#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:20:45 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180852 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/83/2018387.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018387_Fobs loop_ _publ_author_name 'Gerhardt, Valeska' 'Tutughamiarso, Maya' 'Bolte, Michael' _publ_section_title ; Conformational studies of hydantoin-5-acetic acid and orotic acid ; _journal_coeditor_code SK3419 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o92 _journal_page_last o98 _journal_volume 68 _journal_year 2012 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.6148 _cell_length_b 8.5592 _cell_length_c 9.3406 _exptl_crystal_F_000 328.00 _reflns_d_resolution_high 0.8197 _cod_data_source_file sk3419Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' vg2-96 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 73.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 0.27 1.80 5.83 o 4 0 0 536.78 539.78 42.87 o 6 0 0 769.67 834.02 45.61 o 8 0 0 306.55 298.75 22.14 o 1 1 0 1337.83 1191.80 32.13 o 2 1 0 47.01 43.44 4.62 o 3 1 0 1.68 1.19 3.36 o 4 1 0 213.30 218.13 5.55 o 5 1 0 2.29 1.63 3.87 o 6 1 0 58.26 59.73 4.44 o 7 1 0 981.91 928.82 40.34 o 8 1 0 202.72 189.61 7.61 o 9 1 0 46.79 52.45 5.63 o 0 2 0 5472.61 5221.95 414.35 o 1 2 0 1867.70 1941.41 27.85 o 2 2 0 1163.45 1153.10 21.50 o 3 2 0 16.85 19.49 3.78 o 4 2 0 132.65 139.94 5.34 o 5 2 0 13.78 13.43 3.81 o 6 2 0 25.86 23.25 4.27 o 7 2 0 519.83 504.59 14.11 o 8 2 0 48.05 58.58 5.16 o 9 2 0 13.71 7.45 4.97 o 1 3 0 2245.36 2321.92 46.74 o 2 3 0 820.49 857.89 11.21 o 3 3 0 548.76 559.79 11.44 o 4 3 0 353.00 352.40 9.49 o 5 3 0 225.98 234.87 5.43 o 6 3 0 127.48 134.69 5.07 o 7 3 0 1.71 2.43 4.51 o 8 3 0 5.55 9.26 5.30 o 0 4 0 606.46 583.57 10.93 o 1 4 0 25.65 31.02 3.98 o 2 4 0 340.47 322.63 5.92 o 3 4 0 73.94 80.37 4.28 o 4 4 0 0.20 2.57 3.52 o 5 4 0 0.18 1.56 3.75 o 6 4 0 803.22 773.53 41.23 o 7 4 0 0.92 5.76 4.52 o 8 4 0 3.11 5.35 5.31 o 1 5 0 364.50 356.68 14.25 o 2 5 0 365.03 377.41 9.11 o 3 5 0 145.41 151.20 4.49 o 4 5 0 112.90 118.41 4.54 o 5 5 0 96.68 97.06 4.42 o 6 5 0 17.25 20.24 4.45 o 7 5 0 55.52 48.77 5.80 o 8 5 0 3.30 4.66 5.27 o 0 6 0 324.24 333.11 12.33 o 1 6 0 242.14 245.62 5.86 o 2 6 0 1.65 3.78 4.11 o 3 6 0 107.75 112.49 4.37 o 4 6 0 24.21 35.22 4.13 o 5 6 0 208.53 209.02 11.35 o 6 6 0 121.24 117.58 7.48 o 7 6 0 2.34 3.75 4.89 o 1 7 0 123.77 118.17 4.82 o 2 7 0 177.84 183.18 5.67 o 3 7 0 172.32 177.26 6.06 o 4 7 0 110.58 105.46 4.84 o 5 7 0 5.74 7.29 4.63 o 6 7 0 0.37 4.61 4.59 o 0 8 0 13.80 21.66 7.15 o 1 8 0 0.19 2.12 5.42 o 2 8 0 48.88 47.07 4.61 o 3 8 0 3.56 11.50 4.80 o 4 8 0 78.03 81.63 5.32 o 5 8 0 0.66 2.31 5.21 o 1 9 0 42.28 51.15 6.00 o 2 9 0 3.33 3.69 5.39 o 3 9 0 64.97 71.50 5.73 o 4 9 0 5.31 5.76 5.50 o 0 10 0 208.41 191.77 15.64 o 1 10 0 56.74 56.63 6.26 o 2 10 0 9.38 9.93 6.76 o 1 0 1 178.94 153.99 9.42 o 2 0 1 38.99 29.37 4.43 o 3 0 1 37.58 39.05 3.86 o 4 0 1 1572.42 1747.77 65.56 o 5 0 1 44.67 47.39 3.74 o 6 0 1 6.69 4.31 3.66 o 7 0 1 50.75 52.92 4.23 o 8 0 1 63.17 60.22 4.95 o 9 0 1 8.62 10.54 4.80 o 0 1 1 11.25 10.69 9.24 o 1 1 1 155.32 131.83 4.19 o 2 1 1 754.70 738.17 13.30 o 3 1 1 1461.68 1635.28 38.23 o 4 1 1 301.20 299.86 4.55 o 5 1 1 132.38 143.49 4.03 o 6 1 1 180.96 180.11 6.35 o 7 1 1 349.69 337.99 9.72 o 8 1 1 4.00 6.16 3.02 o 9 1 1 19.88 22.66 3.52 o 0 2 1 0.01 1.16 3.82 o 1 2 1 545.31 486.04 12.31 o 2 2 1 236.51 224.05 4.12 o 3 2 1 85.92 88.20 3.08 o 4 2 1 429.63 455.87 10.93 o 5 2 1 608.80 599.64 14.35 o 6 2 1 227.55 224.86 4.44 o 7 2 1 4.81 6.81 3.09 o 8 2 1 53.68 52.90 3.54 o 9 2 1 3.34 6.44 4.12 o 0 3 1 1086.57 1029.55 49.41 o 1 3 1 392.65 357.85 10.48 o 2 3 1 1047.18 1060.14 18.29 o 3 3 1 351.48 382.04 7.17 o 4 3 1 415.94 430.32 12.27 o 5 3 1 65.86 68.73 3.08 o 6 3 1 275.63 283.45 6.39 o 7 3 1 34.90 41.77 3.28 o 8 3 1 79.65 87.59 4.30 o 0 4 1 706.83 710.61 19.16 o 1 4 1 251.08 248.36 4.59 o 2 4 1 254.90 271.13 5.69 o 3 4 1 11.02 11.30 2.55 o 4 4 1 356.32 377.98 5.80 o 5 4 1 285.86 293.71 6.85 o 6 4 1 24.36 24.14 3.26 o 7 4 1 32.77 27.30 3.45 o 8 4 1 167.21 168.61 4.80 o 0 5 1 75.03 74.92 4.65 o 1 5 1 708.98 726.77 13.88 o 2 5 1 243.38 242.78 3.84 o 3 5 1 334.89 340.70 4.84 o 4 5 1 75.86 77.24 3.11 o 5 5 1 70.37 73.00 3.23 o 6 5 1 245.47 242.42 6.71 o 7 5 1 251.25 261.37 10.08 o 8 5 1 3.04 7.50 4.26 o 0 6 1 152.40 161.14 5.22 o 1 6 1 71.05 71.01 3.32 o 2 6 1 28.77 31.39 3.00 o 3 6 1 68.78 71.85 3.06 o 4 6 1 247.20 242.80 3.83 o 5 6 1 44.99 43.49 3.11 o 6 6 1 32.00 36.17 3.14 o 7 6 1 21.38 22.42 3.68 o 0 7 1 384.42 393.51 11.65 o 1 7 1 157.08 146.29 4.80 o 2 7 1 287.56 282.09 4.44 o 3 7 1 144.23 151.13 3.63 o 4 7 1 314.63 322.23 5.32 o 5 7 1 225.21 227.27 5.03 o 6 7 1 35.17 33.32 3.46 o 0 8 1 19.18 17.61 4.76 o 1 8 1 252.18 248.18 4.96 o 2 8 1 18.12 17.01 3.31 o 3 8 1 145.66 145.94 3.95 o 4 8 1 107.00 111.37 3.85 o 5 8 1 95.53 91.86 3.71 o 0 9 1 248.01 252.69 7.53 o 1 9 1 29.34 32.94 3.85 o 2 9 1 79.00 80.70 3.94 o 3 9 1 121.87 121.43 4.10 o 4 9 1 118.43 110.62 4.15 o 0 10 1 1.16 6.74 5.72 o 1 10 1 35.29 41.18 4.33 o 2 10 1 9.02 16.84 4.62 o 0 0 2 113.68 93.85 6.83 o 1 0 2 684.37 595.04 27.34 o 2 0 2 2249.94 2306.22 52.64 o 3 0 2 246.64 265.36 5.78 o 4 0 2 61.08 57.89 4.25 o 5 0 2 48.11 49.34 3.76 o 6 0 2 1.25 0.61 4.00 o 7 0 2 194.09 186.79 11.56 o 8 0 2 293.43 282.50 15.58 o 9 0 2 76.49 76.57 5.09 o 0 1 2 4377.30 4455.27 127.04 o 1 1 2 3495.34 3453.30 75.75 o 2 1 2 1233.31 1202.20 23.88 o 3 1 2 251.92 226.28 7.97 o 4 1 2 234.31 237.02 4.76 o 5 1 2 21.99 21.68 2.88 o 6 1 2 501.53 504.10 12.15 o 7 1 2 56.13 58.27 3.04 o 8 1 2 9.34 12.84 3.45 o 9 1 2 19.14 19.44 3.62 o 0 2 2 326.33 280.12 7.32 o 1 2 2 4573.40 4878.14 118.28 o 2 2 2 527.11 546.24 7.93 o 3 2 2 27.98 30.22 3.00 o 4 2 2 488.60 487.88 13.02 o 5 2 2 116.88 119.67 3.68 o 6 2 2 9.25 9.66 3.39 o 7 2 2 86.06 77.92 4.21 o 8 2 2 70.14 62.34 3.57 o 0 3 2 130.82 119.57 5.13 o 1 3 2 65.25 69.29 2.99 o 2 3 2 595.03 586.25 15.41 o 3 3 2 151.02 157.11 3.27 o 4 3 2 56.66 58.77 3.00 o 5 3 2 142.49 146.85 3.50 o 6 3 2 83.56 80.47 3.44 o 7 3 2 69.10 72.73 3.52 o 8 3 2 142.06 140.62 5.29 o 0 4 2 254.70 260.46 12.79 o 1 4 2 998.77 1015.58 18.55 o 2 4 2 493.73 468.84 10.43 o 3 4 2 386.44 388.03 5.21 o 4 4 2 70.61 71.90 3.17 o 5 4 2 140.14 135.89 3.97 o 6 4 2 58.69 56.55 3.42 o 7 4 2 44.20 39.16 3.48 o 8 4 2 58.27 59.80 3.99 o 0 5 2 482.48 457.70 49.22 o 1 5 2 154.91 157.03 4.14 o 2 5 2 31.25 29.16 2.79 o 3 5 2 62.76 60.08 3.02 o 4 5 2 6.10 7.38 2.78 o 5 5 2 195.54 193.12 3.86 o 6 5 2 240.84 233.60 6.00 o 7 5 2 57.60 57.29 3.91 o 0 6 2 251.75 238.65 13.93 o 1 6 2 6.15 7.04 3.32 o 2 6 2 117.09 119.26 3.20 o 3 6 2 387.02 365.64 6.73 o 4 6 2 132.64 128.89 3.65 o 5 6 2 103.49 93.85 3.43 o 6 6 2 31.67 34.49 3.54 o 7 6 2 106.73 108.59 4.38 o 0 7 2 12.11 13.46 5.65 o 1 7 2 140.30 138.44 5.11 o 2 7 2 181.48 177.32 5.53 o 3 7 2 28.09 29.90 3.04 o 4 7 2 168.15 177.12 3.66 o 5 7 2 14.58 16.06 3.29 o 6 7 2 73.31 77.72 4.33 o 0 8 2 56.94 61.88 4.90 o 1 8 2 99.05 92.91 3.69 o 2 8 2 108.45 110.78 4.03 o 3 8 2 213.80 202.90 4.18 o 4 8 2 156.15 166.64 4.08 o 5 8 2 122.16 119.23 4.38 o 0 9 2 113.48 93.65 7.36 o 1 9 2 1.76 0.78 3.78 o 2 9 2 33.69 38.73 3.82 o 3 9 2 138.25 140.34 4.51 o 4 9 2 4.47 4.53 3.83 o 0 10 2 10.74 10.19 5.83 o 1 10 2 66.15 63.93 4.29 o 1 0 3 2021.56 1983.46 53.22 o 2 0 3 38.96 34.85 3.86 o 3 0 3 624.76 634.91 31.07 o 4 0 3 16.00 14.14 3.77 o 5 0 3 0.57 2.46 3.71 o 6 0 3 20.43 17.38 4.20 o 7 0 3 721.89 717.80 15.84 o 8 0 3 1.14 2.27 4.69 o 0 1 3 3087.96 3015.99 97.50 o 1 1 3 2197.31 2117.61 71.36 o 2 1 3 853.05 861.03 11.19 o 3 1 3 453.73 458.63 14.27 o 4 1 3 1058.15 1141.30 33.96 o 5 1 3 136.45 139.52 6.25 o 6 1 3 210.72 210.98 8.27 o 7 1 3 39.04 44.34 3.31 o 8 1 3 145.21 137.15 5.05 o 0 2 3 1840.94 1803.44 45.13 o 1 2 3 230.69 207.89 4.06 o 2 2 3 89.05 87.52 3.00 o 3 2 3 134.54 132.78 5.35 o 4 2 3 336.32 353.26 8.56 o 5 2 3 261.95 252.67 7.21 o 6 2 3 87.21 82.14 3.39 o 7 2 3 175.24 190.55 5.61 o 8 2 3 74.72 73.89 3.85 o 0 3 3 592.88 593.51 11.76 o 1 3 3 265.35 261.19 5.06 o 2 3 3 529.26 529.51 10.89 o 3 3 3 314.87 332.62 8.64 o 4 3 3 72.84 83.74 3.08 o 5 3 3 22.46 20.68 3.11 o 6 3 3 371.13 387.60 7.71 o 7 3 3 114.93 112.94 3.87 o 8 3 3 69.83 63.14 3.80 o 0 4 3 27.38 30.80 4.13 o 1 4 3 260.39 244.49 6.09 o 2 4 3 291.24 298.35 4.75 o 3 4 3 193.64 196.79 3.72 o 4 4 3 32.81 34.35 2.83 o 5 4 3 384.47 370.72 8.21 o 6 4 3 136.00 136.01 3.88 o 7 4 3 27.73 24.89 3.69 o 8 4 3 23.40 22.18 3.66 o 0 5 3 53.89 52.90 5.13 o 1 5 3 264.56 266.09 6.46 o 2 5 3 404.66 410.66 7.99 o 3 5 3 229.83 231.14 3.85 o 4 5 3 160.83 172.21 3.91 o 5 5 3 342.71 330.24 9.66 o 6 5 3 2.15 5.29 3.16 o 7 5 3 32.09 27.44 3.60 o 0 6 3 243.54 216.03 15.76 o 1 6 3 288.08 287.89 4.96 o 2 6 3 68.21 71.66 3.07 o 3 6 3 131.60 129.40 3.56 o 4 6 3 71.85 76.73 3.21 o 5 6 3 169.15 172.24 3.90 o 6 6 3 146.66 143.11 4.16 o 7 6 3 57.12 57.23 3.93 o 0 7 3 283.06 297.26 10.95 o 1 7 3 103.40 109.28 3.89 o 2 7 3 8.92 10.89 3.08 o 3 7 3 94.68 90.38 3.31 o 4 7 3 16.43 15.89 3.17 o 5 7 3 104.69 100.81 3.80 o 6 7 3 44.94 44.95 4.02 o 0 8 3 224.19 213.72 7.91 o 1 8 3 244.25 244.11 4.46 o 2 8 3 47.53 56.46 3.71 o 3 8 3 39.89 37.77 3.77 o 4 8 3 48.19 48.58 3.56 o 5 8 3 11.60 12.35 3.69 o 0 9 3 5.58 4.18 5.05 o 1 9 3 24.90 24.58 3.63 o 2 9 3 33.44 41.53 4.02 o 3 9 3 30.39 28.92 4.06 o 4 9 3 9.86 7.45 13.67 o 0 10 3 226.98 220.17 7.06 o 0 0 4 955.74 992.36 35.15 o 1 0 4 6.73 8.98 3.57 o 2 0 4 101.97 110.99 4.32 o 3 0 4 1327.79 1389.86 41.88 o 4 0 4 8.87 10.36 3.57 o 5 0 4 294.97 310.70 9.82 o 6 0 4 18.86 21.69 4.87 o 7 0 4 87.46 84.98 5.27 o 8 0 4 0.26 2.39 4.81 o 0 1 4 1433.64 1521.71 43.41 o 1 1 4 471.27 453.91 9.35 o 2 1 4 125.80 129.57 3.02 o 3 1 4 10.42 11.29 2.43 o 4 1 4 50.02 50.68 2.98 o 5 1 4 63.32 62.08 3.31 o 6 1 4 10.94 13.29 2.98 o 7 1 4 68.13 62.32 3.47 o 8 1 4 5.40 8.70 3.67 o 0 2 4 247.09 232.54 6.23 o 1 2 4 174.58 168.42 3.48 o 2 2 4 142.53 143.64 3.22 o 3 2 4 76.04 80.26 3.21 o 4 2 4 385.21 402.92 11.94 o 5 2 4 38.34 36.79 3.17 o 6 2 4 122.07 119.69 3.61 o 7 2 4 46.04 46.84 3.50 o 8 2 4 34.65 36.60 3.74 o 0 3 4 539.73 512.66 22.77 o 1 3 4 391.03 400.18 6.90 o 2 3 4 179.38 176.81 4.72 o 3 3 4 580.91 578.85 7.50 o 4 3 4 37.85 35.77 3.04 o 5 3 4 193.47 183.13 4.32 o 6 3 4 145.63 136.91 6.16 o 7 3 4 6.91 10.00 3.82 o 8 3 4 73.09 72.57 4.00 o 0 4 4 25.72 31.71 3.82 o 1 4 4 912.45 900.23 15.70 o 2 4 4 178.91 178.59 3.41 o 3 4 4 51.28 51.05 2.86 o 4 4 4 14.93 15.41 2.91 o 5 4 4 319.03 303.60 6.68 o 6 4 4 69.56 68.90 3.75 o 7 4 4 22.78 22.20 3.96 o 0 5 4 32.70 31.49 3.98 o 1 5 4 128.22 131.62 3.37 o 2 5 4 338.09 339.34 7.56 o 3 5 4 27.57 29.95 2.92 o 4 5 4 124.45 127.45 3.54 o 5 5 4 6.50 10.49 3.10 o 6 5 4 72.74 74.39 4.09 o 7 5 4 26.34 27.18 4.10 o 0 6 4 30.83 29.94 4.75 o 1 6 4 4.09 6.15 3.13 o 2 6 4 401.70 378.98 10.40 o 3 6 4 132.12 127.25 3.52 o 4 6 4 140.60 138.56 3.67 o 5 6 4 163.63 176.44 3.87 o 6 6 4 30.30 29.00 3.51 o 0 7 4 4.84 8.56 4.45 o 1 7 4 34.00 34.26 3.36 o 2 7 4 289.41 285.03 4.40 o 3 7 4 370.11 366.59 5.24 o 4 7 4 73.66 73.04 3.53 o 5 7 4 37.37 40.27 3.61 o 6 7 4 22.47 26.25 10.62 o 0 8 4 14.08 13.13 4.98 o 1 8 4 13.88 19.07 3.71 o 2 8 4 33.20 36.07 3.77 o 3 8 4 34.27 34.94 3.81 o 4 8 4 57.86 56.93 3.70 o 5 8 4 16.89 20.79 14.43 o 0 9 4 76.72 69.02 5.62 o 1 9 4 52.59 52.16 3.82 o 2 9 4 26.79 25.90 4.07 o 3 9 4 81.87 81.64 4.45 o 1 0 5 649.48 687.72 18.90 o 2 0 5 857.48 909.50 35.17 o 3 0 5 197.80 187.44 6.79 o 4 0 5 32.75 32.74 4.02 o 5 0 5 57.52 68.26 4.32 o 6 0 5 149.25 144.03 8.00 o 7 0 5 0.82 4.68 4.81 o 8 0 5 0.17 -0.19 6.20 o 0 1 5 0.63 0.88 3.21 o 1 1 5 56.01 58.08 2.74 o 2 1 5 334.48 337.76 7.11 o 3 1 5 254.67 249.92 7.78 o 4 1 5 176.98 188.18 3.91 o 5 1 5 81.90 83.41 3.38 o 6 1 5 106.10 96.44 4.24 o 7 1 5 46.67 48.98 3.59 o 8 1 5 73.71 73.86 4.16 o 0 2 5 810.42 831.38 23.73 o 1 2 5 533.23 560.66 8.32 o 2 2 5 573.89 573.10 10.95 o 3 2 5 437.34 446.84 12.05 o 4 2 5 66.97 65.05 3.01 o 5 2 5 306.29 286.94 7.73 o 6 2 5 237.42 232.37 4.93 o 7 2 5 26.95 29.95 3.74 o 8 2 5 48.04 46.17 4.28 o 0 3 5 34.39 24.71 3.88 o 1 3 5 419.27 409.35 6.56 o 2 3 5 17.71 15.68 2.62 o 3 3 5 117.76 112.15 4.26 o 4 3 5 324.22 309.43 14.37 o 5 3 5 292.52 291.67 7.23 o 6 3 5 31.32 33.21 3.48 o 7 3 5 41.32 39.77 3.74 o 0 4 5 279.88 296.27 5.62 o 1 4 5 38.54 38.50 2.83 o 2 4 5 5.53 4.52 2.59 o 3 4 5 128.67 132.94 3.36 o 4 4 5 83.48 82.15 3.64 o 5 4 5 14.44 17.41 3.16 o 6 4 5 103.42 98.22 3.57 o 7 4 5 87.68 83.89 4.50 o 0 5 5 4.18 5.32 3.90 o 1 5 5 64.48 65.88 3.24 o 2 5 5 846.10 821.56 18.96 o 3 5 5 75.58 70.79 3.14 o 4 5 5 13.91 15.65 3.16 o 5 5 5 24.86 24.00 3.46 o 6 5 5 50.65 48.16 3.81 o 7 5 5 2.35 7.01 5.61 o 0 6 5 206.72 211.58 13.22 o 1 6 5 81.10 73.81 3.24 o 2 6 5 13.00 13.87 2.99 o 3 6 5 6.96 8.17 3.05 o 4 6 5 38.00 39.85 3.29 o 5 6 5 152.04 154.20 4.05 o 6 6 5 26.92 31.79 4.08 o 0 7 5 2.13 2.18 4.59 o 1 7 5 212.09 204.31 5.85 o 2 7 5 468.95 464.63 12.19 o 3 7 5 32.64 40.09 3.52 o 4 7 5 4.61 7.77 3.51 o 5 7 5 54.10 56.15 3.68 o 0 8 5 0.07 1.45 4.86 o 1 8 5 8.35 12.18 3.69 o 2 8 5 49.99 48.11 3.92 o 3 8 5 26.42 27.48 3.89 o 4 8 5 14.97 18.40 4.00 o 0 9 5 1.91 3.98 5.88 o 1 9 5 104.15 99.83 4.46 o 2 9 5 1.43 6.51 4.26 o 0 0 6 365.41 369.74 12.78 o 1 0 6 96.12 90.50 4.15 o 2 0 6 153.05 144.45 6.89 o 3 0 6 162.59 166.47 7.86 o 4 0 6 11.36 11.38 4.25 o 5 0 6 648.29 674.13 16.37 o 6 0 6 57.16 64.94 5.18 o 7 0 6 0.81 -2.32 5.13 o 0 1 6 40.02 34.19 3.83 o 1 1 6 72.36 75.00 2.71 o 2 1 6 352.11 370.99 10.65 o 3 1 6 274.34 278.55 6.38 o 4 1 6 3.71 8.76 2.82 o 5 1 6 20.81 21.82 3.17 o 6 1 6 59.81 63.95 3.79 o 7 1 6 140.94 135.08 5.78 o 0 2 6 3.93 4.09 3.38 o 1 2 6 518.69 536.16 7.96 o 2 2 6 757.19 780.28 13.66 o 3 2 6 381.38 381.79 7.72 o 4 2 6 279.11 293.36 5.36 o 5 2 6 71.96 64.12 3.23 o 6 2 6 82.70 84.28 3.65 o 7 2 6 0.84 4.27 3.68 o 0 3 6 47.30 51.43 4.00 o 1 3 6 230.70 238.07 7.56 o 2 3 6 27.33 24.57 2.72 o 3 3 6 120.75 117.07 3.93 o 4 3 6 5.72 5.82 2.77 o 5 3 6 176.81 177.49 4.36 o 6 3 6 17.90 17.99 3.17 o 7 3 6 42.53 42.23 3.83 o 0 4 6 0.00 1.01 3.75 o 1 4 6 60.70 62.35 2.87 o 2 4 6 53.16 57.34 2.89 o 3 4 6 78.47 79.03 3.17 o 4 4 6 402.67 398.03 8.24 o 5 4 6 2.71 5.81 3.13 o 6 4 6 14.55 13.25 3.34 o 0 5 6 34.17 35.10 4.13 o 1 5 6 54.07 55.37 3.16 o 2 5 6 111.24 109.10 3.48 o 3 5 6 371.02 352.73 6.49 o 4 5 6 114.70 116.07 3.68 o 5 5 6 11.54 13.82 3.52 o 6 5 6 38.90 37.41 3.93 o 0 6 6 3.52 4.24 4.48 o 1 6 6 10.25 11.89 3.27 o 2 6 6 64.55 69.64 3.21 o 3 6 6 13.02 15.95 3.27 o 4 6 6 56.67 55.69 3.62 o 5 6 6 2.23 3.25 4.13 o 0 7 6 0.00 -0.88 5.18 o 1 7 6 26.05 28.99 3.48 o 2 7 6 6.55 8.46 3.47 o 3 7 6 34.39 32.06 3.73 o 4 7 6 8.49 7.93 3.81 o 0 8 6 4.54 6.83 5.45 o 1 8 6 40.73 40.41 4.10 o 2 8 6 46.12 53.82 4.03 o 3 8 6 18.92 20.98 4.22 o 1 0 7 102.90 99.55 4.05 o 2 0 7 59.36 56.06 4.01 o 3 0 7 122.85 124.35 5.25 o 4 0 7 425.69 432.79 11.47 o 5 0 7 1.98 2.45 4.49 o 6 0 7 8.41 6.22 4.90 o 7 0 7 44.10 34.26 5.81 o 0 1 7 2.67 3.10 3.84 o 1 1 7 9.84 9.92 2.59 o 2 1 7 35.96 35.90 2.70 o 3 1 7 331.53 324.53 6.15 o 4 1 7 50.08 46.88 3.16 o 5 1 7 69.45 61.71 3.48 o 6 1 7 24.99 19.58 3.61 o 7 1 7 7.36 10.95 4.13 o 0 2 7 13.92 15.93 3.63 o 1 2 7 23.70 28.58 2.68 o 2 2 7 203.12 202.96 3.61 o 3 2 7 186.30 192.36 4.32 o 4 2 7 126.90 122.36 4.79 o 5 2 7 32.98 39.24 3.46 o 6 2 7 17.08 18.31 3.69 o 7 2 7 43.41 46.78 4.03 o 0 3 7 51.55 52.20 4.04 o 1 3 7 123.26 128.13 3.28 o 2 3 7 190.73 187.31 3.74 o 3 3 7 288.91 272.60 9.78 o 4 3 7 123.13 125.81 3.99 o 5 3 7 155.61 153.70 3.72 o 6 3 7 13.14 15.96 3.67 o 0 4 7 24.87 19.83 4.05 o 1 4 7 113.66 116.96 3.21 o 2 4 7 27.66 31.37 2.90 o 3 4 7 108.43 109.52 3.38 o 4 4 7 33.27 27.90 3.40 o 5 4 7 61.92 66.31 3.87 o 6 4 7 14.14 12.58 3.56 o 0 5 7 190.84 185.47 6.36 o 1 5 7 225.49 232.47 4.52 o 2 5 7 39.29 37.77 3.34 o 3 5 7 104.53 106.55 3.45 o 4 5 7 11.90 18.29 3.72 o 5 5 7 13.17 16.94 3.42 o 0 6 7 0.05 3.60 4.46 o 1 6 7 299.32 286.06 6.62 o 2 6 7 171.33 161.84 5.20 o 3 6 7 20.64 24.50 3.49 o 4 6 7 18.05 17.53 3.70 o 0 7 7 16.46 16.91 5.55 o 1 7 7 15.92 18.94 3.78 o 2 7 7 2.50 -0.89 3.49 o 3 7 7 2.33 3.46 3.84 o 0 8 7 7.68 7.18 6.38 o 1 8 7 62.12 62.56 4.27 o 0 0 8 29.11 28.19 5.78 o 1 0 8 31.97 35.01 3.94 o 2 0 8 42.65 49.07 4.45 o 3 0 8 346.22 339.75 20.38 o 4 0 8 5.17 7.55 4.77 o 5 0 8 15.53 14.70 4.53 o 6 0 8 37.28 40.28 5.40 o 0 1 8 3.80 6.08 3.82 o 1 1 8 222.66 220.11 5.37 o 2 1 8 152.06 157.41 3.35 o 3 1 8 25.18 24.12 2.89 o 4 1 8 224.93 217.75 10.22 o 5 1 8 103.20 101.62 3.79 o 6 1 8 5.53 7.07 4.47 o 0 2 8 3.52 7.59 3.88 o 1 2 8 53.14 59.19 2.92 o 2 2 8 26.48 33.09 2.97 o 3 2 8 19.31 20.78 2.90 o 4 2 8 173.70 179.51 3.97 o 5 2 8 112.82 110.34 4.05 o 6 2 8 8.68 11.84 3.78 o 0 3 8 4.86 7.78 3.75 o 1 3 8 16.11 15.49 2.71 o 2 3 8 428.07 426.39 8.40 o 3 3 8 13.42 14.71 2.92 o 4 3 8 49.71 47.33 3.28 o 5 3 8 53.15 62.22 3.95 o 6 3 8 41.69 31.10 15.92 o 0 4 8 96.66 93.66 4.33 o 1 4 8 97.16 100.80 3.94 o 2 4 8 102.41 106.67 3.23 o 3 4 8 45.99 53.52 3.29 o 4 4 8 98.09 99.75 3.60 o 5 4 8 29.31 30.33 3.99 o 0 5 8 20.82 17.45 4.42 o 1 5 8 68.23 66.99 3.34 o 2 5 8 10.36 11.67 3.17 o 3 5 8 13.34 14.94 3.46 o 4 5 8 3.01 5.19 3.52 o 0 6 8 9.91 12.28 4.73 o 1 6 8 26.90 26.68 3.65 o 2 6 8 52.98 52.54 3.88 o 3 6 8 149.17 148.37 4.98 o 0 7 8 2.08 4.38 5.28 o 1 7 8 38.69 37.63 3.82 o 2 7 8 53.70 49.54 8.52 o 1 0 9 3.77 8.63 4.19 o 2 0 9 38.13 39.44 4.51 o 3 0 9 1.06 2.84 4.82 o 4 0 9 61.74 59.41 5.33 o 5 0 9 80.01 81.21 5.52 o 0 1 9 131.84 129.34 4.88 o 1 1 9 1.67 1.92 3.15 o 2 1 9 111.02 110.53 3.48 o 3 1 9 66.47 69.26 3.82 o 4 1 9 29.28 28.73 3.66 o 5 1 9 10.57 9.97 3.67 o 0 2 9 7.00 11.83 4.08 o 1 2 9 82.75 80.22 3.10 o 2 2 9 30.54 29.97 2.99 o 3 2 9 202.18 199.85 8.16 o 4 2 9 155.75 158.50 4.11 o 5 2 9 68.94 67.46 3.93 o 0 3 9 7.96 7.19 4.12 o 1 3 9 16.95 16.99 3.06 o 2 3 9 50.71 51.17 3.36 o 3 3 9 203.34 202.92 3.98 o 4 3 9 129.07 129.93 3.82 o 0 4 9 106.93 100.40 6.57 o 1 4 9 97.59 96.05 3.37 o 2 4 9 40.80 45.72 3.39 o 3 4 9 229.37 243.90 6.65 o 4 4 9 47.97 49.57 3.68 o 0 5 9 7.87 7.47 4.54 o 1 5 9 38.10 36.53 3.44 o 2 5 9 29.35 28.71 3.30 o 3 5 9 20.86 25.10 3.68 o 0 6 9 164.12 151.16 8.68 o 1 6 9 5.22 5.86 3.64 o 0 0 10 166.92 145.40 11.71 o 1 0 10 36.86 38.05 5.39 o 2 0 10 34.38 34.69 4.97 o 3 0 10 19.44 20.62 4.92 o 4 0 10 30.96 26.00 5.21 o 0 1 10 2.15 3.32 4.80 o 1 1 10 0.20 1.54 3.25 o 2 1 10 39.66 35.66 3.79 o 3 1 10 53.91 52.54 3.96 o 4 1 10 1.40 4.56 3.55 o 0 2 10 137.45 124.64 6.68 o 1 2 10 23.53 20.85 3.18 o 2 2 10 36.61 37.87 3.43 o 3 2 10 1.47 4.88 3.44 o 4 2 10 6.42 3.93 20.78 o 0 3 10 20.42 22.73 4.92 o 1 3 10 57.06 54.94 3.20 o 2 3 10 23.61 29.29 3.49 o 3 3 10 95.55 95.53 4.06 o 0 4 10 29.44 31.79 4.85 o 1 4 10 4.96 6.96 3.49 o 2 4 10 38.03 33.51 3.59 o 1 0 11 3.31 4.98 5.04 o 2 0 11 43.34 37.99 5.40 o 0 1 11 10.85 16.98 5.27 o 1 1 11 16.74 16.22 3.57 o 2 1 11 5.74 10.03 5.89 o 0 2 11 21.90 21.33 4.71 o 1 2 11 16.26 15.88 3.66 o