#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/84/2018451.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018451_Fobs loop_ _publ_author_name 'Pourayoubi, Mehrdad' 'Tarahhomi, Atekeh' 'Karimi Ahmadabad, Fatemeh' 'Fejfarov\'a, Karla' 'van der Lee, Arie' 'Du\XP(O)[NHC(CH~3~)~3~]~2~ phosphoramidates, with X = (CH~3~)~2~N and [(CH~3~)~3~CNH]~2~P(O)(O) ; _journal_coeditor_code FA3268 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o164 _journal_page_last o169 _journal_volume 68 _journal_year 2012 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _audit_creation_date 12-01-24 _audit_creation_method CRYSTALS _cell_angle_alpha 90 _cell_angle_beta 90.529(3) _cell_angle_gamma 90 _cell_length_a 12.0615(4) _cell_length_b 21.2567(7) _cell_length_c 17.1877(6) _[local]_cod_data_source_file fa3268Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 1 -19 0 166.00 205.80 23.22 o 2 -19 0 179.55 227.46 33.89 o 0 -18 0 2097.31 2116.97 90.43 o 1 -18 0 81.81 83.16 15.00 o 2 -18 0 614.28 595.47 34.67 o 3 -18 0 1018.02 966.05 60.53 o 4 -18 0 88.27 77.28 16.72 o 1 -17 0 356.90 378.15 21.23 o 2 -17 0 288.69 257.92 30.00 o 3 -17 0 290.17 305.24 31.55 o 4 -17 0 422.70 457.61 41.65 o 5 -17 0 56.86 67.31 15.11 o 6 -17 0 24.78 32.17 15.27 o 10 -17 0 57.93 32.35 54.93 o 11 -17 0 -6.11 33.51 29.96 o 0 -16 0 1324.61 1568.05 50.40 o 1 -16 0 271.89 333.54 15.68 o 2 -16 0 494.65 533.76 26.09 o 3 -16 0 218.27 235.16 19.01 o 4 -16 0 1507.84 1503.55 81.02 o 5 -16 0 4.85 14.03 11.12 o 6 -16 0 57.11 57.06 20.76 o 7 -16 0 210.48 266.28 28.91 o 9 -16 0 30.56 10.62 39.01 o 10 -16 0 136.31 94.42 58.38 o 11 -16 0 75.75 141.92 45.38 o 1 -15 0 222.66 212.13 14.71 o 2 -15 0 1423.13 1633.60 47.71 o 3 -15 0 787.80 805.96 35.60 o 4 -15 0 1299.39 1352.88 51.06 o 5 -15 0 3696.37 3311.92 150.98 o 6 -15 0 1229.78 1187.61 86.18 o 7 -15 0 801.42 888.27 58.04 o 8 -15 0 317.87 282.77 40.38 o 9 -15 0 76.67 76.35 24.41 o 10 -15 0 0.01 27.20 25.15 o 11 -15 0 114.09 48.64 54.71 o 0 -14 0 2390.16 2816.94 68.65 o 1 -14 0 852.66 880.22 27.27 o 2 -14 0 1033.13 1197.46 35.33 o 3 -14 0 871.88 849.05 36.23 o 4 -14 0 1546.44 1512.54 80.22 o 5 -14 0 140.16 141.20 28.40 o 6 -14 0 302.46 294.21 38.39 o 7 -14 0 345.40 327.82 39.07 o 8 -14 0 216.84 233.35 31.71 o 9 -14 0 360.81 393.10 43.09 o 10 -14 0 113.44 112.61 28.28 o 11 -14 0 291.94 318.57 42.58 o 1 -13 0 449.86 538.69 20.76 o 2 -13 0 2045.51 2407.89 52.64 o 3 -13 0 1381.64 1476.27 48.22 o 4 -13 0 977.91 1047.77 62.10 o 5 -13 0 630.64 654.46 57.35 o 6 -13 0 747.42 749.19 57.29 o 7 -13 0 140.84 101.07 30.88 o 8 -13 0 351.22 359.11 38.80 o 9 -13 0 34.93 10.19 22.71 o 10 -13 0 -16.10 2.46 20.54 o 11 -13 0 -15.98 14.21 19.55 o 12 -13 0 100.94 126.83 29.60 o 0 -12 0 2583.10 2818.69 69.42 o 1 -12 0 877.15 982.85 28.92 o 2 -12 0 849.03 1016.05 30.23 o 3 -12 0 708.78 691.19 46.40 o 4 -12 0 1661.56 1574.28 84.94 o 5 -12 0 734.10 641.04 47.17 o 6 -12 0 104.84 74.95 22.07 o 7 -12 0 317.32 322.28 36.48 o 8 -12 0 606.07 570.55 51.47 o 9 -12 0 32.62 66.44 25.35 o 10 -12 0 80.66 34.13 25.80 o 11 -12 0 126.22 117.37 29.62 o 12 -12 0 82.00 82.53 27.33 o 13 -12 0 8.97 37.35 18.74 o 1 -11 0 667.00 715.35 24.39 o 2 -11 0 103.21 99.21 10.90 o 3 -11 0 573.55 852.87 43.03 o 4 -11 0 82.35 94.84 17.37 o 5 -11 0 484.42 542.49 40.27 o 6 -11 0 1421.14 1395.59 71.99 o 7 -11 0 1287.22 1308.40 68.94 o 8 -11 0 317.49 270.24 39.35 o 9 -11 0 386.24 367.30 41.27 o 10 -11 0 891.71 773.77 67.34 o 11 -11 0 11.00 15.06 23.26 o 12 -11 0 39.68 41.58 23.82 o 13 -11 0 34.53 6.61 33.34 o 14 -11 0 9.02 59.95 21.68 o 0 -10 0 1717.75 1518.33 49.82 o 1 -10 0 2277.70 2467.09 49.71 o 2 -10 0 963.53 1019.60 30.85 o 3 -10 0 1900.43 2122.92 66.02 o 4 -10 0 272.89 315.51 25.95 o 5 -10 0 1137.37 1061.92 57.95 o 6 -10 0 518.61 484.75 43.36 o 7 -10 0 520.18 507.24 43.57 o 8 -10 0 2021.25 1808.36 89.55 o 9 -10 0 3.23 3.46 18.06 o 10 -10 0 -1.51 34.94 22.19 o 11 -10 0 1020.34 812.34 75.07 o 12 -10 0 22.53 9.20 23.31 o 13 -10 0 107.90 67.31 41.61 o 14 -10 0 27.74 63.76 25.66 o 15 -10 0 32.82 30.34 27.56 o 1 -9 0 20200.72 19964.28 278.69 o 2 -9 0 1523.90 1714.46 51.13 o 3 -9 0 516.23 476.88 27.51 o 4 -9 0 566.14 485.75 40.62 o 5 -9 0 29.31 38.56 14.27 o 6 -9 0 33.84 32.37 20.55 o 7 -9 0 74.79 63.96 24.07 o 8 -9 0 244.64 221.40 29.62 o 9 -9 0 895.13 812.71 63.58 o 10 -9 0 627.39 534.04 53.90 o 11 -9 0 123.80 118.06 31.64 o 12 -9 0 317.35 324.67 42.03 o 13 -9 0 59.14 61.59 29.03 o 14 -9 0 -40.08 13.58 29.58 o 15 -9 0 32.27 69.29 29.58 o 0 -8 0 3524.19 3616.23 75.04 o 1 -8 0 4865.54 4473.19 81.33 o 2 -8 0 4012.07 4024.21 93.60 o 3 -8 0 4633.74 4548.25 94.04 o 4 -8 0 2580.11 2324.72 83.02 o 5 -8 0 428.67 393.80 31.93 o 6 -8 0 65.39 103.93 23.65 o 7 -8 0 315.74 277.02 32.30 o 8 -8 0 813.20 744.70 54.79 o 9 -8 0 70.39 81.62 19.30 o 10 -8 0 414.33 382.13 46.51 o 11 -8 0 105.84 130.62 21.76 o 12 -8 0 42.26 7.19 25.34 o 13 -8 0 142.59 152.03 31.65 o 14 -8 0 0.01 23.51 19.05 o 15 -8 0 43.45 82.62 25.08 o 1 -7 0 1265.13 1265.04 30.39 o 2 -7 0 3133.51 3214.33 67.69 o 3 -7 0 4563.17 4219.82 91.20 o 4 -7 0 2911.89 2290.09 87.32 o 5 -7 0 1361.90 1233.47 59.99 o 6 -7 0 868.87 880.06 67.75 o 7 -7 0 680.80 648.84 45.22 o 8 -7 0 1432.56 1429.00 72.14 o 9 -7 0 499.06 428.20 46.30 o 10 -7 0 221.93 250.37 31.64 o 11 -7 0 75.58 86.56 23.78 o 12 -7 0 69.77 71.50 27.66 o 13 -7 0 50.54 29.49 22.75 o 14 -7 0 62.90 24.82 43.25 o 15 -7 0 -75.61 19.73 37.63 o 0 -6 0 4863.08 5026.38 129.65 o 1 -6 0 792.93 759.38 28.59 o 2 -6 0 904.23 799.74 30.55 o 3 -6 0 250.36 202.20 20.35 o 4 -6 0 1228.72 1271.05 51.39 o 5 -6 0 3547.68 2969.69 103.22 o 6 -6 0 40.21 44.65 17.03 o 7 -6 0 1288.71 1283.68 62.65 o 8 -6 0 1445.14 1457.66 72.06 o 9 -6 0 506.22 475.51 44.92 o 10 -6 0 691.94 733.41 54.97 o 11 -6 0 18.78 41.17 18.72 o 12 -6 0 60.44 20.23 27.18 o 13 -6 0 0.47 1.13 12.56 o 14 -6 0 33.76 58.45 35.92 o 15 -6 0 149.61 90.38 58.56 o 1 -5 0 21465.67 20929.86 351.56 o 2 -5 0 406.50 369.40 19.64 o 3 -5 0 445.23 518.86 21.42 o 4 -5 0 560.27 552.59 27.56 o 5 -5 0 721.88 607.26 41.41 o 6 -5 0 1620.85 1388.61 65.60 o 7 -5 0 92.65 85.08 19.85 o 8 -5 0 181.32 174.42 27.66 o 9 -5 0 244.21 255.30 33.55 o 10 -5 0 2347.70 2059.35 103.94 o 11 -5 0 44.80 27.24 19.35 o 12 -5 0 112.67 83.69 31.46 o 13 -5 0 419.16 395.30 50.28 o 14 -5 0 29.73 14.95 21.31 o 15 -5 0 42.04 57.17 31.25 o 0 -4 0 2632.30 2673.00 71.61 o 1 -4 0 4682.15 4654.60 75.66 o 2 -4 0 6019.61 6306.44 99.12 o 3 -4 0 1492.14 1390.30 41.74 o 4 -4 0 1152.21 1292.79 39.64 o 5 -4 0 2606.55 2244.85 79.95 o 6 -4 0 701.56 744.30 41.67 o 7 -4 0 1911.48 1937.37 77.78 o 8 -4 0 721.31 747.60 47.62 o 9 -4 0 456.69 451.44 43.12 o 10 -4 0 216.25 219.00 35.04 o 11 -4 0 913.92 886.31 65.36 o 12 -4 0 61.18 54.28 18.92 o 13 -4 0 53.50 48.73 25.92 o 14 -4 0 75.06 66.72 28.10 o 15 -4 0 -28.99 29.88 31.64 o 1 -3 0 6120.48 6097.48 91.27 o 2 -3 0 16863.26 17707.65 296.82 o 3 -3 0 118.69 130.23 13.12 o 4 -3 0 116.31 128.72 17.39 o 5 -3 0 7490.68 6667.09 161.87 o 6 -3 0 146.39 128.93 21.30 o 7 -3 0 4083.45 3703.78 120.96 o 8 -3 0 1415.03 1343.29 71.03 o 9 -3 0 593.41 542.21 47.29 o 10 -3 0 134.07 106.20 29.04 o 11 -3 0 356.50 219.00 44.34 o 12 -3 0 22.94 34.14 19.98 o 13 -3 0 97.44 54.94 27.97 o 14 -3 0 -55.65 0.41 25.60 o 15 -3 0 18.49 6.19 32.98 o 1 -2 0 340.94 342.25 13.40 o 2 -2 0 5125.00 4934.01 102.79 o 3 -2 0 175.76 182.35 16.75 o 4 -2 0 937.51 843.88 38.51 o 5 -2 0 397.79 328.52 30.05 o 6 -2 0 304.57 306.32 28.22 o 7 -2 0 1030.24 915.61 55.02 o 8 -2 0 3110.25 3012.13 108.35 o 9 -2 0 2706.66 2567.54 105.57 o 10 -2 0 178.51 185.53 33.11 o 11 -2 0 827.55 760.19 62.58 o 12 -2 0 72.86 64.14 23.89 o 13 -2 0 36.18 22.00 21.75 o 14 -2 0 42.82 20.50 25.10 o 15 -2 0 9.54 1.19 34.47 o 1 -1 0 548.80 737.24 16.26 x 2 -1 0 6131.47 6466.77 113.30 o 3 -1 0 4242.84 4520.54 71.76 o 4 -1 0 76.53 58.77 9.17 o 5 -1 0 649.47 678.76 27.59 o 6 -1 0 664.16 775.13 30.53 o 7 -1 0 1722.27 1567.22 71.85 o 8 -1 0 739.28 711.34 49.17 o 9 -1 0 3504.41 3241.14 123.90 o 10 -1 0 938.26 833.74 62.74 o 11 -1 0 -0.95 2.88 11.08 o 12 -1 0 259.17 249.56 39.87 o 13 -1 0 12.00 21.16 22.45 o 14 -1 0 51.59 40.25 24.38 o 15 -1 0 51.32 27.49 38.63 o 1 0 0 184.62 283.16 11.79 o 2 0 0 49.16 21.61 7.74 o 3 0 0 32051.36 36955.20 532.60 o 4 0 0 343.50 388.45 24.78 o 5 0 0 81.02 167.11 18.19 o 6 0 0 178.82 162.50 16.77 o 7 0 0 68.45 94.00 14.90 o 8 0 0 642.38 666.17 46.58 o 9 0 0 672.02 619.67 54.78 o 10 0 0 228.32 174.57 36.25 o 11 0 0 343.68 363.90 41.18 o 12 0 0 7.95 8.19 17.68 o 13 0 0 46.79 34.81 24.35 o 14 0 0 15.23 6.94 22.37 o 15 0 0 153.66 124.49 54.26 o 1 1 0 724.39 747.05 31.14 o 2 1 0 5848.10 6455.01 90.37 o 3 1 0 4363.34 4477.06 67.14 o 4 1 0 67.29 53.86 10.50 o 5 1 0 704.00 661.07 30.48 o 6 1 0 753.17 773.69 35.85 o 7 1 0 1680.03 1570.00 72.03 o 8 1 0 768.67 711.84 49.62 o 9 1 0 3314.85 3238.86 120.62 o 10 1 0 883.64 837.50 62.91 o 11 1 0 16.87 3.23 17.18 o 12 1 0 206.07 243.71 30.49 o 13 1 0 23.91 21.62 24.50 o 14 1 0 42.35 39.68 20.19 o 15 1 0 34.50 26.96 24.48 o 1 2 0 301.94 342.74 13.20 o 2 2 0 4742.03 4939.69 66.22 o 3 2 0 158.49 178.32 10.30 o 4 2 0 878.53 847.22 33.25 o 5 2 0 415.34 331.24 25.70 o 6 2 0 305.33 309.21 23.73 o 7 2 0 987.38 907.83 54.75 o 8 2 0 2962.63 3006.36 108.09 o 9 2 0 2563.21 2588.37 97.80 o 10 2 0 155.99 190.63 29.65 o 11 2 0 823.74 758.16 61.20 o 12 2 0 82.33 67.09 24.58 o 13 2 0 -1.45 22.64 20.31 o 14 2 0 35.11 19.85 20.90 o 15 2 0 5.58 1.34 17.08 o 1 3 0 6017.42 6119.50 89.66 o 2 3 0 17322.00 17750.58 205.08 o 3 3 0 121.69 140.15 9.93 o 4 3 0 153.15 114.32 12.11 o 5 3 0 6843.58 6690.14 154.38 o 6 3 0 137.23 116.41 25.97 o 7 3 0 4017.09 3723.44 123.08 o 8 3 0 1421.43 1349.58 70.90 o 9 3 0 567.10 543.47 48.93 o 10 3 0 126.28 101.13 30.04 o 11 3 0 288.88 214.53 38.35 o 12 3 0 17.56 34.61 20.15 o 13 3 0 66.02 57.97 21.81 o 14 3 0 13.30 0.61 18.21 o 15 3 0 -45.88 6.44 29.55 o 0 4 0 2912.68 2636.51 79.41 o 1 4 0 4788.13 4738.73 76.82 o 2 4 0 5966.23 6389.13 96.97 o 3 4 0 1454.44 1372.98 33.14 o 4 4 0 1116.67 1279.84 30.53 o 5 4 0 2434.27 2251.14 58.99 o 6 4 0 764.64 745.48 67.37 o 7 4 0 1921.79 1935.88 80.93 o 8 4 0 650.99 747.39 48.95 o 9 4 0 426.02 452.16 44.32 o 10 4 0 228.33 220.33 38.45 o 11 4 0 904.82 890.31 67.26 o 12 4 0 30.79 54.14 22.94 o 13 4 0 41.59 46.98 24.51 o 14 4 0 82.59 64.63 27.82 o 15 4 0 0.01 30.86 19.93 o 1 5 0 22075.75 21014.31 297.11 o 2 5 0 430.35 356.40 19.28 o 3 5 0 471.87 515.96 18.50 o 4 5 0 562.61 549.84 21.78 o 5 5 0 705.56 638.11 30.13 o 6 5 0 1557.19 1384.51 59.68 o 7 5 0 126.43 88.31 41.78 o 8 5 0 161.10 173.71 29.56 o 9 5 0 281.61 261.37 37.59 o 10 5 0 2251.50 2053.66 103.01 o 11 5 0 36.63 26.60 18.54 o 12 5 0 83.91 82.27 24.17 o 13 5 0 393.51 398.75 47.39 o 14 5 0 14.48 16.62 20.18 o 15 5 0 51.67 57.41 50.17 o 0 6 0 5748.56 5037.37 151.49 o 1 6 0 820.40 748.25 25.90 o 2 6 0 993.06 827.64 30.73 o 3 6 0 253.66 200.16 15.59 o 4 6 0 1098.32 1236.03 32.71 o 5 6 0 3434.56 2934.21 77.24 o 6 6 0 20.34 41.95 11.70 o 7 6 0 1305.57 1330.08 57.53 o 8 6 0 1400.33 1450.00 73.67 o 9 6 0 470.25 466.77 44.65 o 10 6 0 677.00 727.61 58.65 o 11 6 0 33.83 42.05 20.43 o 12 6 0 36.44 20.88 18.02 o 13 6 0 -12.53 1.45 19.69 o 14 6 0 78.25 58.05 28.24 o 15 6 0 104.36 89.66 46.69 o 1 7 0 1281.13 1267.77 35.32 o 2 7 0 3351.42 3212.94 67.27 o 3 7 0 4713.35 4223.49 78.67 o 4 7 0 2824.03 2308.64 58.59 o 5 7 0 1374.14 1261.37 58.02 o 6 7 0 920.15 902.66 46.73 o 7 7 0 668.49 648.62 42.52 o 8 7 0 1362.44 1414.68 103.82 o 9 7 0 480.51 420.31 45.97 o 10 7 0 227.98 255.27 38.00 o 11 7 0 85.47 87.65 25.79 o 12 7 0 60.21 71.07 20.54 o 13 7 0 0.79 28.25 9.90 o 14 7 0 -36.36 24.66 24.25 o 15 7 0 20.66 19.62 30.18 o 0 8 0 4130.85 3596.84 124.09 o 1 8 0 5170.56 4450.88 119.42 o 2 8 0 4310.99 3948.19 82.46 o 3 8 0 4789.83 4621.75 81.86 o 4 8 0 2500.29 2302.68 64.00 o 5 8 0 442.13 408.01 34.53 o 6 8 0 82.11 114.97 16.45 o 7 8 0 300.45 271.53 30.82 o 8 8 0 810.10 753.73 49.87 o 9 8 0 82.33 79.58 38.01 o 10 8 0 397.76 377.56 46.21 o 11 8 0 88.76 131.80 21.89 o 12 8 0 15.79 6.55 22.11 o 13 8 0 132.06 152.25 31.55 o 14 8 0 43.56 23.55 22.79 o 15 8 0 42.09 81.27 34.78 o 1 9 0 21673.86 20066.35 519.96 o 2 9 0 1773.47 1788.27 53.75 o 3 9 0 581.07 476.54 28.31 o 4 9 0 564.69 463.58 28.45 o 5 9 0 18.69 42.66 14.98 o 6 9 0 25.82 32.33 13.13 o 7 9 0 48.87 66.35 20.78 o 8 9 0 233.91 222.87 28.65 o 9 9 0 770.59 815.45 85.58 o 10 9 0 599.23 533.02 54.78 o 11 9 0 112.71 112.73 26.63 o 12 9 0 391.83 328.28 47.64 o 13 9 0 14.59 59.57 19.05 o 14 9 0 9.76 13.83 15.22 o 15 9 0 38.36 68.13 34.81 o 0 10 0 1978.28 1565.74 82.91 o 1 10 0 2502.47 2467.36 100.27 o 2 10 0 975.45 1017.25 39.45 o 3 10 0 2162.09 2131.59 57.55 o 4 10 0 326.88 332.89 22.86 o 5 10 0 1070.23 1083.01 54.07 o 6 10 0 491.68 485.93 38.63 o 7 10 0 490.65 505.73 38.58 o 8 10 0 1896.92 1817.35 82.37 o 9 10 0 13.15 4.47 16.91 o 10 10 0 -18.15 36.34 27.27 o 11 10 0 960.07 802.96 68.98 o 12 10 0 12.29 8.93 17.81 o 13 10 0 104.36 64.84 28.51 o 14 10 0 27.57 62.16 32.51 o 15 10 0 7.79 29.34 20.25 o 1 11 0 818.14 705.86 53.97 o 2 11 0 128.77 97.82 16.18 o 3 11 0 657.93 843.64 30.74 o 4 11 0 106.69 90.78 14.46 o 5 11 0 466.25 540.12 36.37 o 6 11 0 1398.20 1363.13 66.25 o 7 11 0 1301.30 1291.08 66.42 o 8 11 0 282.49 272.29 32.42 o 9 11 0 370.49 374.30 35.99 o 10 11 0 844.73 774.48 93.93 o 11 11 0 29.16 15.37 20.28 o 12 11 0 37.37 41.46 24.99 o 13 11 0 6.71 7.11 20.35 o 14 11 0 0.01 59.86 19.47 o 1 12 0 1100.63 974.89 64.52 o 2 12 0 1008.08 1003.43 62.54 o 3 12 0 764.80 683.24 33.53 o 4 12 0 1607.01 1583.83 53.13 o 5 12 0 736.30 641.98 46.04 o 6 12 0 65.62 71.88 18.62 o 7 12 0 291.12 324.23 34.74 o 8 12 0 584.39 566.35 46.48 o 9 12 0 61.01 63.59 20.06 o 10 12 0 1.85 33.28 26.23 o 11 12 0 115.99 115.99 41.38 o 12 12 0 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