#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:21:37 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180854 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/85/2018570.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018570_Fobs loop_ _publ_author_name 'Broomfield, Lewis M.' 'Bochmann, Manfred' 'Wright, Joseph A.' _publ_section_title ; Tris[3,6-di-tert-butyl-1-(isoquinolin-1-yl)naphthalen-2-olato-\k^2^N,O]aluminium(III) toluene sesquisolvate ; _journal_coeditor_code GZ3214 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m226 _journal_page_last m228 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 75.217 _cell_angle_beta 75.262 _cell_angle_gamma 74.200 _cell_length_a 13.0728 _cell_length_b 15.9452 _cell_length_c 19.4565 _exptl_crystal_F_000 1406.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file gz3214Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2007SRC0759 IN P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 195.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9639.15 9671.89 365.15 o 3 0 0 700.36 789.62 20.13 o 4 0 0 75.92 114.53 11.60 o 5 0 0 2716.25 3004.95 67.80 o 6 0 0 1442.08 1732.37 57.16 o 7 0 0 3139.47 3061.93 89.14 o 8 0 0 124.87 157.31 11.99 o 9 0 0 404.35 375.79 16.71 o 10 0 0 33.67 61.92 14.13 o 11 0 0 2389.21 2448.70 96.55 o 12 0 0 21.54 0.00 24.77 o 13 0 0 123.37 156.80 23.20 o 14 0 0 123.42 163.06 34.69 o 15 0 0 17.66 46.33 16.22 o 16 0 0 17.11 36.38 22.68 o -15 1 0 12.21 0.00 20.51 o -14 1 0 198.29 203.63 20.23 o -13 1 0 98.08 113.67 16.81 o -12 1 0 25.57 2.60 17.59 o -11 1 0 2178.74 1989.41 98.26 o -10 1 0 12.21 0.00 15.08 o -9 1 0 1411.34 1368.84 41.86 o -8 1 0 90.91 88.40 9.74 o -7 1 0 557.16 520.11 22.45 o -6 1 0 2197.85 2358.77 71.10 o -5 1 0 646.20 465.57 12.96 o -4 1 0 2924.46 2711.94 53.81 o -3 1 0 700.73 742.04 15.98 o 2 1 0 919.49 956.55 36.20 o 3 1 0 11156.95 10250.90 201.47 o 4 1 0 25367.33 24340.49 491.36 o 5 1 0 3354.86 3370.35 61.94 o 6 1 0 1786.29 1795.60 42.80 o 7 1 0 1032.32 1046.31 30.36 o 8 1 0 438.94 346.64 17.79 o 9 1 0 1003.16 971.99 30.03 o 10 1 0 226.59 189.77 15.43 o 11 1 0 3487.08 3498.20 152.83 o 12 1 0 13.66 1.11 17.16 o 13 1 0 77.23 75.40 18.88 o 14 1 0 50.52 15.70 18.95 o 15 1 0 231.27 235.89 25.03 o 16 1 0 0.71 25.64 18.92 o -15 2 0 0.08 0.00 15.66 o -14 2 0 133.16 124.91 27.28 o -13 2 0 264.54 273.49 22.64 o -12 2 0 29.07 8.21 18.63 o -11 2 0 160.93 187.68 20.45 o -10 2 0 149.12 194.67 20.16 o -9 2 0 2007.30 1834.18 68.40 o -8 2 0 352.40 330.79 15.00 o -7 2 0 427.34 354.92 9.93 o -6 2 0 775.46 729.94 17.69 o -5 2 0 869.72 784.79 21.11 o -4 2 0 117.60 189.55 8.68 o -3 2 0 214.53 304.97 10.41 o -2 2 0 0.21 0.00 4.38 o -1 2 0 822.33 900.15 29.58 o 2 2 0 5177.81 5024.06 132.21 o 3 2 0 26057.37 25133.33 524.39 o 4 2 0 1057.38 1228.74 28.02 o 5 2 0 7098.74 7265.81 137.60 o 6 2 0 13.33 36.19 6.18 o 7 2 0 33.95 103.96 6.59 o 8 2 0 145.50 164.92 12.27 o 9 2 0 302.42 379.54 17.40 o 10 2 0 258.44 312.57 20.73 o 11 2 0 87.15 77.66 12.97 o 12 2 0 311.12 359.16 39.40 o 13 2 0 39.90 17.74 17.18 o 14 2 0 98.11 112.95 17.46 o 15 2 0 884.25 1115.70 65.41 o 16 2 0 74.37 124.06 20.86 o -15 3 0 24.44 6.24 33.51 o -14 3 0 27.82 17.01 17.18 o -13 3 0 16.50 36.42 16.63 o -12 3 0 99.39 114.25 15.75 o -11 3 0 14.04 67.94 21.92 o -10 3 0 130.32 89.36 17.34 o -9 3 0 580.91 591.80 23.65 o -8 3 0 12.48 0.00 3.40 o -7 3 0 7.06 44.26 8.20 o -6 3 0 224.62 311.25 12.83 o -5 3 0 249.66 290.18 10.24 o -4 3 0 367.53 350.57 11.20 o -3 3 0 869.74 807.97 19.95 o -2 3 0 1046.86 1067.09 26.76 o -1 3 0 105.91 83.55 6.65 o 0 3 0 3276.51 3610.91 118.35 o 1 3 0 38406.53 35520.96 1034.87 o 2 3 0 23439.70 22318.92 460.14 o 3 3 0 1401.72 1507.72 28.84 o 4 3 0 5334.03 5520.67 104.13 o 5 3 0 145.01 165.47 8.15 o 6 3 0 31770.31 33894.05 678.71 o 7 3 0 171.81 220.69 9.06 o 8 3 0 270.29 268.42 9.01 o 9 3 0 39.88 67.26 5.05 o 10 3 0 7.13 11.14 12.73 o 11 3 0 5.99 0.00 24.80 o 12 3 0 136.75 111.14 29.50 o 13 3 0 221.39 206.88 24.92 o 14 3 0 708.96 795.11 51.84 o 15 3 0 134.92 169.31 20.71 o 16 3 0 27.10 64.01 13.93 o -14 4 0 94.83 63.00 18.31 o -13 4 0 42.24 116.72 18.58 o -12 4 0 11.86 0.00 16.97 o -11 4 0 160.42 208.04 23.97 o -10 4 0 194.11 96.44 19.09 o -9 4 0 18.09 10.63 3.80 o -8 4 0 38.16 28.70 5.63 o -7 4 0 40.19 16.01 5.61 o -6 4 0 99.31 119.14 6.78 o -5 4 0 2391.77 2547.03 51.66 o -4 4 0 2465.40 2822.16 57.46 o -3 4 0 17.38 4.70 5.51 o -2 4 0 532.76 486.84 13.44 o -1 4 0 1004.69 950.24 27.51 o 0 4 0 222.06 201.35 14.31 o 1 4 0 821.05 786.08 22.70 o 2 4 0 6.78 10.30 7.23 o 3 4 0 28.88 25.94 7.68 o 4 4 0 255.59 328.28 9.68 o 5 4 0 379.06 334.39 10.10 o 6 4 0 30616.04 33207.96 643.60 o 7 4 0 379.26 389.82 13.54 o 8 4 0 1776.26 1846.81 41.67 o 9 4 0 0.65 3.30 6.08 o 10 4 0 10.09 0.00 4.51 o 11 4 0 11.57 12.18 15.26 o 12 4 0 316.88 261.87 21.98 o 13 4 0 108.39 77.67 20.72 o 14 4 0 153.75 185.47 29.94 o 15 4 0 46.08 46.31 21.04 o 16 4 0 67.35 79.27 17.77 o -14 5 0 50.20 47.22 35.15 o -13 5 0 6.36 0.00 15.63 o -12 5 0 295.29 379.94 38.10 o -11 5 0 112.34 138.62 29.93 o -10 5 0 191.67 134.08 9.01 o -9 5 0 350.04 372.89 13.61 o -8 5 0 748.30 706.25 26.37 o -7 5 0 98.49 145.88 9.73 o -6 5 0 116.86 117.54 7.45 o -5 5 0 213.53 166.38 7.49 o -4 5 0 6717.90 7402.16 149.93 o -3 5 0 2883.75 2756.20 58.57 o -2 5 0 30.11 77.08 10.23 o -1 5 0 1494.59 1509.54 46.63 o 0 5 0 3906.39 3718.75 114.28 o 1 5 0 4441.38 4536.58 253.93 o 2 5 0 273.98 211.12 7.96 o 3 5 0 7561.03 7173.61 137.47 o 4 5 0 1187.47 1307.10 27.58 o 5 5 0 795.92 744.10 16.44 o 6 5 0 373.11 264.82 21.89 o 7 5 0 424.55 389.72 11.72 o 8 5 0 14.51 34.48 8.30 o 9 5 0 435.78 399.80 15.56 o 10 5 0 0.22 0.00 9.92 o 11 5 0 22.91 15.04 6.80 o 12 5 0 25.82 24.64 12.77 o 13 5 0 25.50 25.88 14.97 o 14 5 0 358.00 349.46 39.91 o 15 5 0 9.03 42.07 28.32 o 16 5 0 3.56 0.00 19.35 o -14 6 0 0.02 36.63 27.98 o -13 6 0 19.07 0.00 46.45 o -12 6 0 29.39 0.00 16.46 o -11 6 0 2.36 12.95 13.53 o -10 6 0 1685.54 1482.65 55.46 o -9 6 0 60.68 33.50 6.90 o -8 6 0 591.68 628.91 18.74 o -7 6 0 600.14 588.81 15.66 o -6 6 0 80.41 63.87 5.97 o -5 6 0 33.05 31.80 6.04 o -4 6 0 601.00 622.33 16.69 o -3 6 0 233.08 275.54 12.29 o -2 6 0 15.08 5.35 7.73 o -1 6 0 445.15 459.62 17.33 o 0 6 0 3.45 0.00 9.65 o 1 6 0 1141.70 1210.95 37.22 o 2 6 0 101.29 43.94 9.31 o 3 6 0 0.01 31.53 6.24 o 4 6 0 0.14 18.04 7.60 o 5 6 0 242.45 261.98 12.86 o 6 6 0 217.63 83.53 9.28 o 7 6 0 293.43 365.76 11.15 o 8 6 0 21.98 62.37 6.72 o 9 6 0 14.44 41.13 6.24 o 10 6 0 7.55 23.75 10.67 o 11 6 0 0.07 17.92 10.32 o 12 6 0 301.40 267.45 11.13 o 13 6 0 399.39 398.11 42.14 o 14 6 0 9.99 94.00 23.65 o 15 6 0 12.20 0.00 25.22 o 16 6 0 23.29 0.00 19.57 o -13 7 0 31.37 23.40 59.47 o -12 7 0 15.75 0.00 14.26 o -11 7 0 15.23 10.64 18.10 o -10 7 0 316.90 314.15 21.26 o -9 7 0 288.71 277.52 11.80 o -8 7 0 530.03 472.69 21.78 o -7 7 0 530.85 467.23 14.39 o -6 7 0 51.68 50.96 7.89 o -5 7 0 2.99 1.93 4.77 o -4 7 0 2.13 1.56 10.23 o -3 7 0 580.11 573.53 18.42 o -2 7 0 50.58 75.76 7.58 o -1 7 0 54.60 40.75 16.85 o 0 7 0 48.36 27.77 6.36 o 1 7 0 8036.80 9076.13 247.31 o 2 7 0 293.44 296.70 19.09 o 3 7 0 25.41 31.39 8.92 o 4 7 0 24.62 19.94 7.17 o 5 7 0 163.16 134.76 8.17 o 6 7 0 199.13 133.76 10.61 o 7 7 0 204.91 148.15 12.56 o 8 7 0 1615.67 1666.26 40.87 o 9 7 0 177.73 139.25 7.70 o 10 7 0 2.49 7.30 11.33 o 11 7 0 2.82 18.60 8.27 o 12 7 0 33.58 4.03 18.13 o 13 7 0 239.37 179.51 13.29 o 14 7 0 15.20 58.98 20.75 o 15 7 0 132.45 158.03 25.59 o 16 7 0 0.36 0.00 22.94 o -13 8 0 51.19 62.04 59.74 o -12 8 0 43.98 23.75 28.59 o -11 8 0 133.08 156.22 12.10 o -10 8 0 98.51 77.82 13.11 o -9 8 0 19.24 10.61 7.24 o -8 8 0 32.56 49.67 6.64 o -7 8 0 593.00 506.09 21.68 o -6 8 0 286.17 241.73 10.83 o -5 8 0 41.26 58.19 8.02 o -4 8 0 760.83 753.63 23.05 o -3 8 0 437.43 460.31 17.48 o -2 8 0 440.89 377.08 14.80 o -1 8 0 720.74 681.58 26.45 o 0 8 0 28.94 31.99 9.77 o 1 8 0 3.47 59.86 9.65 o 2 8 0 478.32 513.91 22.79 o 3 8 0 288.30 279.64 20.91 o 4 8 0 125.03 74.37 10.84 o 5 8 0 1746.55 1655.66 37.29 o 6 8 0 45.05 18.60 8.69 o 7 8 0 92.37 104.51 10.25 o 8 8 0 472.57 466.26 15.28 o 9 8 0 33.04 18.28 7.19 o 10 8 0 261.63 206.98 11.24 o 11 8 0 6.17 5.49 9.34 o 12 8 0 127.09 105.58 9.79 o 13 8 0 47.85 69.70 14.36 o 14 8 0 41.76 17.77 18.14 o 15 8 0 1.01 13.10 27.34 o 16 8 0 95.62 99.72 28.49 o -12 9 0 0.00 171.75 64.14 o -11 9 0 0.04 14.26 32.61 o -10 9 0 4.10 26.72 7.29 o -9 9 0 48.87 30.63 7.90 o -8 9 0 328.06 270.41 12.90 o -7 9 0 238.98 223.01 10.36 o -6 9 0 160.49 175.77 11.37 o -5 9 0 5.08 10.08 9.37 o -4 9 0 20.70 33.65 9.13 o -3 9 0 72.99 46.96 9.27 o -2 9 0 916.70 898.13 30.93 o -1 9 0 1290.49 1150.02 38.05 o 0 9 0 899.70 811.34 26.96 o 1 9 0 34.33 35.95 4.78 o 2 9 0 392.29 412.65 18.40 o 3 9 0 1091.46 1208.71 33.45 o 4 9 0 287.46 305.62 15.28 o 5 9 0 331.53 290.75 12.43 o 6 9 0 1333.31 1309.43 32.53 o 7 9 0 33.36 34.07 8.58 o 8 9 0 1199.19 1161.60 34.71 o 9 9 0 149.61 117.57 8.98 o 10 9 0 574.02 505.58 22.16 o 11 9 0 34.05 30.72 6.95 o 12 9 0 97.80 83.08 12.20 o 13 9 0 678.20 739.60 40.47 o 14 9 0 131.17 118.81 17.19 o 15 9 0 0.19 8.34 17.09 o -12 10 0 135.89 215.89 38.97 o -11 10 0 155.43 161.29 30.91 o -10 10 0 76.58 77.74 21.54 o -9 10 0 34.54 0.00 14.98 o -8 10 0 71.40 36.22 9.18 o -7 10 0 11.07 0.00 9.60 o -6 10 0 336.44 298.32 18.36 o -5 10 0 360.47 393.65 20.51 o -4 10 0 2957.38 2978.89 102.47 o -3 10 0 11.92 31.36 24.20 o -2 10 0 457.47 440.15 28.07 o -1 10 0 239.14 201.85 19.29 o 0 10 0 191.40 205.07 11.07 o 1 10 0 1211.62 1155.67 31.47 o 2 10 0 723.75 578.14 27.45 o 3 10 0 478.30 584.98 22.33 o 4 10 0 0.26 0.00 10.18 o 5 10 0 1341.79 1273.83 33.96 o 6 10 0 173.01 134.35 8.83 o 7 10 0 3578.09 3522.35 83.63 o 8 10 0 267.98 251.86 14.44 o 9 10 0 86.89 53.82 8.80 o 10 10 0 7.68 0.00 8.69 o 11 10 0 1.14 0.00 10.91 o 12 10 0 274.08 213.30 16.87 o 13 10 0 2.54 14.26 10.85 o 14 10 0 31.28 75.54 21.58 o 15 10 0 0.63 0.00 37.22 o -11 11 0 10.37 54.77 16.79 o -10 11 0 11.28 1.65 18.46 o -9 11 0 1.40 12.04 15.18 o -8 11 0 44.88 26.45 16.05 o -7 11 0 65.04 36.77 9.22 o -6 11 0 12.61 0.00 10.81 o -5 11 0 1.89 37.76 15.82 o -4 11 0 193.94 127.40 21.27 o -3 11 0 2517.49 2520.97 111.17 o -2 11 0 732.67 705.79 31.92 o -1 11 0 195.12 205.05 16.93 o 0 11 0 174.36 217.26 11.25 o 1 11 0 476.31 454.45 16.73 o 2 11 0 57.22 64.32 9.62 o 3 11 0 5.73 45.94 11.87 o 4 11 0 51.87 57.19 14.07 o 5 11 0 0.52 0.00 8.31 o 6 11 0 704.34 729.04 25.15 o 7 11 0 5381.07 5447.31 126.00 o 8 11 0 27.71 6.26 9.30 o 9 11 0 11.68 0.76 8.25 o 10 11 0 56.61 46.10 9.58 o 11 11 0 0.40 3.52 8.14 o 12 11 0 98.67 21.34 17.44 o 13 11 0 29.96 27.12 10.64 o 14 11 0 64.15 66.90 31.02 o 15 11 0 5.68 0.00 16.42 o -10 12 0 306.18 276.77 28.57 o -9 12 0 8.60 40.76 25.12 o -8 12 0 2.73 53.70 21.92 o -7 12 0 0.42 21.93 11.41 o -6 12 0 61.74 19.93 15.73 o -5 12 0 297.16 241.04 19.40 o -4 12 0 2937.33 3213.18 112.89 o -3 12 0 222.14 227.20 19.44 o -2 12 0 144.03 183.02 19.39 o -1 12 0 178.95 169.50 26.03 o 0 12 0 14.40 20.89 27.09 o 1 12 0 184.92 159.47 10.31 o 2 12 0 0.19 0.00 11.75 o 3 12 0 410.44 404.41 18.08 o 4 12 0 111.85 149.08 17.41 o 5 12 0 138.41 148.45 10.76 o 6 12 0 3.01 0.00 8.36 o 7 12 0 4.76 0.00 9.49 o 8 12 0 10.63 16.80 11.47 o 9 12 0 148.15 117.38 9.98 o 10 12 0 0.86 15.59 9.62 o 11 12 0 4.11 23.56 9.27 o 12 12 0 128.09 108.73 17.80 o 13 12 0 0.82 13.91 14.40 o 14 12 0 0.07 25.27 12.21 o 15 12 0 39.97 58.78 22.02 o -9 13 0 97.99 148.09 19.05 o -8 13 0 1.51 0.00 35.73 o -7 13 0 24.32 55.38 23.34 o -6 13 0 1.65 0.00 12.50 o -5 13 0 102.44 101.68 20.51 o -4 13 0 952.87 907.96 42.06 o -3 13 0 516.18 609.27 30.92 o -2 13 0 1031.68 858.28 45.06 o -1 13 0 61.47 63.33 14.95 o 0 13 0 103.14 53.79 15.99 o 1 13 0 54.68 35.25 9.93 o 2 13 0 0.22 0.00 8.34 o 3 13 0 606.08 636.09 23.29 o 4 13 0 0.20 0.00 13.29 o 5 13 0 360.38 362.08 25.80 o 6 13 0 74.22 64.27 8.30 o 7 13 0 253.91 203.45 14.74 o 8 13 0 17.70 35.37 15.13 o 9 13 0 496.17 564.69 23.95 o 10 13 0 51.93 65.36 15.20 o 11 13 0 31.70 59.65 13.32 o 12 13 0 48.47 34.43 15.11 o 13 13 0 221.27 242.42 18.04 o 14 13 0 0.25 27.90 45.57 o -8 14 0 79.42 106.23 25.20 o -7 14 0 366.62 444.00 53.88 o -6 14 0 0.61 0.00 27.12 o -5 14 0 73.95 52.67 18.55 o -4 14 0 13.81 29.12 18.08 o -3 14 0 13.07 0.00 20.59 o -2 14 0 283.96 426.32 44.80 o -1 14 0 87.98 85.96 17.79 o 0 14 0 835.22 865.65 47.88 o 1 14 0 444.42 432.86 25.03 o 2 14 0 0.96 63.93 20.27 o 3 14 0 184.65 143.29 11.21 o 4 14 0 53.27 74.38 20.81 o 5 14 0 394.40 373.44 22.22 o 6 14 0 80.09 87.27 13.17 o 7 14 0 1086.69 1051.87 39.29 o 8 14 0 493.18 559.61 30.29 o 9 14 0 62.28 39.21 18.70 o 10 14 0 22.98 26.74 13.77 o 11 14 0 169.80 176.63 20.02 o 12 14 0 74.47 106.84 18.67 o 13 14 0 578.58 687.23 37.43 o 14 14 0 7.71 64.91 36.95 o -7 15 0 106.77 242.21 43.88 o -6 15 0 23.85 9.49 26.03 o -5 15 0 165.33 181.86 24.34 o -4 15 0 224.29 265.77 20.03 o -3 15 0 24.64 22.14 23.23 o -2 15 0 19.93 0.00 26.15 o -1 15 0 145.13 231.04 27.80 o 0 15 0 86.06 32.32 32.35 o 1 15 0 131.06 146.32 10.48 o 2 15 0 163.17 119.79 9.81 o 3 15 0 293.77 220.42 21.29 o 4 15 0 42.67 51.18 10.13 o 5 15 0 170.76 54.05 11.44 o 6 15 0 100.37 96.99 16.99 o 7 15 0 383.42 401.03 27.35 o 8 15 0 63.84 53.84 15.07 o 9 15 0 4.63 16.65 18.20 o 10 15 0 13.00 36.56 23.16 o 11 15 0 4.68 64.26 32.65 o 12 15 0 23.77 51.42 17.27 o 13 15 0 137.58 130.43 23.42 o -5 16 0 12.22 50.45 35.08 o -4 16 0 614.83 671.39 38.18 o -3 16 0 47.74 14.89 15.20 o -2 16 0 370.74 390.84 31.07 o -1 16 0 2.83 6.21 15.24 o 0 16 0 8.31 0.00 17.43 o 1 16 0 134.02 102.93 13.71 o 2 16 0 549.94 546.50 24.17 o 3 16 0 72.58 56.18 10.78 o 4 16 0 423.86 364.17 23.43 o 5 16 0 80.91 120.16 20.32 o 6 16 0 18.35 46.74 16.64 o 7 16 0 21.62 0.00 19.20 o 8 16 0 69.68 78.92 16.41 o 9 16 0 21.79 0.07 12.67 o 10 16 0 20.10 15.31 14.74 o 11 16 0 38.93 63.45 23.40 o 12 16 0 28.01 44.36 14.97 o -5 17 0 9.43 69.02 22.08 o -4 17 0 19.76 45.80 20.07 o -3 17 0 37.17 72.74 19.90 o -2 17 0 49.94 95.19 17.60 o -1 17 0 292.02 317.92 30.44 o 0 17 0 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-17 2 0.58 25.30 15.14 o -8 -17 2 337.76 362.46 29.98 o -7 -17 2 0.01 15.22 30.24 o -6 -17 2 34.39 0.00 20.37 o -5 -17 2 0.36 64.39 37.33 o -4 -17 2 6.91 0.00 72.11 o -3 -17 2 17.46 0.00 29.56 o -2 -17 2 321.46 473.30 56.19 o -1 -17 2 303.41 433.79 63.91 o 0 -17 2 10.91 1.04 27.70 o 1 -17 2 0.44 81.74 65.14 o 2 -17 2 158.73 217.51 37.33 o 3 -17 2 67.03 74.79 38.49 o 4 -17 2 110.05 111.18 35.77 o -11 -16 2 0.02 44.54 47.33 o -10 -16 2 259.60 240.28 27.49 o -9 -16 2 7.40 42.35 14.40 o -8 -16 2 0.83 0.00 10.79 o -7 -16 2 128.60 147.73 22.93 o -6 -16 2 61.11 38.30 12.59 o -5 -16 2 7.64 22.85 13.95 o -4 -16 2 69.61 65.91 11.12 o -3 -16 2 178.48 156.61 21.27 o -2 -16 2 159.38 137.75 11.28 o -1 -16 2 29.00 25.65 50.53 o 0 -16 2 21.61 0.00 26.49 o 1 -16 2 174.18 164.51 45.03 o 2 -16 2 37.68 90.07 61.31 o 3 -16 2 23.81 39.50 32.23 o 4 -16 2 244.47 204.29 37.50 o 5 -16 2 54.93 60.16 16.59 o 6 -16 2 0.23 63.05 43.44 o -12 -15 2 26.06 111.44 57.79 o -11 -15 2 66.63 41.92 21.58 o -10 -15 2 23.76 57.48 23.98 o -9 -15 2 631.40 646.02 40.35 o -8 -15 2 8.46 11.14 11.27 o -7 -15 2 2.13 2.57 12.81 o -6 -15 2 0.55 0.00 20.59 o -5 -15 2 113.79 92.19 15.42 o -4 -15 2 106.63 110.15 14.20 o -3 -15 2 302.41 306.51 20.07 o -2 -15 2 186.35 133.08 10.46 o -1 -15 2 8.66 71.84 28.19 o 0 -15 2 9.59 0.00 31.48 o 1 -15 2 38.46 9.60 27.48 o 2 -15 2 202.47 270.29 64.89 o 3 -15 2 36.68 0.00 27.08 o 4 -15 2 210.33 231.22 39.40 o 5 -15 2 78.99 191.17 44.88 o 6 -15 2 18.65 32.07 15.55 o 7 -15 2 141.12 129.89 34.62 o -13 -14 2 141.29 198.03 27.02 o -12 -14 2 52.42 37.23 24.76 o -11 -14 2 61.24 35.04 22.23 o -10 -14 2 40.82 44.51 26.21 o -9 -14 2 5.58 22.84 10.94 o -8 -14 2 67.72 80.01 12.42 o -7 -14 2 630.75 692.08 26.17 o -6 -14 2 120.45 63.61 17.11 o -5 -14 2 24.66 0.00 10.57 o -4 -14 2 57.51 22.99 9.42 o -3 -14 2 62.00 70.97 7.21 o -2 -14 2 22.43 0.00 6.75 o -1 -14 2 210.80 186.28 17.12 o 0 -14 2 2.44 19.44 7.58 o 1 -14 2 128.90 125.97 25.02 o 2 -14 2 469.73 454.18 34.39 o 3 -14 2 170.77 159.72 15.01 o 4 -14 2 3.36 0.00 24.23 o 5 -14 2 168.52 177.93 24.09 o 6 -14 2 105.49 148.59 38.26 o 7 -14 2 10.32 0.00 22.67 o 8 -14 2 17.26 0.00 19.32 o -13 -13 2 1154.78 1462.48 108.73 o -12 -13 2 156.04 156.25 31.13 o -11 -13 2 555.26 682.68 36.19 o -10 -13 2 25.05 23.97 26.23 o -9 -13 2 5.23 3.17 8.19 o -8 -13 2 402.54 408.89 19.94 o -7 -13 2 425.62 444.60 18.01 o -6 -13 2 7.07 0.00 5.13 o -5 -13 2 71.87 50.18 5.80 o -4 -13 2 0.76 0.00 12.22 o -3 -13 2 207.06 212.34 8.69 o -2 -13 2 223.40 150.88 11.02 o -1 -13 2 56.75 55.44 12.04 o 0 -13 2 265.27 229.72 14.52 o 1 -13 2 275.37 259.04 28.67 o 2 -13 2 5.64 9.35 11.38 o 3 -13 2 541.05 498.09 36.04 o 4 -13 2 316.10 321.78 32.52 o 5 -13 2 259.54 298.81 21.31 o 6 -13 2 7.84 48.14 42.81 o 7 -13 2 0.19 0.00 13.28 o 8 -13 2 0.15 15.23 21.13 o 9 -13 2 43.94 0.00 17.04 o -14 -12 2 0.77 17.68 20.07 o -13 -12 2 198.85 203.24 24.13 o -12 -12 2 293.75 336.20 25.07 o -11 -12 2 31.88 16.46 12.12 o -10 -12 2 52.55 67.93 9.62 o -9 -12 2 109.71 87.75 8.66 o -8 -12 2 29.89 0.00 13.28 o -7 -12 2 140.59 153.08 10.85 o -6 -12 2 460.75 434.27 17.11 o -5 -12 2 42.35 36.30 9.90 o -4 -12 2 312.96 302.48 12.48 o -3 -12 2 440.76 472.70 19.43 o -2 -12 2 21.29 36.06 8.29 o -1 -12 2 12.89 0.00 11.74 o 0 -12 2 762.01 748.16 31.48 o 1 -12 2 89.14 88.40 14.76 o 2 -12 2 211.53 212.12 21.08 o 3 -12 2 2.68 0.00 15.08 o 4 -12 2 813.65 893.18 42.44 o 5 -12 2 156.56 134.07 22.65 o 6 -12 2 15.59 16.66 11.07 o 7 -12 2 213.00 223.45 25.83 o 8 -12 2 122.19 118.09 26.37 o 9 -12 2 5.79 0.00 22.42 o 10 -12 2 40.50 68.35 24.51 o -14 -11 2 41.04 0.00 14.09 o -13 -11 2 2.83 12.64 21.98 o -12 -11 2 100.07 67.47 14.58 o -11 -11 2 0.58 6.20 10.79 o -10 -11 2 631.52 649.12 23.23 o -9 -11 2 144.44 142.27 10.16 o -8 -11 2 277.18 277.57 16.62 o -7 -11 2 701.35 743.94 22.05 o -6 -11 2 683.49 633.79 20.65 o -5 -11 2 37.38 11.71 7.65 o -4 -11 2 29.36 41.03 6.41 o -3 -11 2 127.72 141.56 12.07 o -2 -11 2 84.32 78.14 8.57 o -1 -11 2 537.54 558.29 16.85 o 0 -11 2 4.91 0.00 9.79 o 1 -11 2 666.82 693.93 43.44 o 2 -11 2 2231.31 2249.95 89.17 o 3 -11 2 3482.24 3477.38 125.55 o 4 -11 2 854.84 761.30 50.53 o 5 -11 2 295.10 293.55 17.99 o 6 -11 2 142.92 128.41 15.53 o 7 -11 2 4.22 0.00 10.74 o 8 -11 2 16.01 25.19 20.85 o 9 -11 2 173.20 252.72 33.46 o 10 -11 2 102.35 146.47 37.57 o 11 -11 2 15.41 33.14 26.91 o -15 -10 2 77.43 110.09 33.85 o -14 -10 2 5.07 1.05 21.04 o -13 -10 2 129.58 117.66 16.30 o -12 -10 2 0.22 0.00 10.78 o -11 -10 2 173.25 139.90 10.57 o -10 -10 2 164.52 149.68 11.14 o -9 -10 2 329.50 335.82 13.27 o -8 -10 2 575.04 557.20 19.87 o -7 -10 2 4668.42 4709.56 117.19 o -6 -10 2 3838.68 3775.14 88.26 o -5 -10 2 1860.71 1782.06 41.78 o -4 -10 2 844.48 809.24 20.69 o -3 -10 2 163.32 160.94 7.50 o -2 -10 2 82.50 109.23 9.25 o -1 -10 2 485.93 538.96 16.81 o 0 -10 2 82.12 104.08 7.54 o 1 -10 2 448.65 418.88 25.70 o 2 -10 2 8.84 0.00 11.12 o 3 -10 2 723.49 735.44 25.22 o 4 -10 2 93.04 80.31 11.35 o 5 -10 2 776.83 735.53 35.40 o 6 -10 2 0.00 0.00 18.37 o 7 -10 2 230.47 172.05 15.50 o 8 -10 2 175.37 143.29 15.64 o 9 -10 2 363.07 414.21 27.20 o 10 -10 2 10.35 30.72 22.51 o 11 -10 2 255.75 154.15 23.21 o 12 -10 2 16.87 19.58 15.79 o -15 -9 2 57.77 49.59 31.29 o -14 -9 2 2.20 23.28 33.89 o -13 -9 2 1.67 15.92 9.78 o -12 -9 2 100.26 82.07 16.89 o -11 -9 2 412.42 388.70 18.89 o -10 -9 2 0.62 11.24 8.18 o -9 -9 2 625.55 586.33 19.15 o -8 -9 2 100.49 109.97 9.22 o -7 -9 2 4333.31 4447.93 99.49 o -6 -9 2 2988.03 2846.33 63.87 o -5 -9 2 142.89 129.57 9.07 o -4 -9 2 298.59 266.86 11.97 o -3 -9 2 73.25 77.85 10.19 o -2 -9 2 3504.34 3663.09 77.43 o -1 -9 2 656.97 702.10 22.39 o 0 -9 2 497.19 549.27 18.73 o 1 -9 2 180.00 172.60 15.57 o 2 -9 2 1208.55 1309.72 46.11 o 3 -9 2 52.88 49.93 11.98 o 4 -9 2 1860.01 1746.64 57.11 o 5 -9 2 470.06 444.60 18.10 o 6 -9 2 632.08 604.67 30.26 o 7 -9 2 354.29 378.65 14.67 o 8 -9 2 516.10 480.27 21.46 o 9 -9 2 612.02 561.47 29.48 o 10 -9 2 116.69 104.42 23.42 o 11 -9 2 86.48 203.57 46.60 o 12 -9 2 130.33 114.60 17.73 o -15 -8 2 29.38 53.80 29.52 o -14 -8 2 9.78 16.75 15.42 o -13 -8 2 4.94 0.00 22.00 o -12 -8 2 90.30 52.42 11.01 o -11 -8 2 88.17 82.94 10.64 o -10 -8 2 60.79 65.12 8.32 o -9 -8 2 394.41 355.10 11.73 o -8 -8 2 32.34 33.07 9.51 o -7 -8 2 2.64 0.00 9.10 o -6 -8 2 684.68 716.27 18.18 o -5 -8 2 833.35 810.76 20.23 o -4 -8 2 465.58 490.12 16.56 o -3 -8 2 2778.21 2731.09 58.44 o -2 -8 2 4300.72 4506.62 96.51 o -1 -8 2 21.13 11.24 7.36 o 0 -8 2 650.06 663.99 22.95 o 1 -8 2 2.32 0.00 13.40 o 2 -8 2 99.57 43.24 10.89 o 3 -8 2 41.11 15.98 10.93 o 4 -8 2 936.76 916.97 35.78 o 5 -8 2 763.49 820.92 26.59 o 6 -8 2 55.16 50.42 5.63 o 7 -8 2 461.57 424.34 15.76 o 8 -8 2 43.13 70.89 10.17 o 9 -8 2 712.65 661.31 24.13 o 10 -8 2 196.42 156.09 17.00 o 11 -8 2 9.78 50.17 21.36 o 12 -8 2 6.30 39.77 30.11 o 13 -8 2 2.41 0.00 55.22 o -15 -7 2 1.46 0.00 25.77 o -14 -7 2 12.70 0.00 16.03 o -13 -7 2 14.56 0.00 11.96 o -12 -7 2 394.18 315.87 15.20 o -11 -7 2 51.80 11.08 11.87 o -10 -7 2 57.07 56.90 9.04 o -9 -7 2 48.52 45.38 6.47 o -8 -7 2 41.70 42.19 7.17 o -7 -7 2 51.38 87.19 7.93 o -6 -7 2 292.33 316.94 10.36 o -5 -7 2 61.57 71.12 7.29 o -4 -7 2 68.09 30.01 5.89 o -3 -7 2 1369.24 1537.70 32.59 o -2 -7 2 76.23 85.44 8.20 o -1 -7 2 841.75 784.85 19.39 o 0 -7 2 3260.58 3077.11 81.67 o 1 -7 2 0.03 25.53 11.63 o 2 -7 2 446.44 485.44 21.78 o 3 -7 2 60.06 65.38 10.29 o 4 -7 2 1801.45 1828.17 44.98 o 5 -7 2 10.85 24.18 8.42 o 6 -7 2 23.53 38.27 12.48 o 7 -7 2 219.14 206.16 9.55 o 8 -7 2 17.49 11.02 6.68 o 9 -7 2 3620.97 3371.68 92.10 o 10 -7 2 101.46 84.58 7.51 o 11 -7 2 193.51 173.96 15.59 o 12 -7 2 130.24 180.67 15.41 o 13 -7 2 21.64 73.97 32.64 o -15 -6 2 42.61 15.40 21.29 o -14 -6 2 10.91 60.94 25.60 o -13 -6 2 6.79 0.00 17.25 o -12 -6 2 278.13 257.40 13.53 o -11 -6 2 89.50 44.00 10.37 o -10 -6 2 58.13 57.44 6.94 o -9 -6 2 20.77 40.38 7.96 o -8 -6 2 509.50 507.51 14.13 o -7 -6 2 35.02 27.57 6.30 o -6 -6 2 271.17 294.28 9.93 o -5 -6 2 739.29 686.62 21.60 o -4 -6 2 891.26 942.04 19.90 o -3 -6 2 264.90 287.14 10.25 o -2 -6 2 691.58 788.64 19.39 o -1 -6 2 11596.39 12235.71 264.23 o 0 -6 2 354.89 416.96 15.09 o 1 -6 2 1404.44 1494.37 45.13 o 2 -6 2 3.40 0.00 3.97 o 3 -6 2 20.43 17.19 7.32 o 4 -6 2 641.60 550.81 18.76 o 5 -6 2 1164.34 1305.26 32.81 o 6 -6 2 102.23 107.90 9.63 o 7 -6 2 144.88 211.85 9.74 o 8 -6 2 139.71 97.40 8.29 o 9 -6 2 85.39 51.74 7.76 o 10 -6 2 1975.93 2028.53 67.23 o 11 -6 2 184.93 157.49 20.09 o 12 -6 2 8.88 3.67 7.33 o 13 -6 2 269.10 231.65 25.10 o 14 -6 2 31.34 38.83 18.47 o -16 -5 2 6.80 0.00 20.98 o -15 -5 2 169.33 92.10 32.60 o -14 -5 2 42.44 93.53 19.90 o -13 -5 2 121.14 125.11 37.85 o -12 -5 2 3.22 21.75 15.13 o -11 -5 2 6.43 5.85 5.77 o -10 -5 2 19.96 42.05 6.99 o -9 -5 2 75.40 45.65 11.41 o -8 -5 2 19.87 0.48 7.43 o -7 -5 2 1978.41 2204.00 46.88 o -6 -5 2 98.31 88.31 6.72 o -5 -5 2 23.52 23.03 6.15 o -4 -5 2 789.99 854.09 17.23 o -3 -5 2 63.27 66.71 6.01 o -2 -5 2 8924.45 8844.21 193.95 o -1 -5 2 1308.76 1359.43 33.84 o 0 -5 2 2498.61 2357.62 61.68 o 1 -5 2 166.34 201.86 7.90 o 2 -5 2 35.01 7.92 6.45 o 3 -5 2 28.68 0.00 6.59 o 4 -5 2 676.49 667.73 16.23 o 5 -5 2 294.34 307.75 12.06 o 6 -5 2 572.92 599.83 21.90 o 7 -5 2 432.19 437.72 14.96 o 8 -5 2 0.36 0.00 6.08 o 9 -5 2 161.40 167.46 9.64 o 10 -5 2 798.04 769.67 25.89 o 11 -5 2 1326.63 1356.68 44.90 o 12 -5 2 45.74 27.33 15.54 o 13 -5 2 93.81 100.63 19.07 o 14 -5 2 13.06 45.83 13.83 o -16 -4 2 212.03 161.83 39.02 o -15 -4 2 55.95 36.01 17.99 o -14 -4 2 902.32 1007.64 58.72 o -13 -4 2 124.63 137.92 21.33 o -12 -4 2 35.32 39.16 23.10 o -11 -4 2 47.22 61.37 16.21 o -10 -4 2 309.42 289.19 11.08 o -9 -4 2 263.13 276.85 11.24 o -8 -4 2 2.69 1.18 6.93 o -7 -4 2 1035.67 1115.16 24.42 o -6 -4 2 1768.69 1953.14 37.12 o -5 -4 2 2650.54 2508.03 46.62 o -4 -4 2 178.33 190.06 8.27 o -3 -4 2 533.00 570.49 15.96 o -2 -4 2 31.14 12.39 5.52 o -1 -4 2 1340.31 1349.33 33.06 o 0 -4 2 4792.62 4461.07 100.85 o 1 -4 2 2314.70 2272.53 50.25 o 2 -4 2 926.75 919.94 23.56 o 3 -4 2 153.06 139.86 8.28 o 4 -4 2 164.67 199.46 8.56 o 5 -4 2 2203.21 2589.23 54.13 o 6 -4 2 192.38 178.04 8.20 o 7 -4 2 326.54 304.41 11.08 o 8 -4 2 726.95 670.07 22.32 o 9 -4 2 195.91 173.99 9.94 o 10 -4 2 199.22 243.11 16.61 o 11 -4 2 340.59 423.98 29.03 o 12 -4 2 134.81 111.09 19.40 o 13 -4 2 144.54 132.98 23.50 o 14 -4 2 0.42 0.00 15.14 o 15 -4 2 1.24 10.03 27.97 o -16 -3 2 69.22 91.97 24.90 o -15 -3 2 1.74 0.00 15.56 o -14 -3 2 456.11 597.72 33.32 o -13 -3 2 198.82 106.33 22.69 o -12 -3 2 139.99 139.47 20.33 o -11 -3 2 0.66 0.00 25.04 o -10 -3 2 0.61 25.32 12.76 o -9 -3 2 41.18 44.50 4.51 o -8 -3 2 225.82 265.96 9.84 o -7 -3 2 1721.04 2017.06 45.75 o -6 -3 2 5802.98 6039.60 120.56 o -5 -3 2 1235.32 1278.41 24.09 o -4 -3 2 545.91 581.96 12.69 o -3 -3 2 565.03 494.66 11.41 o -2 -3 2 6524.74 6487.08 130.06 o -1 -3 2 15764.27 14931.16 349.01 o 0 -3 2 12841.15 11956.75 318.53 o 1 -3 2 631.67 592.21 15.64 o 2 -3 2 356.34 349.05 12.03 o 3 -3 2 156.21 102.69 10.07 o 4 -3 2 3.84 0.00 6.39 o 5 -3 2 570.10 626.05 17.34 o 6 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89.42 o 3 3 24 177.77 177.24 23.47 o 4 3 24 3.50 31.50 41.24 o 5 3 24 1.58 25.80 49.60 o 6 3 24 28.37 2.62 28.11 o 7 3 24 59.28 131.67 24.81 o 8 3 24 2.71 55.81 23.16 o -1 4 24 107.29 185.63 81.95 o 1 4 24 35.06 123.82 80.28 o 2 4 24 44.62 56.01 51.66 o 3 4 24 183.80 183.16 50.32 o 4 4 24 89.12 81.86 33.08 o 5 4 24 14.37 8.56 18.06 o 6 4 24 22.41 0.00 13.83 o 7 4 24 174.42 164.30 28.21 o 8 4 24 271.70 188.91 34.38 o 0 5 24 170.60 154.90 51.82 o 1 5 24 0.07 137.05 53.90 o 2 5 24 756.58 922.55 90.71 o 3 5 24 6.74 72.85 40.38 o 4 5 24 437.46 489.43 46.61 o 5 5 24 112.81 146.51 18.44 o 6 5 24 30.75 52.77 19.13 o 7 5 24 103.52 123.87 28.28 o 8 5 24 0.75 0.00 31.11 o 9 5 24 12.34 9.08 24.62 o 0 6 24 0.31 54.41 79.38 o 1 6 24 22.02 72.21 68.34 o 2 6 24 50.30 0.00 49.21 o 3 6 24 220.73 313.28 41.73 o 4 6 24 109.87 99.92 23.01 o 5 6 24 39.91 1.94 26.09 o 6 6 24 32.64 8.98 20.45 o 7 6 24 2.32 0.00 19.60 o 8 6 24 426.93 528.35 42.41 o 9 6 24 277.30 400.64 38.03 o 0 7 24 59.86 0.00 37.03 o 1 7 24 12.90 100.37 78.29 o 2 7 24 1533.77 1543.64 138.03 o 3 7 24 71.67 75.52 25.94 o 4 7 24 82.96 167.58 53.45 o 5 7 24 23.29 160.17 43.46 o 6 7 24 57.16 161.75 69.62 o 7 7 24 40.38 0.00 16.58 o 8 7 24 239.61 223.68 37.68 o 9 7 24 7.76 0.00 27.53 o 1 8 24 70.25 386.58 97.69 o 2 8 24 34.91 28.76 21.54 o 3 8 24 25.15 37.51 25.59 o 4 8 24 140.79 235.95 40.48 o 5 8 24 66.06 60.30 25.06 o 6 8 24 385.70 337.93 44.85 o 7 8 24 17.71 3.29 31.86 o 8 8 24 22.58 81.18 65.18 o 9 8 24 0.18 0.00 59.89 o 1 9 24 7.97 0.43 27.94 o 2 9 24 10.65 0.36 24.49 o 3 9 24 86.00 101.65 27.28 o 4 9 24 119.49 119.89 39.82 o 5 9 24 112.89 88.90 24.20 o 6 9 24 0.69 23.82 29.60 o 7 9 24 2.25 0.00 21.40 o 8 9 24 0.12 0.00 24.10 o 2 10 24 2.03 13.75 54.80 o 3 10 24 148.30 134.29 31.13 o 4 10 24 7.71 0.00 21.84 o 5 10 24 11.89 58.47 45.08 o 6 10 24 69.28 46.90 35.35 o 7 10 24 21.87 51.39 87.20 o 8 10 24 357.57 499.17 56.00 o 4 11 24 12.77 0.00 20.61 o 5 11 24 1.82 0.00 23.93 o 6 11 24 50.73 22.80 32.96 o 3 3 25 319.41 217.61 70.92 o 4 3 25 3.64 125.87 93.05 o 5 3 25 7.68 36.29 43.65 o 2 4 25 3.93 22.12 67.36 o 3 4 25 110.71 110.40 40.49 o 4 4 25 116.24 143.45 20.87 o 5 4 25 111.62 88.99 88.90 o 6 4 25 25.56 0.00 32.66 o 2 5 25 2.91 17.94 30.60 o 3 5 25 177.90 85.19 50.51 o 4 5 25 153.15 163.18 29.21 o 5 5 25 23.16 4.79 36.06 o 6 5 25 430.57 356.91 52.18 o 3 6 25 711.26 867.28 131.16 o 4 6 25 2.17 71.73 23.19 o 5 6 25 6.19 114.40 40.80 o 6 6 25 3.62 0.00 24.04 o 3 7 25 90.84 129.67 21.92 o 4 7 25 336.56 172.82 70.73 o 5 7 25 157.95 118.35 39.59 o 6 7 25 2.10 0.36 22.43 o 4 8 25 585.67 484.71 63.92 o 5 8 25 307.23 270.10 37.55 o