#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/85/2018563.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018563_Fobs loop_ _publ_author_name 'Maass, John S.' 'Luck, Rudy L.' 'Zeller, Matthias' _publ_section_title ; The first dinuclear cobalt complex bridged by acetylamidate ligands: di-\m-acetylamido-\k^2^O:N;\k^2^N:O-di-\m-hydroxido-\k^4^O:O-bis[bis(pyridine-\kN)cobalt(III)] bis(perchlorate) acetonitrile disolvate ; _journal_coeditor_code FG3263 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m233 _journal_page_last m234 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.167 _cell_angle_gamma 90.000 _cell_length_a 10.6198 _cell_length_b 10.2440 _cell_length_c 16.5030 _exptl_crystal_F_000 888.00 _reflns_d_resolution_high 0.6729 _[local]_cod_data_source_file fg3263Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 12mz052_0m in P 21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 175.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 663.96 677.26 12.21 o 4 0 0 297.30 222.80 10.61 o 6 0 0 65.71 64.50 7.64 o 8 0 0 189.95 241.37 23.10 o 10 0 0 585.99 526.03 49.31 o 12 0 0 964.74 991.06 60.89 o 14 0 0 52.99 34.14 18.76 o 2 1 0 1264.69 1325.73 36.71 o 3 1 0 2239.49 2542.46 29.35 o 4 1 0 3197.95 3271.48 29.41 o 5 1 0 7845.53 7811.58 69.44 o 6 1 0 3292.89 3336.70 34.06 o 7 1 0 861.91 897.43 20.60 o 8 1 0 283.13 298.72 14.36 o 9 1 0 635.61 584.66 27.89 o 10 1 0 58.79 70.30 11.71 o 11 1 0 1016.45 1073.41 37.18 o 12 1 0 135.60 150.44 17.53 o 13 1 0 1446.03 1528.84 47.37 o 14 1 0 436.81 457.43 32.79 o 15 1 0 518.09 631.77 38.93 o 0 2 0 19507.58 21891.42 190.60 o 1 2 0 2025.47 2256.46 19.70 o 2 2 0 827.48 911.80 16.12 o 3 2 0 2188.68 2284.44 22.74 o 4 2 0 1620.27 1385.45 17.52 o 5 2 0 3956.85 4008.50 44.06 o 6 2 0 2706.41 2608.76 28.26 o 7 2 0 2963.79 2933.52 41.32 o 8 2 0 54.69 63.91 8.27 o 9 2 0 468.05 491.38 20.20 o 10 2 0 0.61 1.93 7.10 o 11 2 0 403.49 406.36 33.91 o 12 2 0 280.27 270.78 23.29 o 13 2 0 180.22 197.13 26.16 o 14 2 0 509.08 478.91 32.94 o 15 2 0 233.82 275.28 26.73 o 1 3 0 3922.38 3933.91 32.23 o 2 3 0 1.37 7.68 7.11 o 3 3 0 3069.03 3365.10 37.63 o 4 3 0 827.29 986.52 15.83 o 5 3 0 4111.01 4327.03 60.18 o 6 3 0 3197.52 3020.86 40.74 o 7 3 0 2.25 -0.18 4.25 o 8 3 0 2661.15 2560.63 41.53 o 9 3 0 391.89 426.08 21.03 o 10 3 0 1732.06 1852.89 64.90 o 11 3 0 54.16 55.84 11.87 o 12 3 0 864.99 971.01 46.85 o 13 3 0 486.68 516.57 32.64 o 14 3 0 74.09 106.87 16.72 o 15 3 0 113.61 77.51 22.84 o 0 4 0 1076.30 955.18 27.12 o 1 4 0 3756.06 3981.10 35.29 o 2 4 0 564.12 544.16 17.92 o 3 4 0 2323.66 2491.05 29.24 o 4 4 0 1.63 12.10 3.29 o 5 4 0 3726.13 3457.03 51.00 o 6 4 0 550.90 623.57 18.31 o 7 4 0 4261.81 4100.82 53.14 o 8 4 0 73.22 78.87 10.17 o 9 4 0 1122.06 1116.57 28.99 o 10 4 0 519.42 485.22 23.85 o 11 4 0 1209.30 1218.86 38.85 o 12 4 0 355.20 383.94 27.43 o 13 4 0 351.20 337.52 26.90 o 14 4 0 23.60 34.47 13.88 o 1 5 0 103.23 98.87 10.29 o 2 5 0 664.33 908.57 40.23 o 3 5 0 3792.29 3923.14 39.26 o 4 5 0 1264.49 1168.72 20.07 o 5 5 0 12.73 9.99 3.37 o 6 5 0 6523.20 6698.72 70.54 o 7 5 0 34.87 40.14 7.64 o 8 5 0 3721.24 3673.52 54.97 o 9 5 0 15.92 17.75 6.66 o 10 5 0 266.07 290.78 19.34 o 11 5 0 128.85 100.06 14.65 o 12 5 0 146.87 124.54 19.98 o 13 5 0 180.95 151.86 22.20 o 14 5 0 1.03 18.17 17.92 o 0 6 0 1000.74 1021.80 26.07 o 1 6 0 85.67 97.01 7.29 o 2 6 0 2782.78 2700.27 41.22 o 3 6 0 1170.61 1214.87 21.00 o 4 6 0 316.56 341.38 13.12 o 5 6 0 5275.08 5116.63 55.47 o 6 6 0 1617.22 1687.67 32.45 o 7 6 0 3372.17 3330.80 58.36 o 8 6 0 774.21 752.01 31.97 o 9 6 0 71.43 59.27 11.84 o 10 6 0 552.07 535.82 40.33 o 11 6 0 133.25 157.45 28.71 o 12 6 0 13.64 21.12 11.70 o 13 6 0 6.13 20.79 15.60 o 1 7 0 878.03 859.23 18.22 o 2 7 0 141.85 173.06 10.02 o 3 7 0 3337.82 3302.98 39.10 o 4 7 0 493.82 499.12 15.91 o 5 7 0 1789.66 1798.83 40.59 o 6 7 0 1845.93 1737.58 45.30 o 7 7 0 209.25 204.29 18.05 o 8 7 0 883.86 867.09 32.60 o 9 7 0 158.40 136.19 16.28 o 10 7 0 109.46 139.49 17.24 o 11 7 0 26.35 25.60 9.40 o 12 7 0 1.97 6.72 11.13 o 13 7 0 92.89 107.51 25.71 o 0 8 0 1480.71 1536.82 37.30 o 1 8 0 290.65 344.93 19.34 o 2 8 0 1967.82 1948.98 35.67 o 3 8 0 465.86 480.29 21.51 o 4 8 0 53.12 81.48 9.47 o 5 8 0 1224.64 1252.39 48.59 o 6 8 0 196.05 166.35 16.70 o 7 8 0 171.30 184.63 18.12 o 8 8 0 33.02 43.60 10.47 o 9 8 0 764.63 758.16 37.56 o 10 8 0 85.25 109.10 15.04 o 11 8 0 257.27 265.73 24.17 o 12 8 0 15.27 56.57 19.62 o 1 9 0 874.10 856.22 29.56 o 2 9 0 245.34 259.46 20.77 o 3 9 0 1617.56 1745.02 36.09 o 4 9 0 804.24 808.42 27.07 o 5 9 0 1.70 4.81 7.08 o 6 9 0 701.60 594.06 35.61 o 7 9 0 942.16 962.99 37.45 o 8 9 0 0.79 -2.43 7.28 o 9 9 0 0.68 0.37 13.61 o 10 9 0 549.21 541.46 45.13 o 11 9 0 68.19 90.09 17.05 o 12 9 0 245.20 369.41 59.31 o 0 10 0 2618.26 2564.60 103.73 o 1 10 0 426.25 424.94 26.39 o 2 10 0 1431.59 1451.79 40.71 o 3 10 0 2.47 11.37 12.64 o 4 10 0 38.59 37.85 12.11 o 5 10 0 69.36 99.28 22.54 o 6 10 0 61.17 78.05 15.43 o 7 10 0 170.74 176.88 19.13 o 8 10 0 192.78 169.34 18.67 o 9 10 0 2.06 -2.40 8.12 o 10 10 0 289.38 336.05 31.74 o 11 10 0 0.21 -6.68 10.38 o 1 11 0 1248.50 1250.08 39.85 o 2 11 0 9.33 30.18 9.79 o 3 11 0 832.96 814.15 35.52 o 4 11 0 12.55 26.51 10.09 o 5 11 0 88.58 63.22 15.16 o 6 11 0 1.15 -1.77 12.64 o 7 11 0 186.66 232.65 46.17 o 8 11 0 57.10 53.32 16.00 o 9 11 0 79.24 109.21 25.58 o 10 11 0 13.17 26.39 15.00 o 0 12 0 523.78 460.98 44.14 o 1 12 0 14.52 24.65 8.14 o 2 12 0 2722.31 2824.61 63.87 o 3 12 0 26.09 33.09 13.16 o 4 12 0 163.41 187.48 41.83 o 5 12 0 17.20 22.30 11.84 o 6 12 0 139.76 136.23 27.61 o 7 12 0 214.82 239.55 42.66 o 8 12 0 143.04 165.96 33.27 o 1 13 0 1250.31 1239.25 43.18 o 2 13 0 264.61 273.51 24.18 o 3 13 0 384.72 341.07 32.64 o 4 13 0 195.55 225.69 26.42 o 5 13 0 104.55 92.10 22.99 o 6 13 0 466.36 549.57 42.76 o 0 14 0 232.46 243.16 48.39 o 1 14 0 31.81 56.43 11.87 o 2 14 0 495.42 559.36 42.52 o 3 14 0 602.43 548.83 42.09 o 4 14 0 79.68 82.74 23.81 o 1 15 0 128.28 139.95 41.35 o 2 15 0 15.66 -15.79 21.65 o -15 0 1 75.21 104.87 33.40 o -13 0 1 88.92 133.09 25.22 o -11 0 1 2.68 1.55 10.23 o -9 0 1 16.87 19.77 11.29 o -7 0 1 136.42 74.83 13.87 o -5 0 1 99.41 142.05 9.65 o -3 0 1 3149.68 3181.87 44.17 o 1 0 1 2496.64 2553.14 25.87 o 3 0 1 28898.48 28826.45 234.46 o 5 0 1 93.68 50.88 6.78 o 7 0 1 260.99 260.34 14.33 o 9 0 1 2673.26 2802.68 124.30 o 11 0 1 108.93 116.61 21.68 o 13 0 1 1660.62 1538.17 67.28 o 15 0 1 617.97 626.95 97.37 o -15 1 1 2.57 5.35 10.34 o -14 1 1 555.14 562.91 35.47 o -13 1 1 281.50 331.25 36.52 o -12 1 1 17.89 36.07 11.19 o -11 1 1 0.84 -4.16 7.58 o -10 1 1 0.06 -6.54 6.54 o -9 1 1 3.12 6.69 6.49 o -8 1 1 19.43 16.97 4.85 o -7 1 1 1407.89 1518.45 44.57 o -6 1 1 2846.11 2769.34 29.12 o -5 1 1 3.25 4.93 2.88 o -4 1 1 234.79 240.36 11.78 o -3 1 1 13865.85 14434.11 99.50 o -2 1 1 28645.34 29538.36 305.08 o -1 1 1 471.35 488.47 7.23 o 0 1 1 7881.00 8096.52 53.52 o 1 1 1 4248.54 4334.05 29.22 o 2 1 1 28440.19 29810.50 497.50 o 3 1 1 275.85 256.57 7.24 o 4 1 1 5221.94 5409.05 43.09 o 5 1 1 1946.99 1954.72 23.61 o 6 1 1 1779.80 1822.85 24.19 o 7 1 1 109.26 102.93 7.16 o 8 1 1 348.64 357.82 19.17 o 9 1 1 1.58 3.66 6.73 o 10 1 1 2834.66 3017.15 73.75 o 11 1 1 286.30 308.07 23.45 o 12 1 1 765.94 784.10 51.75 o 13 1 1 2.51 -0.04 9.56 o 14 1 1 970.06 1058.00 48.53 o 15 1 1 149.23 123.14 24.11 o -15 2 1 582.47 625.72 61.90 o -14 2 1 17.03 16.22 10.88 o -13 2 1 1181.28 1245.03 44.66 o -12 2 1 656.11 685.32 50.15 o -11 2 1 244.87 257.13 21.52 o -10 2 1 1638.69 1598.58 54.12 o -9 2 1 19.38 13.55 5.68 o -8 2 1 2333.46 2257.83 37.62 o -7 2 1 4422.49 4327.31 52.04 o -6 2 1 4566.41 4715.91 52.17 o -5 2 1 996.35 986.77 19.99 o -4 2 1 937.83 877.76 17.24 o -3 2 1 16613.92 17386.92 106.72 o -2 2 1 3794.73 3975.12 33.81 o -1 2 1 27846.29 29250.11 203.59 o 0 2 1 3582.35 3823.66 35.79 o 1 2 1 8445.33 9067.49 57.94 o 2 2 1 815.56 794.66 14.52 o 3 2 1 4400.70 4420.95 36.30 o 4 2 1 2396.59 2205.21 28.41 o 5 2 1 29.44 54.44 5.86 o 6 2 1 387.73 371.29 20.52 o 7 2 1 430.36 447.36 14.59 o 8 2 1 776.99 828.02 22.46 o 9 2 1 245.00 259.13 15.84 o 10 2 1 339.02 320.24 22.41 o 11 2 1 454.96 507.71 29.21 o 12 2 1 457.40 458.02 29.19 o 13 2 1 677.93 734.47 38.53 o 14 2 1 0.92 4.89 11.93 o 15 2 1 785.86 873.06 98.42 o -15 3 1 312.12 318.41 45.42 o -14 3 1 924.10 896.34 44.83 o -13 3 1 570.03 554.79 34.19 o -12 3 1 111.21 98.35 14.90 o -11 3 1 972.89 954.58 36.70 o -10 3 1 665.71 680.65 32.29 o -9 3 1 4258.17 4106.46 56.98 o -8 3 1 2543.05 2430.47 40.53 o -7 3 1 6260.11 6160.84 93.66 o -6 3 1 549.42 465.37 16.84 o -5 3 1 333.92 391.14 14.99 o -4 3 1 1126.47 1213.14 20.30 o -3 3 1 564.52 591.03 12.83 o -2 3 1 5598.43 5506.82 42.21 o -1 3 1 23.37 28.88 3.08 o 0 3 1 2781.22 2863.69 25.47 o 1 3 1 3909.40 4208.18 37.57 o 2 3 1 11.06 5.02 2.97 o 3 3 1 4264.74 4299.35 42.07 o 4 3 1 318.03 309.39 10.34 o 5 3 1 703.80 635.18 13.88 o 6 3 1 4.25 2.70 3.00 o 7 3 1 4834.02 4825.36 57.02 o 8 3 1 0.44 5.30 4.98 o 9 3 1 632.22 637.18 31.12 o 10 3 1 449.08 430.07 25.70 o 11 3 1 213.55 244.64 20.84 o 12 3 1 37.12 48.81 11.65 o 13 3 1 210.55 223.37 22.41 o 14 3 1 310.41 314.62 26.87 o 15 3 1 6.48 7.05 16.51 o -15 4 1 32.47 20.42 25.85 o -14 4 1 198.05 191.37 25.75 o -13 4 1 12.79 20.53 12.00 o -12 4 1 1329.14 1448.23 53.05 o -11 4 1 34.94 32.52 12.21 o -10 4 1 75.13 79.64 10.61 o -9 4 1 819.22 888.02 31.62 o -8 4 1 5674.87 5780.74 68.62 o -7 4 1 2195.35 2171.21 37.03 o -6 4 1 964.84 904.16 21.96 o -5 4 1 5.60 0.53 2.45 o -4 4 1 218.52 207.07 8.76 o -3 4 1 1395.78 1510.77 20.30 o -2 4 1 1536.67 1633.50 20.10 o -1 4 1 542.22 452.57 9.92 o 0 4 1 130.32 166.16 7.13 o 1 4 1 44.43 55.59 4.66 o 2 4 1 664.61 640.98 12.77 o 3 4 1 746.75 1029.85 17.14 o 4 4 1 7305.36 7135.84 63.36 o 5 4 1 5635.93 5806.46 57.45 o 6 4 1 4339.12 4382.19 44.78 o 7 4 1 3.10 2.38 5.28 o 8 4 1 72.31 102.71 10.67 o 9 4 1 3.48 2.47 5.27 o 10 4 1 1792.09 1757.66 38.41 o 11 4 1 85.75 100.07 14.66 o 12 4 1 132.52 140.11 17.56 o 13 4 1 11.18 14.18 10.13 o 14 4 1 9.00 11.33 12.29 o -14 5 1 43.00 39.36 16.00 o -13 5 1 552.31 609.58 43.81 o -12 5 1 104.59 88.61 17.83 o -11 5 1 376.92 431.38 35.66 o -10 5 1 0.85 1.52 6.17 o -9 5 1 993.20 955.86 29.12 o -8 5 1 137.87 129.44 12.28 o -7 5 1 1703.18 1658.70 33.96 o -6 5 1 191.22 197.15 12.98 o -5 5 1 7.82 25.94 6.28 o -4 5 1 964.12 943.06 17.59 o -3 5 1 44.08 78.01 8.13 o -2 5 1 4682.11 4816.82 43.10 o -1 5 1 61.74 61.11 5.31 o 0 5 1 2267.56 2359.97 27.16 o 1 5 1 2876.17 3037.36 32.09 o 2 5 1 875.93 787.54 15.99 o 3 5 1 125.94 51.07 5.59 o 4 5 1 93.88 152.19 8.92 o 5 5 1 3071.25 3244.16 76.91 o 6 5 1 2530.93 2515.05 81.87 o 7 5 1 10826.06 10620.26 111.56 o 8 5 1 34.97 27.78 7.51 o 9 5 1 226.70 242.66 16.86 o 10 5 1 219.33 244.05 26.56 o 11 5 1 126.16 167.16 17.83 o 12 5 1 63.80 59.81 14.74 o 13 5 1 2.75 -10.77 16.80 o 14 5 1 0.04 15.15 14.26 o -13 6 1 24.52 3.30 12.71 o -12 6 1 176.94 203.04 25.51 o -11 6 1 107.29 120.47 18.86 o -10 6 1 6.67 -2.83 7.21 o -9 6 1 177.98 196.14 18.26 o -8 6 1 1025.35 981.86 32.65 o -7 6 1 22.58 27.23 8.26 o -6 6 1 1670.06 1584.97 33.44 o -5 6 1 1216.69 1139.57 27.41 o -4 6 1 770.53 775.21 16.83 o -3 6 1 154.47 138.11 8.34 o -2 6 1 0.82 0.03 2.88 o -1 6 1 545.28 581.45 13.64 o 0 6 1 15.70 10.78 3.50 o 1 6 1 1093.20 1042.04 18.73 o 2 6 1 7441.35 7790.33 64.72 o 3 6 1 1354.27 1386.68 22.95 o 4 6 1 5250.60 5109.01 50.83 o 5 6 1 1379.70 1287.22 24.12 o 6 6 1 4873.29 5065.31 60.88 o 7 6 1 285.09 274.41 17.05 o 8 6 1 1654.04 1687.12 35.78 o 9 6 1 188.01 167.24 14.57 o 10 6 1 263.28 219.43 19.77 o 11 6 1 143.94 151.57 16.54 o 12 6 1 3.86 4.76 13.56 o 13 6 1 155.56 149.53 27.99 o -13 7 1 646.01 673.34 46.46 o -12 7 1 53.95 40.41 22.16 o -11 7 1 36.52 28.98 9.35 o -10 7 1 0.05 2.14 6.88 o -9 7 1 141.68 161.18 17.72 o -8 7 1 328.46 302.39 22.64 o -7 7 1 1202.26 1207.83 36.27 o -6 7 1 50.28 54.95 10.48 o -5 7 1 353.63 305.24 23.32 o -4 7 1 3674.77 3635.83 50.04 o -3 7 1 500.84 536.65 24.15 o -2 7 1 38.16 52.01 5.72 o -1 7 1 2.04 6.60 3.61 o 0 7 1 8418.79 8359.22 69.78 o 1 7 1 1345.13 1435.86 23.92 o 2 7 1 97.51 130.60 9.06 o 3 7 1 1945.93 1854.92 28.65 o 4 7 1 87.97 120.61 9.81 o 5 7 1 3326.42 3221.79 41.24 o 6 7 1 44.91 64.41 8.98 o 7 7 1 1238.20 1239.95 38.95 o 8 7 1 780.19 808.24 38.03 o 9 7 1 532.45 549.50 34.24 o 10 7 1 5.83 4.09 7.70 o 11 7 1 5.98 27.40 14.91 o 12 7 1 715.17 697.55 92.79 o 13 7 1 24.15 18.47 16.42 o -12 8 1 266.00 301.73 30.57 o -11 8 1 94.97 105.50 15.95 o -10 8 1 415.38 357.78 28.40 o -9 8 1 741.79 767.44 38.12 o -8 8 1 873.75 830.36 42.05 o -7 8 1 46.86 38.75 14.70 o -6 8 1 120.88 158.60 29.12 o -5 8 1 2202.01 2079.32 50.53 o -4 8 1 660.35 653.18 24.75 o -3 8 1 934.60 1019.25 26.35 o -2 8 1 259.70 270.65 16.37 o -1 8 1 2511.64 2377.39 39.62 o 0 8 1 3928.22 3993.60 52.50 o 1 8 1 3249.80 3157.28 39.34 o 2 8 1 78.17 101.96 8.68 o 3 8 1 947.25 935.24 24.82 o 4 8 1 9.67 10.73 5.47 o 5 8 1 512.48 570.35 27.93 o 6 8 1 2.83 38.07 21.64 o 7 8 1 2013.82 1996.76 47.65 o 8 8 1 765.37 821.05 37.76 o 9 8 1 514.24 575.36 32.76 o 10 8 1 22.91 16.48 10.15 o 11 8 1 13.72 22.60 9.88 o 12 8 1 314.35 237.65 50.46 o -12 9 1 115.43 74.28 29.35 o -11 9 1 119.32 130.78 17.23 o -10 9 1 82.52 79.65 14.38 o -9 9 1 105.17 89.63 18.65 o -8 9 1 447.75 487.04 31.06 o -7 9 1 669.77 700.90 35.72 o -6 9 1 541.40 554.78 30.76 o -5 9 1 57.51 43.87 12.32 o -4 9 1 3463.95 3549.88 54.49 o -3 9 1 111.03 119.53 13.91 o -2 9 1 115.71 125.95 15.08 o -1 9 1 97.08 131.90 12.07 o 0 9 1 2518.40 2459.30 50.47 o 1 9 1 72.28 79.19 11.94 o 2 9 1 5.30 5.14 5.84 o 3 9 1 259.06 264.05 19.85 o 4 9 1 16.67 18.90 12.27 o 5 9 1 199.99 183.21 17.70 o 6 9 1 246.94 202.16 18.67 o 7 9 1 4.91 29.06 10.52 o 8 9 1 154.27 179.01 22.76 o 9 9 1 51.53 65.19 15.95 o 10 9 1 33.93 17.27 10.61 o 11 9 1 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210.16 248.26 15.97 o -5 2 9 2928.66 2917.48 37.77 o -4 2 9 420.18 431.49 15.48 o -3 2 9 2405.55 2282.32 30.93 o -2 2 9 599.91 705.23 17.13 o -1 2 9 2183.95 1908.18 25.85 o 0 2 9 1485.57 1388.66 20.30 o 1 2 9 131.46 114.31 11.05 o 2 2 9 2063.87 1976.92 30.59 o 3 2 9 391.32 407.29 15.97 o 4 2 9 1173.38 1109.82 24.02 o 5 2 9 717.56 785.37 20.87 o 6 2 9 267.58 323.20 16.89 o 7 2 9 1095.95 1023.48 26.09 o 8 2 9 417.15 369.63 23.55 o 9 2 9 406.94 368.49 27.90 o 10 2 9 6.05 -6.61 7.43 o 11 2 9 251.63 213.46 30.93 o 12 2 9 66.16 75.32 29.69 o 13 2 9 4.24 17.84 18.82 o -14 3 9 0.05 -14.38 19.78 o -13 3 9 149.81 153.36 23.72 o -12 3 9 2.90 8.85 11.33 o -11 3 9 1198.49 1214.09 52.13 o -10 3 9 704.35 690.74 46.11 o -9 3 9 37.04 41.12 12.70 o -8 3 9 137.51 115.97 12.18 o -7 3 9 3.12 5.46 5.95 o -6 3 9 5228.34 5252.90 64.45 o -5 3 9 17.05 32.92 5.60 o -4 3 9 885.47 863.33 23.77 o -3 3 9 26.61 14.19 4.58 o -2 3 9 911.18 762.59 16.82 o -1 3 9 2037.79 1959.44 26.74 o 0 3 9 649.47 633.95 17.03 o 1 3 9 2934.63 2899.41 41.38 o 2 3 9 18.71 14.11 4.83 o 3 3 9 966.32 927.35 21.90 o 4 3 9 20.43 16.70 6.43 o 5 3 9 735.04 787.47 22.26 o 6 3 9 2.08 4.44 4.76 o 7 3 9 409.94 390.37 19.94 o 8 3 9 190.17 182.93 16.75 o 9 3 9 142.91 158.88 19.47 o 10 3 9 993.53 1018.01 44.90 o 11 3 9 10.60 8.11 13.72 o 12 3 9 115.04 121.95 43.99 o 13 3 9 23.15 18.25 25.81 o -13 4 9 42.38 27.68 13.66 o -12 4 9 736.36 765.48 49.57 o -11 4 9 1061.70 1092.21 56.36 o -10 4 9 1126.65 1103.49 51.60 o -9 4 9 48.58 60.99 15.43 o -8 4 9 346.76 350.40 24.57 o -7 4 9 87.00 91.68 13.18 o -6 4 9 6.51 18.60 12.10 o -5 4 9 777.37 726.26 28.58 o -4 4 9 67.88 93.03 8.09 o -3 4 9 32.85 42.67 6.00 o -2 4 9 1241.30 1190.69 21.41 o -1 4 9 1846.65 1803.92 32.26 o 0 4 9 2978.91 2898.37 33.65 o 1 4 9 107.02 158.49 8.75 o 2 4 9 6089.48 6054.89 64.27 o 3 4 9 1756.01 1821.48 32.39 o 4 4 9 5982.98 5932.70 66.23 o 5 4 9 3.60 5.99 5.02 o 6 4 9 31.91 39.88 8.69 o 7 4 9 71.71 56.48 10.07 o 8 4 9 348.07 323.95 19.06 o 9 4 9 173.58 184.82 17.14 o 10 4 9 5.10 -4.18 7.43 o 11 4 9 338.35 271.31 25.35 o 12 4 9 0.31 4.58 12.55 o 13 4 9 22.84 24.93 18.00 o -13 5 9 24.54 23.24 14.60 o -12 5 9 162.83 191.17 25.81 o -11 5 9 1580.25 1595.57 58.82 o -10 5 9 65.57 34.58 13.68 o -9 5 9 914.27 912.09 38.39 o -8 5 9 252.52 255.81 25.88 o -7 5 9 143.06 158.09 16.93 o -6 5 9 85.35 106.75 14.23 o -5 5 9 1.35 6.38 7.44 o -4 5 9 847.05 805.69 24.60 o -3 5 9 204.59 229.92 16.71 o -2 5 9 430.47 445.49 18.65 o -1 5 9 3126.73 2969.52 42.55 o 0 5 9 47.74 52.16 6.01 o 1 5 9 4505.65 4362.71 74.14 o 2 5 9 71.55 72.68 9.42 o 3 5 9 8624.49 8413.95 83.83 o 4 5 9 1633.86 1521.81 31.47 o 5 5 9 818.59 840.69 24.06 o 6 5 9 1.02 2.61 5.27 o 7 5 9 697.22 633.97 25.49 o 8 5 9 217.54 227.68 18.82 o 9 5 9 89.57 80.22 12.17 o 10 5 9 297.38 319.47 30.39 o 11 5 9 0.07 -6.26 6.83 o 12 5 9 0.01 -0.23 14.17 o 13 5 9 59.03 107.75 35.46 o -12 6 9 1454.01 1404.01 88.62 o -11 6 9 126.76 100.81 19.50 o -10 6 9 560.65 542.70 40.57 o -9 6 9 328.04 333.81 26.24 o -8 6 9 257.66 290.03 23.98 o -7 6 9 149.59 136.62 16.52 o -6 6 9 216.58 211.15 19.42 o -5 6 9 450.86 424.94 26.02 o -4 6 9 34.56 22.41 9.42 o -3 6 9 4557.05 4436.42 58.78 o -2 6 9 187.52 203.43 14.40 o -1 6 9 1250.28 1281.67 28.37 o 0 6 9 638.55 611.80 21.55 o 1 6 9 0.78 -4.36 5.96 o 2 6 9 2047.79 1985.32 43.30 o 3 6 9 28.91 31.96 8.37 o 4 6 9 2679.66 2835.61 45.45 o 5 6 9 285.37 287.68 17.77 o 6 6 9 623.99 630.53 25.61 o 7 6 9 512.21 508.61 27.72 o 8 6 9 982.28 1016.69 36.03 o 9 6 9 269.55 309.90 23.11 o 10 6 9 95.75 81.97 12.21 o 11 6 9 7.12 17.38 13.60 o 12 6 9 0.20 6.75 17.11 o -12 7 9 106.00 104.46 19.97 o -11 7 9 1451.01 1475.08 58.90 o -10 7 9 107.75 81.43 19.62 o -9 7 9 527.54 543.30 33.96 o -8 7 9 893.05 965.69 44.46 o -7 7 9 5.21 17.23 8.90 o -6 7 9 12.94 0.68 7.90 o -5 7 9 0.51 -6.95 6.95 o -4 7 9 1205.16 1310.04 37.62 o -3 7 9 90.12 94.02 10.93 o -2 7 9 6.26 1.40 5.09 o -1 7 9 2333.37 2248.76 50.44 o 0 7 9 160.74 204.55 26.79 o 1 7 9 359.71 355.86 23.16 o 2 7 9 2315.65 2136.88 51.26 o 3 7 9 154.67 182.20 17.37 o 4 7 9 686.43 654.08 31.62 o 5 7 9 1124.29 1069.04 32.06 o 6 7 9 662.93 635.34 30.49 o 7 7 9 462.20 423.53 31.60 o 8 7 9 501.39 554.06 31.01 o 9 7 9 863.16 883.36 38.06 o 10 7 9 396.12 385.29 27.41 o 11 7 9 4.77 -5.69 8.48 o 12 7 9 516.64 531.60 69.38 o -11 8 9 11.68 11.78 12.70 o -10 8 9 368.15 407.30 47.01 o -9 8 9 502.70 509.61 33.70 o -8 8 9 21.33 21.58 12.54 o -7 8 9 966.18 1005.09 45.53 o -6 8 9 78.25 81.97 14.09 o -5 8 9 304.12 290.67 23.36 o -4 8 9 11.72 14.73 12.98 o -3 8 9 3213.20 3066.24 95.95 o -2 8 9 2.94 -0.91 5.50 o -1 8 9 156.36 137.77 12.83 o 0 8 9 1086.01 1029.04 33.66 o 1 8 9 2009.44 2004.05 47.46 o 2 8 9 1809.04 1805.19 61.50 o 3 8 9 25.70 22.70 8.89 o 4 8 9 904.51 884.75 33.07 o 5 8 9 203.77 174.30 18.15 o 6 8 9 3.68 -6.63 6.63 o 7 8 9 412.78 432.69 32.70 o 8 8 9 85.87 71.20 14.08 o 9 8 9 597.66 613.86 52.39 o 10 8 9 0.13 29.41 13.84 o 11 8 9 400.34 331.12 47.12 o -10 9 9 3.10 -7.32 11.56 o -9 9 9 38.74 49.71 13.87 o -8 9 9 806.41 802.23 42.36 o -7 9 9 0.59 3.76 9.02 o -6 9 9 372.35 335.46 26.38 o -5 9 9 166.90 161.57 18.84 o -4 9 9 4354.31 4173.98 74.88 o -3 9 9 299.26 341.78 24.59 o -2 9 9 576.82 578.49 27.11 o -1 9 9 9.54 -3.75 6.62 o 0 9 9 894.49 884.99 36.84 o 1 9 9 78.24 58.84 12.00 o 2 9 9 644.83 757.36 36.59 o 3 9 9 3.01 -3.34 10.44 o 4 9 9 282.54 261.64 26.07 o 5 9 9 317.70 301.98 22.92 o 6 9 9 202.79 208.47 23.32 o 7 9 9 188.68 179.85 22.47 o 8 9 9 955.62 1058.10 69.77 o 9 9 9 137.44 159.28 26.92 o 10 9 9 425.09 516.26 48.56 o 11 9 9 70.56 163.64 35.05 o -10 10 9 123.89 104.90 27.27 o -9 10 9 318.86 286.00 38.07 o -8 10 9 3.16 18.08 10.06 o -7 10 9 140.28 113.00 24.10 o -6 10 9 45.04 42.30 11.79 o -5 10 9 1220.29 1251.16 43.62 o -4 10 9 42.39 18.78 10.55 o -3 10 9 4187.65 4021.58 86.96 o -2 10 9 125.87 100.31 14.18 o -1 10 9 222.66 208.01 20.02 o 0 10 9 20.18 21.41 9.15 o 1 10 9 798.85 818.74 39.11 o 2 10 9 71.20 63.51 12.50 o 3 10 9 148.99 153.32 17.52 o 4 10 9 23.36 31.22 10.72 o 5 10 9 64.69 100.81 21.80 o 6 10 9 0.23 11.65 15.58 o 7 10 9 343.37 415.66 60.53 o 8 10 9 22.53 29.55 13.14 o 9 10 9 1139.28 1283.38 130.69 o -9 11 9 187.40 291.29 48.51 o -8 11 9 373.43 374.88 30.16 o -7 11 9 10.07 10.57 10.01 o -6 11 9 20.99 30.98 14.26 o -5 11 9 0.39 4.76 8.80 o -4 11 9 3273.80 3130.67 123.27 o -3 11 9 92.76 42.02 14.41 o -2 11 9 128.66 110.40 18.49 o -1 11 9 0.75 11.54 6.63 o 0 11 9 49.69 35.96 10.20 o 1 11 9 190.82 163.73 20.90 o 2 11 9 115.00 100.13 17.68 o 3 11 9 9.98 -5.89 8.40 o 4 11 9 77.06 72.72 15.62 o 5 11 9 10.61 16.41 13.31 o 6 11 9 7.75 -1.92 19.75 o 7 11 9 2.51 9.89 15.50 o 8 11 9 1047.44 1343.40 119.04 o -7 12 9 336.47 260.30 33.87 o -6 12 9 72.79 73.27 21.79 o -5 12 9 341.42 358.16 35.01 o -4 12 9 90.15 91.44 22.52 o -3 12 9 397.04 445.39 65.41 o -2 12 9 20.42 39.88 16.91 o -1 12 9 18.11 24.46 11.87 o 0 12 9 73.54 92.46 17.60 o 1 12 9 492.66 541.38 40.83 o 2 12 9 946.08 843.81 50.61 o 3 12 9 51.36 32.21 11.91 o 4 12 9 107.23 82.31 21.74 o 5 12 9 192.47 171.42 29.67 o 6 12 9 5.91 10.27 10.89 o -3 13 9 131.18 144.76 30.46 o -2 13 9 3.02 36.83 15.12 o -1 13 9 35.81 76.90 22.45 o 0 13 9 198.73 247.76 33.41 o 1 13 9 347.92 331.38 31.88 o 2 13 9 51.23 74.23 14.40 o 3 13 9 639.79 653.69 45.43 o -14 0 10 85.07 96.68 33.79 o -12 0 10 422.50 418.03 43.56 o -10 0 10 205.49 214.96 28.57 o -8 0 10 3333.70 3368.50 146.86 o -6 0 10 303.82 289.68 21.77 o -4 0 10 8008.88 7584.76 183.43 o -2 0 10 870.55 711.42 23.34 o 0 0 10 1723.27 1755.12 34.39 o 2 0 10 1.15 -1.27 5.21 o 4 0 10 2051.43 2018.28 56.34 o 6 0 10 173.00 167.94 21.13 o 8 0 10 3534.60 3492.91 87.43 o -14 1 10 48.62 -3.27 22.67 o -13 1 10 490.94 532.81 41.41 o -12 1 10 67.31 70.31 14.58 o -11 1 10 537.33 530.77 32.07 o -10 1 10 5.47 3.38 9.37 o -9 1 10 981.16 938.84 35.35 o -8 1 10 1.87 -4.09 6.76 o -7 1 10 2357.60 2390.96 42.32 o -6 1 10 426.38 455.98 19.14 o -5 1 10 485.73 493.66 19.72 o -4 1 10 1240.05 1212.73 23.34 o -3 1 10 4470.10 4551.12 47.75 o -2 1 10 121.35 116.92 8.48 o -1 1 10 81.95 102.13 7.50 o 0 1 10 175.77 155.28 8.37 o 1 1 10 267.85 256.24 8.53 o 2 1 10 312.62 381.16 19.75 o 3 1 10 1739.97 1764.51 29.07 o 4 1 10 623.28 654.92 18.00 o 5 1 10 2151.08 2172.53 57.13 o 6 1 10 1.57 3.56 5.57 o 7 1 10 1591.09 1639.57 45.70 o 8 1 10 18.06 10.19 7.09 o 9 1 10 5022.30 4665.44 75.13 o 10 1 10 170.90 163.79 23.05 o 11 1 10 577.64 559.14 48.14 o 12 1 10 7.17 2.91 14.36 o 13 1 10 179.09 143.77 29.02 o -14 2 10 8.15 11.01 21.69 o -13 2 10 291.42 284.81 30.98 o -12 2 10 839.33 803.80 49.36 o -11 2 10 613.37 610.52 41.87 o -10 2 10 5.83 11.70 8.61 o -9 2 10 73.77 51.39 11.67 o -8 2 10 2506.45 2559.42 52.51 o -7 2 10 598.92 584.14 25.20 o -6 2 10 601.72 627.01 24.20 o -5 2 10 3239.98 3150.42 40.92 o -4 2 10 5068.68 5175.67 58.15 o -3 2 10 1263.18 1275.15 23.37 o -2 2 10 2150.76 2404.24 31.93 o -1 2 10 789.11 783.19 19.19 o 0 2 10 325.44 310.26 11.53 o 1 2 10 1187.25 1232.53 24.49 o 2 2 10 142.34 174.03 11.33 o 3 2 10 1502.59 1327.26 26.22 o 4 2 10 4042.19 4023.66 50.57 o 5 2 10 129.45 134.98 15.50 o 6 2 10 1366.98 1275.34 31.59 o 7 2 10 930.45 874.66 38.21 o 8 2 10 1039.29 1078.29 33.40 o 9 2 10 17.60 24.15 7.64 o 10 2 10 227.07 181.75 21.01 o 11 2 10 108.88 142.81 42.85 o 12 2 10 233.92 229.84 32.70 o 13 2 10 38.92 23.31 17.84 o -13 3 10 7.14 31.97 14.95 o -12 3 10 581.51 565.27 42.36 o -11 3 10 38.85 40.41 13.65 o -10 3 10 204.65 168.93 23.02 o -9 3 10 1011.50 1027.04 47.13 o -8 3 10 279.35 307.99 22.24 o -7 3 10 1021.67 1131.13 29.45 o -6 3 10 189.69 174.04 13.96 o -5 3 10 18.22 24.52 6.33 o -4 3 10 1459.60 1385.64 27.87 o -3 3 10 3351.47 3390.93 40.80 o -2 3 10 5174.03 5018.58 50.21 o -1 3 10 1578.93 1613.30 25.89 o 0 3 10 2693.75 2496.04 30.37 o 1 3 10 243.81 258.39 13.95 o 2 3 10 2973.02 2883.04 45.55 o 3 3 10 1899.35 1936.74 33.45 o 4 3 10 2281.26 2307.27 37.71 o 5 3 10 9.03 21.96 6.59 o 6 3 10 321.82 303.54 17.51 o 7 3 10 24.51 11.20 5.58 o 8 3 10 58.88 56.03 12.18 o 9 3 10 744.91 690.88 56.84 o 10 3 10 436.85 409.85 31.66 o 11 3 10 1.77 7.74 14.65 o 12 3 10 4.15 -4.46 13.36 o 13 3 10 158.10 166.72 44.01 o -13 4 10 183.50 235.10 28.58 o -12 4 10 52.51 33.50 14.48 o -11 4 10 41.72 34.74 18.29 o -10 4 10 7.87 15.68 10.75 o -9 4 10 137.70 153.91 20.78 o -8 4 10 667.18 590.30 31.72 o -7 4 10 726.41 659.61 32.52 o -6 4 10 532.93 460.01 26.22 o -5 4 10 1235.89 1155.47 47.51 o -4 4 10 306.27 286.15 16.31 o -3 4 10 1688.09 1603.83 26.99 o -2 4 10 288.91 290.85 21.25 o -1 4 10 1142.28 1059.66 21.69 o 0 4 10 41.13 30.21 4.88 o 1 4 10 6106.45 6005.90 66.19 o 2 4 10 278.56 251.94 14.65 o 3 4 10 5069.66 5067.35 117.01 o 4 4 10 227.81 246.06 15.39 o 5 4 10 18.96 9.66 7.17 o 6 4 10 861.85 904.33 35.11 o 7 4 10 120.38 113.18 11.85 o 8 4 10 74.76 87.62 10.41 o 9 4 10 192.72 203.69 22.50 o 10 4 10 6.48 14.58 9.21 o 11 4 10 73.33 49.77 15.18 o 12 4 10 53.00 39.16 17.87 o 13 4 10 123.14 100.52 36.20 o -13 5 10 133.74 46.77 28.14 o -12 5 10 508.95 438.05 38.12 o -11 5 10 24.48 22.42 33.46 o -10 5 10 186.12 207.49 25.65 o -9 5 10 29.92 23.60 11.37 o -8 5 10 31.88 22.68 9.78 o -7 5 10 185.70 168.99 17.93 o -6 5 10 41.95 85.20 13.10 o -5 5 10 646.71 643.60 31.02 o -4 5 10 212.12 242.68 15.88 o -3 5 10 28.65 23.15 6.09 o -2 5 10 1841.34 1719.89 41.44 o -1 5 10 1404.66 1362.46 31.98 o 0 5 10 77.83 52.64 12.60 o 1 5 10 447.92 467.98 39.08 o 2 5 10 3126.14 3114.30 45.29 o 3 5 10 1143.62 1040.76 27.77 o 4 5 10 2763.76 2540.50 42.69 o 5 5 10 83.12 92.28 10.35 o 6 5 10 2010.91 1997.55 39.46 o 7 5 10 97.53 105.24 11.68 o 8 5 10 48.76 45.83 9.00 o 9 5 10 82.19 104.81 17.01 o 10 5 10 424.08 382.89 30.50 o 11 5 10 0.06 -3.48 10.39 o 12 5 10 16.22 5.67 15.42 o -12 6 10 45.16 45.93 22.21 o -11 6 10 413.58 480.04 39.57 o -10 6 10 441.89 463.18 37.67 o -9 6 10 73.41 99.89 15.70 o -8 6 10 43.62 39.82 11.61 o -7 6 10 34.68 44.76 11.57 o -6 6 10 476.58 514.14 30.00 o -5 6 10 81.43 97.33 16.79 o -4 6 10 30.29 34.29 7.07 o -3 6 10 1721.86 1734.17 35.46 o -2 6 10 48.35 62.98 11.24 o -1 6 10 86.28 109.65 11.85 o 0 6 10 1450.81 1546.94 38.67 o 1 6 10 3505.93 3508.97 60.19 o 2 6 10 1347.56 1271.81 35.54 o 3 6 10 3940.96 3957.47 98.14 o 4 6 10 25.44 24.89 7.31 o 5 6 10 9.12 11.85 6.97 o 6 6 10 1196.10 1194.80 34.97 o 7 6 10 831.17 842.74 33.12 o 8 6 10 3.07 14.19 8.81 o 9 6 10 31.02 43.91 11.59 o 10 6 10 213.76 209.66 22.97 o 11 6 10 28.51 3.28 20.16 o 12 6 10 20.03 45.75 24.55 o -12 7 10 614.74 495.12 69.73 o -11 7 10 458.12 433.81 38.25 o -10 7 10 422.98 396.61 35.34 o -9 7 10 680.22 731.79 39.48 o -8 7 10 9.57 24.94 10.70 o -7 7 10 433.38 417.57 28.58 o -6 7 10 147.52 167.03 22.58 o -5 7 10 1560.32 1472.59 42.09 o -4 7 10 345.40 345.04 23.96 o -3 7 10 124.68 114.79 12.06 o -2 7 10 230.59 229.24 16.08 o -1 7 10 187.78 196.22 17.99 o 0 7 10 792.16 829.36 30.80 o 1 7 10 690.80 686.32 32.71 o 2 7 10 1960.80 1932.25 45.83 o 3 7 10 171.82 182.95 19.97 o 4 7 10 200.97 180.84 19.69 o 5 7 10 349.94 346.60 23.95 o 6 7 10 173.68 163.05 18.61 o 7 7 10 330.85 388.83 25.34 o 8 7 10 179.43 206.14 18.98 o 9 7 10 111.40 89.08 13.82 o 10 7 10 31.89 26.53 11.17 o 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