#------------------------------------------------------------------------------ #$Date: 2012-02-14 12:59:18 +0200 (Tue, 14 Feb 2012) $ #$Revision: 34292 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/83/2018351.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018351_Fobs loop_ _publ_author_name 'Khan, Saeed I.' 'Knobler, Carolyn B.' 'Maverick, Emily F.' _publ_section_title ; Benz[cd]indol-2(1H)-one at 298 and 100K ; _journal_coeditor_code QS3004 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o1 _journal_page_last o6 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.196 _cell_angle_gamma 90.000 _cell_length_a 9.2508 _cell_length_b 6.7748 _cell_length_c 13.2556 _exptl_crystal_F_000 352.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file qs3004Ia298Ksup2.hkl _[local]_cod_data_source_block Ia298K #BEGIN Tags that were not found in dictionaries: _shelx_title ' EMILYF' _shelx_refln_list_code 4 _shelx_f_calc_maximum 125.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 172.53 146.68 6.11 o 4 0 0 218.74 235.26 10.04 o 6 0 0 230.16 218.71 9.75 o 8 0 0 20.91 18.15 1.95 o 10 0 0 20.77 21.43 2.75 o 1 1 0 2064.82 1790.57 71.19 o 2 1 0 1026.47 988.92 39.53 o 3 1 0 100.76 93.77 4.25 o 4 1 0 637.02 650.26 26.46 o 5 1 0 280.66 305.66 13.07 o 6 1 0 4.50 3.52 0.84 o 7 1 0 14.22 15.59 1.62 o 8 1 0 9.87 10.58 1.57 o 9 1 0 25.42 28.21 2.66 o 10 1 0 3.59 2.05 1.98 o 0 2 0 1246.82 1034.11 41.33 o 1 2 0 461.60 386.92 15.81 o 2 2 0 217.53 202.84 8.59 o 3 2 0 235.72 236.12 10.05 o 4 2 0 173.92 199.72 8.72 o 5 2 0 279.61 296.34 12.71 o 6 2 0 110.25 117.60 5.93 o 7 2 0 6.56 7.32 1.53 o 8 2 0 73.87 71.20 4.46 o 9 2 0 9.39 8.99 1.91 o 10 2 0 32.53 33.61 3.31 o 1 3 0 3.39 4.04 0.62 o 2 3 0 11.83 10.96 1.21 o 3 3 0 70.52 74.71 3.80 o 4 3 0 67.67 77.23 4.07 o 5 3 0 7.08 10.73 1.44 o 6 3 0 136.66 133.08 6.69 o 7 3 0 0.00 0.00 3.33 o 8 3 0 1.66 2.01 1.59 o 9 3 0 0.39 0.00 3.94 o 10 3 0 7.24 10.72 2.03 o 0 4 0 32.41 33.18 2.15 o 1 4 0 92.06 91.16 4.55 o 2 4 0 14.50 11.61 1.29 o 3 4 0 140.55 129.82 6.23 o 4 4 0 1.99 1.56 0.76 o 5 4 0 17.45 18.29 1.82 o 6 4 0 15.31 13.94 1.97 o 7 4 0 30.68 30.49 2.71 o 8 4 0 5.93 6.08 1.47 o 9 4 0 3.87 9.36 2.04 o 1 5 0 24.80 21.00 1.91 o 2 5 0 70.08 77.11 4.27 o 3 5 0 22.03 18.35 1.88 o 4 5 0 20.62 15.72 1.96 o 5 5 0 22.75 19.75 2.16 o 6 5 0 0.00 3.16 1.80 o 7 5 0 2.48 2.73 1.49 o 8 5 0 1.98 2.15 1.93 o 0 6 0 6.93 8.11 1.49 o 1 6 0 2.97 3.18 1.53 o 2 6 0 3.20 1.23 1.37 o 3 6 0 16.91 12.80 1.82 o 4 6 0 1.11 1.54 1.35 o 5 6 0 0.01 0.00 3.65 o 6 6 0 0.96 1.81 1.61 o 7 6 0 6.28 7.99 1.84 o 1 7 0 6.97 6.80 1.90 o 2 7 0 9.95 6.78 2.13 o 3 7 0 6.11 5.96 1.49 o 4 7 0 2.12 1.55 1.54 o 5 7 0 0.62 0.00 3.96 o 0 8 0 0.57 1.20 1.32 o 1 8 0 1.71 2.01 1.67 o -11 0 1 4.26 5.31 2.04 o -9 0 1 3.35 2.34 1.79 o -7 0 1 139.03 140.41 6.92 o -5 0 1 0.15 2.62 0.97 o -3 0 1 198.49 163.67 7.00 o -1 0 1 1020.75 1116.54 44.35 o 1 0 1 8106.87 6648.57 263.69 o 3 0 1 225.56 191.68 8.09 o 5 0 1 4.85 4.13 0.77 o 7 0 1 197.86 194.99 9.07 o 9 0 1 181.32 195.84 9.55 o -10 1 1 3.43 8.06 1.75 o -9 1 1 28.41 28.28 2.61 o -8 1 1 16.95 16.38 1.93 o -7 1 1 24.97 27.72 2.31 o -6 1 1 58.75 62.45 3.58 o -5 1 1 5.18 7.06 1.03 o -4 1 1 169.26 175.54 7.68 o -3 1 1 452.13 451.66 18.47 o -2 1 1 306.54 334.24 13.67 o -1 1 1 53.82 50.79 2.33 o 0 1 1 1080.11 1011.24 40.27 o 1 1 1 7.76 4.77 0.54 o 2 1 1 164.48 154.30 6.56 o 3 1 1 27.91 29.19 1.69 o 4 1 1 288.00 314.71 13.18 o 5 1 1 178.45 196.96 8.72 o 6 1 1 3.85 2.16 1.03 o 7 1 1 2.31 4.87 1.23 o 8 1 1 0.60 0.00 3.60 o 9 1 1 8.76 7.44 2.33 o 10 1 1 54.06 54.04 4.12 o -10 2 1 5.97 8.71 1.89 o -9 2 1 0.97 0.00 3.81 o -8 2 1 4.09 2.99 1.55 o -7 2 1 6.52 5.03 1.18 o -6 2 1 39.71 44.26 2.86 o -5 2 1 32.98 36.63 2.43 o -4 2 1 1.79 1.93 0.57 o -3 2 1 0.02 0.00 1.64 o -2 2 1 413.83 394.49 16.24 o -1 2 1 38.06 38.66 2.01 o 0 2 1 51.20 52.78 2.55 o 1 2 1 1076.07 907.35 36.46 o 2 2 1 5.50 8.38 0.81 o 3 2 1 294.05 308.44 12.97 o 4 2 1 127.49 154.71 6.98 o 5 2 1 169.79 180.84 8.23 o 6 2 1 19.98 21.04 1.82 o 7 2 1 44.35 46.05 3.17 o 8 2 1 17.76 16.53 2.03 o 9 2 1 22.06 21.69 2.52 o 10 2 1 16.97 10.13 1.99 o -10 3 1 4.15 0.00 4.93 o -9 3 1 0.00 0.88 1.34 o -8 3 1 4.67 5.71 1.30 o -7 3 1 15.99 17.42 2.01 o -6 3 1 0.02 0.00 3.14 o -5 3 1 18.64 19.07 1.71 o -4 3 1 11.69 13.17 1.41 o -3 3 1 75.47 79.68 4.05 o -2 3 1 56.76 55.74 3.00 o -1 3 1 297.17 288.42 12.14 o 0 3 1 935.79 854.24 34.56 o 1 3 1 27.22 28.81 1.78 o 2 3 1 51.01 48.46 2.67 o 3 3 1 283.01 271.23 11.70 o 4 3 1 18.33 20.25 1.68 o 5 3 1 13.00 9.89 1.62 o 6 3 1 0.58 0.00 2.68 o 7 3 1 20.92 17.91 1.92 o 8 3 1 16.26 13.86 2.02 o 9 3 1 15.22 14.17 2.09 o 10 3 1 1.88 2.25 1.86 o -9 4 1 12.57 12.92 2.15 o -8 4 1 0.24 7.11 1.64 o -7 4 1 0.96 2.55 1.40 o -6 4 1 64.19 69.28 4.16 o -5 4 1 188.32 185.46 8.72 o -4 4 1 74.40 66.70 3.82 o -3 4 1 0.67 0.95 0.91 o -2 4 1 234.87 224.42 9.94 o -1 4 1 190.18 174.12 7.89 o 0 4 1 79.97 86.88 4.36 o 1 4 1 146.52 139.52 6.51 o 2 4 1 10.43 8.93 1.17 o 3 4 1 273.33 230.34 10.28 o 4 4 1 2.29 1.35 1.15 o 5 4 1 50.22 50.39 3.32 o 6 4 1 0.03 0.00 3.36 o 7 4 1 0.27 0.00 3.50 o 8 4 1 3.10 1.78 1.50 o 9 4 1 10.49 17.51 2.70 o -8 5 1 0.80 1.31 1.46 o -7 5 1 3.36 3.24 1.87 o -6 5 1 5.94 5.37 1.43 o -5 5 1 1.53 3.16 1.45 o -4 5 1 265.69 241.17 11.03 o -3 5 1 19.20 20.55 2.03 o -2 5 1 155.44 139.47 6.84 o -1 5 1 12.69 12.88 1.61 o 0 5 1 0.14 3.36 1.27 o 1 5 1 5.24 4.53 0.96 o 2 5 1 17.19 14.56 1.64 o 3 5 1 134.05 127.85 6.45 o 4 5 1 11.35 9.51 1.56 o 5 5 1 0.50 1.70 1.37 o 6 5 1 2.78 0.50 1.62 o 7 5 1 8.00 10.16 1.80 o 8 5 1 6.98 9.91 2.06 o -7 6 1 8.04 10.00 1.99 o -6 6 1 4.40 2.17 1.72 o -5 6 1 0.01 1.47 1.36 o -4 6 1 38.36 36.63 3.03 o -3 6 1 22.98 20.19 2.14 o -2 6 1 5.96 4.02 1.04 o -1 6 1 2.71 3.22 1.01 o 0 6 1 51.17 51.66 3.46 o 1 6 1 11.34 14.70 1.88 o 2 6 1 118.40 113.04 6.06 o 3 6 1 45.61 42.65 3.30 o 4 6 1 33.82 39.07 3.01 o 5 6 1 2.79 1.66 1.47 o 6 6 1 24.21 29.41 3.02 o 7 6 1 7.63 13.00 2.14 o -5 7 1 10.59 14.74 2.30 o -4 7 1 2.39 3.72 1.73 o -3 7 1 0.18 1.55 1.45 o -2 7 1 3.91 6.09 1.64 o -1 7 1 22.01 21.25 2.46 o 0 7 1 2.95 2.50 1.66 o 1 7 1 2.53 2.79 1.60 o 2 7 1 53.00 62.12 4.35 o 3 7 1 6.06 9.46 1.85 o 4 7 1 5.04 6.52 1.68 o 5 7 1 3.62 1.33 1.72 o -1 8 1 4.78 7.98 2.10 o 0 8 1 0.28 1.10 1.50 o 1 8 1 0.44 0.58 1.38 o -10 0 2 3.61 6.94 1.76 o -8 0 2 0.16 0.70 1.18 o -6 0 2 839.19 823.64 33.80 o -4 0 2 544.44 503.94 20.67 o -2 0 2 6926.82 7395.11 293.38 o 0 0 2 471.10 453.84 18.22 o 2 0 2 1545.32 1387.50 55.36 o 4 0 2 23.69 17.81 1.36 o 6 0 2 298.36 280.31 12.28 o 8 0 2 37.95 35.20 2.80 o 10 0 2 21.08 16.32 2.32 o -10 1 2 45.37 50.76 3.96 o -9 1 2 2.83 2.44 1.77 o -8 1 2 42.75 39.92 3.07 o -7 1 2 1.19 0.69 1.14 o -6 1 2 12.03 12.43 1.57 o -5 1 2 193.90 209.41 9.27 o -4 1 2 70.95 71.04 3.58 o -3 1 2 79.48 86.49 4.00 o -2 1 2 15685.29 16295.37 596.57 o -1 1 2 7203.89 7405.56 293.58 o 0 1 2 8.08 9.28 0.71 o 1 1 2 326.90 285.65 11.69 o 2 1 2 49.76 45.64 2.27 o 3 1 2 900.37 993.63 39.92 o 4 1 2 760.27 794.40 32.27 o 5 1 2 45.39 43.11 2.61 o 6 1 2 34.73 34.40 2.55 o 7 1 2 0.18 0.00 3.00 o 8 1 2 14.58 16.28 2.04 o 9 1 2 2.42 3.41 1.89 o 10 1 2 6.56 7.63 2.05 o -10 2 2 3.76 3.50 1.89 o -9 2 2 3.21 8.57 1.68 o -8 2 2 2.97 5.71 1.36 o -7 2 2 20.84 18.65 1.94 o -6 2 2 10.62 10.95 1.55 o -5 2 2 107.78 118.37 5.75 o -4 2 2 272.98 291.05 12.44 o -3 2 2 0.02 0.81 0.67 o -2 2 2 676.66 695.60 28.10 o -1 2 2 41.34 47.36 2.44 o 0 2 2 0.11 1.61 0.60 o 1 2 2 422.66 397.47 16.30 o 2 2 2 10.22 9.89 0.93 o 3 2 2 114.51 106.77 4.93 o 4 2 2 93.63 88.94 4.41 o 5 2 2 24.67 29.82 2.12 o 6 2 2 5.05 6.04 1.07 o 7 2 2 19.98 21.28 2.09 o 8 2 2 47.79 52.81 3.74 o 9 2 2 0.26 0.68 1.26 o 10 2 2 0.78 2.57 1.67 o -10 3 2 4.77 6.18 1.91 o -9 3 2 0.43 0.00 3.62 o -8 3 2 27.56 27.52 2.65 o -7 3 2 116.36 122.88 6.58 o -6 3 2 0.90 0.48 1.02 o -5 3 2 72.50 62.16 3.57 o -4 3 2 148.84 150.38 6.99 o -3 3 2 6.74 6.53 1.00 o -2 3 2 121.70 111.50 5.23 o -1 3 2 474.84 441.29 18.26 o 0 3 2 208.56 234.83 10.03 o 1 3 2 483.43 467.08 19.29 o 2 3 2 18.93 22.92 1.61 o 3 3 2 4.08 2.70 0.74 o 4 3 2 217.00 212.67 9.47 o 5 3 2 170.81 187.11 8.63 o 6 3 2 33.01 36.60 2.77 o 7 3 2 2.94 2.61 1.52 o 8 3 2 8.63 10.10 1.59 o 9 3 2 0.69 1.62 1.55 o 10 3 2 9.20 9.24 2.20 o -9 4 2 0.24 1.87 1.64 o -8 4 2 9.79 8.34 1.85 o -7 4 2 0.37 0.00 3.47 o -6 4 2 5.56 5.49 1.60 o -5 4 2 2.21 2.96 1.39 o -4 4 2 24.35 23.22 1.98 o -3 4 2 4.72 5.03 0.96 o -2 4 2 14.60 14.44 1.56 o -1 4 2 112.05 110.67 5.41 o 0 4 2 148.42 151.76 6.97 o 1 4 2 54.47 52.13 3.00 o 2 4 2 136.88 139.47 6.57 o 3 4 2 7.10 8.01 1.20 o 4 4 2 5.08 5.21 1.08 o 5 4 2 7.30 8.55 1.46 o 6 4 2 20.04 19.69 2.09 o 7 4 2 0.39 0.62 1.11 o 8 4 2 3.25 4.06 1.89 o 9 4 2 3.05 5.60 2.57 o -8 5 2 2.42 0.00 4.49 o -7 5 2 0.05 0.00 4.04 o -6 5 2 7.45 8.77 1.49 o -5 5 2 2.11 5.17 1.20 o -4 5 2 82.32 79.47 4.58 o -3 5 2 18.65 19.67 2.03 o -2 5 2 3.74 3.36 0.94 o -1 5 2 2.54 0.11 1.53 o 0 5 2 12.47 13.77 1.53 o 1 5 2 20.25 17.79 1.75 o 2 5 2 34.81 34.18 2.62 o 3 5 2 33.20 31.14 2.50 o 4 5 2 12.76 14.01 1.73 o 5 5 2 91.08 101.99 5.66 o 6 5 2 6.30 9.19 2.03 o 7 5 2 31.09 35.03 2.96 o 8 5 2 0.27 1.33 1.65 o -7 6 2 1.82 0.00 4.16 o -6 6 2 0.44 2.03 1.53 o -5 6 2 4.68 0.00 4.00 o -4 6 2 1.32 0.78 1.24 o -3 6 2 7.77 8.26 1.67 o -2 6 2 0.24 0.00 2.98 o -1 6 2 35.15 40.99 3.05 o 0 6 2 12.15 11.31 1.54 o 1 6 2 28.45 25.73 2.30 o 2 6 2 39.80 40.69 3.07 o 3 6 2 8.33 5.34 1.47 o 4 6 2 5.84 8.01 1.63 o 5 6 2 5.47 8.10 1.62 o 6 6 2 34.98 39.36 3.37 o 7 6 2 19.44 23.33 2.84 o -5 7 2 5.55 3.76 1.87 o -4 7 2 0.61 0.00 4.20 o -3 7 2 1.62 1.38 1.37 o -2 7 2 1.56 0.72 1.27 o -1 7 2 0.14 2.85 1.45 o 0 7 2 1.09 2.05 1.54 o 1 7 2 25.05 28.06 2.90 o 2 7 2 1.05 1.62 1.60 o 3 7 2 10.06 3.74 1.65 o 4 7 2 3.49 8.27 1.92 o 5 7 2 0.34 0.00 4.10 o -9 0 3 0.71 0.00 3.89 o -7 0 3 0.65 1.24 1.21 o -5 0 3 74.27 69.01 3.65 o -3 0 3 143.51 149.06 6.50 o -1 0 3 3055.42 3615.34 143.59 o 1 0 3 461.75 435.12 17.64 o 3 0 3 63.83 54.18 2.79 o 5 0 3 5.21 5.48 1.06 o 7 0 3 126.36 110.96 5.81 o 9 0 3 88.35 89.78 5.54 o -10 1 3 3.96 2.64 2.06 o -9 1 3 18.20 20.32 2.57 o -8 1 3 24.39 30.00 2.59 o -7 1 3 12.61 12.85 1.81 o -6 1 3 0.04 0.00 2.74 o -5 1 3 57.14 47.45 2.80 o -4 1 3 78.31 83.35 4.10 o -3 1 3 667.85 697.94 28.27 o -2 1 3 4347.23 5124.00 203.39 o -1 1 3 6910.90 7716.42 306.25 o 0 1 3 28.77 21.38 1.23 o 1 1 3 32.03 31.77 1.69 o 2 1 3 249.34 265.33 11.04 o 3 1 3 212.68 215.96 9.20 o 4 1 3 105.23 124.60 5.74 o 5 1 3 280.55 293.85 12.66 o 6 1 3 11.33 9.38 1.40 o 7 1 3 86.90 93.22 5.10 o 8 1 3 165.30 163.79 8.19 o 9 1 3 6.13 5.50 2.02 o 10 1 3 5.99 6.74 1.86 o -10 2 3 3.30 0.00 5.37 o -9 2 3 0.15 0.65 1.29 o -8 2 3 17.24 19.59 2.28 o -7 2 3 1.47 3.59 1.18 o -6 2 3 42.29 39.95 2.78 o -5 2 3 3.10 3.37 0.90 o -4 2 3 1.62 1.29 0.98 o -3 2 3 60.55 63.86 3.32 o -2 2 3 13.06 14.45 1.19 o -1 2 3 57.91 57.89 2.84 o 0 2 3 183.61 170.13 7.31 o 1 2 3 61.38 58.53 2.93 o 2 2 3 862.88 890.82 35.99 o 3 2 3 293.70 316.29 13.30 o 4 2 3 1.20 1.44 0.95 o 5 2 3 70.35 76.58 4.05 o 6 2 3 10.89 10.11 1.44 o 7 2 3 0.76 1.86 1.36 o 8 2 3 3.55 0.00 3.98 o 9 2 3 37.33 37.77 3.16 o 10 2 3 1.63 3.70 1.44 o -10 3 3 1.16 2.07 1.87 o -9 3 3 12.99 11.59 1.99 o -8 3 3 0.05 0.00 3.66 o -7 3 3 0.17 0.65 1.18 o -6 3 3 77.17 81.48 4.56 o -5 3 3 0.01 0.00 2.59 o -4 3 3 63.11 57.04 3.32 o -3 3 3 27.95 22.08 1.67 o -2 3 3 11.00 13.89 1.27 o -1 3 3 364.07 320.38 13.47 o 0 3 3 224.08 225.47 9.75 o 1 3 3 357.97 353.57 14.85 o 2 3 3 40.35 41.59 2.44 o 3 3 3 23.52 23.85 1.78 o 4 3 3 21.73 23.55 1.86 o 5 3 3 1.28 2.89 1.41 o 6 3 3 52.61 52.37 3.42 o 7 3 3 84.97 82.75 4.80 o 8 3 3 0.00 0.00 3.45 o 9 3 3 6.42 9.51 1.74 o -9 4 3 1.09 0.50 1.83 o -8 4 3 20.62 17.75 2.21 o -7 4 3 19.95 14.14 1.95 o -6 4 3 124.19 119.44 6.33 o -5 4 3 62.85 56.40 3.72 o -4 4 3 0.10 0.00 2.59 o -3 4 3 136.18 124.70 6.11 o -2 4 3 18.18 15.98 1.61 o -1 4 3 85.56 87.41 4.50 o 0 4 3 15.80 14.47 1.42 o 1 4 3 155.23 163.01 7.52 o 2 4 3 0.92 0.65 0.85 o 3 4 3 37.18 37.31 2.60 o 4 4 3 9.85 8.05 1.26 o 5 4 3 56.37 57.07 3.71 o 6 4 3 2.37 1.94 1.33 o 7 4 3 17.20 20.95 2.27 o 8 4 3 1.35 1.41 1.58 o 9 4 3 16.19 23.10 2.74 o -8 5 3 5.87 4.17 1.90 o -7 5 3 8.11 8.21 1.73 o -6 5 3 29.20 26.64 2.65 o -5 5 3 29.71 30.80 2.83 o -4 5 3 84.06 80.55 4.70 o -3 5 3 24.43 21.99 2.21 o -2 5 3 38.19 39.36 2.76 o -1 5 3 40.25 40.31 2.76 o 0 5 3 0.08 1.56 1.06 o 1 5 3 52.92 50.89 3.27 o 2 5 3 106.85 104.94 5.55 o 3 5 3 47.36 46.17 3.18 o 4 5 3 33.53 32.96 2.76 o 5 5 3 1.94 0.00 3.62 o 6 5 3 1.33 2.24 1.57 o 7 5 3 3.27 2.94 2.00 o 8 5 3 6.96 8.79 1.95 o -7 6 3 0.56 1.99 1.66 o -6 6 3 10.88 14.51 2.30 o -5 6 3 0.73 2.57 1.48 o -4 6 3 12.98 10.64 1.84 o -3 6 3 16.34 13.25 1.75 o -2 6 3 3.54 3.58 1.49 o -1 6 3 9.57 9.38 1.66 o 0 6 3 10.69 8.71 1.79 o 1 6 3 118.81 125.70 6.65 o 2 6 3 19.57 19.30 2.26 o 3 6 3 19.91 17.87 2.09 o 4 6 3 30.39 33.45 2.97 o 5 6 3 7.43 2.26 2.12 o 6 6 3 24.64 30.77 2.98 o -5 7 3 0.11 1.40 1.67 o -4 7 3 3.73 4.25 1.95 o -3 7 3 0.24 1.77 1.34 o -2 7 3 3.39 3.39 1.69 o -1 7 3 0.09 3.58 1.65 o 0 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