#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/83/2018376.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018376_Fobs loop_ _publ_author_name 'Daran, Jean-Claude' 'Demirhan, Funda' 'Y\?ild\?ir\?im, \"Ozg\"ur' '\,Cetinkaya, Bekir' _publ_section_title ; 1-Ferrocenylmethyl-3-(2,4,6-trimethylbenzyl)-1H-imidazolidin-3-ium iodide and trans-bis(3-benzyl-1-ferrocenylmethyl-1H-imidazolidin-2-ylidene)diiodidopalladium(II) ; _journal_coeditor_code KY3008 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m48 _journal_page_last m52 _journal_volume 68 _journal_year 2012 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.603 _cell_angle_gamma 90.000 _cell_length_a 10.6277 _cell_length_b 7.4514 _cell_length_c 28.2926 _exptl_crystal_F_000 1064.00 _reflns_d_resolution_high 0.7500 _[local]_cod_data_source_file ky3008Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' FUNDA' _shelx_refln_list_code 4 _shelx_f_calc_maximum 403.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 5 -9 0 75.26 185.49 229.73 o 6 -8 0 340.80 595.19 279.32 o 7 -8 0 441.44 323.83 273.05 o 8 -8 0 595.10 320.15 165.12 o 5 -7 0 2020.71 2295.51 281.54 o 6 -7 0 573.50 440.64 198.75 o 7 -7 0 1596.92 1242.89 205.97 o 8 -7 0 181.06 199.19 187.92 o 9 -7 0 525.70 537.28 193.95 o 10 -7 0 449.64 474.50 219.77 o 0 -6 0 1109.14 1138.10 118.22 o 1 -6 0 6295.89 6601.48 175.14 o 2 -6 0 629.88 583.76 98.41 o 3 -6 0 3608.02 3706.57 163.32 o 4 -6 0 2555.25 2666.48 133.96 o 5 -6 0 878.95 1141.84 119.98 o 6 -6 0 421.91 507.20 112.00 o 7 -6 0 462.27 536.96 253.39 o 9 -6 0 58.09 28.84 147.81 o 10 -6 0 95.23 159.66 170.76 o 11 -6 0 234.31 193.91 138.80 o 1 -5 0 501.72 746.76 84.94 o 2 -5 0 266.70 228.70 75.39 o 3 -5 0 275.38 344.09 88.69 o 4 -5 0 1341.10 1356.00 108.64 o 5 -5 0 6126.97 6316.15 187.05 o 6 -5 0 65.39 31.08 53.33 o 7 -5 0 4279.52 4591.48 209.30 o 8 -5 0 106.07 48.54 63.44 o 9 -5 0 427.13 450.34 124.18 o 10 -5 0 336.41 229.37 132.26 o 11 -5 0 78.79 52.37 85.67 o 12 -5 0 211.46 111.42 84.14 o 1 -4 0 6934.94 7239.35 145.52 o 2 -4 0 6328.66 6677.84 132.78 o 3 -4 0 15260.47 15534.07 199.79 o 4 -4 0 14542.87 15301.08 260.86 o 5 -4 0 1538.97 1694.98 117.35 o 6 -4 0 1095.11 1018.91 110.15 o 7 -4 0 1591.44 1513.03 131.42 o 8 -4 0 793.28 902.13 129.15 o 9 -4 0 530.04 434.07 118.79 o 10 -4 0 954.47 955.17 168.72 o 11 -4 0 37.66 81.84 85.52 o 12 -4 0 602.13 449.09 132.16 o 1 -3 0 3268.53 3313.77 87.08 o 2 -3 0 129.64 203.91 66.90 o 3 -3 0 14371.08 14388.55 180.48 o 4 -3 0 6622.43 6954.29 129.84 o 5 -3 0 2798.88 2779.74 119.85 o 6 -3 0 2834.01 2765.44 133.15 o 7 -3 0 1764.26 1861.18 129.31 o 8 -3 0 3065.46 2955.47 146.32 o 9 -3 0 2020.00 2053.53 152.29 o 10 -3 0 145.20 167.16 117.60 o 11 -3 0 1303.60 1271.54 143.30 o 12 -3 0 314.58 357.84 142.12 o 13 -3 0 432.93 500.97 165.68 o 0 -2 0 19877.80 20683.42 152.23 o 1 -2 0 10704.93 11269.69 114.11 o 2 -2 0 11156.16 10790.16 127.07 o 3 -2 0 3324.49 3314.65 86.00 o 4 -2 0 11621.54 11171.97 437.14 o 5 -2 0 1599.61 1517.61 99.30 o 6 -2 0 3036.46 3304.57 117.72 o 7 -2 0 927.16 949.19 106.20 o 8 -2 0 3416.61 3682.85 171.63 o 9 -2 0 1368.83 1378.81 136.18 o 10 -2 0 1012.13 1064.25 155.77 o 11 -2 0 891.73 820.13 128.42 o 12 -2 0 355.00 441.60 139.90 o 13 -2 0 232.96 259.48 132.55 o 2 -1 0 15090.76 15722.03 785.06 o 3 -1 0 3224.10 2965.41 118.39 o 4 -1 0 4928.37 4824.60 102.66 o 5 -1 0 4367.83 4390.08 118.23 o 6 -1 0 6852.83 6771.03 270.42 o 7 -1 0 1142.29 1073.28 102.79 o 8 -1 0 6092.95 6125.58 177.94 o 9 -1 0 1279.44 1216.10 136.46 o 10 -1 0 1036.01 1071.70 125.64 o 11 -1 0 3055.72 2878.44 212.03 o 12 -1 0 393.51 364.60 128.79 o 13 -1 0 188.20 329.10 232.30 o 14 -1 0 93.19 140.62 176.47 o 2 0 0 291.28 323.54 21.34 o 3 0 0 83.55 92.39 22.30 o 4 0 0 614.83 582.71 30.76 o 5 0 0 2812.18 2961.97 60.98 o 6 0 0 2000.84 2103.11 62.53 o 7 0 0 2434.73 2530.15 70.00 o 8 0 0 1311.44 1223.19 117.38 o 9 0 0 1515.76 1396.68 133.59 o 10 0 0 1.66 47.14 67.60 o 11 0 0 639.21 557.74 135.77 o 12 0 0 1559.86 1484.36 231.55 o 13 0 0 258.92 520.33 245.09 o 14 0 0 150.52 298.51 189.17 o 1 1 0 12817.13 9166.27 281.64 o 2 1 0 14870.12 15533.72 312.45 o 3 1 0 3409.16 3306.43 62.94 o 4 1 0 5226.71 5173.76 78.80 o 5 1 0 4456.34 4588.76 116.65 o 6 1 0 6732.91 6615.54 97.60 o 7 1 0 1145.03 1050.42 63.85 o 8 1 0 6071.00 6315.43 114.76 o 9 1 0 1277.29 1445.60 201.80 o 10 1 0 1063.40 1089.79 213.54 o 11 1 0 3093.89 3521.66 282.75 o 12 1 0 399.52 440.44 206.98 o 13 1 0 195.77 213.85 147.22 o 14 1 0 94.53 108.29 161.23 o 0 2 0 19500.13 19674.29 371.22 o 1 2 0 11024.38 11138.15 211.65 o 2 2 0 11038.71 10608.69 78.98 o 3 2 0 3512.64 3516.21 42.44 o 4 2 0 11753.97 11887.72 278.75 o 5 2 0 1603.01 1524.08 117.71 o 6 2 0 3026.86 3115.65 233.87 o 7 2 0 930.77 851.98 116.51 o 8 2 0 3422.01 3782.18 142.86 o 9 2 0 1399.77 1477.86 106.00 o 10 2 0 1006.61 1011.74 225.53 o 11 2 0 895.74 883.20 218.57 o 12 2 0 329.45 370.95 191.22 o 13 2 0 233.56 255.10 190.39 o 1 3 0 3198.64 3269.28 140.05 o 2 3 0 92.13 164.63 31.18 o 3 3 0 14371.81 14140.62 93.37 o 4 3 0 6954.72 7434.51 154.01 o 5 3 0 2690.77 2629.31 92.64 o 6 3 0 2804.38 2765.75 117.06 o 7 3 0 1782.25 1810.16 209.61 o 8 3 0 3048.97 3084.56 148.20 o 9 3 0 1995.44 2117.74 145.94 o 10 3 0 135.95 104.79 133.80 o 12 3 0 298.60 269.82 168.27 o 13 3 0 426.66 550.58 267.95 o 0 4 0 8102.05 9093.33 173.24 o 1 4 0 6905.85 7082.59 216.30 o 2 4 0 6474.11 6852.19 107.50 o 3 4 0 15311.01 15387.60 245.72 o 4 4 0 14406.44 15143.00 160.20 o 5 4 0 1500.16 1491.15 75.95 o 6 4 0 1120.81 1269.06 70.76 o 7 4 0 1655.10 1599.74 160.15 o 8 4 0 771.16 798.09 186.75 o 9 4 0 522.53 533.47 135.28 o 10 4 0 946.11 1001.56 137.25 o 11 4 0 37.56 25.49 161.68 o 12 4 0 636.47 943.49 297.36 o 1 5 0 507.57 544.27 76.40 o 2 5 0 244.67 261.07 43.87 o 3 5 0 286.14 306.95 97.33 o 4 5 0 1361.88 1365.10 67.72 o 5 5 0 6141.37 6150.19 152.95 o 6 5 0 65.63 51.60 66.59 o 7 5 0 4311.54 4440.27 191.02 o 8 5 0 106.57 19.34 47.92 o 9 5 0 415.65 371.24 171.94 o 10 5 0 343.99 278.99 123.33 o 11 5 0 76.55 103.88 77.60 o 0 6 0 1126.05 1108.37 98.48 o 1 6 0 6391.89 6803.23 201.55 o 2 6 0 627.16 536.54 62.24 o 3 6 0 3606.22 3513.43 177.14 o 4 6 0 2424.62 2432.83 125.38 o 6 6 0 456.18 408.56 137.41 o 7 6 0 467.48 471.19 214.41 o 8 6 0 476.28 389.74 111.98 o 9 6 0 64.99 11.61 100.38 o 10 6 0 81.84 114.22 119.41 o 11 6 0 230.35 271.85 149.43 o 1 7 0 770.52 740.31 66.16 o 2 7 0 127.21 106.83 72.58 o 3 7 0 2176.04 2098.42 191.94 o 4 7 0 210.17 181.40 62.10 o 5 7 0 2016.86 1961.74 304.58 o 6 7 0 559.12 405.36 116.62 o 7 7 0 1594.40 1839.58 222.66 o 8 7 0 176.32 171.59 188.57 o 9 7 0 510.29 625.71 213.79 o 10 7 0 435.09 347.42 177.51 o 0 8 0 423.73 344.19 142.15 o 1 8 0 1951.64 2172.54 127.97 o 2 8 0 817.82 911.15 139.66 o 3 8 0 411.81 410.57 94.54 o 4 8 0 1570.19 1386.74 135.44 o 5 8 0 173.12 72.28 83.17 o 6 8 0 335.44 301.95 101.59 o 7 8 0 437.19 426.31 134.28 o 8 8 0 602.90 734.07 188.06 o 1 9 0 56.47 104.15 116.52 o 2 9 0 738.73 730.01 140.66 o 3 9 0 479.09 660.09 164.79 o 4 9 0 434.83 282.47 124.71 o 5 9 0 79.23 82.40 94.43 o -5 -9 1 76.38 128.96 194.41 o 5 -9 1 574.71 838.75 331.69 o -8 -8 1 1111.54 907.39 280.31 o -7 -8 1 413.28 524.60 240.13 o 6 -8 1 166.11 193.73 222.30 o 7 -8 1 702.12 593.41 283.23 o 8 -8 1 438.49 527.28 271.02 o -10 -7 1 475.68 661.94 333.44 o -9 -7 1 113.45 41.19 169.31 o -7 -7 1 1853.27 1716.57 282.36 o -6 -7 1 16.61 133.73 241.65 o 5 -7 1 719.11 544.07 226.29 o 6 -7 1 707.72 590.72 237.02 o 7 -7 1 75.22 136.44 192.66 o 8 -7 1 39.40 46.77 102.20 o 9 -7 1 977.22 505.11 195.49 o -11 -6 1 351.38 247.51 193.35 o -10 -6 1 479.45 577.25 292.20 o -9 -6 1 1066.79 846.95 228.03 o -7 -6 1 2060.71 1898.56 272.42 o -6 -6 1 199.73 444.60 213.35 o -5 -6 1 2320.87 2671.15 315.75 o -4 -6 1 790.95 787.86 105.55 o -3 -6 1 2586.02 2663.94 130.19 o -2 -6 1 357.77 366.54 67.45 o -1 -6 1 77.57 97.19 51.23 o 0 -6 1 563.37 536.10 129.00 o 1 -6 1 405.78 510.71 115.38 o 2 -6 1 260.65 216.63 86.60 o 3 -6 1 1035.56 1095.85 131.31 o 4 -6 1 819.60 781.94 111.93 o 5 -6 1 1846.37 1829.87 135.64 o 6 -6 1 483.54 455.28 103.67 o 7 -6 1 1953.83 1978.98 146.14 o 8 -6 1 763.51 706.57 126.07 o 9 -6 1 701.71 729.55 225.14 o 10 -6 1 233.37 433.71 196.38 o 11 -6 1 327.27 378.75 259.32 o -12 -5 1 149.85 134.03 129.58 o -11 -5 1 1014.22 990.54 186.05 o -10 -5 1 451.91 414.66 143.89 o -9 -5 1 8.61 20.00 96.05 o -8 -5 1 912.63 822.33 181.94 o -7 -5 1 1321.32 1321.74 128.85 o -6 -5 1 1168.25 1154.31 107.74 o -5 -5 1 2948.32 3116.29 140.36 o -4 -5 1 1169.87 1154.93 111.28 o -3 -5 1 1151.15 1187.57 102.42 o -2 -5 1 1057.62 1126.29 76.47 o -1 -5 1 6876.42 7301.58 123.50 o 0 -5 1 973.19 1035.12 62.62 o 1 -5 1 22627.61 23276.41 182.50 o 2 -5 1 903.44 1030.48 89.71 o 3 -5 1 5565.73 5715.69 160.79 o 4 -5 1 1060.15 1057.23 114.21 o 5 -5 1 1319.04 1374.41 118.15 o 6 -5 1 2746.51 2815.96 192.37 o 7 -5 1 2.06 31.82 61.88 o 8 -5 1 954.81 836.28 137.45 o 9 -5 1 1250.40 1270.65 154.15 o 10 -5 1 656.55 599.99 147.10 o 11 -5 1 11.72 31.38 68.72 o 12 -5 1 164.67 124.64 99.00 o -12 -4 1 296.22 182.95 127.69 o -11 -4 1 503.07 431.42 136.39 o -10 -4 1 1426.85 1495.94 166.58 o -9 -4 1 1875.71 2061.91 225.03 o -8 -4 1 2392.96 2191.50 134.59 o -7 -4 1 1755.36 1777.98 163.04 o -6 -4 1 644.47 640.22 104.83 o -5 -4 1 2814.04 2913.84 166.83 o -4 -4 1 2566.11 2703.49 126.29 o -3 -4 1 1244.29 1284.05 102.16 o -2 -4 1 6605.74 7046.03 128.78 o -1 -4 1 2168.91 2280.15 83.73 o 0 -4 1 2806.37 2259.82 86.02 o 1 -4 1 3.23 29.52 57.98 o 2 -4 1 6295.91 6642.23 149.24 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1 2163.78 2102.40 141.45 o 9 -3 1 1947.69 1935.00 161.00 o 10 -3 1 494.05 523.34 128.51 o 11 -3 1 572.97 679.13 177.78 o 12 -3 1 331.68 355.88 124.53 o 13 -3 1 19.21 59.65 91.91 o -13 -2 1 117.57 94.50 171.56 o -12 -2 1 1810.10 1827.60 205.16 o -11 -2 1 314.27 327.93 181.04 o -10 -2 1 2098.69 2094.58 167.21 o -9 -2 1 915.65 848.59 134.64 o -8 -2 1 4845.68 5076.82 170.73 o -7 -2 1 1281.02 1123.05 94.16 o -6 -2 1 8568.91 8764.81 255.93 o -5 -2 1 5140.22 5220.86 407.86 o -4 -2 1 2272.73 2214.29 160.51 o -3 -2 1 938.91 982.63 76.48 o -2 -2 1 3421.50 3634.76 88.29 o 1 -2 1 7568.98 8052.88 117.10 o 2 -2 1 4141.75 4337.88 101.40 o 3 -2 1 1894.41 1916.79 83.15 o 4 -2 1 11572.12 11490.01 588.59 o 5 -2 1 4830.62 4941.35 131.16 o 6 -2 1 4304.05 4069.99 132.88 o 7 -2 1 1361.61 1314.34 110.97 o 8 -2 1 3147.00 2834.09 148.13 o 9 -2 1 1041.66 977.01 138.00 o 10 -2 1 2186.72 2076.69 177.61 o 11 -2 1 398.32 416.56 128.85 o 12 -2 1 982.81 827.35 147.00 o 13 -2 1 548.84 480.62 166.71 o -14 -1 1 171.49 206.86 188.89 o -13 -1 1 190.95 198.73 179.94 o -12 -1 1 450.50 494.99 188.66 o -11 -1 1 3895.11 3955.88 204.92 o -10 -1 1 145.34 156.45 80.93 o -9 -1 1 1762.71 1779.46 129.61 o -8 -1 1 205.14 340.12 101.87 o -7 -1 1 1481.00 1413.53 101.06 o -6 -1 1 3075.41 3271.33 173.07 o -5 -1 1 982.88 915.74 82.13 o -4 -1 1 2924.91 2805.84 92.99 o -3 -1 1 5743.10 5560.19 114.03 o -2 -1 1 72499.56 74098.02 253.64 o -1 -1 1 4698.22 4223.41 52.54 o 1 -1 1 11864.10 9122.66 85.97 o 2 -1 1 95649.52 91113.38 4766.18 o 3 -1 1 2194.20 2311.60 84.86 o 4 -1 1 15338.53 14855.48 147.03 o 5 -1 1 13603.51 13159.98 149.38 o 6 -1 1 594.14 590.54 88.10 o 7 -1 1 3168.25 3081.85 123.21 o 8 -1 1 622.02 649.47 119.41 o 9 -1 1 1177.01 1084.05 130.98 o 10 -1 1 194.17 200.72 98.27 o 11 -1 1 463.28 536.16 143.72 o 12 -1 1 23.89 133.74 103.48 o 13 -1 1 917.23 906.76 200.69 o -14 0 1 480.35 384.87 245.21 o -13 0 1 327.49 454.69 242.73 o -12 0 1 1997.67 1964.10 269.11 o -11 0 1 488.75 476.55 190.51 o -10 0 1 678.99 753.85 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