85 45.86 o 11 7 0 913.23 831.50 98.52 o -14 8 0 54.08 67.58 38.22 o -13 8 0 124.19 72.23 40.45 o -12 8 0 148.62 122.02 25.37 o -11 8 0 121.64 104.55 22.77 o -10 8 0 1022.55 937.52 42.16 o -9 8 0 0.52 -11.36 10.04 o -8 8 0 2743.12 2669.88 65.37 o -7 8 0 1776.35 1877.70 50.08 o -6 8 0 15.23 54.21 13.30 o -5 8 0 120.76 121.96 13.28 o -4 8 0 1569.27 1817.81 41.12 o -3 8 0 8697.79 8977.17 187.37 o -2 8 0 306.06 382.93 25.45 o -1 8 0 582.46 520.64 23.21 o 0 8 0 5223.79 5662.23 101.02 o 1 8 0 5964.69 5608.65 160.25 o 2 8 0 885.48 1151.56 39.54 o 3 8 0 2955.54 2808.82 70.86 o 4 8 0 7918.41 7380.54 167.68 o 5 8 0 264.24 203.20 28.36 o 6 8 0 48.52 31.31 21.52 o 7 8 0 519.83 371.04 114.24 o 8 8 0 219.63 148.32 84.51 o 9 8 0 1422.68 1488.62 91.73 o 10 8 0 3258.62 3270.28 122.73 o -14 9 0 217.39 255.98 40.51 o -13 9 0 133.01 158.54 28.96 o -12 9 0 982.45 947.80 47.50 o -11 9 0 4971.94 5122.97 111.89 o -10 9 0 64.16 100.15 23.88 o -9 9 0 4966.63 4762.59 99.81 o -8 9 0 2297.26 2323.24 78.41 o -7 9 0 794.67 865.31 46.20 o -6 9 0 1374.73 1269.79 37.73 o -5 9 0 470.85 515.46 36.01 o -4 9 0 4611.00 4814.87 121.30 o -3 9 0 1058.10 1083.79 50.72 o -2 9 0 7712.49 7927.37 130.37 o -1 9 0 2350.85 2677.26 87.31 o 0 9 0 8134.18 7583.77 155.27 o 1 9 0 556.02 677.51 30.98 o 2 9 0 163.44 112.58 17.48 o 3 9 0 124.00 125.97 25.29 o 4 9 0 13.84 36.44 16.78 o 5 9 0 7.46 -18.51 14.90 o 6 9 0 1370.90 1286.68 50.97 o 7 9 0 153.88 167.67 33.51 o 8 9 0 667.44 629.36 78.99 o 9 9 0 5591.77 5702.94 166.96 o 10 9 0 926.91 1061.68 106.17 o -14 10 0 311.04 238.66 62.00 o -13 10 0 416.46 395.94 47.94 o -12 10 0 4549.89 4488.91 106.58 o -11 10 0 1525.16 1533.57 70.50 o -10 10 0 57.55 34.19 18.28 o -9 10 0 481.46 504.57 30.86 o -8 10 0 764.36 752.00 33.56 o -7 10 0 4467.63 4633.82 91.40 o -6 10 0 730.71 655.95 26.62 o -5 10 0 195.09 209.38 23.93 o -4 10 0 1139.03 1092.94 53.75 o -3 10 0 1086.81 1130.91 55.25 o -2 10 0 685.45 570.94 33.79 o -1 10 0 401.08 292.15 20.25 o 0 10 0 26.92 41.68 16.03 o 1 10 0 1358.24 1407.35 45.47 o 2 10 0 4186.23 4359.80 112.10 o 3 10 0 229.54 193.89 22.61 o 4 10 0 37.53 46.36 19.03 o 5 10 0 1515.29 1308.39 51.57 o 6 10 0 785.79 788.98 56.13 o 7 10 0 312.22 377.44 56.06 o 8 10 0 2767.02 1764.93 122.31 o 9 10 0 903.73 1175.49 108.72 o -14 11 0 100.64 108.72 52.66 o -13 11 0 1102.13 1076.20 70.52 o -12 11 0 7.10 21.21 21.61 o -11 11 0 352.18 429.41 49.26 o -10 11 0 69.10 78.83 29.36 o -9 11 0 213.29 262.00 43.74 o -8 11 0 1693.84 1510.76 127.83 o -7 11 0 1257.21 1165.89 61.86 o -6 11 0 270.76 219.43 44.59 o -5 11 0 761.30 729.68 47.12 o -4 11 0 192.56 156.21 27.61 o -3 11 0 220.59 149.74 27.55 o -2 11 0 2542.55 2600.96 85.22 o -1 11 0 1027.03 1201.64 65.71 o 0 11 0 115.31 186.58 20.67 o 1 11 0 8488.98 8011.69 145.10 o 2 11 0 2974.47 3208.24 133.77 o 3 11 0 112.37 84.08 24.02 o 4 11 0 458.80 431.00 32.44 o 5 11 0 432.80 432.05 34.37 o 6 11 0 1655.56 1636.83 98.52 o 7 11 0 16.51 8.77 29.97 o 8 11 0 152.62 274.80 78.14 o -14 12 0 128.21 99.84 39.91 o -13 12 0 56.38 40.55 30.29 o -12 12 0 160.66 188.75 47.14 o -11 12 0 142.59 160.34 81.96 o -10 12 0 56.45 92.66 36.10 o -9 12 0 4.58 -17.88 24.54 o -8 12 0 16.16 1.96 30.15 o -7 12 0 239.91 268.92 36.24 o -6 12 0 260.15 292.35 35.37 o -5 12 0 1048.38 961.89 56.42 o -4 12 0 1060.44 1096.44 59.91 o -3 12 0 7634.99 7278.31 177.47 o -2 12 0 5071.75 4983.28 137.23 o -1 12 0 192.29 207.35 27.85 o 0 12 0 1954.14 2260.07 62.38 o 1 12 0 911.98 852.58 46.51 o 2 12 0 93.10 130.50 31.85 o 3 12 0 1464.07 1382.48 53.58 o 4 12 0 0.53 10.36 19.16 o 5 12 0 2107.16 2319.90 74.81 o 6 12 0 425.47 330.99 44.85 o 7 12 0 105.03 47.47 33.49 o 8 12 0 359.81 365.32 50.68 o -13 13 0 333.96 206.28 169.87 o -12 13 0 11.57 -17.87 28.15 o -11 13 0 344.69 363.87 47.67 o -10 13 0 1.35 21.38 28.88 o -9 13 0 556.29 584.85 53.93 o -8 13 0 135.38 137.77 53.51 o -7 13 0 6.16 20.77 24.92 o -6 13 0 1395.76 1231.71 78.56 o -5 13 0 495.36 679.83 50.44 o -4 13 0 791.12 721.78 52.49 o -3 13 0 574.06 625.33 51.04 o -2 13 0 131.47 172.02 31.81 o -1 13 0 328.16 209.97 33.63 o 0 13 0 847.01 841.30 56.44 o 1 13 0 1522.77 1404.93 73.27 o 3 13 0 422.11 448.08 40.35 o 4 13 0 152.83 114.08 29.29 o 5 13 0 225.05 269.76 37.16 o 6 13 0 27.94 3.00 48.41 o 7 13 0 99.93 48.76 35.30 o -13 14 0 9.89 32.39 36.33 o -12 14 0 49.15 47.04 34.59 o -11 14 0 539.63 504.04 86.63 o -10 14 0 1149.97 1138.85 84.93 o -9 14 0 465.25 545.02 50.68 o -8 14 0 771.13 653.63 54.61 o -7 14 0 434.45 551.40 50.68 o -6 14 0 65.18 40.94 50.96 o -5 14 0 614.92 639.44 53.44 o -4 14 0 106.19 73.32 29.96 o -3 14 0 216.85 216.22 37.53 o -2 14 0 70.01 33.32 27.61 o -1 14 0 524.36 469.00 46.74 o 0 14 0 1347.60 1396.16 75.61 o 1 14 0 2001.57 1902.60 86.59 o 2 14 0 113.92 124.85 50.11 o 3 14 0 304.98 249.71 59.45 o 4 14 0 234.18 208.11 39.91 o 5 14 0 271.74 188.55 66.25 o 6 14 0 152.72 199.60 63.70 o -12 15 0 128.72 7.72 45.86 o -11 15 0 2984.89 2929.30 116.76 o -10 15 0 1253.72 1192.27 74.41 o -9 15 0 420.41 527.37 53.44 o -8 15 0 925.41 991.99 66.80 o -7 15 0 689.42 676.60 57.35 o -6 15 0 6137.09 6360.36 176.87 o -5 15 0 75.95 85.65 33.83 o -4 15 0 88.57 29.49 29.35 o -3 15 0 423.92 469.39 56.48 o -2 15 0 14.67 45.88 30.61 o -1 15 0 2215.55 2108.45 182.18 o 0 15 0 693.41 856.06 95.55 o 1 15 0 11.89 18.16 37.80 o 2 15 0 798.35 621.72 82.39 o 3 15 0 220.86 165.88 41.32 o 4 15 0 41.99 -1.70 43.32 o -12 16 0 782.46 860.86 83.24 o -11 16 0 1093.79 973.00 73.27 o -10 16 0 1245.25 1238.89 132.92 o -9 16 0 1411.61 1321.10 86.63 o -8 16 0 1594.38 1427.07 138.87 o -7 16 0 3792.85 3737.54 131.22 o -6 16 0 1242.74 1315.87 78.67 o -5 16 0 74.72 76.90 36.58 o -4 16 0 10.83 -0.23 29.35 o -3 16 0 0.45 5.07 29.72 o -2 16 0 0.33 -5.86 28.48 o -1 16 0 316.33 332.71 47.40 o 0 16 0 483.25 485.05 57.76 o 1 16 0 102.23 -2.12 32.43 o 2 16 0 348.36 84.57 132.07 o 3 16 0 696.89 655.53 89.61 o 4 16 0 7.69 32.27 54.36 o -11 17 0 182.26 70.04 38.57 o -10 17 0 1453.53 1467.22 87.98 o -9 17 0 312.37 414.90 62.85 o -8 17 0 2155.94 2031.06 98.78 o -7 17 0 2051.05 2230.56 103.88 o -6 17 0 5.39 46.68 33.57 o -5 17 0 2.46 19.73 32.97 o -4 17 0 38.67 14.37 31.41 o -3 17 0 1225.99 1397.98 98.52 o -2 17 0 681.74 775.32 67.23 o -1 17 0 1314.16 1217.23 84.51 o 0 17 0 202.11 264.65 48.85 o 1 17 0 1430.41 1326.24 118.06 o 2 17 0 1276.76 1244.28 122.31 o -10 18 0 40.53 36.60 38.21 o -9 18 0 8.67 0.23 32.62 o -8 18 0 453.74 449.25 55.84 o -7 18 0 6.76 -15.09 31.42 o -6 18 0 23.48 21.16 47.56 o -5 18 0 7.06 0.00 32.09 o -4 18 0 92.97 93.80 89.61 o -3 18 0 1762.73 1711.08 168.17 o -2 18 0 2135.35 2366.69 112.01 o -1 18 0 602.90 643.75 65.16 o 0 18 0 843.89 574.35 63.05 o 1 18 0 419.98 517.62 121.03 o -8 19 0 279.66 326.30 55.21 o -7 19 0 5.91 -8.89 32.97 o -6 19 0 97.20 124.35 43.79 o -5 19 0 680.39 837.18 105.32 o -4 19 0 0.98 -10.49 35.42 o -3 19 0 1211.93 1400.40 91.19 o -2 19 0 138.50 296.21 120.61 o -1 19 0 198.86 196.77 50.44 o 1 -19 1 157.98 150.78 48.00 o 2 -19 1 205.14 306.11 55.21 o 3 -19 1 649.48 738.78 70.84 o 4 -19 1 2134.15 2230.03 112.00 o 5 -19 1 34.01 2.74 36.24 o 6 -19 1 298.33 241.43 50.35 o 7 -19 1 125.77 132.43 65.40 o 8 -19 1 1370.55 1496.57 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