#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/85/2018575.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018575_Fobs loop_ _publ_author_name 'Valkonen, Arto' 'Kolehmainen, Erkki' 'Grzeg\'orska, Aleksandra' 'O\'smia\/lowski, Borys' 'Gawinecki, Ryszard' 'Rissanen, Kari' _publ_section_title ; Two (E)-2-({[4-(dialkylamino)phenyl]imino}methyl)-4-nitrophenols ; _journal_coeditor_code LG3082 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o279 _journal_page_last o282 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.545 _cell_angle_gamma 90.000 _cell_length_a 31.6882 _cell_length_b 6.7674 _cell_length_c 13.1460 _exptl_crystal_F_000 1200.00 _reflns_d_resolution_high 0.8301 _[local]_cod_data_source_file lg3082Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ac-5 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 771.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 4832.54 4808.58 197.74 o 8 0 0 5209.48 5063.56 198.56 o 10 0 0 3260.86 3043.31 148.27 o 12 0 0 294.45 376.46 44.68 o 14 0 0 166.30 214.76 44.01 o 16 0 0 11.39 19.55 26.98 o 18 0 0 17.61 -5.95 12.49 o 20 0 0 534.82 769.25 111.08 o 22 0 0 10.97 78.01 102.46 o 24 0 0 12213.05 13258.42 517.52 o 26 0 0 12379.73 13208.20 469.53 o 28 0 0 134.24 148.34 75.99 o 30 0 0 563.25 406.32 75.77 o 32 0 0 122.26 450.59 178.05 o 34 0 0 63.39 8.98 160.76 o 36 0 0 175.65 67.17 181.88 o 1 1 0 22648.60 22410.11 818.61 o 3 1 0 28871.66 28733.18 650.49 o 5 1 0 6726.16 6533.25 147.33 o 7 1 0 2242.35 2311.60 70.08 o 9 1 0 642.99 666.93 47.94 o 11 1 0 174.19 244.95 51.72 o 13 1 0 3933.07 4351.59 118.29 o 15 1 0 119.28 118.21 49.29 o 17 1 0 2458.85 2361.88 77.03 o 19 1 0 3.13 10.68 36.29 o 21 1 0 63.77 191.29 54.69 o 23 1 0 838.65 708.47 63.75 o 25 1 0 2135.92 2273.00 102.21 o 27 1 0 2.01 23.80 63.73 o 29 1 0 13.70 80.31 63.44 o 31 1 0 402.84 559.54 182.12 o 33 1 0 21.36 112.52 122.76 o 35 1 0 17.49 -104.08 136.52 o 0 2 0 6797.96 6369.44 258.64 o 2 2 0 2.41 -7.88 41.30 o 4 2 0 1961.10 1858.29 86.99 o 6 2 0 137.64 126.51 44.84 o 8 2 0 20.80 40.19 41.64 o 10 2 0 283.49 300.45 47.13 o 12 2 0 2001.61 2118.13 74.06 o 14 2 0 684.56 718.44 57.20 o 16 2 0 1830.31 1935.84 78.88 o 18 2 0 206.34 150.30 42.27 o 20 2 0 1178.72 1238.00 72.33 o 22 2 0 28.90 89.74 102.80 o 24 2 0 1003.12 947.71 157.25 o 26 2 0 29.84 24.33 158.11 o 28 2 0 525.10 775.69 178.35 o 30 2 0 24.63 56.95 38.03 o 32 2 0 97.18 327.24 97.48 o 34 2 0 31.73 -5.39 302.74 o 1 3 0 23671.93 24874.12 648.93 o 3 3 0 436.87 349.77 66.64 o 5 3 0 9.76 19.06 64.91 o 7 3 0 503.09 575.17 50.64 o 9 3 0 407.65 539.98 64.15 o 11 3 0 90.61 206.54 127.20 o 13 3 0 2329.96 2731.62 106.13 o 15 3 0 86.93 32.63 86.67 o 17 3 0 49.53 52.06 47.97 o 19 3 0 0.29 53.38 51.17 o 21 3 0 1304.15 1144.46 76.41 o 23 3 0 197.43 160.20 58.19 o 25 3 0 1778.28 1641.49 96.95 o 27 3 0 1062.85 944.13 118.37 o 29 3 0 504.36 438.12 96.33 o 31 3 0 103.75 53.78 98.08 o 33 3 0 6.99 196.15 161.87 o 0 4 0 10507.65 12855.10 767.22 o 2 4 0 1914.81 1725.48 80.74 o 4 4 0 1122.96 1112.87 71.31 o 6 4 0 772.53 691.97 75.66 o 8 4 0 4314.36 4588.02 150.25 o 10 4 0 190.55 188.49 49.38 o 12 4 0 226.86 174.23 53.63 o 14 4 0 2285.62 2227.43 95.54 o 16 4 0 4801.42 4553.32 183.12 o 18 4 0 18.42 43.73 79.80 o 20 4 0 7.76 122.67 109.29 o 22 4 0 15.26 10.66 77.37 o 24 4 0 1.03 2.19 68.10 o 26 4 0 686.62 575.38 100.48 o 28 4 0 328.77 324.77 91.21 o 30 4 0 15.24 -15.88 153.75 o 1 5 0 372.03 283.41 82.27 o 3 5 0 2.56 66.64 49.65 o 5 5 0 1110.64 1019.03 85.93 o 7 5 0 663.87 703.50 86.20 o 9 5 0 31.93 81.06 111.58 o 11 5 0 3214.48 3180.16 131.24 o 13 5 0 376.59 448.05 51.45 o 15 5 0 439.24 335.36 85.09 o 17 5 0 119.87 116.34 78.74 o 19 5 0 0.04 111.05 72.13 o 21 5 0 285.96 309.04 74.40 o 23 5 0 219.50 172.25 89.03 o 25 5 0 24.03 9.88 85.33 o 27 5 0 8.81 17.42 95.21 o 0 6 0 531.45 450.38 355.62 o 2 6 0 501.00 496.43 115.78 o 4 6 0 25.75 363.39 157.72 o 6 6 0 451.40 271.86 89.52 o 8 6 0 1258.32 1285.56 111.15 o 10 6 0 41.47 290.56 100.26 o 12 6 0 2204.80 1706.90 278.74 o 14 6 0 46.71 11.32 87.80 o 16 6 0 71.58 400.07 163.73 o 18 6 0 211.68 460.92 451.84 o 20 6 0 1.14 86.23 102.72 o 22 6 0 4.13 -36.46 119.81 o 24 6 0 0.80 -18.42 142.42 o 1 7 0 1332.93 1284.43 199.17 o 3 7 0 768.15 822.73 186.26 o 5 7 0 457.78 -64.62 190.86 o 7 7 0 20.26 56.78 63.37 o 9 7 0 45.83 159.51 95.64 o 11 7 0 439.31 215.88 115.52 o 13 7 0 1.82 2.45 116.36 o 15 7 0 423.69 426.30 140.59 o 17 7 0 307.21 337.23 132.61 o 0 8 0 85.79 245.36 272.18 o 2 8 0 82.32 510.69 215.75 o 4 8 0 7.54 257.92 209.33 o 6 8 0 2.73 67.33 201.26 o -35 1 1 0.01 108.86 173.79 o -33 1 1 29.86 195.68 111.41 o -31 1 1 25.00 294.88 122.78 o -29 1 1 394.02 311.43 79.31 o -27 1 1 3388.64 3015.54 187.05 o -25 1 1 0.34 19.22 65.17 o -23 1 1 31.29 6.49 46.25 o -21 1 1 0.18 -1.23 55.08 o -19 1 1 75.41 28.44 51.24 o -17 1 1 1753.83 1698.39 72.85 o -15 1 1 26422.63 28406.50 637.96 o -13 1 1 0.93 -32.86 32.86 o -11 1 1 1530.72 1507.08 50.91 o -9 1 1 7402.30 7477.67 217.84 o -7 1 1 4280.47 4179.49 98.84 o -5 1 1 2133.15 2135.43 59.97 o -3 1 1 90.91 53.00 52.08 o -1 1 1 13556.60 12942.46 277.64 o 1 1 1 30104.54 29209.02 681.12 o 3 1 1 1269.53 1211.98 58.47 o 5 1 1 300.37 209.79 79.69 o 7 1 1 218.50 300.21 39.48 o 9 1 1 1754.93 1779.48 72.52 o 11 1 1 2232.81 2332.51 110.68 o 13 1 1 47.25 16.29 40.03 o 15 1 1 38.70 -39.15 39.15 o 17 1 1 115.29 93.60 42.38 o 19 1 1 317.54 237.53 130.10 o 21 1 1 1498.34 1379.15 76.54 o 23 1 1 985.12 1045.02 94.00 o 25 1 1 6958.38 7071.44 190.10 o 27 1 1 0.80 -34.58 34.58 o 29 1 1 132.07 157.50 67.02 o 31 1 1 3.61 -31.94 79.14 o 33 1 1 67.11 241.53 127.04 o 35 1 1 32.82 -158.36 158.36 o -36 2 1 153.73 -82.31 134.41 o -34 2 1 32.52 -169.54 169.54 o -32 2 1 121.72 61.51 145.03 o -30 2 1 905.58 874.44 88.61 o -28 2 1 2465.93 2225.94 180.59 o -26 2 1 80.89 -2.75 145.37 o -24 2 1 311.79 195.12 55.29 o -22 2 1 143.58 201.80 53.88 o -20 2 1 484.17 524.12 50.99 o -18 2 1 1902.03 1905.08 123.48 o -16 2 1 45.81 141.50 57.18 o -14 2 1 528.74 636.18 53.42 o -12 2 1 5818.86 6135.42 312.09 o -10 2 1 12789.93 13292.32 298.86 o -8 2 1 81.15 81.98 40.36 o -6 2 1 1846.68 1671.39 72.27 o -4 2 1 787.13 778.19 58.14 o -2 2 1 418.71 510.78 41.56 o 0 2 1 2468.29 2549.18 93.99 o 2 2 1 1131.46 1215.72 60.79 o 4 2 1 6569.43 6449.48 230.89 o 6 2 1 2368.33 2626.39 97.58 o 8 2 1 1700.34 1651.70 67.73 o 10 2 1 388.27 437.84 54.30 o 12 2 1 38.45 85.09 50.63 o 14 2 1 252.92 193.04 83.54 o 16 2 1 2288.96 2095.11 115.81 o 18 2 1 1.49 33.18 45.73 o 20 2 1 53.77 130.48 45.58 o 22 2 1 0.19 26.80 51.88 o 24 2 1 1085.14 950.65 70.51 o 26 2 1 1634.96 1606.17 88.19 o 28 2 1 334.39 264.90 66.27 o 30 2 1 163.09 178.78 68.34 o 32 2 1 174.95 197.19 91.18 o 34 2 1 3.95 -93.01 120.40 o -33 3 1 17.11 -108.91 196.38 o -31 3 1 10.15 -20.99 72.74 o -29 3 1 2.08 18.65 67.44 o -27 3 1 187.07 150.64 72.06 o -25 3 1 181.80 309.39 70.48 o -23 3 1 344.59 279.91 139.66 o -21 3 1 150.77 333.20 137.83 o -19 3 1 559.13 504.74 58.20 o -17 3 1 1028.73 831.83 68.53 o -15 3 1 43.92 105.03 93.79 o -13 3 1 3020.94 3328.61 102.86 o -11 3 1 256.05 252.36 76.13 o -9 3 1 353.20 444.85 68.99 o -7 3 1 405.10 520.59 46.65 o -5 3 1 66.18 133.83 34.58 o -3 3 1 5861.12 5966.54 168.23 o -1 3 1 350.14 303.72 35.71 o 1 3 1 5424.85 6273.89 175.58 o 3 3 1 23.10 9.83 176.21 o 5 3 1 258.05 314.14 39.88 o 7 3 1 0.39 58.96 48.76 o 9 3 1 31.78 56.39 51.02 o 11 3 1 124.44 191.69 53.09 o 13 3 1 2260.75 1949.57 250.50 o 15 3 1 1150.52 1250.32 75.80 o 17 3 1 509.58 515.64 81.97 o 19 3 1 26.18 58.89 52.22 o 21 3 1 949.86 822.90 139.18 o 23 3 1 248.45 290.50 69.97 o 25 3 1 1447.45 1130.86 85.76 o 27 3 1 9.26 -9.94 61.71 o 29 3 1 40.83 117.91 78.29 o 31 3 1 4.41 37.40 103.42 o 33 3 1 464.48 422.34 159.04 o -32 4 1 141.91 113.00 221.61 o -30 4 1 28.19 88.09 152.16 o -28 4 1 203.84 6.18 163.99 o -26 4 1 25.26 83.16 85.12 o -24 4 1 69.63 147.95 81.28 o -22 4 1 27.24 122.58 112.85 o -20 4 1 353.22 265.59 90.01 o -18 4 1 2.02 0.38 64.54 o -16 4 1 8115.46 8243.90 215.30 o -14 4 1 5218.24 4894.90 185.64 o -12 4 1 116.81 143.16 47.70 o -10 4 1 3.38 -6.21 41.84 o -8 4 1 679.72 540.42 84.40 o -6 4 1 543.93 578.26 75.52 o -4 4 1 87.22 140.13 69.79 o -2 4 1 2431.65 2717.72 199.70 o 0 4 1 39.93 120.95 43.36 o 2 4 1 135.81 124.18 49.47 o 4 4 1 180.21 171.98 52.78 o 6 4 1 915.35 713.12 104.12 o 8 4 1 315.71 312.34 68.87 o 10 4 1 2497.51 2199.70 111.68 o 12 4 1 1869.55 1666.31 193.01 o 14 4 1 471.77 504.08 106.60 o 16 4 1 1776.59 1530.52 107.25 o 18 4 1 234.78 216.86 100.48 o 20 4 1 522.28 351.83 74.82 o 22 4 1 456.30 461.85 102.11 o 24 4 1 81.23 84.04 68.53 o 26 4 1 65.31 32.53 70.59 o 28 4 1 49.27 50.56 107.03 o 30 4 1 13.15 99.28 96.08 o -29 5 1 0.76 155.29 213.97 o -27 5 1 113.98 -25.64 101.16 o -25 5 1 127.83 224.96 92.61 o -23 5 1 69.66 98.19 76.46 o -21 5 1 47.61 151.57 97.78 o -19 5 1 297.21 353.11 99.40 o -17 5 1 345.00 395.70 55.23 o -15 5 1 5801.13 5827.70 172.64 o -13 5 1 1832.65 1698.13 74.73 o -11 5 1 4679.21 4612.70 176.16 o -9 5 1 3658.91 3416.75 133.70 o -7 5 1 400.05 407.39 82.39 o -5 5 1 1.45 -0.95 55.24 o -3 5 1 215.30 135.77 49.04 o -1 5 1 106.86 99.53 91.38 o 1 5 1 150.93 166.20 47.67 o 3 5 1 199.62 198.70 58.95 o 5 5 1 628.60 596.81 72.16 o 7 5 1 1.11 13.18 67.19 o 9 5 1 236.46 190.40 81.22 o 11 5 1 772.25 625.14 86.91 o 13 5 1 1429.13 1491.18 233.40 o 15 5 1 45.75 106.06 83.18 o 17 5 1 1836.35 2046.93 193.32 o 19 5 1 46.51 -26.39 69.04 o 21 5 1 11.41 -26.83 82.37 o 23 5 1 190.20 250.42 158.09 o 25 5 1 66.79 21.30 92.43 o 27 5 1 242.31 413.10 112.03 o -24 6 1 0.05 2.16 149.07 o -22 6 1 26.91 87.16 125.42 o -20 6 1 779.57 729.55 152.67 o -18 6 1 207.36 101.12 36.99 o -16 6 1 34.34 92.80 98.26 o -14 6 1 151.87 180.95 121.55 o -12 6 1 3186.31 2940.20 404.70 o -10 6 1 2375.78 2606.15 301.59 o -8 6 1 381.02 520.61 90.93 o -6 6 1 1094.07 1110.79 87.65 o -4 6 1 583.52 391.83 183.74 o -2 6 1 349.57 594.45 233.48 o 0 6 1 1520.16 1433.06 131.17 o 2 6 1 39.47 182.73 174.03 o 4 6 1 78.21 104.80 69.26 o 6 6 1 434.67 467.47 88.19 o 8 6 1 5.94 -93.06 163.74 o 10 6 1 508.58 477.36 97.57 o 12 6 1 658.07 506.07 122.08 o 14 6 1 544.24 681.69 177.39 o 16 6 1 230.35 232.19 96.36 o 18 6 1 336.05 547.01 120.45 o 20 6 1 119.95 164.38 108.84 o 22 6 1 67.38 145.89 143.57 o -19 7 1 243.80 436.93 263.90 o -17 7 1 972.27 1881.49 224.02 o -15 7 1 57.95 -54.23 126.09 o -13 7 1 238.43 502.51 247.84 o -11 7 1 134.34 89.44 95.47 o -9 7 1 18.77 106.05 113.37 o -7 7 1 549.79 474.05 63.27 o -5 7 1 35.08 14.36 162.30 o -3 7 1 618.31 484.73 167.47 o -1 7 1 35.41 287.25 191.25 o 1 7 1 0.56 218.67 168.50 o 3 7 1 184.55 441.98 177.96 o 5 7 1 72.10 64.71 44.50 o 7 7 1 206.22 278.68 97.58 o 9 7 1 339.27 501.67 190.37 o 11 7 1 31.20 105.33 113.25 o 13 7 1 255.70 281.64 136.33 o 15 7 1 123.17 109.55 207.05 o 17 7 1 107.87 98.99 138.53 o -6 8 1 99.91 135.76 168.61 o -4 8 1 168.45 172.53 189.93 o -2 8 1 51.90 -41.02 165.43 o 0 8 1 1.33 142.24 181.86 o 2 8 1 2.20 -188.42 255.73 o 4 8 1 237.46 266.18 219.29 o -36 0 2 18.56 60.27 256.34 o -34 0 2 340.03 319.24 240.35 o -32 0 2 759.30 793.63 216.95 o -30 0 2 7760.08 7506.32 420.07 o -28 0 2 81.56 200.21 150.62 o -26 0 2 3495.91 3101.48 235.59 o -24 0 2 1440.41 1401.53 176.85 o -22 0 2 1321.59 1375.96 121.96 o -20 0 2 682.33 756.64 106.19 o -18 0 2 1202.02 801.23 120.21 o -16 0 2 2419.12 2215.44 135.03 o -14 0 2 3828.82 4017.66 192.71 o -12 0 2 350.51 360.82 46.84 o -10 0 2 11919.98 11721.88 487.37 o -8 0 2 257.57 355.20 71.96 o -6 0 2 588.48 576.93 68.68 o -4 0 2 2615.23 2487.62 96.80 o -2 0 2 103.09 -43.76 43.76 o 0 0 2 1737.17 1595.61 71.16 o 2 0 2 530.58 404.93 76.83 o 4 0 2 61.59 225.48 55.90 o 6 0 2 8648.52 8250.47 318.28 o 8 0 2 13.58 20.31 56.84 o 10 0 2 1499.39 1508.50 90.24 o 12 0 2 2453.96 2620.88 142.86 o 14 0 2 607.40 622.80 88.78 o 16 0 2 180.39 181.72 84.66 o 18 0 2 1862.60 1982.70 142.72 o 20 0 2 5097.63 5614.60 239.16 o 22 0 2 6408.92 6848.46 281.91 o 24 0 2 120.81 169.27 89.07 o 26 0 2 6593.65 6447.51 332.54 o 28 0 2 1297.85 1313.48 77.90 o 30 0 2 1031.44 875.16 129.83 o 32 0 2 69.21 208.61 146.39 o 34 0 2 2.24 23.28 142.22 o -37 1 2 309.99 311.35 154.65 o -35 1 2 192.84 249.49 160.37 o -33 1 2 287.45 311.44 168.08 o -31 1 2 22.28 133.93 120.12 o -29 1 2 144.11 67.54 96.18 o -27 1 2 6714.24 7458.07 428.75 o -25 1 2 1088.39 1208.97 107.85 o -23 1 2 72.39 119.81 65.46 o -21 1 2 13.27 26.70 67.44 o -19 1 2 1054.79 1148.33 60.00 o -17 1 2 232.45 227.55 30.92 o -15 1 2 4218.25 4420.47 112.07 o -13 1 2 94.88 190.07 33.61 o -11 1 2 8110.91 7805.59 170.17 o -9 1 2 2497.23 2358.19 104.82 o -7 1 2 7053.00 6813.71 153.37 o -5 1 2 19945.72 19935.37 430.32 o -3 1 2 1670.06 1538.57 47.02 o -1 1 2 5914.77 6011.28 143.76 o 1 1 2 14858.21 15092.02 411.98 o 3 1 2 8969.25 8856.19 239.38 o 5 1 2 1446.89 1326.47 73.49 o 7 1 2 12632.44 12453.00 338.24 o 9 1 2 609.66 715.64 102.31 o 11 1 2 4724.61 5010.43 297.63 o 13 1 2 493.35 383.66 91.36 o 15 1 2 767.84 974.84 125.67 o 17 1 2 172.89 140.76 59.81 o 19 1 2 898.76 1051.20 101.09 o 21 1 2 779.40 695.23 104.20 o 23 1 2 11018.82 11209.65 293.03 o 25 1 2 155.01 219.58 59.74 o 27 1 2 247.24 266.87 54.44 o 29 1 2 105.13 87.61 50.77 o 31 1 2 73.47 209.76 86.30 o 33 1 2 255.84 100.41 111.29 o -36 2 2 0.09 -29.10 163.22 o -34 2 2 40.93 118.96 145.53 o -32 2 2 22.39 -20.27 24.05 o -30 2 2 915.77 908.77 73.42 o -28 2 2 104.19 192.89 58.97 o -26 2 2 6.77 -30.24 52.37 o -24 2 2 21.36 73.92 48.03 o -22 2 2 9.57 80.40 44.83 o -20 2 2 0.02 20.77 41.72 o -18 2 2 4.17 9.79 36.17 o -16 2 2 5173.98 5670.33 137.52 o -14 2 2 29247.00 30682.29 643.77 o -12 2 2 492.12 439.86 90.61 o -10 2 2 226.97 176.33 73.38 o -8 2 2 70.90 112.32 38.24 o -6 2 2 5480.56 5629.79 139.40 o -4 2 2 5973.12 5756.33 130.24 o -2 2 2 52.63 -57.24 97.92 o 0 2 2 11241.29 10471.22 356.27 o 2 2 2 2403.69 2572.04 83.32 o 4 2 2 1.18 -19.32 37.78 o 6 2 2 203.15 236.74 59.39 o 8 2 2 1146.23 1267.15 75.85 o 10 2 2 42347.70 46114.99 1152.76 o 12 2 2 4333.32 4963.19 142.09 o 14 2 2 37.02 82.60 70.65 o 16 2 2 32.84 23.99 43.55 o 18 2 2 37.50 13.10 42.64 o 20 2 2 70.37 138.38 50.86 o 22 2 2 1.54 -9.53 51.51 o 24 2 2 30.74 77.94 74.47 o 26 2 2 1152.04 955.95 77.70 o 28 2 2 0.48 33.43 57.92 o 30 2 2 10.68 4.59 66.55 o 32 2 2 10.83 18.98 105.66 o -35 3 2 18.64 -39.45 166.19 o -33 3 2 17.78 252.17 183.18 o -31 3 2 405.38 193.79 117.68 o -29 3 2 173.25 254.66 164.33 o -27 3 2 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