#------------------------------------------------------------------------------ #$Date: 2012-02-14 12:59:18 +0200 (Tue, 14 Feb 2012) $ #$Revision: 34292 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/83/2018347.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018347_Fobs loop_ _publ_author_name 'Aparici Plaza, Luis' 'Chojnacki, Jaroslaw' _publ_section_title ; Influence of chloroform on crystalline products yielded in reactions of 5,10,15,20-tetraphenylporphyrin with HCl and copper(II) salts ; _journal_coeditor_code FN3092 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m24 _journal_page_last m28 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 87.706 _cell_angle_beta 82.025 _cell_angle_gamma 76.356 _cell_length_a 11.6031 _cell_length_b 12.6132 _cell_length_c 24.5118 _exptl_crystal_F_000 1644.00 _reflns_d_resolution_high 0.8255 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824.29 794.33 48.07 o 2 5 27 340.68 247.26 46.06 o 3 5 27 4.58 64.82 46.10 o 4 5 27 18.65 -0.40 43.18 o 5 5 27 191.45 140.06 47.53 o 6 5 27 711.34 719.26 85.42 o 1 6 27 301.75 151.25 62.78 o 2 6 27 221.68 66.70 44.06 o 3 6 27 4.36 5.05 45.39 o 4 6 27 705.63 530.95 50.15 o 5 6 27 118.75 244.21 49.96 o -1 -4 28 6.01 62.91 76.05 o 0 -4 28 204.89 216.21 70.72 o 1 -4 28 124.36 207.84 79.44 o 2 -4 28 187.88 277.40 73.75 o -2 -3 28 316.27 195.55 67.47 o -1 -3 28 9.40 14.69 67.89 o 0 -3 28 4.98 -3.58 70.20 o 1 -3 28 64.22 44.40 76.26 o 2 -3 28 38.50 -16.95 70.76 o 3 -3 28 209.94 206.66 72.47 o 4 -3 28 469.15 417.36 73.01 o -2 -2 28 50.51 115.27 47.39 o -1 -2 28 202.09 232.73 52.10 o 0 -2 28 42.26 102.35 74.77 o 1 -2 28 93.46 15.11 72.50 o 2 -2 28 34.33 112.00 71.84 o 3 -2 28 0.05 13.21 72.64 o 4 -2 28 6.83 -11.83 75.20 o 5 -2 28 121.96 112.23 70.29 o -2 -1 28 407.05 555.80 49.74 o -1 -1 28 269.69 186.21 47.35 o 0 -1 28 20.59 47.13 44.71 o 1 -1 28 71.65 161.11 67.02 o 2 -1 28 377.23 489.58 77.70 o 3 -1 28 101.23 14.26 72.99 o 4 -1 28 243.21 189.73 78.59 o 5 -1 28 347.10 444.33 77.64 o -2 0 28 140.33 181.75 44.66 o -1 0 28 11.93 29.94 44.95 o 0 0 28 205.76 234.85 47.76 o 1 0 28 175.21 191.41 70.83 o 2 0 28 28.82 111.07 69.64 o 3 0 28 34.66 -44.84 69.96 o 4 0 28 120.96 154.06 74.52 o 5 0 28 269.62 166.44 75.72 o 6 0 28 95.71 137.97 73.72 o -2 1 28 254.68 249.63 46.72 o -1 1 28 1082.01 1152.37 73.33 o 0 1 28 2.32 -28.19 43.28 o 1 1 28 177.94 116.24 72.14 o 2 1 28 563.90 662.88 78.64 o 3 1 28 10.28 -1.79 70.69 o 4 1 28 202.89 275.87 72.03 o 5 1 28 707.24 642.64 78.59 o 6 1 28 22.94 14.53 76.65 o -2 2 28 622.96 679.71 48.46 o -1 2 28 4.66 2.74 43.50 o 0 2 28 301.65 412.33 97.28 o 1 2 28 62.96 70.61 68.45 o 2 2 28 1102.88 953.32 77.46 o 3 2 28 744.86 631.99 76.96 o 4 2 28 822.14 872.14 80.69 o 5 2 28 10.84 38.70 76.55 o 6 2 28 0.30 28.24 76.87 o -1 3 28 34.44 17.05 42.73 o 0 3 28 432.72 176.23 63.98 o 1 3 28 125.85 187.52 67.01 o 2 3 28 131.71 170.58 67.09 o 3 3 28 249.08 341.92 68.40 o 4 3 28 464.21 422.48 74.65 o 5 3 28 15.78 13.94 44.47 o 6 3 28 364.48 358.12 48.42 o 0 4 28 63.09 -9.43 57.16 o 1 4 28 43.73 62.91 60.41 o 2 4 28 556.98 675.04 74.41 o 3 4 28 8.13 46.11 44.70 o 4 4 28 5.46 18.77 43.87 o 5 4 28 31.97 48.17 46.06 o 1 5 28 52.28 38.53 41.61 o 2 5 28 272.71 318.71 45.09 o 3 5 28 634.58 587.76 52.14 o 4 5 28 270.17 275.77 48.23 o 5 5 28 129.74 82.10 48.17 o 0 -2 29 207.54 294.31 79.18 o 1 -2 29 389.37 280.09 76.97 o 2 -2 29 1213.09 1145.24 83.56 o 3 -2 29 85.71 6.88 68.48 o 0 -1 29 123.93 113.76 46.37 o 1 -1 29 236.09 263.88 71.61 o 2 -1 29 69.78 144.57 77.85 o 3 -1 29 93.31 86.76 70.65 o 4 -1 29 59.07 113.84 68.87 o -1 0 29 52.54 87.33 44.79 o 0 0 29 0.80 20.72 43.01 o 1 0 29 79.71 77.15 71.29 o 2 0 29 619.94 527.86 74.94 o 3 0 29 80.04 124.35 77.45 o 4 0 29 410.11 488.18 79.20 o 0 1 29 330.17 244.23 66.55 o 1 1 29 45.93 42.72 68.97 o 2 1 29 240.54 217.58 75.11 o 3 1 29 2.41 -26.32 70.03 o 4 1 29 238.45 157.60 77.37 o 0 2 29 14.45 -40.47 59.06 o 1 2 29 0.51 -6.11 67.10 o 2 2 29 273.68 275.85 73.26 o 3 2 29 74.37 127.80 74.32 o 4 2 29 128.97 178.01 71.72 o 1 3 29 801.93 812.02 73.45 o 2 3 29 12.38 16.84 68.00 o 3 3 29 34.49 139.93 72.37 o 4 3 29 150.98 43.28 67.04 o