#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:21:09 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180853 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/84/2018442.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018442_Fobs loop_ _publ_author_name 'Szczesio, Ma\/lgorzata' 'Olczak, Andrzej' 'Gobis, Katarzyna' 'Foks, Henryk' 'G\/l\'owka, Marek L.' _publ_section_title ; Planarity of heteroaryldithiocarbazic acid derivatives showing tuberculostatic activity. IV. Diesters of benzoylcarbonohydrazonodithioic acid ; _journal_coeditor_code WQ3009 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o99 _journal_page_last o103 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.415 _cell_angle_gamma 90.000 _cell_length_a 13.3680 _cell_length_b 8.1817 _cell_length_c 13.5158 _exptl_crystal_F_000 656.00 _reflns_d_resolution_high 0.8216 _cod_data_source_file wq3009D4sup5.hkl _cod_data_source_block D4 #BEGIN Tags that were not found in dictionaries: _shelx_title ' cm27_0m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 153.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 25.59 26.62 1.37 o 2 0 0 262.30 315.82 11.50 o 3 0 0 18615.98 18813.77 646.65 o 4 0 0 1.67 0.48 0.28 o 5 0 0 450.26 464.18 13.66 o 6 0 0 2495.71 2811.78 60.70 o 7 0 0 133.35 183.47 3.44 o 8 0 0 1481.46 1429.75 27.62 o 9 0 0 2.75 2.02 0.23 o 10 0 0 116.02 122.95 2.91 o 11 0 0 734.73 732.03 12.82 o 12 0 0 871.13 904.18 23.29 o 13 0 0 67.21 89.91 3.07 o 14 0 0 10.94 19.00 1.45 o 15 0 0 191.53 207.41 6.83 o 1 1 0 1160.52 1168.16 45.17 o 2 1 0 180.07 166.91 4.00 o 3 1 0 3246.27 3541.63 73.06 o 4 1 0 9111.08 9195.96 193.01 o 5 1 0 116.67 96.55 2.32 o 6 1 0 374.15 409.62 5.77 o 7 1 0 51.14 51.34 0.87 o 8 1 0 48.93 48.60 0.87 o 9 1 0 62.47 60.95 1.15 o 10 1 0 48.44 51.09 1.26 o 11 1 0 388.69 411.18 6.04 o 12 1 0 52.15 58.58 1.16 o 13 1 0 240.26 246.43 4.78 o 14 1 0 13.34 12.84 0.45 o 15 1 0 10.55 9.72 0.36 o 0 2 0 152.87 121.38 7.71 o 1 2 0 9831.95 9809.33 365.32 o 2 2 0 1334.62 1400.87 50.88 o 3 2 0 11.35 3.77 0.34 o 4 2 0 6935.53 7121.03 160.22 o 5 2 0 1170.01 1278.35 18.79 o 6 2 0 620.62 648.16 7.88 o 7 2 0 665.33 645.46 8.91 o 8 2 0 2.45 2.65 0.26 o 9 2 0 191.70 178.80 3.44 o 10 2 0 368.59 370.97 9.91 o 11 2 0 333.43 320.53 5.28 o 12 2 0 276.10 285.53 4.62 o 13 2 0 35.39 43.46 1.07 o 14 2 0 22.84 22.79 0.62 o 15 2 0 12.22 11.34 0.32 o 1 3 0 7924.67 7882.20 318.29 o 2 3 0 127.25 90.99 2.47 o 3 3 0 917.11 960.09 21.73 o 4 3 0 308.73 314.29 3.99 o 5 3 0 1397.47 1421.59 17.04 o 6 3 0 161.21 160.90 2.13 o 7 3 0 2558.78 2524.22 32.22 o 8 3 0 426.80 428.95 6.24 o 9 3 0 392.88 372.81 7.08 o 10 3 0 896.06 892.79 14.84 o 11 3 0 9.36 10.23 0.36 o 12 3 0 26.58 33.95 0.87 o 13 3 0 0.27 0.79 0.20 o 14 3 0 7.65 10.87 0.35 o 0 4 0 919.43 1061.05 36.63 o 1 4 0 4288.56 4400.36 86.79 o 2 4 0 490.34 404.89 5.57 o 3 4 0 45.25 65.07 1.00 o 4 4 0 271.20 255.13 3.55 o 5 4 0 7.26 13.87 0.37 o 6 4 0 869.82 835.12 10.76 o 7 4 0 599.70 659.78 9.23 o 8 4 0 231.56 199.15 2.95 o 9 4 0 723.45 673.55 7.77 o 10 4 0 5.47 3.85 0.21 o 11 4 0 73.58 76.28 1.49 o 12 4 0 0.01 -0.13 0.14 o 13 4 0 2.01 2.27 0.20 o 14 4 0 77.40 67.18 1.34 o 1 5 0 684.31 668.62 8.64 o 2 5 0 866.02 872.46 11.18 o 3 5 0 2449.09 2376.49 32.40 o 4 5 0 30.00 26.03 0.58 o 5 5 0 1084.06 1132.15 18.20 o 6 5 0 505.72 525.29 8.60 o 7 5 0 8.51 7.72 0.40 o 8 5 0 5.44 5.67 0.18 o 9 5 0 21.39 14.94 0.33 o 10 5 0 17.36 14.44 0.36 o 11 5 0 275.77 256.29 4.64 o 12 5 0 74.07 62.53 1.67 o 13 5 0 0.89 0.57 0.15 o 0 6 0 12.38 10.07 0.64 o 1 6 0 38.66 34.32 0.76 o 2 6 0 1515.94 1607.62 23.84 o 3 6 0 57.00 62.75 1.26 o 4 6 0 147.21 135.67 3.06 o 5 6 0 79.66 86.44 1.65 o 6 6 0 17.08 18.06 0.33 o 7 6 0 33.89 31.43 0.46 o 8 6 0 239.75 226.01 2.44 o 9 6 0 24.52 33.22 0.55 o 10 6 0 281.09 245.95 3.98 o 11 6 0 28.55 29.98 0.56 o 12 6 0 0.91 0.26 0.12 o 1 7 0 448.40 445.58 4.92 o 2 7 0 699.33 706.46 7.31 o 3 7 0 73.35 67.14 0.81 o 4 7 0 4.52 3.28 0.16 o 5 7 0 20.05 18.30 0.34 o 6 7 0 7.83 6.61 0.23 o 7 7 0 152.45 155.81 2.12 o 8 7 0 20.83 19.53 0.43 o 9 7 0 63.24 61.20 0.89 o 10 7 0 8.45 14.31 0.36 o 0 8 0 556.09 540.54 9.19 o 1 8 0 11.23 6.16 0.28 o 2 8 0 342.15 348.95 4.19 o 3 8 0 2.51 3.11 0.21 o 4 8 0 165.94 171.13 2.31 o 5 8 0 20.48 27.18 0.50 o 6 8 0 54.87 54.46 0.85 o 7 8 0 0.31 0.41 0.11 o 8 8 0 20.82 17.61 0.32 o 9 8 0 0.60 0.06 0.10 o 1 9 0 1.58 2.70 0.20 o 2 9 0 1.85 1.28 0.24 o 3 9 0 144.65 153.73 2.82 o 4 9 0 22.93 21.87 0.46 o 5 9 0 23.46 26.56 0.47 o 6 9 0 29.60 29.84 0.55 o -15 1 1 3.11 4.26 0.28 o -14 1 1 104.80 112.00 2.20 o -13 1 1 45.79 47.27 0.96 o -12 1 1 0.55 1.16 0.22 o -11 1 1 7.15 6.63 0.23 o -10 1 1 335.89 358.60 5.95 o -9 1 1 9.27 10.58 0.65 o -8 1 1 1052.44 1123.32 14.97 o -7 1 1 211.18 234.17 3.07 o -6 1 1 6282.75 6662.54 88.67 o -5 1 1 130.81 144.30 3.36 o -4 1 1 2100.88 2032.74 41.76 o -3 1 1 10809.80 9965.68 504.35 o -2 1 1 3448.15 3151.99 129.02 o -1 1 1 3092.75 2762.82 184.61 o 0 1 1 1154.55 1128.96 43.99 o 1 1 1 11635.68 11400.63 322.51 o 2 1 1 3651.24 3777.19 78.10 o 3 1 1 4300.77 4425.31 91.70 o 4 1 1 22.23 28.35 0.74 o 5 1 1 3686.19 3906.36 82.03 o 6 1 1 2.54 3.56 0.17 o 7 1 1 381.50 406.61 5.80 o 8 1 1 7.53 6.99 0.35 o 9 1 1 6.26 3.83 0.39 o 10 1 1 62.81 65.80 2.36 o 11 1 1 40.39 40.42 0.90 o 12 1 1 0.02 0.09 0.17 o 13 1 1 111.32 113.37 2.32 o 14 1 1 3.33 3.07 0.20 o 15 1 1 63.74 68.00 2.39 o -15 2 1 1.73 1.63 0.14 o -14 2 1 1.51 1.97 0.20 o -13 2 1 180.58 206.96 4.06 o -12 2 1 98.27 103.59 1.66 o -11 2 1 255.33 257.56 3.49 o -10 2 1 1903.93 1945.56 34.55 o -9 2 1 5.43 7.12 0.44 o -8 2 1 0.79 0.87 0.15 o -7 2 1 353.74 265.28 3.57 o -6 2 1 3334.25 3593.83 42.20 o -5 2 1 707.09 770.19 13.99 o -4 2 1 110.70 110.82 4.03 o -3 2 1 32.70 45.58 1.14 o -2 2 1 814.19 789.71 17.95 o -1 2 1 21194.71 20769.74 1047.40 o 0 2 1 23513.08 24622.38 1166.58 o 1 2 1 2570.09 2453.24 81.89 o 2 2 1 2218.12 2364.35 48.63 o 3 2 1 219.51 206.62 4.33 o 4 2 1 10.76 19.34 0.67 o 5 2 1 85.62 78.17 1.12 o 6 2 1 938.55 1127.26 14.04 o 7 2 1 422.30 395.31 6.65 o 8 2 1 58.46 53.20 1.18 o 9 2 1 226.79 258.68 12.93 o 10 2 1 27.94 26.25 0.65 o 11 2 1 350.43 374.84 5.99 o 12 2 1 0.25 0.85 0.68 o 13 2 1 61.75 60.33 1.37 o 14 2 1 14.58 11.47 0.39 o 15 2 1 4.50 2.04 0.17 o -15 3 1 0.95 0.87 0.10 o -14 3 1 1.71 1.48 0.20 o -13 3 1 5.16 6.68 0.35 o -12 3 1 167.09 160.49 4.11 o -11 3 1 0.31 0.85 0.22 o -10 3 1 102.07 98.67 1.57 o -9 3 1 1070.62 1050.17 16.94 o -8 3 1 199.89 198.08 3.05 o -7 3 1 1391.31 1491.31 19.06 o -6 3 1 1626.84 1610.83 19.89 o -5 3 1 8.56 6.72 0.22 o -4 3 1 1310.99 1384.66 18.05 o -3 3 1 148.98 158.60 3.75 o -2 3 1 408.16 336.93 8.71 o -1 3 1 3764.78 3768.11 112.27 o 0 3 1 2763.59 2782.66 84.23 o 1 3 1 122.08 98.45 3.53 o 2 3 1 344.11 289.64 6.66 o 3 3 1 1034.72 1022.75 15.27 o 4 3 1 1771.52 1786.66 21.72 o 5 3 1 34.96 35.01 0.56 o 6 3 1 2250.44 2199.92 27.16 o 7 3 1 97.16 93.89 1.47 o 8 3 1 263.58 265.82 4.65 o 9 3 1 20.88 21.65 0.81 o 10 3 1 9.80 5.84 0.27 o 11 3 1 37.05 41.21 0.90 o 12 3 1 18.84 21.02 0.67 o 13 3 1 13.60 13.70 0.45 o 14 3 1 72.15 65.80 1.37 o -14 4 1 113.13 100.78 1.99 o -13 4 1 9.12 6.71 0.32 o -12 4 1 10.72 12.84 0.47 o -11 4 1 162.39 149.93 1.75 o -10 4 1 0.53 0.74 0.13 o -9 4 1 62.89 70.92 1.05 o -8 4 1 1.62 2.38 0.22 o -7 4 1 88.96 93.72 1.48 o -6 4 1 180.18 155.11 2.28 o -5 4 1 491.70 471.21 6.89 o -4 4 1 0.53 0.24 0.13 o -3 4 1 703.30 690.63 9.37 o -2 4 1 49.08 44.00 0.73 o -1 4 1 1049.47 1029.59 13.52 o 0 4 1 674.73 635.88 8.02 o 1 4 1 123.79 130.00 1.97 o 2 4 1 2214.71 2167.31 30.98 o 3 4 1 858.13 828.25 11.23 o 4 4 1 1394.91 1411.47 18.49 o 5 4 1 89.79 110.64 1.57 o 6 4 1 65.93 64.04 1.10 o 7 4 1 167.24 151.11 2.52 o 8 4 1 272.52 264.74 4.26 o 9 4 1 123.07 115.42 1.52 o 10 4 1 4.40 1.91 0.19 o 11 4 1 7.46 7.71 0.54 o 12 4 1 132.09 126.97 2.55 o 13 4 1 7.49 4.18 0.25 o 14 4 1 0.67 0.34 0.17 o -13 5 1 54.27 47.58 1.26 o -12 5 1 21.73 13.75 0.42 o -11 5 1 3.48 2.16 0.23 o -10 5 1 229.96 213.07 2.29 o -9 5 1 98.24 84.26 0.95 o -8 5 1 428.62 410.97 4.00 o -7 5 1 143.01 151.20 2.67 o -6 5 1 12.20 14.02 0.54 o -5 5 1 218.49 219.59 4.10 o -4 5 1 572.36 583.24 8.82 o -3 5 1 485.21 489.13 6.70 o -2 5 1 40.53 44.01 0.78 o -1 5 1 402.20 403.52 5.12 o 0 5 1 77.80 81.81 1.14 o 1 5 1 1012.27 1077.63 14.36 o 2 5 1 75.64 82.12 1.21 o 3 5 1 122.73 115.30 1.79 o 4 5 1 265.22 274.01 4.31 o 5 5 1 24.18 28.05 0.70 o 6 5 1 14.54 18.57 0.65 o 7 5 1 25.57 26.82 0.61 o 8 5 1 36.26 35.68 0.57 o 9 5 1 67.98 71.16 0.93 o 10 5 1 0.75 1.14 0.18 o 11 5 1 53.87 58.08 1.30 o 12 5 1 3.87 2.25 0.20 o 13 5 1 34.05 32.20 1.36 o -12 6 1 0.40 0.23 0.10 o -11 6 1 92.86 87.88 1.11 o -10 6 1 30.17 41.10 0.66 o -9 6 1 70.64 77.27 1.11 o -8 6 1 77.78 77.32 0.89 o -7 6 1 495.93 502.34 5.31 o -6 6 1 169.60 171.18 1.82 o -5 6 1 36.84 36.16 0.92 o -4 6 1 257.11 272.70 4.61 o -3 6 1 144.31 148.21 2.62 o -2 6 1 127.83 151.29 2.48 o -1 6 1 2099.63 2212.51 35.69 o 0 6 1 0.22 0.88 0.21 o 1 6 1 3.01 8.55 0.40 o 2 6 1 280.22 281.57 4.38 o 3 6 1 668.50 663.88 10.00 o 4 6 1 249.66 247.30 4.22 o 5 6 1 0.35 0.30 0.11 o 6 6 1 448.44 449.18 4.55 o 7 6 1 227.40 233.20 2.78 o 8 6 1 42.80 38.20 0.74 o 9 6 1 160.81 181.13 3.01 o 10 6 1 69.27 69.97 1.23 o 11 6 1 6.76 6.36 0.29 o -11 7 1 0.15 0.23 0.11 o -10 7 1 0.02 0.33 0.09 o -9 7 1 17.05 17.40 0.39 o -8 7 1 1.41 1.02 0.31 o -7 7 1 28.23 25.02 0.48 o -6 7 1 0.15 0.61 0.16 o -5 7 1 1.67 2.00 0.20 o -4 7 1 87.57 93.54 1.08 o -3 7 1 0.29 0.09 0.13 o -2 7 1 0.05 -0.07 0.18 o -1 7 1 193.55 191.73 2.21 o 0 7 1 18.87 13.82 0.36 o 1 7 1 85.49 78.21 0.98 o 2 7 1 0.04 0.49 0.17 o 3 7 1 0.18 -0.07 0.10 o 4 7 1 58.75 55.70 0.75 o 5 7 1 19.05 20.69 0.38 o 6 7 1 2.79 3.10 0.17 o 7 7 1 60.96 62.79 0.88 o 8 7 1 7.93 6.94 0.32 o 9 7 1 9.68 13.41 0.38 o 10 7 1 1.51 1.60 0.13 o -9 8 1 8.83 8.29 0.23 o -8 8 1 4.88 2.48 0.15 o -7 8 1 12.86 13.89 0.32 o -6 8 1 119.99 115.49 1.59 o -5 8 1 140.65 157.96 2.15 o -4 8 1 27.67 23.29 0.45 o -3 8 1 24.68 25.26 0.62 o -2 8 1 181.69 182.73 2.61 o -1 8 1 25.78 29.05 0.74 o 0 8 1 33.60 26.25 0.54 o 1 8 1 30.64 30.78 0.55 o 2 8 1 62.67 73.42 1.29 o 3 8 1 231.30 242.33 3.52 o 4 8 1 111.90 103.11 1.46 o 5 8 1 13.24 16.13 0.37 o 6 8 1 89.73 99.09 1.37 o 7 8 1 34.73 32.71 0.69 o 8 8 1 6.57 6.99 0.26 o 9 8 1 0.52 0.51 0.12 o -6 9 1 68.29 63.63 0.99 o -5 9 1 62.54 61.53 0.88 o -4 9 1 5.76 3.37 0.20 o -3 9 1 11.88 10.12 0.37 o -2 9 1 0.18 0.47 0.17 o -1 9 1 96.21 81.47 2.09 o 0 9 1 113.91 112.00 3.25 o 1 9 1 6.46 4.88 0.29 o 2 9 1 50.50 44.72 0.85 o 3 9 1 11.01 11.01 0.36 o 4 9 1 0.39 0.46 0.12 o 5 9 1 8.16 10.37 0.35 o 6 9 1 14.25 15.67 0.85 o -15 0 2 0.31 0.43 0.12 o -14 0 2 169.51 202.80 4.70 o -13 0 2 150.11 122.67 2.72 o -12 0 2 264.55 239.92 3.60 o -11 0 2 174.79 188.53 4.98 o -10 0 2 2136.22 2195.96 46.18 o -9 0 2 61.31 60.30 1.42 o -8 0 2 568.60 594.16 10.72 o -7 0 2 807.87 1073.52 17.40 o -6 0 2 78.28 63.38 1.48 o -5 0 2 436.81 371.34 13.82 o -4 0 2 4671.38 4089.75 205.70 o -3 0 2 4396.10 3844.88 336.99 o -2 0 2 7256.49 6579.13 340.93 o -1 0 2 3280.36 3074.63 90.19 o 0 0 2 228.87 248.94 7.30 o 1 0 2 2311.63 2601.17 94.70 o 2 0 2 6929.50 7179.27 258.43 o 3 0 2 647.10 562.18 33.95 o 4 0 2 265.27 205.62 6.35 o 5 0 2 1242.14 1362.22 37.22 o 6 0 2 116.88 104.69 2.14 o 7 0 2 4021.35 3884.08 87.22 o 8 0 2 3128.75 3373.52 92.36 o 9 0 2 1.03 2.01 0.41 o 10 0 2 564.97 575.51 16.23 o 11 0 2 39.51 38.79 1.00 o 12 0 2 0.72 0.68 0.24 o 13 0 2 33.38 29.13 1.36 o 14 0 2 2.22 1.53 0.34 o -15 1 2 70.80 72.25 1.41 o -14 1 2 9.05 9.50 0.39 o -13 1 2 409.33 408.35 4.24 o -12 1 2 0.38 0.22 0.10 o -11 1 2 1.62 1.98 0.18 o -10 1 2 606.77 618.18 10.05 o -9 1 2 878.14 895.89 12.03 o -8 1 2 1601.27 1702.78 21.38 o -7 1 2 615.04 601.98 7.71 o -6 1 2 4861.41 4881.24 61.94 o -5 1 2 6384.75 6613.26 190.12 o -4 1 2 806.71 734.37 21.15 o -3 1 2 1835.10 1956.74 51.79 o -2 1 2 2547.68 2400.51 56.01 o -1 1 2 4566.24 4204.91 159.49 o 0 1 2 5567.24 5571.49 125.66 o 1 1 2 292.06 286.03 6.05 o 2 1 2 2699.42 2653.78 54.76 o 3 1 2 10375.42 11152.01 252.73 o 4 1 2 299.24 407.59 9.37 o 5 1 2 166.12 138.53 2.64 o 6 1 2 4942.34 4963.56 69.77 o 7 1 2 714.59 736.95 12.19 o 8 1 2 50.61 51.11 1.61 o 9 1 2 26.23 28.62 1.31 o 10 1 2 1093.68 1124.75 19.47 o 11 1 2 38.37 41.20 0.90 o 12 1 2 64.79 66.58 1.23 o 13 1 2 19.31 19.27 0.59 o 14 1 2 99.91 95.62 3.58 o -15 2 2 23.54 21.47 0.52 o -14 2 2 52.81 53.17 0.99 o -13 2 2 58.21 56.27 0.84 o -12 2 2 445.89 435.05 4.55 o -11 2 2 214.27 197.06 2.08 o -10 2 2 175.17 178.50 2.84 o -9 2 2 52.23 50.86 0.90 o -8 2 2 168.42 166.63 2.31 o -7 2 2 413.45 462.09 6.33 o -6 2 2 404.04 413.95 5.81 o -5 2 2 146.98 136.43 2.30 o -4 2 2 7344.44 7371.46 233.59 o -3 2 2 3812.54 3878.18 79.91 o -2 2 2 175.84 172.71 3.68 o -1 2 2 384.01 388.46 8.82 o 0 2 2 1654.14 1592.83 38.46 o 1 2 2 1392.97 1342.93 30.03 o 2 2 2 3243.84 3233.43 66.81 o 3 2 2 927.59 899.35 20.48 o 4 2 2 586.13 595.22 14.36 o 5 2 2 723.85 698.87 9.01 o 6 2 2 83.73 112.61 1.81 o 7 2 2 1041.71 1063.85 22.05 o 8 2 2 74.66 60.06 1.69 o 9 2 2 9.21 11.71 0.64 o 10 2 2 106.59 111.44 1.96 o 11 2 2 190.61 184.45 3.09 o 12 2 2 16.59 16.91 0.57 o 13 2 2 177.08 175.93 3.46 o 14 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o -8 4 2 684.25 669.04 10.92 o -7 4 2 1482.97 1603.88 24.47 o -6 4 2 24.82 21.08 0.53 o -5 4 2 256.38 249.47 3.41 o -4 4 2 143.13 163.59 2.29 o -3 4 2 222.18 218.05 3.07 o -2 4 2 1358.56 1454.57 18.51 o -1 4 2 829.67 931.40 12.05 o 0 4 2 4141.80 4025.97 51.83 o 1 4 2 305.62 303.75 5.34 o 2 4 2 1738.00 1669.55 21.93 o 3 4 2 1380.18 1427.31 19.20 o 4 4 2 157.91 152.47 2.20 o 5 4 2 1441.23 1539.19 20.22 o 6 4 2 519.24 510.19 7.26 o 7 4 2 92.87 90.57 1.79 o 8 4 2 86.71 108.24 1.70 o 9 4 2 1016.49 1078.41 14.40 o 10 4 2 21.56 17.84 0.48 o 11 4 2 18.70 18.88 0.53 o 12 4 2 15.42 10.60 0.36 o 13 4 2 24.58 26.19 0.62 o -13 5 2 102.16 103.87 2.05 o -12 5 2 20.09 24.60 0.49 o -11 5 2 450.61 425.01 6.24 o -10 5 2 61.58 68.45 1.05 o -9 5 2 1.79 1.09 0.13 o -8 5 2 130.03 115.40 1.42 o -7 5 2 475.75 480.60 7.33 o -6 5 2 740.64 777.80 12.54 o -5 5 2 281.08 254.65 5.55 o -4 5 2 730.34 738.02 10.31 o -3 5 2 450.39 438.94 6.25 o -2 5 2 40.70 35.15 0.61 o -1 5 2 63.15 56.25 0.89 o 0 5 2 721.53 717.37 8.80 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