#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:21:37 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180854 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/85/2018590.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018590_Fobs loop_ _publ_author_name 'Paton, Andrew S.' 'Lough, Alan J.' 'Bender, Timothy P.' _publ_section_title ; Sulfonate pseudohalides of boron subphthalocyanine ; _journal_coeditor_code BI3045 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o459 _journal_page_last o464 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.466 _cell_angle_gamma 90.000 _cell_length_a 13.8349 _cell_length_b 13.8988 _cell_length_c 14.3887 _exptl_crystal_F_000 1224.00 _reflns_d_resolution_high 0.8464 _cod_data_source_file bi3045IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' cu_d1212_0m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 301.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5.14 56.34 6.04 o 2 0 0 7.71 2.01 5.03 o 3 0 0 13429.80 13370.76 483.92 o 4 0 0 449.61 515.90 21.62 o 5 0 0 368.56 310.10 18.36 o 6 0 0 8204.04 8328.41 220.75 o 7 0 0 962.97 1109.70 52.32 o 8 0 0 826.54 993.27 29.71 o 9 0 0 760.95 676.34 21.33 o 10 0 0 161.87 117.21 20.12 o 11 0 0 3821.52 3785.22 132.30 o 12 0 0 18.73 8.05 19.12 o 13 0 0 12.37 -2.01 19.12 o 14 0 0 237.82 208.26 30.18 o 3 1 0 6489.19 6617.50 170.74 o 4 1 0 100.64 117.27 10.21 o 5 1 0 1783.64 1405.01 34.24 o 6 1 0 1290.10 1482.77 45.78 o 7 1 0 1597.98 1954.97 84.01 o 8 1 0 326.19 301.19 18.27 o 9 1 0 4.58 1.03 7.35 o 10 1 0 752.79 841.12 27.68 o 11 1 0 1106.22 1168.06 63.38 o 12 1 0 412.84 437.15 29.52 o 13 1 0 1.06 8.57 13.15 o 14 1 0 79.57 77.54 11.39 o 4 2 0 1554.22 2336.11 89.54 o 5 2 0 336.08 454.76 21.48 o 6 2 0 2261.78 2540.45 72.52 o 7 2 0 735.89 728.10 30.18 o 8 2 0 174.09 154.47 8.97 o 9 2 0 1.71 6.96 4.69 o 10 2 0 294.44 293.62 13.12 o 11 2 0 280.76 200.06 16.47 o 12 2 0 418.27 426.15 29.47 o 13 2 0 178.41 207.01 34.21 o 14 2 0 98.32 64.07 13.75 o 1 3 0 2510.53 2289.16 54.07 o 2 3 0 4603.07 4402.59 141.86 o 3 3 0 1081.62 966.84 36.22 o 4 3 0 9378.67 9935.55 223.74 o 5 3 0 11862.97 12100.63 647.41 o 6 3 0 2266.52 2545.32 72.85 o 7 3 0 77.69 80.49 19.12 o 8 3 0 182.67 144.99 8.21 o 9 3 0 4.91 -4.42 7.20 o 10 3 0 1840.13 1848.51 43.53 o 11 3 0 1570.49 1577.90 65.30 o 12 3 0 16.35 7.04 19.12 o 13 3 0 47.49 30.18 19.12 o 14 3 0 72.27 78.30 13.46 o 0 4 0 254.00 332.01 20.12 o 1 4 0 66.94 67.31 6.73 o 2 4 0 1534.82 1740.51 60.36 o 3 4 0 1259.87 1500.06 53.32 o 4 4 0 2285.91 2739.90 65.09 o 5 4 0 0.81 194.17 22.13 o 6 4 0 219.03 201.59 29.18 o 7 4 0 217.43 255.82 13.58 o 8 4 0 86.59 110.79 12.47 o 9 4 0 8.42 9.89 5.43 o 10 4 0 209.61 198.70 13.73 o 11 4 0 94.27 96.47 18.00 o 12 4 0 2.57 7.44 9.58 o 13 4 0 290.57 350.11 35.21 o 14 4 0 43.71 50.48 14.59 o 1 5 0 7509.05 8599.27 194.57 o 2 5 0 35.05 120.26 12.81 o 3 5 0 3871.35 4317.04 99.95 o 4 5 0 419.91 394.91 29.18 o 5 5 0 7556.85 8272.46 188.88 o 6 5 0 490.12 541.27 34.21 o 7 5 0 177.36 146.36 10.11 o 8 5 0 25.49 32.96 5.90 o 9 5 0 43.34 32.32 6.50 o 10 5 0 205.16 235.94 15.39 o 11 5 0 422.80 420.59 17.06 o 12 5 0 426.87 378.08 20.06 o 13 5 0 181.41 179.08 29.18 o 14 5 0 125.12 110.67 17.10 o 0 6 0 6400.20 8340.38 268.62 o 1 6 0 1750.69 2216.49 54.42 o 2 6 0 10701.61 11710.12 264.64 o 3 6 0 1905.61 2491.92 49.95 o 4 6 0 11575.46 12834.55 290.96 o 5 6 0 56.18 86.10 10.87 o 6 6 0 416.53 452.32 16.20 o 7 6 0 48.80 83.15 6.10 o 8 6 0 132.93 141.59 9.23 o 9 6 0 1131.98 1168.87 27.15 o 10 6 0 1835.92 1767.78 36.45 o 11 6 0 23.09 13.42 7.44 o 12 6 0 0.04 3.59 9.29 o 13 6 0 246.55 232.02 22.68 o 1 7 0 1530.22 2004.74 36.47 o 2 7 0 931.14 1446.34 32.52 o 3 7 0 7902.38 9732.78 181.61 o 4 7 0 0.30 35.48 18.11 o 5 7 0 238.64 288.58 14.82 o 6 7 0 126.64 141.25 7.69 o 7 7 0 60.89 55.07 5.46 o 8 7 0 235.92 292.07 11.66 o 9 7 0 530.91 550.67 18.55 o 10 7 0 619.69 622.63 19.61 o 11 7 0 170.82 163.74 12.75 o 12 7 0 221.56 237.26 11.76 o 13 7 0 0.25 8.52 7.94 o 0 8 0 324.55 272.22 19.05 o 1 8 0 132.49 173.19 11.54 o 2 8 0 3205.08 4327.30 84.61 o 3 8 0 0.14 1.40 8.36 o 4 8 0 1935.10 2202.69 78.71 o 5 8 0 20.90 40.80 5.61 o 6 8 0 39.61 95.01 6.92 o 7 8 0 292.54 346.26 14.95 o 8 8 0 359.79 411.07 15.36 o 9 8 0 215.14 322.08 20.43 o 10 8 0 506.43 493.02 26.33 o 11 8 0 3.76 2.06 6.89 o 12 8 0 27.39 35.80 8.86 o 1 9 0 787.70 949.05 22.59 o 2 9 0 1430.98 1687.20 61.57 o 3 9 0 593.98 667.40 17.85 o 4 9 0 1.64 19.26 7.66 o 5 9 0 22.68 33.50 6.07 o 6 9 0 100.83 112.25 7.66 o 7 9 0 59.46 39.72 6.68 o 8 9 0 27.34 46.65 8.09 o 9 9 0 1602.06 1784.80 42.81 o 10 9 0 1.44 4.91 8.75 o 11 9 0 80.53 57.40 9.95 o 12 9 0 25.29 20.01 6.28 o 0 10 0 577.70 544.68 20.33 o 1 10 0 22.96 35.63 7.21 o 2 10 0 1185.51 1143.92 27.26 o 3 10 0 253.19 314.57 15.12 o 4 10 0 331.43 398.91 16.84 o 5 10 0 602.74 828.35 22.90 o 6 10 0 856.86 919.83 22.76 o 7 10 0 570.95 697.34 17.16 o 8 10 0 355.38 362.29 16.42 o 9 10 0 22.82 26.51 8.95 o 10 10 0 3.71 11.69 9.17 o 11 10 0 3.58 -5.67 7.73 o 1 11 0 1093.09 1018.43 20.48 o 2 11 0 35.92 41.42 8.46 o 3 11 0 1947.55 2034.07 39.02 o 4 11 0 52.84 94.27 10.84 o 5 11 0 199.03 194.10 13.46 o 6 11 0 387.95 443.03 20.72 o 7 11 0 9.64 18.30 7.39 o 8 11 0 0.07 2.27 7.77 o 9 11 0 20.69 13.43 8.36 o 10 11 0 18.87 16.30 8.87 o 0 12 0 3028.15 2887.74 60.16 o 1 12 0 0.45 16.26 8.84 o 2 12 0 2225.73 2190.55 56.49 o 3 12 0 431.55 403.68 17.37 o 4 12 0 76.47 89.50 10.36 o 5 12 0 2024.34 2562.24 67.41 o 6 12 0 799.69 852.01 23.51 o 7 12 0 16.16 54.34 10.67 o 8 12 0 3.64 -3.30 21.63 o 9 12 0 52.04 62.10 8.27 o 1 13 0 1253.55 1159.87 30.93 o 2 13 0 32.37 30.96 22.13 o 3 13 0 25.48 64.98 13.86 o 4 13 0 89.15 130.79 13.86 o 5 13 0 107.84 92.20 18.11 o 6 13 0 31.99 62.57 10.06 o 7 13 0 2.87 2.65 7.48 o 8 13 0 189.85 156.44 14.47 o 0 14 0 31.41 14.30 13.15 o 1 14 0 3.20 5.20 11.34 o 2 14 0 14.75 5.61 12.43 o 3 14 0 1.21 -6.04 11.38 o 4 14 0 133.59 157.88 16.71 o 5 14 0 197.17 233.36 16.61 o 6 14 0 1.73 5.89 9.12 o 7 14 0 129.80 123.75 18.11 o 1 15 0 42.90 56.12 8.42 o 2 15 0 99.90 115.81 9.13 o 3 15 0 1.06 -1.75 14.29 o 4 15 0 118.25 79.25 8.36 o 5 15 0 17.59 52.04 6.97 o 6 15 0 137.86 216.31 21.13 o 0 16 0 31.01 48.66 9.88 o 1 16 0 0.26 4.24 9.77 o 2 16 0 21.53 -8.16 8.16 o 3 16 0 103.04 113.10 10.87 o -15 1 1 15.63 -5.03 14.09 o -14 1 1 0.12 -7.04 11.38 o -13 1 1 10.37 6.04 13.52 o -12 1 1 1432.96 1295.78 27.80 o -11 1 1 236.32 222.69 12.55 o -10 1 1 180.16 162.86 11.18 o -9 1 1 153.23 143.57 8.39 o -8 1 1 164.60 146.33 9.57 o -7 1 1 606.82 540.13 24.16 o -6 1 1 948.76 577.03 23.76 o -5 1 1 1682.76 1552.94 53.00 o -4 1 1 768.68 450.86 15.04 o -3 1 1 42.35 18.11 7.04 o 2 1 1 371.51 199.20 18.11 o 3 1 1 589.60 406.36 15.09 o 4 1 1 59.75 47.15 6.95 o 5 1 1 5890.49 5011.98 109.12 o 6 1 1 0.25 13.44 10.60 o 7 1 1 0.92 -4.76 15.09 o 8 1 1 84.71 70.65 5.15 o 9 1 1 347.01 289.39 15.39 o 10 1 1 1179.53 1095.93 34.44 o 11 1 1 1070.76 1048.84 42.68 o 12 1 1 2.36 0.11 17.10 o 13 1 1 0.01 9.96 10.95 o 14 1 1 11.21 11.65 13.08 o -15 2 1 3.23 -10.06 14.09 o -14 2 1 8.22 -16.10 16.10 o -13 2 1 47.44 65.66 14.94 o -12 2 1 127.83 117.65 14.38 o -11 2 1 370.14 343.63 15.02 o -10 2 1 39.33 37.45 6.26 o -9 2 1 470.09 448.61 11.99 o -8 2 1 429.92 422.45 13.36 o -7 2 1 152.70 164.73 19.12 o -6 2 1 216.87 246.03 18.33 o -5 2 1 37.03 32.09 5.51 o -4 2 1 347.85 258.75 13.86 o -3 2 1 1186.01 658.98 29.18 o 3 2 1 1.45 15.09 10.06 o 4 2 1 156.44 183.82 16.90 o 5 2 1 81.60 58.90 10.39 o 6 2 1 381.70 487.12 24.06 o 7 2 1 5.37 -1.60 11.54 o 8 2 1 86.02 102.45 4.80 o 9 2 1 457.89 400.28 14.30 o 10 2 1 435.20 455.68 24.20 o 11 2 1 0.07 19.55 13.86 o 12 2 1 431.29 476.29 30.18 o 13 2 1 49.83 45.90 14.74 o 14 2 1 57.67 41.25 17.10 o -15 3 1 13.57 22.13 14.09 o -14 3 1 0.42 -4.02 16.10 o -13 3 1 52.51 62.80 9.80 o -12 3 1 180.25 161.54 13.32 o -11 3 1 73.09 75.34 8.53 o -10 3 1 119.12 125.98 9.08 o -9 3 1 671.26 596.26 14.42 o -8 3 1 42.41 25.82 4.89 o -7 3 1 133.48 76.74 12.31 o -6 3 1 10.27 27.02 7.87 o -5 3 1 978.04 647.80 20.98 o -4 3 1 2630.40 1799.27 44.46 o -3 3 1 69.30 61.77 7.44 o -2 3 1 4088.67 2396.17 74.95 o -1 3 1 11.14 -2.09 4.36 o 0 3 1 1395.41 827.79 31.11 o 1 3 1 4475.60 2404.09 45.89 o 4 3 1 501.65 514.11 31.19 o 5 3 1 81.84 25.76 10.05 o 6 3 1 3774.64 3552.37 99.47 o 7 3 1 325.53 238.29 17.86 o 8 3 1 97.16 72.36 5.36 o 9 3 1 57.90 60.62 5.61 o 10 3 1 1581.15 1492.15 42.72 o 11 3 1 16.41 23.21 8.40 o 12 3 1 829.71 796.81 52.32 o 13 3 1 73.86 48.86 14.47 o 14 3 1 13.39 28.17 15.09 o -14 4 1 47.31 48.29 16.10 o -13 4 1 0.17 14.59 17.61 o -12 4 1 0.41 9.50 7.18 o -11 4 1 1373.46 1406.00 38.06 o -10 4 1 343.11 336.41 14.85 o -9 4 1 207.78 230.02 14.63 o -8 4 1 40.43 59.16 6.08 o -7 4 1 559.33 516.96 29.18 o -6 4 1 1271.52 986.59 93.06 o -5 4 1 947.74 675.22 22.73 o -4 4 1 195.27 172.53 18.11 o -3 4 1 17.36 13.48 7.01 o -2 4 1 276.79 189.50 14.47 o -1 4 1 353.63 258.61 18.51 o 0 4 1 327.71 200.66 11.08 o 1 4 1 843.42 627.21 16.24 o 2 4 1 508.44 407.69 12.96 o 3 4 1 986.41 767.42 21.31 o 5 4 1 406.46 526.33 24.63 o 6 4 1 163.98 144.04 14.99 o 7 4 1 421.49 398.87 16.45 o 8 4 1 74.22 62.80 5.68 o 9 4 1 12.30 16.47 6.95 o 10 4 1 1158.68 1110.51 31.37 o 11 4 1 28.58 38.75 10.07 o 12 4 1 0.66 14.09 18.11 o 13 4 1 65.14 59.66 14.02 o 14 4 1 18.47 30.18 14.09 o -14 5 1 0.41 7.04 14.09 o -13 5 1 43.50 39.84 10.56 o -12 5 1 818.25 883.97 24.11 o -11 5 1 52.42 67.87 8.80 o -10 5 1 554.41 552.11 18.73 o -9 5 1 2.10 -2.93 5.87 o -8 5 1 370.73 382.04 11.49 o -7 5 1 840.03 724.58 18.42 o -6 5 1 240.55 239.42 15.99 o -5 5 1 180.49 156.54 14.74 o -4 5 1 119.85 150.02 16.10 o -3 5 1 1439.10 1243.28 34.45 o -2 5 1 1214.86 1007.94 38.73 o -1 5 1 20.67 9.33 6.23 o 0 5 1 211.37 219.47 11.67 o 1 5 1 11.99 28.62 5.88 o 2 5 1 816.64 614.45 16.64 o 3 5 1 1166.57 832.91 24.16 o 4 5 1 577.67 441.67 24.15 o 6 5 1 289.92 253.75 14.53 o 7 5 1 358.77 328.41 11.15 o 8 5 1 18.51 24.33 6.45 o 9 5 1 27.12 17.14 6.50 o 10 5 1 248.04 224.21 14.27 o 11 5 1 9.21 -2.96 8.65 o 12 5 1 190.27 183.11 33.20 o 13 5 1 100.37 139.00 29.68 o -14 6 1 198.33 206.25 24.15 o -13 6 1 1.17 -1.51 8.19 o -12 6 1 58.23 60.66 8.33 o -11 6 1 624.74 718.36 22.63 o -10 6 1 474.74 555.04 20.77 o -9 6 1 126.30 108.89 8.23 o -8 6 1 41.17 42.16 5.77 o -7 6 1 384.27 340.27 10.57 o -6 6 1 0.95 -5.05 5.78 o -5 6 1 12.59 10.91 9.17 o -4 6 1 1176.50 1193.05 55.33 o -3 6 1 1435.10 1172.73 45.27 o -2 6 1 144.78 120.42 12.75 o -1 6 1 397.70 301.75 14.15 o 0 6 1 113.05 109.33 8.24 o 1 6 1 3119.20 2608.58 51.89 o 2 6 1 696.33 521.76 16.41 o 3 6 1 46.79 72.01 8.87 o 4 6 1 910.59 824.98 36.22 o 5 6 1 367.14 300.82 26.16 o 6 6 1 1683.95 1616.52 53.41 o 7 6 1 288.63 272.26 12.49 o 8 6 1 936.57 829.90 19.46 o 9 6 1 0.55 -5.67 7.95 o 10 6 1 4.94 18.15 7.27 o 11 6 1 59.31 37.68 13.58 o 12 6 1 61.89 43.30 20.12 o 13 6 1 283.58 324.55 22.72 o -13 7 1 85.01 82.91 7.26 o -12 7 1 97.00 146.03 13.96 o -11 7 1 15.67 20.68 8.14 o -10 7 1 244.87 209.55 14.51 o -9 7 1 60.19 67.26 16.37 o -8 7 1 29.25 30.72 6.02 o -7 7 1 6.52 6.17 5.08 o -6 7 1 337.81 308.39 12.67 o -5 7 1 111.73 133.41 9.73 o -4 7 1 98.44 116.70 12.75 o -3 7 1 1484.98 1406.64 39.76 o -2 7 1 117.27 172.99 18.61 o -1 7 1 1608.97 1505.90 38.13 o 0 7 1 58.33 60.35 7.97 o 1 7 1 3329.71 3331.04 65.25 o 2 7 1 123.61 134.06 10.13 o 3 7 1 83.02 93.30 11.57 o 4 7 1 9.04 7.04 10.56 o 5 7 1 1366.97 1232.43 24.42 o 6 7 1 926.19 860.24 18.28 o 7 7 1 2282.53 2218.36 37.63 o 8 7 1 389.87 401.34 16.46 o 9 7 1 905.95 978.03 24.20 o 10 7 1 167.72 177.61 14.64 o 11 7 1 22.95 19.02 6.57 o 12 7 1 132.26 199.04 17.51 o -13 8 1 14.48 6.71 7.55 o -12 8 1 65.52 61.17 7.33 o -11 8 1 18.47 17.22 8.24 o -10 8 1 240.96 260.36 16.94 o -9 8 1 308.71 236.12 13.62 o -8 8 1 5.49 17.97 7.23 o -7 8 1 790.33 742.61 15.59 o -6 8 1 649.57 646.06 16.37 o -5 8 1 52.42 56.75 6.56 o -4 8 1 795.70 743.01 21.08 o -3 8 1 570.75 547.82 19.48 o -2 8 1 33.78 34.04 10.87 o -1 8 1 1721.83 1620.78 36.39 o 0 8 1 38.29 42.78 8.61 o 1 8 1 6.06 1.33 7.89 o 2 8 1 3.27 11.07 9.96 o 3 8 1 498.15 416.91 16.76 o 4 8 1 554.76 461.02 20.55 o 5 8 1 19.10 30.96 6.80 o 6 8 1 58.40 49.92 6.00 o 7 8 1 815.30 773.98 20.03 o 8 8 1 2317.83 2494.70 54.96 o 9 8 1 8.28 -2.15 10.75 o 10 8 1 461.09 501.51 17.06 o 11 8 1 43.00 49.47 7.16 o 12 8 1 49.38 41.91 8.90 o -12 9 1 48.64 46.32 13.58 o -11 9 1 0.34 11.82 8.12 o -10 9 1 50.52 63.34 11.01 o -9 9 1 114.23 110.28 9.91 o -8 9 1 27.03 30.65 7.95 o -7 9 1 70.64 74.25 7.43 o -6 9 1 1537.78 1539.95 24.92 o -5 9 1 233.58 204.42 11.98 o -4 9 1 1562.11 1413.97 25.76 o -3 9 1 743.01 609.92 15.76 o -2 9 1 821.88 829.55 25.80 o -1 9 1 156.18 181.87 14.50 o 0 9 1 208.86 199.91 13.21 o 1 9 1 905.71 864.63 23.02 o 2 9 1 444.88 421.68 13.83 o 3 9 1 702.13 563.06 17.00 o 4 9 1 16.30 21.80 7.81 o 5 9 1 283.92 269.94 12.41 o 6 9 1 109.76 132.98 8.53 o 7 9 1 1810.89 1857.05 36.50 o 8 9 1 518.87 570.41 20.34 o 9 9 1 413.94 525.18 21.20 o 10 9 1 123.72 133.68 11.53 o 11 9 1 14.83 27.27 7.17 o -12 10 1 46.35 45.27 10.06 o -11 10 1 181.79 226.69 15.99 o -10 10 1 13.58 12.00 9.58 o -9 10 1 396.98 452.79 25.36 o -8 10 1 15.33 21.07 8.26 o -7 10 1 1778.60 1728.82 30.01 o -6 10 1 158.37 208.33 14.71 o -5 10 1 1.67 0.75 8.20 o -4 10 1 1099.11 944.42 23.07 o -3 10 1 771.02 618.47 16.83 o -2 10 1 154.02 156.91 9.47 o -1 10 1 76.05 72.14 7.04 o 0 10 1 1651.20 1448.04 22.67 o 1 10 1 1253.12 1091.92 25.08 o 2 10 1 810.93 635.24 16.91 o 3 10 1 233.61 142.98 10.55 o 4 10 1 1869.44 1721.52 34.08 o 5 10 1 429.39 448.52 13.91 o 6 10 1 118.25 93.89 7.60 o 7 10 1 271.26 346.28 15.44 o 8 10 1 304.07 235.16 19.92 o 9 10 1 96.35 115.37 11.72 o 10 10 1 8.96 17.06 8.87 o 11 10 1 38.03 32.55 14.09 o -11 11 1 40.13 37.58 8.45 o -10 11 1 291.44 285.23 17.79 o -9 11 1 46.69 55.37 9.15 o -8 11 1 473.72 449.65 16.14 o -7 11 1 490.42 508.74 18.61 o -6 11 1 21.26 22.48 8.72 o -5 11 1 161.54 211.69 13.00 o -4 11 1 682.47 667.98 23.67 o 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