#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:21:37 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180854 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/85/2018584.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018584_Fobs loop_ _publ_author_name 'Santos, L. M.' 'Legendre, A. O.' 'Villis, P. C. M.' 'Viegas Jr, C.' 'Doriguetto, A. C.' _publ_section_title ; (+-)-2,2-Dimethyl-5-oxotetrahydrofuran-3-carboxylic acid (terebic acid): a racemic layered structure ; _journal_coeditor_code UK3046 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o294 _journal_page_last o297 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.070 _cell_angle_gamma 90.000 _cell_length_a 5.9890 _cell_length_b 5.6630 _cell_length_c 22.2820 _exptl_crystal_F_000 336.00 _reflns_d_resolution_high 0.8000 _cod_data_source_file uk3046Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p21_c in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 42.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 45.70 35.80 0.71 o 2 0 0 258.61 237.51 3.98 o 3 0 0 10.69 9.64 0.54 o 4 0 0 693.96 683.91 15.14 o 5 0 0 1.76 2.24 0.54 o 6 0 0 5.85 6.58 1.40 o 7 0 0 0.39 -0.29 1.40 o 2 1 0 468.35 478.01 5.54 o 3 1 0 7.35 9.25 0.54 o 4 1 0 24.13 25.28 0.83 o 5 1 0 2.15 1.99 0.60 o 6 1 0 0.08 -0.75 0.75 o 7 1 0 0.00 -0.17 1.22 o 0 2 0 857.94 803.10 16.52 o 1 2 0 853.50 891.02 12.17 o 2 2 0 639.43 647.71 11.92 o 3 2 0 83.89 85.53 4.15 o 4 2 0 12.90 11.32 0.44 o 5 2 0 85.77 84.39 1.83 o 6 2 0 12.66 14.09 1.57 o 7 2 0 1.18 0.37 2.11 o 1 3 0 116.15 102.25 1.83 o 2 3 0 117.00 121.38 1.92 o 3 3 0 606.25 655.18 12.38 o 4 3 0 64.55 53.44 2.76 o 5 3 0 2.15 2.40 0.92 o 6 3 0 2.06 2.16 1.17 o 0 4 0 349.93 340.72 31.33 o 1 4 0 3.76 3.84 0.52 o 2 4 0 146.07 151.19 3.25 o 3 4 0 29.63 29.61 1.69 o 4 4 0 4.45 3.93 0.79 o 5 4 0 9.85 10.88 2.31 o 6 4 0 15.72 14.45 1.92 o 1 5 0 331.54 354.08 8.28 o 2 5 0 54.62 63.81 3.29 o 3 5 0 23.17 26.73 1.49 o 4 5 0 15.58 16.79 2.25 o 5 5 0 23.86 28.30 3.73 o 0 6 0 46.52 46.44 4.59 o 1 6 0 64.94 62.38 3.78 o 2 6 0 0.02 0.32 1.97 o 3 6 0 2.48 3.06 1.39 o 1 7 0 0.83 -1.59 1.59 o -7 1 1 8.13 6.41 1.04 o -6 1 1 55.03 61.15 2.18 o -5 1 1 37.56 37.47 2.35 o -4 1 1 117.94 128.68 4.94 o -3 1 1 325.10 351.98 5.26 o -2 1 1 941.30 908.43 12.16 o 0 1 1 1.83 1.35 0.15 o 2 1 1 131.10 129.30 1.64 o 3 1 1 7.51 8.40 0.32 o 4 1 1 185.01 189.42 2.38 o 5 1 1 14.39 8.16 3.33 o 6 1 1 4.41 5.07 1.04 o 7 1 1 6.03 9.74 1.98 o -7 2 1 0.44 -0.26 1.64 o -6 2 1 14.50 12.70 1.19 o -5 2 1 79.46 81.63 3.30 o -4 2 1 0.99 1.30 0.34 o -3 2 1 689.30 698.78 12.95 o -2 2 1 491.33 518.02 12.26 o -1 2 1 0.98 1.62 0.46 o 0 2 1 1313.80 1211.54 22.56 o 1 2 1 702.80 674.43 63.96 o 2 2 1 33.80 28.87 0.71 o 3 2 1 13.94 12.76 0.45 o 4 2 1 12.48 11.45 0.67 o 5 2 1 7.83 8.25 1.31 o 6 2 1 4.42 5.09 1.18 o 7 2 1 0.01 -0.32 1.19 o -6 3 1 26.23 31.64 2.29 o -5 3 1 30.43 25.23 1.26 o -4 3 1 299.48 320.73 14.98 o -3 3 1 7.54 8.09 0.46 o -2 3 1 74.52 64.17 1.19 o -1 3 1 43.01 39.86 0.88 o 0 3 1 37.23 37.98 1.07 o 1 3 1 20.73 22.83 0.69 o 2 3 1 70.34 76.70 2.00 o 3 3 1 16.88 16.86 0.98 o 4 3 1 2.58 2.20 0.53 o 5 3 1 0.50 0.50 0.71 o 6 3 1 2.93 1.78 1.21 o -6 4 1 6.07 7.87 1.62 o -5 4 1 9.87 7.54 2.05 o -4 4 1 23.41 25.31 1.48 o -3 4 1 185.03 193.51 10.69 o -2 4 1 415.73 451.81 13.73 o -1 4 1 2.57 1.33 1.38 o 0 4 1 31.87 29.02 1.13 o 1 4 1 6.94 6.95 0.60 o 2 4 1 44.85 55.17 1.82 o 3 4 1 14.33 12.68 1.53 o 4 4 1 6.41 4.60 1.02 o 5 4 1 13.23 13.30 1.51 o 6 4 1 4.23 3.35 1.39 o -5 5 1 0.31 0.96 1.15 o -4 5 1 0.41 2.20 2.43 o -3 5 1 0.09 0.18 1.74 o -2 5 1 73.30 73.77 2.36 o -1 5 1 55.47 49.26 6.50 o 0 5 1 146.84 130.68 18.97 o 1 5 1 2.42 2.47 0.64 o 2 5 1 9.69 8.69 1.33 o 3 5 1 149.58 171.27 6.29 o 4 5 1 8.31 8.03 1.15 o 5 5 1 0.31 1.01 1.10 o -3 6 1 12.54 11.91 1.58 o -2 6 1 22.08 25.99 4.01 o -1 6 1 0.57 2.41 1.44 o 0 6 1 0.23 -0.40 0.76 o 1 6 1 1.36 1.28 1.05 o 2 6 1 19.49 19.10 1.73 o 3 6 1 0.48 2.22 1.06 o -1 7 1 13.96 8.09 1.86 o 0 7 1 2.60 4.32 2.05 o 1 7 1 14.22 12.23 2.33 o -7 0 2 2.63 2.18 1.49 o -6 0 2 8.55 8.00 1.36 o -5 0 2 98.91 108.99 3.37 o -4 0 2 19.82 19.84 1.05 o -3 0 2 506.73 490.51 8.17 o -2 0 2 0.08 0.36 0.19 o 2 0 2 5.57 3.44 0.29 o 3 0 2 640.86 617.61 13.09 o 4 0 2 143.69 143.88 3.79 o 5 0 2 283.96 296.81 7.58 o 6 0 2 65.94 72.37 3.29 o 7 0 2 0.17 -0.80 1.05 o -7 1 2 6.94 9.36 1.37 o -6 1 2 0.07 -0.05 0.79 o -5 1 2 23.21 23.24 0.97 o -4 1 2 51.15 47.25 1.74 o -3 1 2 71.26 58.65 0.98 o -2 1 2 302.01 288.44 3.23 o -1 1 2 181.69 158.10 2.02 o 1 1 2 443.83 412.38 4.82 o 2 1 2 607.10 651.39 8.31 o 3 1 2 46.15 41.83 0.93 o 4 1 2 23.91 25.20 1.40 o 5 1 2 31.52 28.25 1.31 o 6 1 2 0.00 0.19 0.79 o 7 1 2 4.30 3.13 1.11 o -7 2 2 3.75 3.42 1.92 o -6 2 2 3.69 3.48 1.41 o -5 2 2 302.00 343.85 5.93 o -4 2 2 124.00 125.17 7.33 o -3 2 2 37.35 38.61 0.83 o -2 2 2 401.89 424.66 5.09 o -1 2 2 1169.38 1223.39 32.34 o 0 2 2 260.34 264.06 3.34 o 1 2 2 1586.38 1677.51 45.73 o 2 2 2 674.89 710.41 13.82 o 3 2 2 66.06 74.60 1.19 o 4 2 2 76.40 77.88 1.44 o 5 2 2 75.04 82.07 1.77 o 6 2 2 15.02 15.00 1.51 o 7 2 2 13.14 11.35 3.74 o -6 3 2 1.97 1.79 1.68 o -5 3 2 9.43 12.64 1.62 o -4 3 2 112.86 104.89 2.04 o -3 3 2 10.21 10.96 0.62 o -2 3 2 257.79 266.46 3.40 o -1 3 2 248.89 262.02 4.63 o 0 3 2 112.39 132.56 2.04 o 1 3 2 590.17 640.67 9.73 o 2 3 2 503.14 535.87 39.12 o 3 3 2 68.62 69.72 8.10 o 4 3 2 0.02 1.62 0.67 o 5 3 2 0.00 0.22 0.95 o 6 3 2 4.43 5.85 1.13 o -6 4 2 7.32 6.31 1.63 o -5 4 2 0.14 0.16 1.09 o -4 4 2 1.08 3.15 1.36 o -3 4 2 0.00 0.00 0.42 o -2 4 2 0.92 0.48 0.49 o -1 4 2 85.12 84.68 1.92 o 0 4 2 66.09 63.77 1.46 o 1 4 2 0.88 1.26 0.38 o 2 4 2 11.45 10.36 0.59 o 3 4 2 18.97 24.44 3.24 o 4 4 2 25.56 22.21 1.62 o 5 4 2 3.50 2.65 1.97 o 6 4 2 0.64 -1.77 1.77 o -5 5 2 1.48 1.51 1.08 o -4 5 2 0.98 -0.03 0.91 o -3 5 2 14.92 18.96 3.44 o -2 5 2 16.51 17.32 1.11 o -1 5 2 117.87 131.54 2.96 o 0 5 2 26.41 23.26 4.22 o 1 5 2 46.13 48.51 3.24 o 2 5 2 1.55 1.63 0.95 o 3 5 2 6.92 4.15 1.32 o 4 5 2 8.44 10.06 1.63 o 5 5 2 10.07 10.46 1.40 o -3 6 2 2.07 1.10 1.28 o -2 6 2 12.65 12.21 3.67 o -1 6 2 0.85 0.66 1.00 o 0 6 2 5.77 4.57 1.10 o 1 6 2 43.10 50.59 4.23 o 2 6 2 13.81 11.03 1.49 o 3 6 2 3.98 3.26 1.31 o -1 7 2 4.99 6.98 1.89 o 0 7 2 41.83 45.96 5.61 o -7 1 3 2.16 0.21 1.99 o -6 1 3 0.57 1.10 0.89 o -5 1 3 7.33 7.24 0.67 o -4 1 3 298.71 298.92 3.93 o -3 1 3 98.63 102.93 4.27 o -2 1 3 499.77 479.92 5.23 o -1 1 3 0.34 0.71 0.36 o 0 1 3 209.06 197.15 2.65 o 1 1 3 18.37 21.87 0.49 o 2 1 3 635.45 618.35 7.66 o 3 1 3 176.73 181.81 2.25 o 4 1 3 176.38 183.19 5.59 o 5 1 3 0.09 0.36 0.53 o 6 1 3 148.24 158.62 4.21 o 7 1 3 3.89 3.92 1.21 o -7 2 3 0.08 -0.73 1.54 o -6 2 3 9.75 9.25 1.10 o -5 2 3 4.51 4.31 0.57 o -4 2 3 1.81 2.31 0.43 o -3 2 3 3.37 1.04 0.49 o -2 2 3 0.02 0.57 0.32 o -1 2 3 3.46 4.78 0.69 o 0 2 3 509.82 476.27 8.54 o 1 2 3 22.14 23.56 0.74 o 2 2 3 249.06 257.09 6.56 o 3 2 3 247.85 246.40 15.31 o 4 2 3 73.37 76.84 1.54 o 5 2 3 136.66 142.28 4.97 o 6 2 3 1.00 1.89 0.97 o -6 3 3 28.92 24.97 2.13 o -5 3 3 39.96 40.31 1.73 o -4 3 3 114.96 110.60 6.06 o -3 3 3 11.61 8.47 0.61 o -2 3 3 422.72 447.29 6.33 o -1 3 3 414.67 444.82 6.66 o 0 3 3 202.09 203.04 3.56 o 1 3 3 2.34 4.72 0.40 o 2 3 3 370.72 369.47 9.90 o 3 3 3 90.12 90.90 3.64 o 4 3 3 16.59 18.20 2.59 o 5 3 3 4.59 3.74 0.89 o 6 3 3 26.65 30.15 2.34 o -6 4 3 1.69 -0.74 2.24 o -5 4 3 5.72 8.86 1.74 o -4 4 3 0.71 1.08 0.95 o -3 4 3 5.12 4.25 0.46 o -2 4 3 6.89 7.29 0.55 o -1 4 3 5.63 5.10 0.46 o 0 4 3 34.96 36.06 1.35 o 1 4 3 1.18 1.77 0.35 o 2 4 3 60.11 70.42 7.24 o 3 4 3 210.49 228.34 14.70 o 4 4 3 26.10 26.23 1.77 o 5 4 3 12.45 10.00 1.35 o -5 5 3 0.54 1.56 1.44 o -4 5 3 0.43 -0.07 1.00 o -3 5 3 22.18 19.64 1.33 o -2 5 3 7.29 5.81 0.83 o -1 5 3 46.45 43.69 2.42 o 0 5 3 14.23 10.15 1.46 o 1 5 3 0.00 0.48 0.60 o 2 5 3 65.24 64.24 3.29 o 3 5 3 23.32 18.24 1.78 o 4 5 3 0.48 -1.19 1.19 o 5 5 3 1.01 4.75 1.70 o -3 6 3 3.60 1.58 1.31 o -2 6 3 0.39 -0.05 0.88 o -1 6 3 0.34 -0.20 0.96 o 0 6 3 31.73 37.09 4.42 o 1 6 3 26.69 30.28 7.40 o 2 6 3 19.42 23.49 1.90 o 3 6 3 1.37 3.27 1.43 o 0 7 3 0.75 -2.28 2.28 o -7 0 4 3.75 5.63 1.76 o -6 0 4 95.76 101.24 3.39 o -5 0 4 38.37 38.06 1.59 o -4 0 4 235.76 241.01 5.19 o -3 0 4 393.68 426.50 6.35 o -2 0 4 1147.74 1154.83 27.57 o -1 0 4 197.66 170.19 2.74 o 1 0 4 1294.41 1122.85 30.29 o 3 0 4 169.56 168.33 3.08 o 4 0 4 14.25 16.46 0.71 o 5 0 4 17.87 17.53 1.19 o 6 0 4 24.18 23.94 1.89 o 7 0 4 36.49 30.29 2.41 o -7 1 4 0.10 1.22 1.91 o -6 1 4 36.98 38.69 1.52 o -5 1 4 2.03 1.14 0.32 o -4 1 4 22.62 24.72 0.92 o -3 1 4 109.99 109.67 1.58 o -2 1 4 14.77 12.79 0.68 o -1 1 4 7.47 6.65 0.27 o 0 1 4 1208.66 1138.28 24.09 o 2 1 4 149.26 162.05 4.56 o 3 1 4 0.12 0.17 0.23 o 4 1 4 92.49 98.30 1.60 o 5 1 4 1.35 1.23 0.40 o 6 1 4 93.62 99.40 2.77 o 7 1 4 7.39 6.25 1.32 o -7 2 4 0.95 0.13 1.35 o -6 2 4 0.70 1.13 0.77 o -5 2 4 229.37 248.20 13.89 o -4 2 4 14.46 13.87 0.61 o -3 2 4 467.75 500.47 5.72 o -2 2 4 3.00 3.47 1.26 o -1 2 4 916.86 932.30 13.22 o 0 2 4 898.02 852.40 14.85 o 2 2 4 609.17 635.03 11.09 o 3 2 4 281.15 263.96 3.42 o 4 2 4 48.58 49.85 1.39 o 5 2 4 331.63 340.28 12.82 o 6 2 4 17.96 17.88 1.69 o -6 3 4 11.14 14.81 3.59 o -5 3 4 15.95 13.32 1.20 o -4 3 4 90.76 90.46 5.30 o -3 3 4 3.74 4.01 0.82 o -2 3 4 211.79 215.65 3.00 o -1 3 4 97.58 101.99 3.34 o 0 3 4 778.08 815.91 12.39 o 1 3 4 1.43 2.07 0.21 o 2 3 4 48.26 50.06 6.80 o 3 3 4 500.54 570.73 45.17 o 4 3 4 397.28 424.60 10.20 o 5 3 4 0.81 0.17 1.96 o 6 3 4 0.03 -0.34 1.24 o -6 4 4 1.95 1.18 1.71 o -5 4 4 0.67 2.29 1.08 o -4 4 4 26.63 31.07 1.66 o -3 4 4 79.37 75.97 1.95 o -2 4 4 93.68 85.73 3.70 o -1 4 4 65.59 62.11 1.42 o 0 4 4 159.61 155.49 5.67 o 1 4 4 42.15 47.26 1.08 o 2 4 4 0.01 -0.48 1.60 o 3 4 4 46.52 41.82 6.23 o 4 4 4 5.47 8.77 2.13 o 5 4 4 2.95 5.19 1.56 o -5 5 4 41.50 39.95 2.15 o -4 5 4 19.08 18.79 2.31 o -3 5 4 1.38 2.45 0.95 o -2 5 4 5.14 5.18 0.84 o -1 5 4 161.11 176.58 9.04 o 0 5 4 32.83 25.41 4.85 o 1 5 4 25.08 28.25 2.97 o 2 5 4 9.70 8.67 1.34 o 3 5 4 45.13 49.22 6.24 o 4 5 4 18.18 20.01 1.77 o 5 5 4 17.45 15.77 1.93 o -3 6 4 1.47 3.63 1.46 o -2 6 4 11.01 9.02 2.69 o -1 6 4 0.27 0.20 0.97 o 0 6 4 29.98 32.34 3.14 o 1 6 4 22.52 18.71 2.20 o 2 6 4 0.28 -0.04 1.39 o 3 6 4 18.78 22.28 4.22 o 0 7 4 21.65 18.64 4.23 o -7 1 5 33.41 31.87 3.27 o -6 1 5 10.60 10.29 1.09 o -5 1 5 0.48 0.91 0.45 o -4 1 5 20.84 18.32 0.63 o -3 1 5 1531.62 1661.09 45.08 o -2 1 5 42.25 47.74 0.88 o 0 1 5 15.41 14.93 0.42 o 2 1 5 10.31 8.74 0.41 o 3 1 5 63.64 57.99 1.75 o 4 1 5 12.80 12.69 0.83 o 5 1 5 7.53 7.69 0.81 o 6 1 5 0.16 -0.73 0.73 o 7 1 5 8.32 8.16 1.89 o -7 2 5 0.00 -0.54 1.94 o -6 2 5 21.80 19.18 1.41 o -5 2 5 31.23 30.00 1.03 o -4 2 5 1.60 1.99 0.48 o -3 2 5 4.42 4.28 0.66 o -2 2 5 985.94 1123.17 29.58 o -1 2 5 358.84 369.11 13.20 o 0 2 5 35.16 36.84 1.93 o 1 2 5 773.36 772.65 11.12 o 2 2 5 398.76 404.41 6.36 o 3 2 5 0.05 0.46 0.24 o 4 2 5 0.54 0.85 0.38 o 5 2 5 49.89 53.71 1.83 o 6 2 5 0.18 0.95 1.18 o -6 3 5 3.26 2.25 1.20 o -5 3 5 14.06 15.66 2.61 o -4 3 5 36.95 34.73 1.24 o -3 3 5 0.21 -0.12 0.50 o -2 3 5 240.41 241.76 6.01 o -1 3 5 124.47 116.21 1.90 o 0 3 5 128.59 131.66 2.14 o 1 3 5 57.84 55.34 0.96 o 2 3 5 74.89 78.33 2.16 o 3 3 5 15.80 12.30 1.23 o 4 3 5 55.96 57.60 3.79 o 5 3 5 13.66 14.04 1.45 o 6 3 5 7.95 7.96 1.82 o -6 4 5 16.02 15.75 1.56 o -5 4 5 0.94 0.61 1.00 o -4 4 5 73.15 75.43 2.63 o -3 4 5 29.64 27.68 2.24 o -2 4 5 186.13 205.28 4.93 o -1 4 5 83.38 80.53 1.72 o 0 4 5 282.23 283.21 7.74 o 1 4 5 3.12 1.90 0.32 o 2 4 5 41.66 45.18 6.09 o 3 4 5 10.90 10.27 3.59 o 4 4 5 30.79 30.49 2.21 o 5 4 5 0.04 1.23 1.66 o -5 5 5 6.63 7.00 1.39 o -4 5 5 0.07 -1.04 1.04 o -3 5 5 27.98 28.07 1.72 o -2 5 5 29.77 26.86 2.85 o -1 5 5 0.46 0.48 0.58 o 0 5 5 46.88 45.13 3.66 o 1 5 5 14.13 16.10 1.14 o 2 5 5 63.85 69.44 4.75 o 3 5 5 23.05 27.67 2.13 o 4 5 5 2.93 2.58 1.63 o -3 6 5 15.81 15.71 1.67 o -2 6 5 18.03 16.28 1.57 o -1 6 5 9.25 10.32 1.05 o 0 6 5 0.02 0.90 1.83 o 1 6 5 3.02 8.21 5.89 o 2 6 5 37.01 39.29 5.65 o 3 6 5 2.94 4.63 4.40 o -7 0 6 0.03 0.21 1.34 o -6 0 6 153.27 160.10 4.67 o -5 0 6 28.80 32.07 1.72 o -4 0 6 786.73 870.71 20.05 o -3 0 6 426.12 451.19 6.60 o -2 0 6 92.14 87.68 1.72 o -1 0 6 476.88 421.87 6.10 o 2 0 6 964.72 961.35 15.77 o 3 0 6 19.75 18.31 0.71 o 4 0 6 0.89 1.61 0.46 o 5 0 6 189.53 207.04 7.52 o 6 0 6 100.18 118.45 4.73 o 7 0 6 1.00 2.37 2.35 o -7 1 6 0.47 2.62 1.15 o -6 1 6 0.09 0.81 1.35 o -5 1 6 101.18 96.34 2.15 o -4 1 6 3.59 4.45 0.44 o -3 1 6 396.84 440.69 5.66 o -2 1 6 67.88 57.92 0.87 o -1 1 6 54.82 58.72 0.92 o 0 1 6 10.36 8.11 0.47 o 1 1 6 13.81 15.76 0.42 o 2 1 6 0.93 0.73 0.21 o 3 1 6 83.13 83.42 1.25 o 4 1 6 0.04 0.10 0.43 o 5 1 6 78.27 79.87 2.46 o 6 1 6 20.13 21.94 1.18 o -7 2 6 10.40 9.33 1.70 o -6 2 6 0.30 0.30 0.74 o -5 2 6 47.44 49.15 1.30 o -4 2 6 269.52 256.88 3.80 o -3 2 6 64.25 63.48 1.28 o -2 2 6 153.10 189.04 4.86 o -1 2 6 0.44 2.17 0.35 o 0 2 6 61.90 54.44 1.13 o 1 2 6 46.10 47.80 0.90 o 2 2 6 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