#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:21:09 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180853 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/84/2018452.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018452_Fobs loop_ _publ_author_name 'Pourayoubi, Mehrdad' 'Tarahhomi, Atekeh' 'Karimi Ahmadabad, Fatemeh' 'Fejfarov\'a, Karla' 'van der Lee, Arie' 'Du\XP(O)[NHC(CH~3~)~3~]~2~ phosphoramidates, with X = (CH~3~)~2~N and [(CH~3~)~3~CNH]~2~P(O)(O) ; _journal_coeditor_code FA3268 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o164 _journal_page_last o169 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90 _cell_angle_beta 119.371(4) _cell_angle_gamma 90 _cell_length_a 11.3715(4) _cell_length_b 17.7755(7) _cell_length_c 13.6956(5) _exptl_crystal_F_000 872 _reflns_d_resolution_high 0.8365 _cod_data_source_file fa3268IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 265.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2813.29 3004.38 27.52 o 2 0 0 4127.34 4130.76 66.48 o 3 0 0 2230.91 2664.27 49.84 o 4 0 0 174.44 183.37 17.49 o 5 0 0 191.91 121.40 17.79 o 6 0 0 42.61 49.62 8.71 o 7 0 0 137.30 105.11 11.95 o 8 0 0 1336.63 1285.55 26.45 o 9 0 0 53.39 44.98 7.44 o 10 0 0 301.57 268.10 10.50 o 11 0 0 1.09 -8.56 3.35 < 1 1 0 31732.99 33825.34 92.54 o 2 1 0 156.80 118.46 6.87 o 3 1 0 1222.46 1359.72 22.78 o 4 1 0 620.21 762.55 22.88 o 5 1 0 524.65 543.75 26.38 o 6 1 0 494.18 457.54 12.78 o 7 1 0 78.67 61.33 7.46 o 8 1 0 212.52 181.55 12.30 o 9 1 0 68.59 61.83 5.36 o 10 1 0 0.88 -1.62 3.39 < 11 1 0 89.16 66.70 3.90 o 0 2 0 46820.96 49258.79 107.75 o 1 2 0 2257.16 2348.96 25.16 o 2 2 0 8600.54 9095.98 58.40 o 3 2 0 2839.16 3046.31 42.63 o 4 2 0 206.43 238.24 15.74 o 5 2 0 64.09 25.02 9.07 < 6 2 0 15.50 5.65 4.57 < 7 2 0 709.50 675.13 19.09 o 8 2 0 683.82 668.45 15.93 o 9 2 0 51.98 44.67 4.26 o 10 2 0 57.78 45.88 4.92 o 11 2 0 11.00 11.08 3.12 o 1 3 0 19234.10 19129.03 81.36 o 2 3 0 8109.42 8508.95 58.69 o 3 3 0 4.15 6.99 5.06 < 4 3 0 545.30 541.05 19.92 o 5 3 0 127.71 111.58 14.10 o 6 3 0 163.28 146.97 8.93 o 7 3 0 729.65 658.87 19.11 o 8 3 0 153.36 143.86 7.11 o 9 3 0 4.05 8.49 3.83 < 10 3 0 0.66 1.89 4.44 < 11 3 0 51.86 46.33 3.91 o 0 4 0 4622.78 4443.68 47.50 o 1 4 0 5731.15 5539.12 50.23 o 2 4 0 25763.92 25810.84 136.08 o 3 4 0 421.61 501.86 18.52 o 4 4 0 843.63 880.62 28.45 o 5 4 0 91.01 80.85 12.28 o 6 4 0 0.25 -0.90 5.25 < 7 4 0 1919.42 1868.10 30.99 o 8 4 0 586.65 617.67 15.51 o 9 4 0 11.65 8.79 4.14 < 10 4 0 53.51 45.61 4.15 o 11 4 0 1.83 -1.76 2.69 < 1 5 0 19779.90 19657.81 106.09 o 2 5 0 1628.64 1524.52 35.53 o 3 5 0 161.44 186.21 12.70 o 4 5 0 457.51 503.95 22.21 o 5 5 0 586.76 641.08 22.32 o 6 5 0 1882.73 1705.81 22.53 o 7 5 0 1387.67 1391.24 26.30 o 8 5 0 3.21 6.05 4.50 < 9 5 0 419.34 428.36 11.90 o 10 5 0 38.13 29.97 4.33 o 11 5 0 169.80 148.63 7.46 o 0 6 0 1202.56 1144.95 30.17 o 1 6 0 2030.26 1912.28 31.91 o 2 6 0 167.34 131.87 11.62 o 3 6 0 2619.81 3151.24 49.13 o 4 6 0 101.83 100.37 11.71 o 5 6 0 695.11 628.61 18.29 o 6 6 0 17.56 10.81 5.35 < 7 6 0 1374.38 1314.58 21.89 o 8 6 0 398.82 402.73 12.93 o 9 6 0 35.21 37.30 4.99 o 10 6 0 105.12 103.05 6.05 o 11 6 0 10.52 6.85 3.37 < 1 7 0 39.75 70.20 7.50 o 2 7 0 445.26 366.59 16.90 o 3 7 0 1141.29 1067.14 30.38 o 4 7 0 25.37 30.31 8.47 o 5 7 0 78.22 85.84 7.28 o 6 7 0 4254.10 4367.73 39.47 o 7 7 0 118.21 112.74 7.37 o 8 7 0 49.88 37.92 5.10 o 9 7 0 1088.97 1173.09 21.73 o 10 7 0 164.18 162.47 6.78 o 11 7 0 109.51 110.93 9.92 o 0 8 0 49.30 66.27 10.48 o 1 8 0 1027.79 1056.35 24.66 o 2 8 0 1348.93 1566.21 47.93 o 3 8 0 1034.63 991.84 28.18 o 4 8 0 783.64 784.83 14.45 o 5 8 0 2091.97 2018.53 34.47 o 6 8 0 53.12 55.27 9.44 o 7 8 0 869.24 906.94 19.56 o 8 8 0 561.04 569.80 11.63 o 9 8 0 47.67 40.31 4.97 o 10 8 0 7.80 6.02 3.14 < 1 9 0 98.96 117.00 9.67 o 2 9 0 239.10 143.03 14.68 o 3 9 0 500.34 481.01 12.79 o 4 9 0 103.53 59.21 5.24 o 5 9 0 100.61 109.46 10.44 o 6 9 0 2196.86 2254.55 40.36 o 7 9 0 318.00 289.79 8.57 o 8 9 0 597.64 593.43 11.84 o 9 9 0 431.14 451.16 11.20 o 10 9 0 97.80 92.01 4.85 o 0 10 0 76.60 51.20 11.75 o 1 10 0 164.92 149.04 7.13 o 2 10 0 168.74 174.39 8.56 o 3 10 0 1485.82 1602.71 23.79 o 4 10 0 746.05 753.26 15.90 o 5 10 0 2227.41 2383.72 40.01 o 6 10 0 125.57 93.12 8.24 o 7 10 0 603.23 606.95 11.90 o 8 10 0 714.62 746.36 12.85 o 9 10 0 3.64 4.54 3.33 < 10 10 0 22.20 24.76 2.80 o 1 11 0 1.62 1.56 3.29 < 2 11 0 96.17 87.82 6.18 o 3 11 0 158.63 133.50 8.07 o 4 11 0 233.38 253.07 10.34 o 5 11 0 423.33 364.76 16.92 o 6 11 0 768.33 772.75 20.58 o 7 11 0 568.84 590.35 11.64 o 8 11 0 467.24 499.68 10.30 o 9 11 0 28.81 22.37 3.30 o 10 11 0 8.80 3.65 4.56 < 0 12 0 24.28 25.75 4.20 o 1 12 0 1382.98 1326.76 15.59 o 2 12 0 169.19 159.23 7.09 o 3 12 0 154.72 136.82 7.49 o 4 12 0 770.98 721.07 16.21 o 5 12 0 860.22 902.21 28.11 o 6 12 0 326.62 329.13 14.03 o 7 12 0 280.53 284.55 9.33 o 8 12 0 60.20 55.73 4.61 o 9 12 0 5.95 -5.89 3.30 < 1 13 0 17.15 21.98 3.34 o 2 13 0 750.70 723.61 14.11 o 3 13 0 32.99 16.25 4.97 o 4 13 0 4.00 3.98 7.75 < 5 13 0 170.75 197.57 11.36 o 6 13 0 266.74 257.18 12.63 o 7 13 0 81.77 98.52 5.92 o 8 13 0 140.63 159.37 6.37 o 9 13 0 110.27 97.76 6.15 o 0 14 0 502.41 464.62 12.01 o 1 14 0 772.95 704.53 13.54 o 2 14 0 5.31 8.38 3.69 < 3 14 0 539.00 535.19 12.65 o 4 14 0 1296.33 1461.63 19.58 o 5 14 0 152.11 156.36 10.39 o 6 14 0 165.82 171.66 10.46 o 7 14 0 231.16 235.86 7.95 o 8 14 0 189.13 200.22 5.74 o 1 15 0 602.50 611.29 11.18 o 2 15 0 1030.86 1094.84 14.77 o 3 15 0 965.13 980.34 12.98 o 4 15 0 20.98 23.66 5.04 o 5 15 0 40.31 57.28 6.00 o 6 15 0 172.41 192.28 7.42 o 7 15 0 38.28 39.65 3.54 o 8 15 0 0.05 1.37 2.48 < 0 16 0 684.55 701.17 19.32 o 1 16 0 0.57 -2.22 3.33 < 2 16 0 17.73 11.44 3.39 o 3 16 0 432.97 449.82 11.13 o 4 16 0 605.40 651.03 15.04 o 5 16 0 31.66 29.39 4.61 o 6 16 0 33.75 31.79 3.71 o 7 16 0 57.49 51.69 3.31 o 1 17 0 315.96 314.21 9.52 o 2 17 0 313.09 340.23 8.50 o 3 17 0 423.32 443.15 10.66 o 4 17 0 46.64 39.57 4.92 o 5 17 0 90.29 81.84 5.55 o 6 17 0 108.71 112.42 4.90 o 7 17 0 71.87 76.19 7.65 o 0 18 0 28.39 19.28 5.29 o 1 18 0 7.86 4.55 3.41 < 2 18 0 5.52 5.53 3.18 < 3 18 0 257.27 283.18 11.91 o 4 18 0 254.68 263.56 8.71 o 5 18 0 14.38 11.39 2.73 o 6 18 0 16.98 12.70 2.74 o 1 19 0 49.53 48.26 4.74 o 2 19 0 192.69 206.85 8.15 o 3 19 0 233.00 259.82 10.23 o 4 19 0 46.41 43.20 4.84 o 5 19 0 206.43 229.27 8.14 o 0 20 0 32.86 33.94 6.99 o 1 20 0 117.33 114.97 5.85 o 2 20 0 22.47 19.65 4.05 o 3 20 0 102.95 100.34 6.06 o 4 20 0 318.79 357.00 14.16 o 1 21 0 7.67 1.10 2.74 < -12 1 1 53.07 44.63 3.83 o -11 1 1 11.14 6.52 2.75 < -10 1 1 34.01 34.70 4.45 o -9 1 1 36.30 36.09 4.38 o -8 1 1 0.21 -2.32 6.15 < -7 1 1 49.12 43.48 6.20 o -6 1 1 13.20 18.16 5.11 o -5 1 1 782.22 732.64 25.25 o -4 1 1 0.73 -2.09 6.25 < -3 1 1 1069.68 1173.35 30.15 o -2 1 1 2128.14 2114.84 25.32 o -1 1 1 76.12 86.18 3.84 o 0 1 1 130.92 155.13 6.52 o 1 1 1 757.06 825.52 17.78 o 2 1 1 1140.85 1225.14 20.94 o 3 1 1 1.86 4.19 5.23 < 4 1 1 294.44 323.90 18.94 o 5 1 1 4.52 12.33 9.03 < 6 1 1 23.88 26.43 4.82 o 7 1 1 1.97 1.65 3.19 < 8 1 1 221.22 189.01 8.98 o 9 1 1 27.46 19.97 4.88 o 10 1 1 95.86 87.50 4.47 o 11 1 1 15.87 11.02 2.82 o -12 2 1 8.01 5.34 3.22 < -11 2 1 55.98 53.44 4.58 o -10 2 1 775.06 805.24 15.65 o -9 2 1 93.17 74.94 5.58 o -8 2 1 6.21 13.59 5.98 < -7 2 1 8.68 14.97 5.30 < -6 2 1 101.65 84.03 6.48 o -5 2 1 700.40 703.54 28.97 o -4 2 1 106.72 120.37 12.00 o -3 2 1 4.33 5.68 5.17 < -2 2 1 111.99 113.49 8.35 o -1 2 1 1765.50 1750.02 21.53 o 0 2 1 74.10 81.56 6.46 o 1 2 1 10348.33 10737.93 51.41 o 2 2 1 553.20 605.66 15.00 o 3 2 1 816.12 936.04 22.54 o 4 2 1 1122.38 1270.69 30.32 o 5 2 1 576.31 564.71 27.18 o 6 2 1 177.85 168.41 6.99 o 7 2 1 121.14 105.44 8.71 o 8 2 1 403.59 389.10 10.66 o 9 2 1 3.42 0.50 3.22 < 10 2 1 352.14 321.46 7.31 o 11 2 1 0.34 -5.64 2.65 < -12 3 1 23.94 18.48 3.70 o -11 3 1 146.53 141.79 6.44 o -10 3 1 35.79 34.22 4.40 o -9 3 1 2.60 -0.32 3.61 < -8 3 1 140.27 125.08 9.46 o -7 3 1 414.69 367.39 14.45 o -6 3 1 11.37 11.40 5.28 < -5 3 1 141.71 132.21 13.98 o -4 3 1 366.53 443.06 17.25 o -3 3 1 3697.70 4053.71 42.20 o -2 3 1 3882.63 3713.77 36.98 o -1 3 1 3334.97 3360.37 35.36 o 0 3 1 2141.43 2121.98 26.60 o 1 3 1 1925.60 1962.08 30.67 o 2 3 1 112.56 90.21 8.00 o 3 3 1 155.20 130.13 11.00 o 4 3 1 576.93 645.29 25.24 o 5 3 1 101.74 78.77 14.61 o 6 3 1 2.49 -1.04 3.72 < 7 3 1 111.08 80.23 5.51 o 8 3 1 199.21 185.50 7.86 o 9 3 1 174.71 150.78 6.26 o 10 3 1 30.76 25.45 4.52 o 11 3 1 9.41 3.59 3.56 < -11 4 1 24.82 21.92 4.32 o -10 4 1 383.04 405.65 11.53 o -9 4 1 0.18 -1.10 4.15 < -8 4 1 308.49 326.24 15.05 o -7 4 1 2.95 -7.86 6.10 < -6 4 1 144.54 116.61 8.81 o -5 4 1 75.76 89.39 13.12 o -4 4 1 81.23 63.55 8.70 o -3 4 1 39.41 22.93 5.73 o -2 4 1 131.23 121.51 9.47 o -1 4 1 1916.99 1813.01 30.03 o 0 4 1 1491.66 1460.61 22.71 o 1 4 1 1263.66 1295.99 32.01 o 2 4 1 606.05 642.93 18.28 o 3 4 1 34.11 20.13 6.12 o 4 4 1 99.65 96.08 11.63 o 5 4 1 1.06 -3.90 5.56 < 6 4 1 126.23 98.17 6.18 o 7 4 1 305.81 256.60 9.08 o 8 4 1 1410.67 1390.80 19.21 o 9 4 1 64.79 49.02 5.62 o 10 4 1 88.55 64.75 6.25 o 11 4 1 0.37 0.74 3.31 < -11 5 1 265.87 269.30 9.53 o -10 5 1 197.32 184.37 7.31 o -9 5 1 131.05 132.72 7.68 o -8 5 1 1021.78 1022.13 19.49 o -7 5 1 580.50 559.18 17.59 o -6 5 1 293.79 251.52 14.21 o -5 5 1 48.69 69.18 11.70 o -4 5 1 317.35 388.96 19.34 o -3 5 1 151.09 156.70 11.52 o -2 5 1 4438.23 4492.90 54.63 o -1 5 1 3052.60 3125.99 37.53 o 0 5 1 5213.03 5157.13 40.77 o 1 5 1 868.43 891.14 20.79 o 2 5 1 4556.84 5058.94 53.32 o 3 5 1 1234.35 1359.90 31.94 o 4 5 1 630.88 683.40 26.36 o 5 5 1 20.78 23.87 5.10 o 6 5 1 392.72 358.56 10.04 o 7 5 1 1203.48 1180.43 18.45 o 8 5 1 32.16 28.35 5.24 o 9 5 1 359.26 322.39 10.10 o 10 5 1 3.97 1.38 3.31 < 11 5 1 1.72 -4.02 3.28 < -11 6 1 0.13 2.18 3.12 < -10 6 1 166.71 165.88 7.74 o -9 6 1 31.97 32.26 4.52 o -8 6 1 599.33 616.39 16.26 o -7 6 1 772.57 723.83 19.11 o -6 6 1 187.77 187.60 12.96 o -5 6 1 266.09 289.81 12.88 o -4 6 1 855.89 829.95 28.68 o -3 6 1 2281.83 2407.10 51.97 o -2 6 1 59.88 36.20 7.63 o -1 6 1 2.60 2.24 5.06 < 0 6 1 660.13 696.90 16.77 o 1 6 1 149.71 98.85 9.11 o 2 6 1 11.18 4.69 5.60 < 3 6 1 481.40 587.10 22.07 o 4 6 1 104.98 72.43 10.96 o 5 6 1 292.41 313.69 12.27 o 6 6 1 75.42 81.32 6.32 o 7 6 1 148.99 128.53 9.18 o 8 6 1 1442.26 1367.34 22.37 o 9 6 1 32.41 35.47 4.69 o 10 6 1 26.24 20.94 4.14 o -11 7 1 104.95 105.37 5.05 o -10 7 1 1.15 -0.23 3.55 < -9 7 1 687.15 713.64 15.32 o -8 7 1 297.74 305.16 10.56 o -7 7 1 686.08 689.32 13.82 o -6 7 1 32.42 22.54 6.59 o -5 7 1 71.78 68.87 6.47 o -4 7 1 1613.86 1740.54 42.12 o -3 7 1 691.66 730.24 30.89 o -2 7 1 770.18 801.54 27.26 o -1 7 1 827.25 889.77 21.16 o 0 7 1 453.33 445.56 14.89 o 1 7 1 0.32 -0.44 5.78 < 2 7 1 2866.56 3193.11 52.86 o 3 7 1 58.80 32.05 7.11 o 4 7 1 336.94 379.91 13.47 o 5 7 1 6.59 12.12 5.73 < 6 7 1 23.04 30.72 6.35 o 7 7 1 2859.60 2905.55 27.10 o 8 7 1 10.39 6.78 3.68 < 9 7 1 238.39 208.38 8.17 o 10 7 1 8.73 7.11 3.11 < -11 8 1 0.02 -0.33 2.30 < -10 8 1 54.19 46.31 4.68 o -9 8 1 9.22 8.03 4.18 < -8 8 1 78.10 67.42 5.93 o -7 8 1 1533.87 1563.00 21.23 o -6 8 1 1061.93 1045.75 22.40 o -5 8 1 917.71 938.39 22.71 o -4 8 1 0.88 7.75 3.71 < -3 8 1 152.61 237.37 19.66 o -2 8 1 395.70 383.77 16.39 o -1 8 1 1011.54 955.81 23.47 o 0 8 1 143.34 129.67 9.78 o 1 8 1 30.52 48.57 8.54 o 2 8 1 288.58 281.51 17.63 o 3 8 1 187.15 189.44 11.50 o 4 8 1 436.85 400.76 15.89 o 5 8 1 237.01 215.26 13.32 o 6 8 1 696.40 613.49 18.42 o 7 8 1 63.16 58.91 5.25 o 8 8 1 366.62 326.20 8.85 o 9 8 1 27.74 15.89 3.90 o 10 8 1 82.83 77.47 4.97 o -11 9 1 70.17 67.07 7.48 o -10 9 1 43.54 39.17 4.18 o -9 9 1 84.16 83.60 6.05 o -8 9 1 0.31 -2.93 4.11 < -7 9 1 803.70 796.14 19.50 o -6 9 1 1264.21 1192.58 24.06 o -5 9 1 774.36 774.38 18.43 o -4 9 1 2489.69 2670.37 27.37 o -3 9 1 642.16 600.30 14.48 o -2 9 1 1429.25 1482.01 31.95 o -1 9 1 157.11 152.36 11.23 o 0 9 1 197.72 191.49 12.04 o 1 9 1 1150.78 1197.34 35.13 o 2 9 1 1619.57 1566.50 41.49 o 3 9 1 10.74 19.99 4.97 o 4 9 1 12.53 9.97 5.61 < 5 9 1 680.20 714.39 22.14 o 6 9 1 835.26 783.23 21.87 o 7 9 1 1227.47 1244.41 18.08 o 8 9 1 126.83 119.86 5.81 o 9 9 1 117.24 102.65 5.52 o 10 9 1 4.67 -2.48 3.01 < -10 10 1 45.39 47.45 4.05 o -9 10 1 289.86 317.75 9.74 o -8 10 1 37.85 20.52 3.81 o -7 10 1 169.89 170.38 7.63 o -6 10 1 567.08 557.51 18.40 o -5 10 1 2080.23 2038.76 34.36 o -4 10 1 1232.19 1214.58 19.66 o -3 10 1 24.47 8.43 4.84 < -2 10 1 67.36 54.98 5.31 o -1 10 1 696.12 699.01 15.64 o 0 10 1 29.18 20.16 5.78 o 1 10 1 94.89 71.54 5.68 o 2 10 1 6.60 7.04 4.10 < 3 10 1 72.17 89.74 7.73 o 4 10 1 1015.72 1099.04 22.69 o 5 10 1 2.11 6.27 9.89 < 6 10 1 1064.88 1011.07 18.79 o 7 10 1 6.04 4.27 3.29 < 8 10 1 34.76 32.34 3.72 o 9 10 1 11.81 0.38 3.17 < -10 11 1 10.25 10.02 3.88 < -9 11 1 5.35 2.76 3.20 < -8 11 1 254.41 241.82 7.90 o -7 11 1 199.51 203.16 8.09 o -6 11 1 830.33 871.04 26.68 o -5 11 1 742.46 762.03 24.83 o -4 11 1 1428.62 1500.86 22.17 o -3 11 1 1189.92 1255.43 22.35 o -2 11 1 66.42 60.22 4.67 o -1 11 1 5.21 0.33 2.72 < 0 11 1 14.35 16.49 3.24 o 1 11 1 13.00 6.16 3.74 < 2 11 1 268.69 270.76 11.06 o 3 11 1 586.88 608.37 16.08 o 4 11 1 6.50 4.96 6.62 < 5 11 1 568.49 509.10 22.35 o 6 11 1 59.14 52.02 5.53 o 7 11 1 157.76 161.48 6.42 o 8 11 1 5.46 4.75 2.74 < 9 11 1 192.48 171.54 6.74 o -10 12 1 49.38 46.90 4.71 o -9 12 1 175.84 169.55 7.63 o -8 12 1 104.99 99.80 6.14 o -7 12 1 376.46 393.62 12.39 o -6 12 1 512.46 494.62 17.25 o -5 12 1 983.77 923.66 26.85 o -4 12 1 576.72 584.24 15.08 o -3 12 1 2004.00 2008.23 28.78 o -2 12 1 465.11 440.43 9.51 o -1 12 1 1157.90 1146.26 15.69 o 0 12 1 3.18 2.56 3.31 < 1 12 1 874.86 878.72 14.80 o 2 12 1 3.64 -1.56 3.49 < 3 12 1 34.98 8.97 4.97 < 4 12 1 336.99 366.51 14.55 o 5 12 1 119.61 100.59 8.76 o 6 12 1 702.06 731.48 16.12 o 7 12 1 7.20 3.89 3.44 < 8 12 1 149.17 143.77 5.93 o 9 12 1 26.37 20.21 5.42 o -9 13 1 4.54 4.94 4.13 < -8 13 1 312.13 331.58 9.13 o -7 13 1 42.61 49.97 5.68 o -6 13 1 1151.41 1272.96 26.73 o -5 13 1 673.64 638.88 19.24 o -4 13 1 1005.21 935.57 19.11 o -3 13 1 635.88 646.15 12.41 o -2 13 1 0.72 -0.98 2.45 < -1 13 1 591.30 556.56 11.87 o 0 13 1 267.14 250.26 7.92 o 1 13 1 723.11 741.30 13.91 o 2 13 1 476.40 436.10 11.70 o 3 13 1 318.90 321.40 10.16 o 4 13 1 27.99 22.37 5.45 o 5 13 1 293.84 265.06 12.64 o 6 13 1 1.60 4.28 3.98 < 7 13 1 177.20 185.56 7.04 o 8 13 1 11.82 10.50 2.58 o -9 14 1 1.03 2.28 2.26 < -8 14 1 88.63 87.46 5.01 o -7 14 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