#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/85/2018533.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018533_Fobs loop_ _publ_author_name 'Ojala, William H.' 'Arola, Trina M.' 'Brigino, Ann M.' 'Leavell, Jeremy D.' 'Ojala, Charles R.' _publ_section_title ; Competing intermolecular interactions in some `bridge-flipped' isomeric phenylhydrazones ; _journal_coeditor_code FG3255 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o270 _journal_page_last o278 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.500 _cell_angle_gamma 90.000 _cell_length_a 10.6804 _cell_length_b 7.3150 _cell_length_c 16.5427 _exptl_crystal_F_000 600.00 _reflns_d_resolution_high 0.8400 _[local]_cod_data_source_file fg3255Ibsup3.hkl _[local]_cod_data_source_block Ib #BEGIN Tags that were not found in dictionaries: _shelx_title ' 02213m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 262.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14442.97 12831.79 402.26 o 4 0 0 899.97 1042.10 22.22 o 6 0 0 5350.15 5785.31 98.75 o 8 0 0 916.07 904.42 21.79 o 10 0 0 170.32 171.17 10.17 o 12 0 0 1.33 0.05 9.70 o 1 1 0 179.39 142.63 2.46 o 2 1 0 218.01 208.54 5.96 o 3 1 0 4944.96 5281.05 69.01 o 4 1 0 1607.70 1584.13 19.49 o 5 1 0 3505.73 3452.84 41.91 o 6 1 0 2204.05 2240.28 27.62 o 7 1 0 427.10 447.72 6.83 o 8 1 0 12.76 11.49 3.82 o 9 1 0 187.99 214.88 8.90 o 10 1 0 61.58 71.66 5.93 o 11 1 0 284.82 302.99 13.07 o 12 1 0 76.28 91.25 9.18 o 0 2 0 69034.59 57654.20 1655.73 o 1 2 0 7373.33 7591.48 99.86 o 2 2 0 1787.14 2038.19 27.22 o 3 2 0 372.60 357.29 5.44 o 4 2 0 62.14 86.52 2.55 o 5 2 0 207.12 214.20 3.80 o 6 2 0 894.44 997.30 13.01 o 7 2 0 33.19 38.93 4.82 o 8 2 0 52.82 67.11 6.33 o 9 2 0 367.91 385.12 23.64 o 10 2 0 36.52 31.47 6.86 o 11 2 0 45.33 39.88 7.89 o 1 3 0 168.33 163.63 3.35 o 2 3 0 1320.33 1251.82 17.16 o 3 3 0 90.93 72.70 2.62 o 4 3 0 3021.79 2998.44 40.12 o 5 3 0 197.60 190.70 5.71 o 6 3 0 5850.46 5811.01 70.23 o 7 3 0 363.30 346.76 7.03 o 8 3 0 45.96 48.55 4.85 o 9 3 0 2.29 1.50 6.14 o 10 3 0 126.27 144.23 11.85 o 11 3 0 36.68 40.24 8.16 o 0 4 0 1928.85 1867.09 47.50 o 1 4 0 2111.49 2212.96 33.22 o 2 4 0 1470.66 1450.71 20.05 o 3 4 0 88.88 122.15 7.61 o 4 4 0 56.20 59.71 5.44 o 5 4 0 20.51 23.46 3.90 o 6 4 0 813.91 796.81 12.12 o 7 4 0 166.60 172.35 6.13 o 8 4 0 512.46 504.94 10.51 o 9 4 0 187.55 190.29 7.13 o 10 4 0 16.46 18.95 7.45 o 1 5 0 6.18 9.79 3.31 o 2 5 0 91.32 115.31 5.34 o 3 5 0 1830.84 1806.41 27.88 o 4 5 0 86.04 102.71 6.02 o 5 5 0 1851.40 1821.27 28.93 o 6 5 0 1227.72 1208.17 19.78 o 7 5 0 1188.28 1143.78 19.26 o 8 5 0 19.50 17.45 5.78 o 9 5 0 52.04 64.54 6.71 o 10 5 0 0.07 2.32 8.25 o 0 6 0 5089.59 5139.12 109.10 o 1 6 0 275.17 270.57 6.87 o 2 6 0 1064.37 1111.50 18.23 o 3 6 0 103.62 108.35 5.35 o 4 6 0 17.57 29.57 4.87 o 5 6 0 114.02 121.52 6.39 o 6 6 0 728.33 742.60 13.80 o 7 6 0 651.75 647.79 17.79 o 8 6 0 356.57 354.31 11.57 o 1 7 0 9.56 2.99 6.77 o 2 7 0 157.22 168.64 6.47 o 3 7 0 337.55 334.38 8.49 o 4 7 0 270.19 307.82 8.43 o 5 7 0 317.51 326.86 8.91 o 6 7 0 3.68 7.30 7.62 o 7 7 0 180.07 172.74 10.48 o 0 8 0 317.57 311.16 17.35 o 1 8 0 678.90 649.92 17.77 o 2 8 0 0.03 -7.00 8.24 o 3 8 0 144.89 125.86 8.25 o 4 8 0 0.10 5.91 6.87 o -11 0 1 325.15 319.90 12.67 o -9 0 1 578.43 574.64 15.64 o -7 0 1 791.85 882.28 16.69 o -5 0 1 3388.51 3290.07 56.39 o -3 0 1 20464.02 17344.81 293.13 o -1 0 1 508.76 636.49 11.17 o 1 0 1 340.75 455.37 14.36 o 3 0 1 2327.18 2297.21 48.41 o 5 0 1 8238.22 8188.85 139.03 o 7 0 1 111.22 98.03 4.86 o 9 0 1 19.64 22.48 7.18 o 11 0 1 164.62 155.51 10.48 o -12 1 1 30.66 31.25 8.49 o -11 1 1 3.29 3.85 7.30 o -10 1 1 104.53 100.55 6.08 o -9 1 1 273.43 271.00 7.28 o -8 1 1 334.96 331.13 5.94 o -7 1 1 1262.49 1247.38 18.91 o -6 1 1 2959.35 2916.10 35.61 o -5 1 1 604.08 599.50 8.05 o -4 1 1 986.37 962.26 12.09 o -3 1 1 33.62 47.55 1.56 o -2 1 1 2945.56 2957.99 39.25 o -1 1 1 3445.46 3366.63 60.94 o 0 1 1 2242.46 2526.74 33.37 o 1 1 1 471.88 513.10 7.06 o 2 1 1 21343.53 20207.79 265.24 o 3 1 1 1578.22 1595.77 23.91 o 4 1 1 237.95 237.12 4.59 o 5 1 1 14.78 13.95 1.96 o 6 1 1 279.39 297.76 5.41 o 7 1 1 282.91 290.07 6.39 o 8 1 1 3661.34 3580.42 54.28 o 9 1 1 202.31 198.09 6.59 o 10 1 1 314.54 303.88 8.34 o 11 1 1 68.12 66.26 8.14 o -12 2 1 180.52 193.57 10.01 o -11 2 1 19.14 26.66 7.55 o -10 2 1 373.66 376.34 13.81 o -9 2 1 47.89 48.70 5.22 o -8 2 1 145.26 160.38 4.27 o -7 2 1 306.38 329.36 5.56 o -6 2 1 5.83 13.14 2.43 o -5 2 1 263.89 237.61 4.05 o -4 2 1 5149.64 5059.16 60.91 o -3 2 1 3345.95 3294.59 43.80 o -2 2 1 4018.43 3922.04 51.98 o -1 2 1 15.31 14.90 2.26 o 0 2 1 7715.27 7902.38 103.76 o 1 2 1 391.13 417.04 9.67 o 2 2 1 28.91 47.94 4.69 o 3 2 1 93.48 99.04 2.41 o 4 2 1 4878.24 4822.79 63.80 o 5 2 1 1993.08 2045.83 25.14 o 6 2 1 3328.87 3232.36 39.47 o 7 2 1 36.36 33.94 3.47 o 8 2 1 255.81 241.42 6.64 o 9 2 1 1.85 7.73 5.00 o 10 2 1 180.11 186.81 10.69 o 11 2 1 6.38 8.83 7.79 o -11 3 1 19.26 16.19 7.83 o -10 3 1 20.22 23.13 6.99 o -9 3 1 672.53 644.72 12.31 o -8 3 1 305.29 308.39 8.10 o -7 3 1 2900.96 2799.06 37.65 o -6 3 1 153.64 170.24 4.42 o -5 3 1 1062.07 1012.40 13.13 o -4 3 1 44.70 51.02 3.57 o -3 3 1 7.11 15.43 2.16 o -2 3 1 12.18 15.79 2.00 o -1 3 1 7871.52 7935.29 132.61 o 0 3 1 662.00 625.07 20.38 o 1 3 1 990.95 990.87 17.19 o 2 3 1 476.62 509.58 7.77 o 3 3 1 3756.55 3874.87 51.56 o 4 3 1 19.90 25.01 2.54 o 5 3 1 47.29 54.75 2.75 o 6 3 1 106.02 110.43 4.33 o 7 3 1 651.62 642.26 11.69 o 8 3 1 50.88 57.30 5.15 o 9 3 1 381.31 383.50 10.99 o 10 3 1 10.74 17.60 7.12 o 11 3 1 149.67 156.30 9.41 o -11 4 1 196.15 218.24 10.57 o -10 4 1 121.27 128.59 14.94 o -9 4 1 241.30 253.48 10.45 o -8 4 1 19.66 20.28 5.18 o -7 4 1 0.76 1.34 3.86 o -6 4 1 17.16 35.71 3.70 o -5 4 1 1184.92 1172.83 18.66 o -4 4 1 2386.62 2341.80 35.49 o -3 4 1 1735.01 1710.06 23.43 o -2 4 1 778.12 795.02 12.91 o -1 4 1 1116.32 1133.45 15.99 o 0 4 1 1297.03 1456.96 31.84 o 1 4 1 1351.99 1398.29 33.08 o 2 4 1 26.80 34.80 3.12 o 3 4 1 1159.59 1171.66 16.58 o 4 4 1 1939.61 1916.04 26.26 o 5 4 1 445.60 441.65 8.52 o 6 4 1 1648.82 1567.56 21.86 o 7 4 1 4.05 9.74 4.96 o 8 4 1 224.62 210.87 11.83 o 9 4 1 0.40 3.51 6.75 o 10 4 1 89.38 88.84 8.14 o -10 5 1 97.73 92.65 15.63 o -9 5 1 49.74 56.87 6.66 o -8 5 1 833.80 817.76 14.99 o -7 5 1 67.79 65.91 4.86 o -6 5 1 1843.09 1835.50 28.70 o -5 5 1 17.58 36.11 5.35 o -4 5 1 611.09 634.12 11.40 o -3 5 1 13.31 15.22 3.91 o -2 5 1 411.09 437.47 8.43 o -1 5 1 1012.02 1055.99 15.19 o 0 5 1 2998.63 3051.39 41.02 o 1 5 1 43.16 43.73 3.53 o 2 5 1 1680.44 1640.60 22.83 o 3 5 1 508.41 529.85 10.19 o 4 5 1 16.05 18.32 4.16 o 5 5 1 15.54 20.15 4.47 o 6 5 1 371.22 380.24 10.18 o 7 5 1 25.79 47.58 6.13 o 8 5 1 476.27 491.71 10.81 o 9 5 1 6.16 19.40 7.55 o -9 6 1 228.31 233.56 9.12 o -8 6 1 19.65 22.93 6.58 o -7 6 1 17.47 13.11 5.84 o -6 6 1 5.32 16.01 5.48 o -5 6 1 840.32 844.77 14.91 o -4 6 1 29.14 30.25 4.91 o -3 6 1 1891.25 1910.86 39.47 o -2 6 1 510.40 498.08 9.78 o -1 6 1 506.20 492.46 11.15 o 0 6 1 124.98 145.13 5.52 o 1 6 1 426.87 454.47 8.98 o 2 6 1 36.46 50.78 5.27 o 3 6 1 520.96 531.94 10.23 o 4 6 1 16.89 19.54 4.82 o 5 6 1 722.29 744.92 13.50 o 6 6 1 3.83 6.28 6.51 o 7 6 1 8.17 6.75 5.98 o 8 6 1 8.41 4.95 6.53 o -7 7 1 449.45 452.64 13.19 o -6 7 1 578.28 566.52 12.15 o -5 7 1 558.52 564.13 11.85 o -4 7 1 245.78 237.83 10.97 o -3 7 1 42.75 34.82 5.61 o -2 7 1 118.20 131.12 6.76 o -1 7 1 69.57 70.78 8.08 o 0 7 1 535.97 545.47 14.81 o 1 7 1 800.25 749.44 18.83 o 2 7 1 479.15 494.33 10.45 o 3 7 1 58.48 59.54 5.81 o 4 7 1 2.06 -3.32 5.83 o 5 7 1 2.73 6.10 6.08 o 6 7 1 15.15 26.50 7.89 o 7 7 1 90.24 99.76 17.36 o -4 8 1 349.69 364.02 10.01 o -3 8 1 43.10 49.11 7.45 o -2 8 1 548.08 556.12 16.29 o -1 8 1 6.48 11.12 9.57 o 0 8 1 322.72 326.93 12.05 o 1 8 1 32.19 70.34 8.89 o 2 8 1 28.88 24.83 8.46 o 3 8 1 12.86 18.80 7.24 o 4 8 1 157.63 167.81 8.97 o -12 0 2 435.05 408.10 21.54 o -10 0 2 9.50 19.68 7.16 o -8 0 2 1382.22 1365.17 25.09 o -6 0 2 232.14 155.04 13.27 o -4 0 2 704.38 701.22 12.89 o -2 0 2 21.90 62.93 6.58 o 0 0 2 1848.95 1921.43 29.79 o 2 0 2 15781.09 15137.67 380.87 o 4 0 2 771.05 715.18 13.10 o 6 0 2 27.28 43.94 14.59 o 8 0 2 163.96 160.41 8.34 o 10 0 2 343.09 362.63 26.63 o -12 1 2 76.27 61.54 9.43 o -11 1 2 150.77 158.56 8.59 o -10 1 2 346.12 354.87 16.15 o -9 1 2 810.53 790.28 17.51 o -8 1 2 302.58 311.26 5.75 o -7 1 2 6.89 4.42 2.88 o -6 1 2 11.30 15.22 2.43 o -5 1 2 10827.01 11524.04 138.02 o -4 1 2 1593.78 1624.41 19.94 o -3 1 2 4261.49 4268.82 51.35 o -2 1 2 2046.87 2100.91 28.02 o -1 1 2 57.13 53.97 1.67 o 0 1 2 299.90 310.82 4.38 o 1 1 2 14811.97 14917.73 195.98 o 2 1 2 230.61 243.52 3.40 o 3 1 2 1374.97 1332.76 17.97 o 4 1 2 1022.00 1003.75 12.64 o 5 1 2 1548.70 1471.51 23.93 o 6 1 2 1306.01 1313.11 16.71 o 7 1 2 3501.50 3483.91 52.78 o 8 1 2 1088.16 1057.09 17.87 o 9 1 2 586.87 572.51 13.30 o 10 1 2 0.07 1.46 5.74 o 11 1 2 6.79 21.05 6.59 o -12 2 2 244.57 238.99 11.51 o -11 2 2 106.65 116.54 14.42 o -10 2 2 11.46 15.96 6.55 o -9 2 2 47.76 37.52 5.29 o -8 2 2 426.64 419.14 7.65 o -7 2 2 1504.91 1424.45 18.10 o -6 2 2 13.06 12.82 2.45 o -5 2 2 3111.34 3098.92 37.68 o -4 2 2 4.51 8.13 2.81 o -3 2 2 1578.28 1588.48 23.92 o -2 2 2 10.30 40.00 2.43 o -1 2 2 2656.42 2659.62 36.94 o 0 2 2 26.54 33.34 2.42 o 1 2 2 61802.22 56789.32 1578.47 o 2 2 2 2241.49 2353.96 31.39 o 3 2 2 7401.57 7632.81 100.56 o 4 2 2 41.13 38.51 2.57 o 5 2 2 7.10 11.97 2.21 o 6 2 2 83.33 84.10 2.98 o 7 2 2 2491.12 2528.52 34.50 o 8 2 2 470.34 470.18 9.85 o 9 2 2 470.80 483.04 14.12 o 10 2 2 68.04 81.70 10.78 o 11 2 2 128.12 139.04 9.18 o -11 3 2 88.32 94.08 8.28 o -10 3 2 803.88 782.19 33.87 o -9 3 2 10.03 11.16 5.20 o -8 3 2 785.04 784.69 12.17 o -7 3 2 64.09 70.43 3.86 o -6 3 2 2.11 1.25 3.88 o -5 3 2 228.43 287.02 4.77 o -4 3 2 3007.96 2994.53 44.70 o -3 3 2 75.94 69.03 3.03 o -2 3 2 4293.63 4270.75 56.53 o -1 3 2 234.62 253.51 6.20 o 0 3 2 1396.83 1323.60 18.02 o 1 3 2 2946.99 3150.59 41.93 o 2 3 2 240.40 281.38 4.80 o 3 3 2 6.69 16.92 2.27 o 4 3 2 1944.61 1915.27 26.04 o 5 3 2 141.99 145.50 3.75 o 6 3 2 2950.35 2934.69 39.74 o 7 3 2 41.88 45.73 3.90 o 8 3 2 3000.82 2850.32 50.75 o 9 3 2 88.18 88.24 9.80 o 10 3 2 2.26 1.43 7.33 o 11 3 2 2.78 13.22 8.37 o -11 4 2 45.78 50.05 14.76 o -10 4 2 15.79 19.52 6.43 o -9 4 2 36.49 45.59 5.59 o -8 4 2 19.38 20.96 4.37 o -7 4 2 586.36 550.79 9.31 o -6 4 2 344.11 324.60 6.42 o -5 4 2 421.75 411.12 9.85 o -4 4 2 749.80 748.30 12.53 o -3 4 2 106.59 135.85 4.45 o -2 4 2 33.92 33.94 3.21 o -1 4 2 392.79 419.86 6.77 o 0 4 2 2210.36 2229.14 37.92 o 1 4 2 19927.74 20177.07 394.67 o 2 4 2 2483.98 2618.18 35.25 o 3 4 2 2634.37 2775.90 37.44 o 4 4 2 449.35 470.95 9.57 o 5 4 2 8.01 27.20 3.98 o 6 4 2 173.35 187.49 5.82 o 7 4 2 1584.17 1571.98 24.95 o 8 4 2 675.65 698.93 15.41 o 9 4 2 150.24 145.92 8.14 o 10 4 2 33.63 39.34 7.89 o -10 5 2 14.65 8.84 7.00 o -9 5 2 281.56 287.87 8.79 o -8 5 2 93.67 92.26 6.29 o -7 5 2 159.04 163.53 5.61 o -6 5 2 322.79 324.50 7.89 o -5 5 2 652.07 636.01 11.70 o -4 5 2 126.77 149.56 6.32 o -3 5 2 1542.50 1482.38 29.19 o -2 5 2 135.55 150.54 5.05 o -1 5 2 1542.36 1500.00 20.91 o 0 5 2 240.95 234.86 5.12 o 1 5 2 134.28 122.38 5.06 o 2 5 2 14.63 17.70 3.48 o 3 5 2 313.51 333.75 7.86 o 4 5 2 34.91 54.27 4.32 o 5 5 2 838.52 819.63 14.10 o 6 5 2 100.91 100.49 7.69 o 7 5 2 661.58 658.87 12.67 o 8 5 2 370.48 322.13 13.39 o 9 5 2 1.01 -6.20 7.58 o -9 6 2 4.03 7.74 7.19 o -8 6 2 110.67 116.38 7.25 o -7 6 2 56.25 60.50 5.37 o -6 6 2 170.79 174.09 8.45 o -5 6 2 956.91 931.18 16.19 o -4 6 2 297.02 282.37 7.43 o -3 6 2 214.63 220.22 8.98 o -2 6 2 10.50 20.69 4.45 o -1 6 2 164.09 158.42 9.13 o 0 6 2 935.65 970.88 18.74 o 1 6 2 108.45 125.23 5.16 o 2 6 2 2590.49 2594.81 39.55 o 3 6 2 122.49 132.07 5.67 o 4 6 2 293.37 301.38 7.61 o 5 6 2 6.73 15.84 5.27 o 6 6 2 32.31 29.40 7.49 o 7 6 2 25.00 25.92 11.23 o 8 6 2 98.31 114.50 7.95 o -7 7 2 56.33 62.67 7.33 o -6 7 2 448.95 426.90 10.47 o -5 7 2 259.45 265.61 10.11 o -4 7 2 209.00 222.89 7.60 o -3 7 2 222.83 233.51 7.33 o -2 7 2 548.33 534.58 12.50 o -1 7 2 294.83 310.04 10.78 o 0 7 2 39.28 39.13 7.19 o 1 7 2 16.69 21.18 5.75 o 2 7 2 1.41 -1.40 5.87 o 3 7 2 58.17 74.28 5.81 o 4 7 2 344.34 333.07 8.79 o 5 7 2 82.99 80.81 7.55 o 6 7 2 358.34 380.22 11.47 o -5 8 2 935.00 914.58 17.23 o -4 8 2 20.63 27.71 6.89 o -3 8 2 230.61 224.42 11.00 o -2 8 2 6.69 16.19 8.67 o -1 8 2 158.24 170.80 9.94 o 0 8 2 13.46 15.26 8.04 o 1 8 2 568.72 571.76 16.50 o 2 8 2 109.63 101.41 7.93 o 3 8 2 477.19 496.95 12.89 o 4 8 2 0.31 4.20 7.68 o -11 0 3 458.45 484.60 15.02 o -9 0 3 761.16 727.60 14.85 o -7 0 3 2167.35 2141.46 62.52 o -5 0 3 22.39 66.58 8.08 o -3 0 3 9306.35 9168.04 155.37 o -1 0 3 10453.62 9823.46 205.31 o 1 0 3 5549.22 5793.69 98.29 o 3 0 3 51.59 74.80 5.98 o 5 0 3 2463.95 2481.68 53.29 o 7 0 3 3467.23 3354.06 72.12 o 9 0 3 63.88 58.66 7.91 o 11 0 3 19.23 36.85 9.78 o -12 1 3 191.35 209.32 16.25 o -11 1 3 21.53 36.25 9.67 o -10 1 3 4.72 13.72 5.42 o -9 1 3 12.23 9.41 3.87 o -8 1 3 457.02 484.18 8.31 o -7 1 3 425.18 415.58 9.77 o -6 1 3 3176.85 3019.39 36.83 o -5 1 3 2979.27 2999.63 36.46 o -4 1 3 4289.45 4239.00 51.07 o -3 1 3 1943.49 1974.15 23.96 o -2 1 3 62.09 67.83 1.65 o -1 1 3 159.17 169.86 4.66 o 0 1 3 13052.03 12703.23 166.83 o 1 1 3 3419.12 3583.32 47.29 o 2 1 3 244.42 266.70 3.88 o 3 1 3 3415.00 3326.66 46.28 o 4 1 3 4699.47 4559.51 60.44 o 5 1 3 272.26 259.39 4.96 o 6 1 3 8.95 13.41 2.98 o 7 1 3 59.78 64.70 4.65 o 8 1 3 56.88 89.64 8.12 o 9 1 3 442.68 441.33 9.77 o 10 1 3 31.00 30.25 6.00 o 11 1 3 52.48 56.97 6.95 o -12 2 3 127.08 144.63 9.33 o -11 2 3 140.99 133.98 8.62 o -10 2 3 482.99 495.59 13.25 o -9 2 3 59.02 54.04 4.93 o -8 2 3 918.01 914.53 13.62 o -7 2 3 599.34 586.23 8.40 o -6 2 3 25.30 53.02 3.19 o -5 2 3 11.57 26.74 2.07 o -4 2 3 1283.32 1224.47 16.79 o 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