#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/85/2018556.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018556_Fobs loop_ _publ_author_name 'Huang, Yu' 'Zhong, Jia-Liang' 'Hanbin, Shan' 'Li, Min' 'Yuan, Zhe-Dong' _publ_section_title ; (1-{[2-(6-Methoxynaphthalen-1-yl)ethyl]amino}ethylidene)oxidanium bromide monohydrate ; _journal_coeditor_code BI3043 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o308 _journal_page_last o310 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.979 _cell_angle_gamma 90.000 _cell_length_a 11.9376 _cell_length_b 7.3761 _cell_length_c 18.1618 _exptl_crystal_F_000 704.00 _reflns_d_resolution_high 0.8408 _[local]_cod_data_source_file bi30433sup2.hkl _[local]_cod_data_source_block 3 #BEGIN Tags that were not found in dictionaries: _shelx_title 'S103_0m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 208.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 27.65 29.55 1.17 o 2 0 0 1082.06 1285.65 27.17 o 3 0 0 5338.75 5626.06 128.28 o 4 0 0 4557.18 4815.45 110.94 o 5 0 0 339.55 354.93 11.65 o 6 0 0 380.98 340.00 11.86 o 7 0 0 5461.39 5742.15 134.04 o 8 0 0 71.48 55.71 4.93 o 9 0 0 2187.19 2139.11 35.78 o 10 0 0 2719.52 2545.51 41.92 o 11 0 0 1510.11 1482.74 26.37 o 12 0 0 623.16 704.47 14.38 o 1 1 0 939.69 904.49 19.07 o 2 1 0 9774.47 9714.33 199.20 o 3 1 0 6218.00 6403.84 290.62 o 4 1 0 4370.30 4716.74 56.65 o 5 1 0 5339.26 5374.76 64.70 o 6 1 0 15711.38 16303.97 261.02 o 7 1 0 1828.26 1744.85 22.09 o 8 1 0 640.30 613.89 11.69 o 9 1 0 761.39 795.04 11.41 o 10 1 0 27.22 29.85 2.09 o 11 1 0 47.15 32.31 3.07 o 12 1 0 142.13 138.97 5.28 o 1 2 0 387.81 386.74 9.34 o 2 2 0 3228.66 3483.41 71.47 o 3 2 0 2128.28 2196.16 31.62 o 4 2 0 1459.28 1605.09 35.06 o 5 2 0 532.18 549.68 14.45 o 6 2 0 755.08 793.02 13.48 o 7 2 0 68.48 60.87 2.98 o 8 2 0 548.19 541.14 8.22 o 9 2 0 1448.09 1477.37 19.99 o 10 2 0 299.99 301.37 4.82 o 11 2 0 247.30 242.55 6.00 o 2 3 0 2.34 3.17 1.17 o 3 3 0 1183.73 1284.44 28.86 o 4 3 0 684.66 713.59 10.26 o 5 3 0 1141.30 1207.01 23.37 o 6 3 0 264.17 279.97 8.27 o 7 3 0 11.36 16.03 2.52 o 8 3 0 34.59 31.75 3.38 o 9 3 0 0.10 3.26 1.32 o 10 3 0 3.79 4.68 1.04 o 11 3 0 20.52 22.77 1.39 o 12 3 0 4.10 4.48 1.45 o 0 4 0 17.75 18.24 1.69 o 1 4 0 1389.51 1419.22 14.36 o 2 4 0 652.79 649.75 11.96 o 3 4 0 2.16 2.52 1.14 o 4 4 0 454.33 479.98 7.45 o 5 4 0 91.21 101.21 3.07 o 6 4 0 42.58 52.54 3.73 o 7 4 0 3.27 0.59 1.72 o 8 4 0 814.79 833.30 19.10 o 9 4 0 67.88 57.38 1.93 o 10 4 0 164.42 169.36 3.89 o 11 4 0 19.19 22.80 1.57 o 12 4 0 53.73 56.54 2.83 o 1 5 0 321.75 322.79 7.75 o 2 5 0 856.72 900.81 16.41 o 3 5 0 1625.66 1583.34 26.34 o 4 5 0 870.49 867.05 16.24 o 5 5 0 620.86 625.84 9.74 o 6 5 0 522.02 518.06 13.44 o 7 5 0 659.65 664.63 8.19 o 8 5 0 373.78 406.76 5.83 o 9 5 0 164.10 163.83 3.85 o 10 5 0 142.67 134.32 3.19 o 11 5 0 27.38 28.99 1.50 o 0 6 0 851.13 892.53 16.93 o 1 6 0 1868.08 1893.27 31.48 o 2 6 0 781.82 805.30 15.86 o 3 6 0 572.49 562.98 12.27 o 4 6 0 20.41 24.48 1.79 o 5 6 0 17.02 17.14 1.61 o 6 6 0 12.74 16.55 2.24 o 7 6 0 207.81 224.23 6.24 o 8 6 0 954.05 994.85 16.72 o 9 6 0 2.14 4.52 1.02 o 10 6 0 631.02 637.17 10.62 o 1 7 0 59.33 55.83 3.16 o 2 7 0 295.77 295.59 7.20 o 3 7 0 87.11 83.29 3.69 o 4 7 0 565.20 567.94 11.06 o 5 7 0 404.06 417.32 8.93 o 6 7 0 345.12 338.17 7.51 o 7 7 0 217.67 225.92 5.62 o 8 7 0 258.90 258.05 5.62 o 2 8 0 76.36 72.23 2.28 o 3 8 0 36.70 33.03 1.67 o 4 8 0 4.83 8.12 2.26 o 5 8 0 14.71 13.48 1.13 o -12 1 1 16.78 18.00 2.38 o -11 1 1 46.51 47.98 2.43 o -10 1 1 159.45 159.75 4.11 o -9 1 1 622.90 630.88 7.95 o -8 1 1 1595.85 1589.19 16.48 o -7 1 1 67.01 55.07 2.30 o -6 1 1 3.68 2.49 1.41 o -5 1 1 4851.67 5290.76 67.72 o -4 1 1 6.59 8.66 1.24 o -3 1 1 560.80 604.54 10.45 o -2 1 1 2080.56 2189.17 45.20 o -1 1 1 240.36 288.35 6.87 o 1 1 1 258.78 258.66 5.93 o 2 1 1 23986.78 20942.55 544.50 o 3 1 1 4180.32 4113.42 49.29 o 4 1 1 604.79 605.06 8.62 o 5 1 1 657.54 678.41 12.15 o 6 1 1 115.38 152.07 18.86 o 7 1 1 39.00 37.97 2.93 o 8 1 1 21.82 24.02 2.80 o 9 1 1 17.52 20.55 2.69 o 10 1 1 20.17 33.44 3.21 o 11 1 1 111.51 106.60 3.76 o 12 1 1 263.23 259.59 7.41 o -12 2 1 419.04 402.36 9.68 o -11 2 1 75.68 81.37 2.98 o -10 2 1 499.90 455.17 7.25 o -9 2 1 504.43 522.12 7.38 o -8 2 1 54.63 58.56 2.43 o -7 2 1 50.54 78.18 3.29 o -6 2 1 748.68 819.96 13.74 o -5 2 1 980.84 911.21 21.92 o -4 2 1 8485.06 8280.93 168.45 o -3 2 1 11467.93 11174.50 225.54 o -2 2 1 6903.30 7101.50 143.80 o -1 2 1 2776.87 3061.60 62.95 o 1 2 1 3784.00 4051.42 80.46 o 2 2 1 137.23 154.26 3.27 o 3 2 1 753.21 745.46 11.79 o 4 2 1 29.97 40.67 1.58 o 5 2 1 905.77 920.24 24.44 o 6 2 1 922.54 826.99 13.76 o 7 2 1 2884.99 2771.86 34.60 o 8 2 1 2176.77 2150.69 24.53 o 9 2 1 1024.96 1030.43 14.98 o 10 2 1 557.78 548.27 6.24 o 11 2 1 471.10 459.48 11.03 o -13 3 1 0.02 1.03 1.07 o -12 3 1 22.49 34.51 2.69 o -11 3 1 213.52 222.88 3.75 o -10 3 1 450.18 478.41 5.70 o -9 3 1 1131.15 1148.21 16.80 o -8 3 1 1166.49 1196.56 24.68 o -7 3 1 1909.76 1870.45 35.30 o -6 3 1 4710.65 4622.94 79.39 o -5 3 1 3522.41 3603.38 40.68 o -4 3 1 327.62 303.81 5.36 o -3 3 1 11.64 10.86 1.90 o -2 3 1 1159.74 1223.69 27.27 o -1 3 1 80.05 96.32 3.97 o 0 3 1 4526.00 4642.87 89.71 o 1 3 1 3980.07 3884.55 54.92 o 2 3 1 5687.21 5794.90 81.27 o 3 3 1 4524.74 4490.76 92.73 o 4 3 1 5454.86 5285.49 77.22 o 5 3 1 772.79 689.71 14.96 o 6 3 1 3485.47 3524.50 61.68 o 7 3 1 634.04 623.75 12.07 o 8 3 1 97.53 110.80 5.45 o 9 3 1 63.41 69.00 2.84 o 10 3 1 566.37 559.65 7.40 o 11 3 1 449.34 419.71 15.17 o 12 3 1 325.52 306.17 7.27 o -12 4 1 300.46 307.21 7.13 o -11 4 1 55.25 64.77 3.23 o -10 4 1 325.59 319.15 12.36 o -9 4 1 111.58 104.34 2.45 o -8 4 1 12.24 14.96 2.73 o -7 4 1 49.14 56.06 4.17 o -6 4 1 378.98 398.32 10.86 o -5 4 1 1082.25 1083.18 14.28 o -4 4 1 1396.24 1448.73 17.98 o -3 4 1 2241.53 2176.41 33.86 o -2 4 1 3148.92 3212.32 48.41 o -1 4 1 2484.59 2386.90 22.80 o 0 4 1 2432.18 2426.98 23.12 o 1 4 1 4951.74 5021.46 60.41 o 2 4 1 130.90 132.46 4.17 o 3 4 1 180.19 195.21 4.01 o 4 4 1 810.83 848.59 15.81 o 5 4 1 543.34 525.72 8.17 o 6 4 1 1118.74 1163.64 23.99 o 7 4 1 283.41 255.57 8.58 o 8 4 1 2761.98 2652.14 21.10 o 9 4 1 104.11 104.27 2.67 o 10 4 1 528.73 534.03 8.10 o 11 4 1 470.57 493.84 16.52 o 12 4 1 21.81 30.31 2.17 o -11 5 1 147.47 140.23 2.99 o -10 5 1 57.34 57.75 2.27 o -9 5 1 30.39 28.47 1.91 o -8 5 1 572.74 559.37 7.21 o -7 5 1 190.41 204.99 4.78 o -6 5 1 366.42 371.34 6.93 o -5 5 1 225.75 223.49 9.96 o -4 5 1 77.67 71.85 3.62 o -3 5 1 227.93 242.78 6.69 o -2 5 1 15.23 17.17 2.00 o -1 5 1 432.13 410.34 6.37 o 0 5 1 154.07 170.01 3.66 o 1 5 1 294.67 301.14 7.44 o 2 5 1 1488.85 1542.53 25.72 o 3 5 1 414.94 429.04 9.62 o 4 5 1 1482.63 1526.63 25.65 o 5 5 1 149.93 155.52 4.10 o 6 5 1 95.41 105.88 3.46 o 7 5 1 115.83 120.95 2.54 o 8 5 1 116.77 124.74 2.54 o 9 5 1 33.61 35.93 1.97 o 10 5 1 167.16 169.75 3.55 o 11 5 1 5.89 6.79 0.94 o -10 6 1 3.17 3.53 1.10 o -9 6 1 211.02 214.92 5.45 o -8 6 1 214.77 222.92 6.07 o -7 6 1 10.69 16.24 2.21 o -6 6 1 1.08 3.19 2.45 o -5 6 1 1.96 26.48 2.76 o -4 6 1 15.16 14.65 2.17 o -3 6 1 263.47 268.43 7.51 o -2 6 1 106.66 122.04 4.93 o -1 6 1 50.84 50.47 3.28 o 0 6 1 4.03 5.87 1.57 o 1 6 1 23.51 71.54 3.76 o 2 6 1 28.99 42.37 3.07 o 3 6 1 12.90 14.27 2.21 o 4 6 1 62.19 59.41 3.52 o 5 6 1 136.67 133.66 3.54 o 6 6 1 0.87 1.10 1.55 o 7 6 1 103.50 99.39 4.17 o 8 6 1 149.64 154.14 4.83 o 9 6 1 68.24 62.48 2.14 o -8 7 1 47.18 52.92 2.48 o -7 7 1 50.14 52.97 3.98 o -6 7 1 67.34 67.60 3.28 o -5 7 1 11.98 15.14 2.00 o -4 7 1 1.42 4.86 1.55 o -3 7 1 0.84 1.55 1.45 o -2 7 1 4.36 8.51 1.76 o -1 7 1 35.99 37.61 2.02 o 0 7 1 83.59 79.50 3.69 o 1 7 1 0.26 0.95 1.00 o 2 7 1 6.72 12.65 1.97 o 3 7 1 348.04 322.96 7.55 o 4 7 1 0.45 -0.97 1.31 o 5 7 1 43.85 47.23 3.07 o 6 7 1 2.67 2.93 1.45 o 7 7 1 4.41 6.18 1.45 o 8 7 1 0.53 2.35 1.03 o -5 8 1 163.12 152.87 3.04 o -4 8 1 50.65 56.19 1.96 o -3 8 1 19.66 25.59 1.53 o -2 8 1 249.78 266.25 6.66 o 0 8 1 21.62 22.92 2.07 o 1 8 1 25.38 22.03 2.04 o 2 8 1 9.93 12.63 1.24 o 3 8 1 40.68 40.20 2.48 o 4 8 1 93.94 94.50 2.49 o 5 8 1 99.60 102.12 3.52 o -12 0 2 248.21 211.33 6.55 o -11 0 2 46.38 33.82 3.14 o -10 0 2 15.12 19.07 2.48 o -9 0 2 1157.50 1174.23 15.65 o -8 0 2 2724.76 2665.92 28.19 o -7 0 2 1905.15 1630.85 23.95 o -6 0 2 8926.29 9371.20 213.82 o -5 0 2 1306.22 1254.07 31.65 o -4 0 2 3717.80 3635.41 84.05 o -3 0 2 5728.99 5942.87 89.93 o -2 0 2 3003.82 3413.28 69.95 o -1 0 2 322.97 306.10 7.17 o 0 0 2 1667.02 1646.45 52.16 o 1 0 2 6858.64 6274.93 178.89 o 2 0 2 2056.05 1972.26 58.54 o 3 0 2 18419.06 16113.64 310.45 o 4 0 2 10140.59 9518.35 182.51 o 5 0 2 8609.01 8498.23 194.75 o 6 0 2 1299.92 1246.73 33.27 o 7 0 2 2960.78 2720.09 67.16 o 8 0 2 1482.03 1459.30 39.51 o 9 0 2 4.16 5.00 1.76 o 10 0 2 8.35 9.30 1.60 o 11 0 2 53.78 49.12 3.45 o -12 1 2 562.47 537.86 8.39 o -11 1 2 696.94 656.92 11.08 o -10 1 2 1007.56 949.16 10.87 o -9 1 2 690.18 669.09 8.24 o -8 1 2 1693.49 1736.59 19.40 o -7 1 2 653.86 668.72 19.56 o -6 1 2 1984.44 2514.40 33.79 o -5 1 2 3799.40 4550.35 58.58 o -4 1 2 1878.03 1998.91 26.44 o -3 1 2 6453.18 6369.71 96.27 o -2 1 2 17815.08 16389.92 332.89 o -1 1 2 2808.84 3033.88 61.85 o 1 1 2 1338.32 1489.53 30.75 o 2 1 2 10630.90 10151.65 200.00 o 3 1 2 657.79 687.07 8.54 o 4 1 2 450.31 454.44 6.89 o 5 1 2 43.19 42.49 2.28 o 6 1 2 759.68 819.09 14.84 o 7 1 2 170.29 169.97 5.10 o 8 1 2 1225.56 1146.13 22.99 o 9 1 2 687.81 690.16 15.00 o 10 1 2 817.69 841.62 10.37 o 11 1 2 637.51 659.74 7.23 o -12 2 2 69.38 59.25 2.46 o -11 2 2 168.55 153.49 3.99 o -10 2 2 22.00 26.53 1.43 o -9 2 2 73.29 70.48 3.61 o -8 2 2 57.30 58.70 2.87 o -7 2 2 1256.80 1266.77 19.97 o -6 2 2 1208.78 1186.86 18.53 o -5 2 2 1386.36 1401.80 23.78 o -4 2 2 1851.34 1898.07 54.95 o -3 2 2 1049.37 1099.75 24.51 o -2 2 2 3637.30 3719.53 76.40 o -1 2 2 3822.49 4291.02 87.60 o 0 2 2 43512.88 34463.53 659.37 o 1 2 2 2460.73 2683.22 56.75 o 2 2 2 48.95 42.58 1.58 o 3 2 2 1343.07 1420.56 23.77 o 4 2 2 1343.69 1357.12 28.58 o 5 2 2 2227.81 2208.17 45.23 o 6 2 2 500.10 479.66 11.31 o 7 2 2 106.33 119.07 4.30 o 8 2 2 3537.13 3490.59 42.24 o 9 2 2 4.02 1.82 1.18 o 10 2 2 8.92 9.42 1.43 o 11 2 2 8.90 5.76 1.90 o -13 3 2 7.18 6.45 1.31 o -12 3 2 13.68 11.72 1.90 o -11 3 2 106.40 96.49 3.23 o -10 3 2 1.43 0.49 0.81 o -9 3 2 4.95 3.46 1.37 o -8 3 2 60.63 67.78 4.42 o -7 3 2 83.04 90.12 4.73 o -6 3 2 299.18 319.45 8.93 o -5 3 2 418.61 420.25 6.51 o -4 3 2 0.16 1.98 0.81 o -3 3 2 516.01 567.97 14.65 o -2 3 2 12.79 24.54 2.21 o -1 3 2 118.79 128.28 4.86 o 0 3 2 487.22 483.16 11.41 o 1 3 2 1555.99 1734.07 25.51 o 2 3 2 14.36 18.10 1.86 o 3 3 2 91.17 89.47 3.97 o 4 3 2 183.50 189.07 5.78 o 5 3 2 41.85 45.75 3.31 o 6 3 2 660.50 716.19 15.96 o 7 3 2 0.91 3.03 1.43 o 8 3 2 57.49 61.18 2.88 o 9 3 2 49.61 58.70 3.70 o 10 3 2 288.44 283.20 4.77 o 11 3 2 3.54 4.00 1.62 o 12 3 2 36.19 39.27 2.59 o -12 4 2 42.37 43.44 2.62 o -11 4 2 3.14 3.32 1.04 o -10 4 2 56.90 55.61 2.44 o -9 4 2 5.07 1.69 0.85 o -8 4 2 173.59 169.96 6.93 o -7 4 2 329.23 343.99 10.17 o -6 4 2 15.66 14.93 1.93 o -5 4 2 583.00 580.61 8.76 o -4 4 2 900.72 942.57 12.55 o -3 4 2 561.78 581.52 11.17 o -2 4 2 675.87 715.26 13.00 o -1 4 2 2003.58 2233.14 21.47 o 0 4 2 534.37 535.90 6.32 o 1 4 2 2.51 0.44 0.73 o 2 4 2 362.55 362.23 7.82 o 3 4 2 1348.88 1299.84 16.30 o 4 4 2 6.73 10.71 1.85 o 5 4 2 393.72 438.39 11.34 o 6 4 2 637.19 675.30 15.86 o 7 4 2 82.82 90.02 5.04 o 8 4 2 114.74 116.14 2.32 o 9 4 2 745.32 718.77 7.39 o 10 4 2 91.27 92.80 4.28 o 11 4 2 1.92 2.28 1.31 o -11 5 2 219.30 226.38 3.98 o -10 5 2 429.06 445.96 6.69 o -9 5 2 175.68 190.65 5.02 o -8 5 2 161.13 163.29 3.44 o -7 5 2 11.75 10.00 1.52 o -6 5 2 107.28 100.75 3.35 o -5 5 2 81.73 77.83 2.89 o -4 5 2 313.85 337.34 8.20 o -3 5 2 301.03 315.72 6.28 o -2 5 2 1176.12 1182.46 16.40 o -1 5 2 359.44 321.16 5.44 o 0 5 2 2429.10 2458.13 37.01 o 1 5 2 713.83 737.59 14.03 o 2 5 2 476.97 463.73 10.03 o 3 5 2 1897.51 2015.49 32.62 o 4 5 2 240.40 225.47 6.45 o 5 5 2 297.97 331.88 7.29 o 6 5 2 53.35 58.72 2.76 o 7 5 2 96.34 91.60 2.24 o 8 5 2 463.37 448.69 5.19 o 9 5 2 7.80 8.32 1.97 o 10 5 2 199.45 214.74 3.95 o 11 5 2 159.32 169.07 4.62 o -10 6 2 86.24 93.11 3.17 o -9 6 2 88.00 98.74 3.66 o -8 6 2 246.33 253.22 6.52 o -7 6 2 143.02 143.42 4.93 o -6 6 2 458.14 445.09 7.02 o -5 6 2 1059.50 1055.82 13.22 o -4 6 2 834.49 823.92 16.20 o -3 6 2 387.61 356.99 8.96 o -2 6 2 413.08 412.05 9.79 o -1 6 2 4.18 4.69 1.55 o 0 6 2 0.01 0.14 1.31 o 1 6 2 175.28 178.75 5.93 o 2 6 2 431.16 415.87 9.86 o 3 6 2 97.21 95.28 2.95 o 4 6 2 988.81 964.95 9.89 o 5 6 2 737.25 726.58 8.03 o 6 6 2 797.30 822.51 10.52 o 7 6 2 74.27 85.42 2.71 o 8 6 2 56.47 66.51 2.35 o 9 6 2 223.12 246.06 4.15 o -8 7 2 81.56 72.74 2.86 o -7 7 2 20.41 19.74 2.41 o -6 7 2 61.42 57.25 2.18 o -5 7 2 3.20 4.07 1.55 o -4 7 2 91.02 96.49 3.97 o -2 7 2 352.13 348.20 7.86 o -1 7 2 458.14 424.53 8.17 o 0 7 2 521.83 523.03 7.82 o 1 7 2 266.27 264.62 5.03 o 2 7 2 230.19 232.95 6.31 o 3 7 2 128.13 127.18 4.55 o 4 7 2 32.24 37.02 2.73 o 5 7 2 27.67 30.62 2.55 o 6 7 2 38.91 32.69 2.41 o 7 7 2 29.02 31.75 2.28 o -5 8 2 44.53 45.06 2.55 o -4 8 2 69.60 69.23 3.21 o -3 8 2 1.42 0.86 1.24 o -1 8 2 38.94 33.89 2.38 o 0 8 2 2.71 1.55 1.24 o 1 8 2 0.03 2.10 1.24 o 2 8 2 39.60 40.61 2.52 o 3 8 2 17.64 23.44 2.04 o 4 8 2 192.12 186.96 4.86 o 5 8 2 39.29 34.82 2.10 o -12 1 3 461.75 405.59 6.92 o -11 1 3 101.30 96.71 2.68 o -10 1 3 66.57 59.75 2.77 o 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78.98 o 3 2 3 8126.60 8339.71 160.18 o 4 2 3 2870.52 2783.08 55.88 o 5 2 3 2329.88 2318.00 34.01 o 6 2 3 489.37 500.76 9.44 o 7 2 3 449.56 464.28 11.65 o 8 2 3 437.80 419.66 7.76 o 9 2 3 24.75 31.46 3.21 o 10 2 3 719.47 702.32 7.39 o -13 3 3 337.67 347.20 7.44 o -12 3 3 583.11 585.18 11.93 o -11 3 3 323.47 321.07 7.08 o -10 3 3 816.04 757.55 7.03 o -9 3 3 27.98 25.93 2.24 o -8 3 3 78.96 78.22 4.66 o -7 3 3 21.35 16.79 2.48 o -6 3 3 1960.72 1953.74 35.99 o -5 3 3 2432.80 2378.36 27.67 o -4 3 3 3377.61 3154.13 47.23 o -3 3 3 8287.96 8241.56 168.31 o -2 3 3 15303.72 14552.47 293.66 o -1 3 3 2853.31 2883.09 45.85 o 0 3 3 7611.22 7533.51 144.59 o 1 3 3 1391.30 1413.17 29.41 o 2 3 3 1480.37 1729.44 35.68 o 3 3 3 2.56 11.21 4.24 o 4 3 3 629.19 618.73 7.54 o 5 3 3 1555.98 1540.80 29.17 o 6 3 3 2302.60 2325.53 42.47 o 7 3 3 1855.67 1894.55 31.81 o 8 3 3 2658.33 2654.22 33.34 o 9 3 3 619.04 621.28 8.02 o 10 3 3 245.46 244.43 5.09 o 11 3 3 295.60 302.13 5.35 o -12 4 3 1.82 5.21 1.38 o -11 4 3 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