#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:21:09 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180853 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/84/2018472.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018472_Fobs loop_ _publ_author_name 'De Candia, Ariel G.' 'Molnar, Matias' 'Slep, Leonardo D.' 'Baggio, Ricardo' _publ_section_title ; Four Ni^II^ complexes with the new cyclam--methylimidazole ligand 1-[(1-methyl-1H-imidazol-2-yl)methyl]-1,4,8,11-tetraazacyclotetradecane ; _journal_coeditor_code FA3274 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m121 _journal_page_last m126 _journal_volume 68 _journal_year 2012 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.4280 _cell_length_b 16.0470 _cell_length_c 16.0600 _exptl_crystal_F_000 1192.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file fa32742sup3.hkl _cod_data_source_block 2 #BEGIN Tags that were not found in dictionaries: _shelx_refln_list_code 4 _shelx_f_calc_maximum 242.36 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 58736.82 64680.13 1565.10 o 4 0 0 940.82 907.31 53.57 o 6 0 0 683.07 640.67 47.50 o 8 0 0 628.59 567.42 76.87 o 10 0 0 41.09 25.57 16.79 o 2 1 0 13167.49 14458.83 525.62 o 3 1 0 395.67 491.05 36.45 o 4 1 0 2293.03 2141.35 137.79 o 5 1 0 700.07 869.06 67.54 o 6 1 0 1537.72 1357.22 203.48 o 7 1 0 420.73 358.78 30.33 o 8 1 0 16.12 9.14 7.93 o 9 1 0 1.34 5.62 11.53 o 10 1 0 58.70 50.80 19.56 o 11 1 0 0.71 -13.33 10.36 o 2 2 0 1490.94 1689.98 89.05 o 3 2 0 5157.50 4884.57 203.43 o 4 2 0 7914.46 8155.41 321.18 o 5 2 0 12.27 -4.21 9.95 o 6 2 0 811.79 809.23 52.54 o 7 2 0 478.03 464.94 38.44 o 8 2 0 230.98 206.53 23.66 o 9 2 0 230.28 227.22 38.45 o 10 2 0 0.21 -17.24 11.49 o 11 2 0 123.84 85.02 38.14 o 2 3 0 5.17 1.19 4.63 o 4 3 0 106.29 141.12 25.19 o 5 3 0 211.03 234.76 35.02 o 6 3 0 2.02 -5.99 8.70 o 7 3 0 656.56 714.51 46.24 o 8 3 0 22.36 25.55 20.96 o 9 3 0 116.04 139.67 42.49 o 10 3 0 3.70 -7.37 11.83 o 11 3 0 0.16 24.78 22.33 o 1 4 0 1663.98 1435.11 60.92 o 4 4 0 381.77 393.11 47.33 o 5 4 0 7134.28 7164.63 311.62 o 6 4 0 134.18 138.94 31.41 o 7 4 0 193.56 168.18 29.98 o 8 4 0 180.04 146.06 26.19 o 9 4 0 52.68 143.31 42.99 o 10 4 0 21.78 2.51 13.39 o 11 4 0 26.98 74.62 34.02 o 4 5 0 606.78 567.07 38.35 o 5 5 0 476.98 513.06 59.57 o 6 5 0 1018.33 1022.27 65.49 o 7 5 0 206.30 153.59 31.69 o 8 5 0 12.36 14.50 26.80 o 9 5 0 47.43 70.45 31.05 o 10 5 0 300.20 311.73 61.47 o 11 5 0 6.73 -4.15 11.69 o 2 6 0 4662.58 4931.54 193.75 o 4 6 0 123.32 69.57 22.60 o 5 6 0 565.88 631.75 68.92 o 6 6 0 601.45 611.56 71.46 o 7 6 0 57.56 77.57 19.66 o 8 6 0 969.72 1034.58 76.03 o 9 6 0 43.88 107.34 37.95 o 10 6 0 88.44 83.62 34.67 o 11 6 0 3.31 22.96 20.54 o 2 7 0 3.08 8.64 3.82 o 4 7 0 637.57 603.01 38.19 o 5 7 0 457.73 524.07 32.08 o 6 7 0 13.66 7.21 6.89 o 7 7 0 2.58 4.27 7.15 o 8 7 0 31.12 37.23 15.32 o 9 7 0 18.69 5.91 18.14 o 10 7 0 126.26 164.05 47.70 o 3 8 0 3476.06 3785.12 165.50 o 4 8 0 1625.30 1542.45 87.67 o 5 8 0 4005.95 4365.68 147.51 o 6 8 0 602.18 591.25 76.58 o 7 8 0 117.22 142.71 37.68 o 8 8 0 618.45 591.72 59.68 o 9 8 0 38.76 23.32 13.64 o 10 8 0 35.12 7.67 12.83 o 3 9 0 1166.08 1227.49 54.67 o 4 9 0 211.33 217.45 25.98 o 5 9 0 54.66 34.20 10.21 o 6 9 0 151.92 192.73 44.57 o 7 9 0 271.73 310.23 60.54 o 8 9 0 254.93 291.27 54.25 o 9 9 0 201.26 204.43 36.63 o 10 9 0 23.87 8.81 12.79 o 3 10 0 167.37 132.01 21.88 o 4 10 0 115.60 108.07 18.84 o 5 10 0 76.45 63.51 13.01 o 6 10 0 32.45 17.99 18.88 o 7 10 0 5.38 -1.97 15.38 o 8 10 0 19.17 26.31 14.82 o 9 10 0 25.50 21.02 21.59 o 10 10 0 0.28 1.68 11.99 o 2 11 0 846.88 1029.07 92.30 o 3 11 0 1810.42 1756.33 93.37 o 4 11 0 668.99 822.30 59.87 o 5 11 0 463.28 514.76 77.84 o 6 11 0 68.18 87.55 35.19 o 7 11 0 286.32 305.10 64.68 o 8 11 0 2.89 -5.03 15.90 o 9 11 0 4.30 -15.42 10.36 o 0 12 0 3008.54 2835.42 127.17 o 1 12 0 181.69 147.31 36.09 o 2 12 0 1803.05 1807.88 99.71 o 3 12 0 785.55 804.09 62.60 o 4 12 0 13.74 -1.45 8.77 o 5 12 0 1052.48 1108.73 122.06 o 6 12 0 226.78 198.60 50.98 o 7 12 0 46.40 41.34 22.58 o 8 12 0 224.95 167.09 50.95 o 9 12 0 0.27 -12.90 11.91 o 1 13 0 2132.23 2346.59 120.94 o 2 13 0 366.48 368.07 43.59 o 3 13 0 527.96 536.37 52.34 o 4 13 0 507.49 459.26 48.44 o 5 13 0 197.11 197.74 51.29 o 6 13 0 317.33 353.32 72.65 o 7 13 0 54.06 20.32 16.08 o 8 13 0 0.75 -9.58 13.77 o 0 14 0 216.90 250.16 50.24 o 1 14 0 284.43 311.71 40.76 o 2 14 0 62.94 37.59 13.51 o 3 14 0 750.02 802.11 68.29 o 4 14 0 34.43 53.58 16.40 o 5 14 0 377.62 504.07 87.71 o 6 14 0 131.27 223.23 60.35 o 7 14 0 4.80 -6.09 22.15 o 8 14 0 4.09 3.36 14.55 o 1 15 0 76.75 104.48 33.69 o 2 15 0 1.42 12.49 9.36 o 3 15 0 34.02 18.15 17.56 o 4 15 0 293.07 330.18 70.37 o 5 15 0 257.86 219.96 60.13 o 6 15 0 45.13 46.48 30.71 o 7 15 0 292.87 331.15 77.60 o 0 16 0 380.25 411.42 73.61 o 1 16 0 21.74 -8.17 15.30 o 2 16 0 739.51 851.30 76.41 o 3 16 0 51.55 42.60 14.52 o 4 16 0 2.71 1.09 12.69 o 5 16 0 23.31 14.29 13.11 o 6 16 0 5.52 -39.94 34.23 o 1 17 0 44.60 50.72 27.41 o 2 17 0 365.48 332.83 48.64 o 3 17 0 48.22 50.96 19.46 o 4 17 0 660.95 693.61 112.59 o 5 17 0 3.16 26.55 26.41 o 0 18 0 4.23 -32.41 26.74 o 1 18 0 9.82 13.18 12.23 o 2 18 0 0.90 7.26 9.17 o 3 18 0 175.24 210.30 66.51 o 4 18 0 36.92 94.93 49.30 o 1 19 0 124.16 152.18 35.15 o 2 19 0 6.09 -33.19 39.32 o 3 19 0 11.30 24.96 20.76 o 2 0 1 183.47 169.02 10.37 o 3 0 1 1436.49 1524.06 51.70 o 4 0 1 1.22 7.33 5.08 o 5 0 1 977.02 1120.65 45.96 o 6 0 1 60.97 30.96 16.23 o 7 0 1 492.73 527.86 27.39 o 8 0 1 149.21 158.94 28.00 o 9 0 1 49.34 73.32 27.87 o 10 0 1 12.18 1.37 8.57 o 11 0 1 199.04 209.41 43.79 o -11 1 1 56.00 54.06 24.04 o -10 1 1 79.92 95.73 26.32 o -9 1 1 405.94 446.27 55.21 o -8 1 1 47.74 50.99 17.27 o -7 1 1 4125.56 4233.15 145.52 o -6 1 1 60.32 50.69 7.39 o -5 1 1 1606.27 1500.69 103.84 o -4 1 1 218.79 226.26 20.45 o -3 1 1 264.83 248.17 19.38 o -2 1 1 170.92 142.52 14.22 o 2 1 1 234.96 230.71 12.57 o 3 1 1 297.47 302.98 18.14 o 4 1 1 152.29 158.05 9.85 o 5 1 1 1507.08 1303.93 49.98 o 6 1 1 76.65 65.64 8.46 o 7 1 1 4076.55 4372.86 119.22 o 8 1 1 52.54 53.62 24.90 o 9 1 1 399.36 480.97 54.81 o 10 1 1 71.27 97.12 36.73 o 11 1 1 52.74 18.65 11.14 o -11 2 1 31.91 121.15 44.32 o -10 2 1 187.50 218.85 38.28 o -9 2 1 258.20 265.85 83.13 o -8 2 1 1861.08 2078.36 85.22 o -7 2 1 239.65 267.69 25.58 o -6 2 1 2548.52 2640.80 124.22 o -5 2 1 4659.74 4022.67 180.65 o -1 2 1 9576.68 10405.26 367.92 o 2 2 1 13232.77 15558.28 380.88 o 3 2 1 2829.16 2595.84 80.50 o 4 2 1 1569.26 1483.10 52.92 o 5 2 1 4567.43 4572.03 212.58 o 6 2 1 2638.32 2523.43 183.75 o 7 2 1 217.48 210.67 22.53 o 8 2 1 1885.63 1988.43 97.83 o 9 2 1 268.75 227.61 52.50 o 10 2 1 187.25 186.46 48.71 o 11 2 1 39.57 41.45 28.03 o -11 3 1 19.60 35.95 27.62 o -10 3 1 279.00 318.92 63.96 o -9 3 1 83.43 58.26 44.26 o -8 3 1 6.63 7.64 7.60 o -7 3 1 323.03 313.45 28.89 o -6 3 1 809.80 937.59 48.68 o -5 3 1 1133.24 1084.14 91.10 o -4 3 1 1284.72 1313.18 92.53 o -3 3 1 689.60 794.84 63.85 o -2 3 1 9315.68 9797.85 349.01 o -1 3 1 508.36 504.47 24.06 o 0 3 1 7498.99 7194.93 273.56 o 1 3 1 481.26 477.05 39.18 o 2 3 1 9660.19 9204.00 364.95 o 3 3 1 677.43 272.90 361.62 o 4 3 1 1188.85 1200.79 85.25 o 5 3 1 1165.24 1146.97 87.15 o 6 3 1 845.32 1045.31 64.54 o 7 3 1 338.66 302.41 33.97 o 8 3 1 6.30 -3.06 7.04 o 9 3 1 79.04 80.24 30.14 o 10 3 1 273.07 268.36 58.30 o 11 3 1 19.52 5.58 20.66 o -11 4 1 98.71 132.85 46.13 o -10 4 1 40.06 18.47 16.16 o -9 4 1 153.42 206.12 49.86 o -8 4 1 553.07 635.12 62.32 o -7 4 1 706.95 682.22 53.63 o -6 4 1 1796.98 1918.71 92.11 o -5 4 1 721.06 638.51 67.50 o -3 4 1 3488.55 3179.99 125.21 o -2 4 1 2731.05 2980.87 127.93 o -1 4 1 8728.11 8355.20 218.68 o 0 4 1 1005.54 1087.27 66.65 o 1 4 1 8438.83 8699.37 339.48 o 2 4 1 2481.82 2938.95 334.49 o 3 4 1 3472.95 3481.82 171.99 o 4 4 1 614.39 660.22 32.14 o 5 4 1 864.33 819.77 75.87 o 6 4 1 1761.96 1902.42 94.11 o 7 4 1 723.85 722.02 57.09 o 8 4 1 555.75 561.75 51.72 o 9 4 1 150.03 156.41 44.17 o 10 4 1 43.98 19.60 22.79 o 11 4 1 95.74 148.41 50.36 o -11 5 1 50.38 65.26 33.12 o -10 5 1 33.30 22.64 20.27 o -9 5 1 1279.77 1521.62 142.26 o -8 5 1 47.62 79.12 18.98 o -7 5 1 2637.69 2801.63 187.15 o -6 5 1 351.04 349.80 49.01 o -4 5 1 1576.14 1537.92 67.28 o -3 5 1 464.20 507.82 37.29 o -2 5 1 687.44 796.13 37.52 o -1 5 1 455.59 461.78 40.93 o 0 5 1 2556.52 2297.43 118.49 o 1 5 1 357.03 390.92 24.58 o 2 5 1 745.75 709.89 61.82 o 3 5 1 519.29 468.08 51.81 o 4 5 1 1580.10 1604.60 63.11 o 5 5 1 1485.56 1525.45 115.50 o 6 5 1 323.64 310.71 50.04 o 7 5 1 2563.24 2907.07 132.76 o 8 5 1 45.84 55.33 16.59 o 9 5 1 1262.64 1477.42 140.41 o 10 5 1 33.18 39.85 23.88 o 11 5 1 49.29 47.57 24.11 o -11 6 1 133.45 71.44 35.73 o -10 6 1 22.93 37.08 22.14 o -9 6 1 202.13 222.20 52.97 o -8 6 1 306.55 358.09 42.60 o -7 6 1 4.10 -3.16 8.13 o -6 6 1 768.83 766.76 68.20 o -4 6 1 7.54 1.27 3.22 o -3 6 1 5839.26 6148.41 247.35 o -2 6 1 1634.01 1681.06 63.04 o -1 6 1 53.16 38.60 11.43 o 0 6 1 1723.36 1782.95 105.85 o 1 6 1 35.72 26.38 7.28 o 2 6 1 1627.83 1703.85 111.79 o 3 6 1 5781.31 5357.07 254.67 o 4 6 1 4.90 -6.94 15.13 o 5 6 1 2586.79 689.57 1291.43 o 6 6 1 788.84 806.68 86.98 o 7 6 1 1.47 8.10 8.15 o 8 6 1 317.10 353.37 43.44 o 9 6 1 202.49 193.57 33.56 o 10 6 1 24.29 -2.40 13.01 o 11 6 1 138.42 94.41 39.75 o -10 7 1 120.36 134.00 42.51 o -9 7 1 313.66 371.97 47.08 o -8 7 1 71.39 86.28 23.17 o -7 7 1 975.28 1097.38 75.68 o -6 7 1 985.02 975.75 95.29 o -5 7 1 1267.42 1240.41 62.09 o -4 7 1 2516.62 2788.81 131.92 o -3 7 1 136.18 127.52 21.86 o -2 7 1 5696.56 5352.05 156.93 o -1 7 1 1698.94 1646.78 101.90 o 0 7 1 370.12 317.42 40.44 o 1 7 1 1675.68 1698.47 67.58 o 2 7 1 5667.28 4996.75 326.32 o 3 7 1 136.56 95.53 24.27 o 4 7 1 2532.11 2391.07 156.19 o 5 7 1 1246.90 1239.63 58.41 o 6 7 1 975.37 943.18 100.95 o 7 7 1 941.49 926.87 101.41 o 8 7 1 74.16 100.60 23.38 o 9 7 1 314.77 342.94 59.08 o 10 7 1 125.96 176.21 49.63 o -10 8 1 114.98 124.84 41.35 o -9 8 1 51.94 34.41 46.34 o -8 8 1 770.67 921.63 74.46 o -7 8 1 184.72 188.86 30.36 o -6 8 1 1184.47 1470.02 125.94 o -5 8 1 2.86 0.92 2.70 o -4 8 1 282.25 228.47 30.30 o -3 8 1 400.57 375.46 42.22 o -2 8 1 2711.68 2596.76 141.78 o -1 8 1 357.22 380.29 46.26 o 0 8 1 2315.73 2113.02 131.48 o 1 8 1 392.04 477.00 31.38 o 2 8 1 2581.82 2711.63 165.04 o 3 8 1 441.00 465.70 60.67 o 4 8 1 283.25 258.81 46.97 o 5 8 1 0.87 -2.07 6.06 o 6 8 1 1212.85 1301.30 122.03 o 7 8 1 185.36 160.11 43.29 o 8 8 1 732.57 873.39 73.20 o 9 8 1 55.80 52.73 18.70 o 10 8 1 116.26 140.03 43.33 o -10 9 1 71.01 65.30 32.10 o -9 9 1 59.95 103.80 26.76 o -8 9 1 109.57 132.22 28.16 o -7 9 1 538.84 465.14 50.13 o -6 9 1 838.39 931.99 101.89 o -5 9 1 462.36 500.96 45.20 o -4 9 1 3478.59 3806.77 184.73 o -3 9 1 207.15 225.20 34.60 o -2 9 1 3647.75 3474.83 181.16 o -1 9 1 515.38 422.01 52.36 o 0 9 1 784.48 767.69 74.42 o 1 9 1 555.43 522.98 34.48 o 2 9 1 3505.95 3283.14 192.16 o 3 9 1 212.41 155.70 15.90 o 4 9 1 3385.34 3247.73 202.80 o 5 9 1 443.45 440.52 36.67 o 6 9 1 771.18 890.17 104.03 o 7 9 1 501.55 512.82 79.61 o 8 9 1 113.81 93.36 34.26 o 9 9 1 57.30 12.74 57.70 o 10 9 1 77.11 24.14 10.67 o -10 10 1 29.40 101.90 38.59 o -9 10 1 91.22 84.02 25.03 o -8 10 1 196.56 207.18 34.82 o -7 10 1 49.15 36.33 20.02 o -6 10 1 46.06 66.86 25.96 o -5 10 1 1066.96 1035.62 62.58 o -4 10 1 35.81 17.45 11.17 o -3 10 1 1175.03 1038.27 86.12 o -2 10 1 1619.45 1643.94 116.18 o -1 10 1 1308.60 1207.59 100.40 o 0 10 1 2700.13 2774.55 169.93 o 1 10 1 1294.39 1369.98 63.94 o 2 10 1 1666.10 1877.51 141.29 o 3 10 1 1278.61 1215.47 112.55 o 4 10 1 35.83 25.20 13.65 o 5 10 1 1100.33 1040.05 63.80 o 6 10 1 58.75 132.11 38.94 o 7 10 1 55.53 111.13 36.27 o 8 10 1 183.84 255.87 58.74 o 9 10 1 87.22 106.01 26.48 o 10 10 1 25.97 5.75 12.01 o -9 11 1 249.72 233.71 39.74 o -8 11 1 37.82 47.51 18.41 o -7 11 1 427.46 452.33 78.37 o -6 11 1 26.22 14.36 15.96 o -5 11 1 675.72 695.02 91.30 o -4 11 1 9.18 3.72 6.18 o -3 11 1 173.78 182.67 34.70 o -2 11 1 490.13 575.70 67.16 o -1 11 1 2440.63 2220.17 150.73 o 0 11 1 396.16 358.59 23.93 o 1 11 1 2460.77 2399.04 167.21 o 2 11 1 478.78 533.70 72.89 o 3 11 1 191.03 208.31 46.17 o 4 11 1 8.23 34.55 21.39 o 5 11 1 679.48 530.61 81.15 o 6 11 1 29.44 16.13 19.46 o 7 11 1 445.83 624.15 97.16 o 8 11 1 40.19 47.08 26.74 o 9 11 1 247.89 272.77 44.95 o -9 12 1 2.39 12.64 16.29 o -8 12 1 204.25 256.21 41.04 o -7 12 1 126.17 156.04 47.96 o -6 12 1 372.01 407.20 74.43 o -5 12 1 1151.91 1151.02 123.41 o -4 12 1 197.44 270.77 45.09 o -3 12 1 441.51 450.09 60.88 o -2 12 1 19.92 26.13 13.43 o -1 12 1 437.24 428.70 61.41 o 0 12 1 18.89 12.44 3.21 o 1 12 1 419.33 385.48 62.60 o 2 12 1 20.96 7.48 10.31 o 3 12 1 435.66 523.98 78.36 o 4 12 1 208.79 236.47 33.51 o 5 12 1 1183.42 1211.39 131.34 o 6 12 1 367.80 459.89 80.28 o 7 12 1 130.74 105.20 35.90 o 8 12 1 201.99 191.48 55.69 o 9 12 1 5.23 1.25 18.19 o -8 13 1 28.80 54.86 19.72 o -7 13 1 125.79 150.92 45.09 o -6 13 1 163.23 191.03 52.59 o -5 13 1 19.41 45.53 24.88 o -4 13 1 930.05 1002.01 74.52 o -3 13 1 528.94 541.47 71.57 o -2 13 1 1055.04 1221.39 112.76 o -1 13 1 2276.35 2365.26 169.63 o 0 13 1 472.42 513.95 74.51 o 1 13 1 2220.44 2375.71 176.97 o 2 13 1 955.76 871.53 102.11 o 3 13 1 530.70 538.63 81.06 o 4 13 1 849.71 878.48 67.84 o 5 13 1 23.33 3.62 18.58 o 6 13 1 144.21 147.11 47.98 o 7 13 1 131.39 126.82 45.28 o 8 13 1 30.63 28.77 26.62 o -8 14 1 125.05 114.05 28.48 o -7 14 1 7.33 -23.67 23.86 o -6 14 1 203.63 231.35 60.08 o -5 14 1 71.48 18.36 14.50 o -4 14 1 156.48 156.20 28.58 o -3 14 1 522.11 597.74 59.76 o -2 14 1 424.79 487.08 71.24 o -1 14 1 220.05 229.87 49.00 o 0 14 1 422.40 466.71 73.56 o 1 14 1 219.02 188.37 46.50 o 2 14 1 413.96 430.72 72.98 o 3 14 1 523.86 554.48 56.54 o 4 14 1 159.03 174.33 30.50 o 5 14 1 73.84 44.94 26.74 o 6 14 1 207.71 272.87 67.34 o 7 14 1 8.00 18.33 21.24 o 8 14 1 122.41 158.83 53.62 o -7 15 1 74.63 65.41 34.10 o -6 15 1 133.51 125.96 44.45 o -5 15 1 202.76 249.66 61.19 o -4 15 1 645.42 791.73 108.96 o -3 15 1 8.98 0.06 11.38 o -2 15 1 211.07 191.64 34.13 o -1 15 1 76.18 76.35 19.97 o 0 15 1 4.78 -21.46 14.31 o 1 15 1 79.45 80.89 22.44 o 2 15 1 207.63 233.07 38.41 o 3 15 1 8.12 9.20 7.72 o 4 15 1 642.09 555.39 94.28 o 5 15 1 203.27 254.47 67.10 o 6 15 1 132.14 92.61 37.68 o 7 15 1 78.63 69.89 36.62 o -6 16 1 35.28 21.88 27.96 o -5 16 1 213.18 185.00 56.36 o -4 16 1 131.74 147.12 46.95 o -3 16 1 545.59 590.00 64.04 o -2 16 1 229.61 274.34 43.58 o -1 16 1 35.67 39.99 22.82 o 0 16 1 264.20 317.39 46.28 o 1 16 1 38.66 29.69 9.77 o 2 16 1 216.33 215.55 39.53 o 3 16 1 525.15 605.56 65.17 o 4 16 1 136.28 206.63 59.63 o 5 16 1 213.42 176.60 58.83 o 6 16 1 41.52 8.19 16.77 o -5 17 1 46.05 109.82 47.01 o -4 17 1 50.04 54.36 31.60 o -3 17 1 68.40 48.04 16.02 o -2 17 1 210.41 225.90 40.64 o -1 17 1 218.12 350.24 58.79 o 0 17 1 181.52 168.25 34.31 o 1 17 1 221.85 277.51 73.03 o 2 17 1 200.78 219.59 38.82 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