#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:20:45 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180852 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/83/2018391.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018391_Fobs loop_ _publ_author_name 'Gelbrich, Thomas' 'Rossi, Denise' 'Griesser, Ulrich J.' _publ_section_title ; Two polymorphs and the diethylammonium salt of the barbiturate eldoral ; _journal_coeditor_code SK3420 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o65 _journal_page_last o70 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.189 _cell_angle_gamma 90.000 _cell_length_a 7.8761 _cell_length_b 12.7102 _cell_length_c 11.9438 _exptl_crystal_F_000 512.00 _reflns_d_resolution_high 0.8357 _cod_data_source_file sk3420Iasup2.hkl _cod_data_source_block Ia #BEGIN Tags that were not found in dictionaries: _shelx_title ' s92 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 86.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 607.66 735.20 4.65 o 2 0 0 4.71 9.38 1.13 o 3 0 0 25.45 29.44 3.57 o 4 0 0 1313.31 1387.90 13.29 o 5 0 0 1309.40 1272.57 16.14 o 6 0 0 405.64 460.47 19.52 o 7 0 0 174.74 186.20 5.71 o 8 0 0 9.50 9.95 1.66 o 9 0 0 0.22 -0.29 1.19 o 2 1 0 3042.35 3206.46 54.05 o 3 1 0 270.69 294.29 6.53 o 4 1 0 419.06 422.56 7.69 o 5 1 0 145.31 133.41 2.89 o 6 1 0 10.40 9.70 1.06 o 7 1 0 1.74 2.18 1.26 o 8 1 0 211.83 236.86 7.93 o 9 1 0 112.10 116.21 3.39 o 1 2 0 219.41 231.01 2.23 o 2 2 0 1281.54 1360.25 9.80 o 3 2 0 474.12 524.71 7.21 o 4 2 0 852.25 868.29 7.74 o 5 2 0 14.78 14.18 0.96 o 6 2 0 36.82 42.61 1.68 o 7 2 0 542.36 630.97 10.10 o 8 2 0 187.92 222.31 3.99 o 9 2 0 49.13 55.26 2.30 o 1 3 0 79.50 94.51 1.24 o 2 3 0 31.66 34.29 1.10 o 3 3 0 1648.17 1834.17 14.56 o 4 3 0 65.84 64.93 3.30 o 5 3 0 1048.39 1018.31 21.99 o 6 3 0 59.26 63.76 1.98 o 7 3 0 32.38 33.20 1.92 o 8 3 0 8.55 5.59 1.25 o 9 3 0 1.87 0.68 1.03 o 0 4 0 3006.06 2755.88 162.56 o 1 4 0 1727.21 1804.95 13.59 o 2 4 0 192.84 207.86 4.88 o 3 4 0 235.37 258.23 5.93 o 4 4 0 670.55 585.19 9.70 o 5 4 0 399.52 403.49 9.74 o 6 4 0 84.50 85.48 2.06 o 7 4 0 3.05 3.97 1.37 o 8 4 0 545.08 589.05 8.09 o 9 4 0 13.10 17.34 1.73 o 1 5 0 7.74 14.92 2.81 o 2 5 0 597.93 645.07 5.99 o 3 5 0 346.40 348.98 7.36 o 4 5 0 67.93 58.34 3.88 o 5 5 0 86.73 85.43 2.04 o 6 5 0 374.30 385.73 5.45 o 7 5 0 16.51 16.62 1.67 o 8 5 0 16.20 20.47 1.83 o 0 6 0 108.21 104.12 1.79 o 1 6 0 778.24 792.27 5.70 o 2 6 0 1235.11 1259.12 9.38 o 3 6 0 521.30 479.88 5.36 o 4 6 0 22.15 18.92 1.04 o 5 6 0 12.21 14.70 1.22 o 6 6 0 12.35 12.21 1.28 o 7 6 0 13.90 12.76 2.44 o 8 6 0 0.53 2.78 2.33 o 1 7 0 131.30 155.16 4.50 o 2 7 0 56.82 31.47 3.27 o 3 7 0 89.58 83.72 3.43 o 4 7 0 18.01 14.27 1.15 o 5 7 0 4.36 2.61 1.24 o 6 7 0 176.30 192.86 4.48 o 7 7 0 100.54 100.66 5.63 o 8 7 0 0.38 0.85 1.69 o 0 8 0 426.17 356.62 23.91 o 1 8 0 1.44 2.44 0.56 o 2 8 0 155.98 155.61 3.47 o 3 8 0 6.89 6.20 1.19 o 4 8 0 121.54 133.11 3.46 o 5 8 0 178.64 171.11 5.07 o 6 8 0 70.60 74.24 4.88 o 7 8 0 121.31 118.00 5.55 o 1 9 0 443.56 430.75 6.17 o 2 9 0 4.10 2.78 0.88 o 3 9 0 3.37 5.09 1.11 o 4 9 0 104.89 135.44 3.60 o 5 9 0 256.96 290.99 6.34 o 6 9 0 88.62 98.01 6.04 o 7 9 0 43.02 39.95 1.83 o 0 10 0 1255.65 1242.34 26.80 o 1 10 0 18.87 20.80 1.24 o 2 10 0 20.14 18.88 1.56 o 3 10 0 102.76 119.13 3.34 o 4 10 0 26.14 36.57 2.11 o 5 10 0 4.97 1.62 1.51 o 6 10 0 243.26 255.42 4.68 o 7 10 0 105.19 106.14 3.68 o 1 11 0 1394.78 1417.52 8.77 o 2 11 0 33.37 33.05 1.88 o 3 11 0 11.81 15.49 1.30 o 4 11 0 146.55 164.78 3.24 o 5 11 0 15.20 24.37 1.86 o 6 11 0 0.18 1.14 1.09 o 0 12 0 1109.38 1189.48 32.54 o 1 12 0 689.16 692.50 8.06 o 2 12 0 187.86 208.14 5.70 o 3 12 0 23.99 18.17 1.45 o 4 12 0 127.65 149.52 4.19 o 5 12 0 122.17 96.56 20.61 o 1 13 0 313.75 347.74 18.80 o 2 13 0 51.56 60.19 3.00 o 3 13 0 60.92 69.67 2.65 o 4 13 0 5.36 3.00 1.43 o 0 14 0 2.42 1.58 1.65 o 1 14 0 64.39 66.25 6.12 o 2 14 0 5.56 3.94 1.05 o 3 14 0 40.68 37.53 2.85 o -9 1 1 47.22 51.41 2.40 o -8 1 1 86.56 105.44 4.13 o -7 1 1 258.80 301.19 5.15 o -6 1 1 2.09 2.52 1.05 o -5 1 1 171.15 158.46 4.93 o -4 1 1 1.17 1.51 0.59 o -3 1 1 1518.46 1686.20 26.69 o -2 1 1 43.76 40.48 1.24 o -1 1 1 16.25 84.29 58.10 o 0 1 1 374.59 379.18 1.63 o 1 1 1 578.59 677.21 3.26 o 2 1 1 1.64 6.98 0.46 o 3 1 1 1257.82 1394.37 29.54 o 4 1 1 470.57 466.04 5.70 o 5 1 1 70.12 67.46 4.07 o 6 1 1 0.46 0.92 0.97 o 7 1 1 289.07 332.03 5.18 o 8 1 1 18.26 18.98 1.46 o 9 1 1 12.27 10.19 1.08 o -9 2 1 60.93 57.13 1.86 o -8 2 1 30.65 38.39 1.75 o -7 2 1 30.04 31.58 1.91 o -6 2 1 106.32 120.78 2.84 o -5 2 1 4.17 4.63 0.77 o -4 2 1 130.82 126.71 3.27 o -3 2 1 835.31 909.95 9.38 o -2 2 1 4072.30 4148.31 47.43 o -1 2 1 1160.98 1265.85 14.94 o 1 2 1 1465.66 1466.23 17.65 o 3 2 1 1598.37 1702.13 13.36 o 4 2 1 25.23 23.44 1.46 o 5 2 1 157.30 159.79 2.72 o 6 2 1 17.61 18.70 1.36 o 7 2 1 385.85 446.29 12.27 o 8 2 1 35.72 38.29 1.76 o 9 2 1 0.15 0.02 1.05 o -9 3 1 46.57 42.72 1.92 o -8 3 1 74.35 87.55 2.92 o -7 3 1 51.80 59.24 3.14 o -6 3 1 460.48 484.05 6.22 o -5 3 1 203.98 177.59 2.81 o -4 3 1 892.62 821.08 11.41 o -3 3 1 30.82 36.71 2.18 o -2 3 1 2281.84 2412.75 45.15 o -1 3 1 158.58 169.77 1.32 o 0 3 1 461.36 514.15 22.07 o 1 3 1 4.50 7.05 1.21 o 2 3 1 1887.19 1880.30 8.77 o 3 3 1 1542.61 1588.93 13.89 o 4 3 1 106.89 92.35 3.10 o 5 3 1 240.21 244.81 4.83 o 6 3 1 171.80 179.84 5.73 o 7 3 1 29.80 31.42 1.70 o 8 3 1 20.57 21.38 1.63 o 9 3 1 8.27 5.60 1.03 o -9 4 1 1.43 2.85 1.35 o -8 4 1 5.58 5.57 1.17 o -7 4 1 101.32 100.15 4.34 o -6 4 1 320.74 342.83 6.62 o -5 4 1 346.68 349.32 3.94 o -4 4 1 186.41 168.50 4.73 o -3 4 1 1214.23 1227.78 12.69 o -2 4 1 7484.82 7064.22 214.76 o -1 4 1 707.78 772.59 20.46 o 0 4 1 2796.68 2557.48 67.00 o 1 4 1 0.46 1.36 0.32 o 2 4 1 2538.49 2505.60 91.68 o 3 4 1 30.46 33.55 2.33 o 4 4 1 200.78 169.48 2.73 o 5 4 1 0.36 2.16 0.82 o 6 4 1 86.76 89.08 3.30 o 7 4 1 14.92 14.88 1.37 o 8 4 1 107.02 124.83 4.01 o -8 5 1 23.10 25.65 1.60 o -7 5 1 3.25 2.78 1.10 o -6 5 1 229.91 232.95 4.18 o -5 5 1 31.81 27.80 1.25 o -4 5 1 220.62 192.26 6.03 o -3 5 1 1617.15 1560.55 15.39 o -2 5 1 1134.20 1192.35 48.57 o -1 5 1 146.67 185.30 2.77 o 0 5 1 49.19 55.00 2.21 o 1 5 1 403.91 502.02 16.48 o 2 5 1 1415.91 1415.23 9.19 o 3 5 1 25.36 20.87 2.03 o 4 5 1 141.44 128.67 2.01 o 5 5 1 1162.68 1150.69 14.98 o 6 5 1 154.38 160.95 4.01 o 7 5 1 211.90 244.03 6.69 o 8 5 1 32.95 35.33 2.25 o -8 6 1 3.83 2.49 1.58 o -7 6 1 15.18 23.32 1.53 o -6 6 1 13.79 14.75 1.25 o -5 6 1 0.82 1.06 0.91 o -4 6 1 0.45 0.84 0.74 o -3 6 1 48.50 33.40 1.72 o -2 6 1 3127.64 3178.77 18.54 o -1 6 1 0.70 0.59 0.45 o 0 6 1 31.68 19.95 0.93 o 1 6 1 574.41 603.68 8.48 o 2 6 1 134.60 148.82 3.36 o 3 6 1 1.26 2.25 0.60 o 4 6 1 42.25 40.90 1.30 o 5 6 1 422.16 440.34 8.90 o 6 6 1 46.99 46.80 2.54 o 7 6 1 9.36 9.46 1.85 o 8 6 1 16.39 12.76 2.10 o -8 7 1 45.07 44.14 2.40 o -6 7 1 79.33 64.13 2.05 o -5 7 1 0.63 1.71 0.97 o -4 7 1 0.69 2.10 0.88 o -3 7 1 52.78 48.26 5.29 o -2 7 1 292.66 263.88 19.52 o -1 7 1 661.48 680.33 8.71 o 0 7 1 117.73 103.46 3.34 o 1 7 1 504.12 489.51 8.41 o 2 7 1 78.20 73.48 3.64 o 3 7 1 9.98 7.69 0.98 o 4 7 1 13.30 14.56 1.05 o 5 7 1 104.60 108.07 3.41 o 6 7 1 2.78 3.98 2.55 o 7 7 1 29.68 32.05 3.68 o 8 7 1 0.27 0.30 1.95 o -8 8 1 178.97 149.98 3.75 o -7 8 1 8.48 8.93 1.73 o -6 8 1 108.45 110.64 7.21 o -5 8 1 187.66 154.63 7.39 o -4 8 1 35.77 35.66 1.80 o -3 8 1 140.25 112.81 6.08 o -2 8 1 3.24 3.09 0.83 o -1 8 1 0.52 0.20 0.79 o 0 8 1 13.76 10.46 0.76 o 1 8 1 4.38 6.03 0.61 o 2 8 1 72.58 67.05 2.14 o 3 8 1 67.19 70.00 2.29 o 4 8 1 10.66 14.81 2.50 o 5 8 1 68.30 62.91 4.65 o 6 8 1 216.98 233.68 8.48 o 7 8 1 33.59 32.95 3.23 o -7 9 1 0.54 0.73 0.93 o -6 9 1 108.61 116.28 3.00 o -5 9 1 0.80 3.40 2.55 o -4 9 1 31.81 26.43 1.56 o -3 9 1 54.46 54.77 2.75 o -2 9 1 39.05 32.20 1.93 o -1 9 1 22.04 19.43 1.30 o 0 9 1 182.76 154.01 8.04 o 1 9 1 30.94 27.88 2.14 o 2 9 1 40.97 49.80 2.93 o 3 9 1 304.64 325.55 4.40 o 4 9 1 193.70 186.07 8.29 o 5 9 1 201.59 225.72 8.26 o 6 9 1 15.95 17.14 1.78 o 7 9 1 1.12 0.11 0.83 o -7 10 1 88.79 78.03 7.88 o -6 10 1 37.67 43.91 2.15 o -5 10 1 45.96 59.27 3.41 o -4 10 1 0.97 2.01 1.32 o -3 10 1 65.10 77.37 4.52 o -2 10 1 131.21 145.08 3.57 o -1 10 1 1650.20 1645.94 13.53 o 0 10 1 440.08 449.12 6.88 o 1 10 1 133.24 142.51 2.97 o 2 10 1 385.38 409.45 7.16 o 3 10 1 36.54 30.19 1.91 o 4 10 1 75.48 74.38 2.75 o 5 10 1 65.08 66.98 3.07 o 6 10 1 0.73 1.17 0.98 o -6 11 1 3.94 3.51 1.00 o -5 11 1 1.69 3.87 1.24 o -4 11 1 1.53 0.60 1.20 o -3 11 1 195.11 243.89 7.29 o -2 11 1 142.73 156.53 3.70 o -1 11 1 116.08 113.97 3.72 o 0 11 1 136.05 141.90 3.21 o 1 11 1 174.33 192.50 3.71 o 2 11 1 0.01 0.15 1.38 o 3 11 1 138.08 125.40 5.29 o 4 11 1 18.44 12.12 1.18 o 5 11 1 16.61 16.98 1.79 o 6 11 1 2.78 1.88 1.43 o -5 12 1 1.04 1.00 1.06 o -4 12 1 17.48 15.97 1.34 o -3 12 1 12.18 15.32 1.14 o -2 12 1 5.52 8.16 1.36 o -1 12 1 748.87 741.05 8.78 o 0 12 1 89.64 87.48 3.41 o 1 12 1 0.30 0.41 1.17 o 2 12 1 0.16 2.93 1.08 o 3 12 1 0.50 2.96 1.09 o 4 12 1 1.58 3.72 1.11 o 5 12 1 16.69 17.87 2.03 o -4 13 1 21.29 25.90 2.03 o -3 13 1 3.08 1.08 1.21 o -2 13 1 94.16 110.30 5.07 o -1 13 1 8.93 9.68 1.38 o 0 13 1 80.09 83.96 5.07 o 1 13 1 150.63 172.44 4.28 o 2 13 1 0.00 0.48 0.96 o 3 13 1 291.97 374.17 15.46 o 4 13 1 197.27 211.39 5.55 o -3 14 1 130.57 92.41 3.68 o -2 14 1 127.77 125.51 4.73 o -1 14 1 7.91 11.11 1.95 o 0 14 1 0.28 -0.54 1.09 o 1 14 1 63.07 67.93 4.35 o 2 14 1 576.32 612.73 22.67 o 3 14 1 282.60 250.07 18.20 o -1 15 1 19.82 7.51 1.43 o 0 15 1 0.22 1.88 1.43 o 1 15 1 43.83 44.21 2.55 o -9 0 2 105.39 105.34 4.88 o -8 0 2 6.10 4.71 1.60 o -7 0 2 78.86 88.53 4.24 o -6 0 2 36.96 35.08 1.98 o -5 0 2 11.97 12.00 1.28 o -4 0 2 39.34 40.84 2.25 o -3 0 2 223.33 217.99 4.28 o 0 0 2 154.73 186.09 2.78 o 1 0 2 73.04 72.42 1.14 o 2 0 2 3068.07 3207.42 145.14 o 3 0 2 2322.53 2592.84 10.33 o 4 0 2 114.29 91.28 3.68 o 5 0 2 949.94 838.24 21.32 o 6 0 2 44.61 35.78 2.53 o 7 0 2 297.04 336.02 8.12 o 8 0 2 215.64 236.61 5.71 o 9 0 2 193.06 213.86 6.01 o -9 1 2 14.16 13.19 1.06 o -8 1 2 207.04 243.90 4.34 o -7 1 2 31.86 35.91 1.76 o -6 1 2 24.31 25.52 1.38 o -5 1 2 18.48 18.27 1.24 o -4 1 2 5.28 2.75 0.64 o -3 1 2 1186.07 1269.65 12.12 o -2 1 2 2870.36 2891.17 12.23 o -1 1 2 126.00 147.20 1.69 o 0 1 2 526.97 524.03 2.10 o 2 1 2 168.60 149.88 2.52 o 3 1 2 6705.14 7322.11 180.27 o 4 1 2 153.58 144.34 3.26 o 5 1 2 510.77 456.01 6.02 o 6 1 2 279.15 301.95 4.53 o 7 1 2 776.88 877.01 10.41 o 8 1 2 62.81 64.13 2.59 o 9 1 2 122.43 114.93 4.43 o -9 2 2 65.41 59.88 5.11 o -8 2 2 31.62 32.08 1.53 o -7 2 2 134.17 149.77 3.26 o -6 2 2 492.96 534.96 7.58 o -5 2 2 85.77 83.01 2.08 o -4 2 2 640.45 657.59 6.51 o -3 2 2 2.92 0.91 0.33 o -2 2 2 463.55 451.89 3.19 o -1 2 2 1040.27 1105.96 14.32 o 0 2 2 1960.60 1990.37 24.39 o 1 2 2 2296.00 2398.90 8.84 o 2 2 2 2516.93 2561.94 16.89 o 3 2 2 87.26 94.66 3.30 o 4 2 2 586.09 518.05 6.05 o 5 2 2 671.70 647.54 8.05 o 6 2 2 246.21 267.83 5.01 o 7 2 2 297.55 316.40 8.04 o 8 2 2 0.80 -0.18 1.19 o -9 3 2 64.89 68.52 2.39 o -8 3 2 0.01 0.75 0.85 o -7 3 2 879.80 1015.05 8.94 o -6 3 2 138.08 150.20 3.13 o -5 3 2 439.59 427.36 6.63 o -4 3 2 106.88 109.57 2.78 o -3 3 2 97.08 106.37 3.53 o -2 3 2 97.50 87.44 1.94 o -1 3 2 290.14 256.54 2.58 o 0 3 2 25.83 43.19 1.55 o 1 3 2 1394.88 1469.33 19.68 o 2 3 2 517.13 532.72 7.09 o 3 3 2 1841.61 1916.37 15.69 o 4 3 2 133.73 108.16 1.99 o 5 3 2 927.95 904.21 17.22 o 6 3 2 279.17 313.60 6.15 o 7 3 2 5.40 5.33 1.16 o 8 3 2 13.07 12.07 1.70 o -9 4 2 80.56 65.76 3.23 o -8 4 2 8.60 7.83 0.89 o -7 4 2 263.71 290.92 4.20 o -6 4 2 130.82 139.94 3.38 o -5 4 2 0.01 1.06 0.94 o -4 4 2 277.91 233.99 6.42 o -3 4 2 150.36 156.66 4.58 o -2 4 2 885.43 942.76 10.06 o -1 4 2 206.31 232.05 6.50 o 0 4 2 2518.14 2675.05 109.52 o 1 4 2 48.29 66.18 1.41 o 2 4 2 16.51 18.33 1.11 o 3 4 2 4.22 5.40 1.13 o 4 4 2 975.11 905.38 5.30 o 5 4 2 827.22 819.61 7.00 o 6 4 2 534.28 585.50 6.06 o 7 4 2 102.07 115.23 3.71 o 8 4 2 0.09 -0.26 1.27 o -8 5 2 5.09 5.61 0.84 o -7 5 2 179.14 186.48 3.65 o -6 5 2 1.62 1.51 1.04 o -5 5 2 7.56 8.54 0.97 o -4 5 2 484.07 444.10 7.06 o -3 5 2 6.15 6.01 1.20 o -2 5 2 482.79 513.30 8.33 o -1 5 2 278.75 327.99 5.03 o 0 5 2 784.26 870.28 26.01 o 1 5 2 477.22 565.73 19.48 o 2 5 2 11.73 6.41 0.87 o 3 5 2 269.98 221.78 2.75 o 4 5 2 737.14 655.63 4.01 o 5 5 2 2.93 4.07 0.80 o 6 5 2 401.85 450.83 7.07 o 7 5 2 30.57 37.88 2.36 o 8 5 2 24.53 28.38 2.85 o -8 6 2 8.32 8.26 1.43 o -7 6 2 45.45 38.65 1.78 o -6 6 2 86.60 98.79 3.69 o -5 6 2 2.06 1.97 0.89 o -4 6 2 166.39 151.19 3.30 o -3 6 2 1538.88 1156.40 13.66 o -2 6 2 465.74 487.10 13.47 o -1 6 2 131.40 144.21 2.61 o 0 6 2 25.66 22.27 1.03 o 1 6 2 1378.39 1462.97 14.04 o 2 6 2 51.24 53.97 1.73 o 3 6 2 10.87 8.68 1.37 o 4 6 2 3.61 3.83 0.66 o 5 6 2 83.78 81.99 3.23 o 6 6 2 0.08 0.57 1.43 o 7 6 2 27.50 30.46 2.39 o 8 6 2 0.90 2.78 1.88 o -8 7 2 2.96 2.30 0.90 o -7 7 2 52.65 54.82 2.86 o -6 7 2 589.25 586.49 11.45 o -5 7 2 7.92 4.56 1.03 o -4 7 2 242.66 224.45 5.77 o -3 7 2 356.54 315.74 5.36 o -2 7 2 368.71 334.66 20.04 o -1 7 2 20.83 19.29 1.73 o 0 7 2 257.31 195.40 8.78 o 1 7 2 1371.15 1215.58 36.90 o 2 7 2 1.18 0.81 0.87 o 3 7 2 144.89 159.13 3.90 o 4 7 2 136.51 135.46 2.91 o 5 7 2 1361.75 1372.94 14.64 o 6 7 2 58.39 60.85 3.37 o 7 7 2 45.29 47.74 3.83 o -8 8 2 140.16 108.25 3.23 o -7 8 2 145.13 152.18 3.71 o -6 8 2 9.48 12.73 1.43 o -5 8 2 37.65 55.94 7.51 o -4 8 2 235.73 234.11 16.29 o -3 8 2 727.39 702.23 32.92 o -2 8 2 518.14 479.43 17.30 o -1 8 2 13.73 14.42 1.06 o 0 8 2 1674.76 1459.19 19.25 o 1 8 2 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