#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/86/2018605.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018605_Fobs loop_ _publ_author_name 'Domasevitch, Konstantin V.' 'Rusanova, Julia A.' 'Gural'skiy, Ilya A.' 'Solntsev, Pavlo V.' _publ_section_title ; Cadmium(II) chloride, bromide and iodide complexes with 4,4'-bipyridazine: when are diazine and halide bridges (in)compatible? ; _journal_coeditor_code EG3098 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m295 _journal_page_last m299 _journal_volume 68 _journal_year 2012 _space_group_IT_number 63 _symmetry_space_group_name_Hall '-C 2c 2' _symmetry_space_group_name_H-M 'C m c m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.7549 _cell_length_b 11.9619 _cell_length_c 7.8690 _exptl_crystal_F_000 800.00 _reflns_d_resolution_high 0.7450 _[local]_cod_data_source_file eg3098IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' ip77 in Cmcm' _shelx_refln_list_code 4 _shelx_f_calc_maximum 432.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x, y, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y, -z-1/2' 'x, -y, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z-1/2' 'x+1/2, -y+1/2, z-1/2' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 109450.60 108764.10 259.85 o 4 0 0 151911.94 150060.78 592.23 o 6 0 0 61652.66 68597.23 243.56 o 8 0 0 77263.93 79451.62 232.16 o 10 0 0 33166.42 33572.46 153.34 o 12 0 0 19812.47 20880.33 124.74 o 14 0 0 15550.75 15480.30 136.98 o 1 1 0 56738.07 51944.66 203.45 o 3 1 0 86448.02 87159.73 480.43 o 5 1 0 94576.08 90782.50 195.86 o 7 1 0 36286.02 36619.77 355.30 o 9 1 0 25516.75 26483.61 238.71 o 11 1 0 27256.41 29576.36 281.45 o 13 1 0 8888.20 9768.99 81.78 o 15 1 0 7587.10 8121.55 104.84 o 0 2 0 42146.71 42056.10 197.41 o 2 2 0 376.30 393.54 29.70 o 4 2 0 6053.18 6894.15 55.26 o 6 2 0 1253.93 1310.54 47.10 o 8 2 0 1755.98 1585.41 40.89 o 10 2 0 2022.41 2001.52 48.06 o 12 2 0 1092.63 1198.26 67.45 o 14 2 0 2637.14 2711.42 95.66 o 1 3 0 5501.99 5922.13 116.96 o 3 3 0 14142.36 13822.69 232.06 o 5 3 0 638.65 579.75 33.12 o 7 3 0 1121.51 1081.48 39.53 o 9 3 0 216.82 187.52 40.67 o 11 3 0 62.73 68.34 40.08 o 13 3 0 36.87 84.24 57.11 o 15 3 0 381.98 323.61 65.97 o 0 4 0 825.92 728.92 35.27 o 2 4 0 2641.81 3055.81 59.61 o 4 4 0 648.36 688.37 28.33 o 6 4 0 1657.06 1675.09 31.04 o 8 4 0 2160.89 1941.24 37.68 o 10 4 0 2206.64 2132.47 46.69 o 12 4 0 453.38 370.48 47.38 o 14 4 0 2276.50 2682.70 70.97 o 1 5 0 50083.26 51522.91 854.22 o 3 5 0 13768.83 13109.45 166.36 o 5 5 0 35542.18 37172.96 344.35 o 7 5 0 22298.29 22969.13 184.89 o 9 5 0 27212.67 26426.60 310.41 o 11 5 0 6195.41 5993.29 51.37 o 13 5 0 5343.24 5038.56 56.60 o 0 6 0 79540.38 83956.86 144.31 o 2 6 0 106531.92 115256.71 1313.21 o 4 6 0 71591.53 72935.03 1143.10 o 6 6 0 61923.76 62936.45 554.42 o 8 6 0 17037.72 17266.62 119.71 o 10 6 0 33134.00 32727.96 202.57 o 12 6 0 14186.35 15835.17 65.84 o 14 6 0 13786.34 13135.33 176.50 o 1 7 0 49819.00 52265.31 1025.88 o 3 7 0 31184.81 29645.47 491.12 o 5 7 0 44603.59 43316.38 364.53 o 7 7 0 26431.66 26759.91 322.21 o 9 7 0 25855.58 27533.07 163.10 o 11 7 0 11605.03 10732.57 74.12 o 13 7 0 6774.53 6405.93 76.04 o 0 8 0 9068.81 8809.30 330.83 o 2 8 0 1781.15 1821.41 52.01 o 4 8 0 2934.20 2940.15 37.99 o 6 8 0 1718.67 1833.75 28.78 o 8 8 0 1017.85 1009.84 34.80 o 10 8 0 1932.45 2018.38 41.84 o 12 8 0 758.42 671.22 49.08 o 1 9 0 6010.67 5392.87 173.21 o 3 9 0 2995.69 2774.75 46.84 o 5 9 0 633.21 705.53 31.81 o 7 9 0 1667.69 1628.80 35.81 o 9 9 0 602.96 669.64 32.71 o 11 9 0 155.73 156.69 60.53 o 13 9 0 90.66 78.56 96.69 o 0 10 0 1235.42 1304.81 104.10 o 2 10 0 3853.42 3616.18 134.72 o 4 10 0 483.83 495.28 26.41 o 6 10 0 1802.09 1589.01 26.56 o 8 10 0 53.81 84.64 37.55 o 10 10 0 232.54 293.63 48.73 o 12 10 0 55.71 151.08 136.98 o 1 11 0 3026.35 2885.43 95.97 o 3 11 0 4977.61 4936.06 151.40 o 5 11 0 6866.71 6142.23 141.85 o 7 11 0 2861.48 2680.10 32.20 o 9 11 0 2271.15 2191.77 52.36 o 11 11 0 4138.68 4081.48 79.47 o 0 12 0 32926.15 34074.49 1347.62 o 2 12 0 16143.14 15788.75 464.84 o 4 12 0 19691.51 18052.76 395.21 o 6 12 0 11473.56 10930.18 207.01 o 8 12 0 10585.19 10989.91 192.91 o 10 12 0 6838.52 7584.05 179.88 o 1 13 0 13824.60 14165.28 407.31 o 3 13 0 10381.95 10326.85 397.10 o 5 13 0 12995.28 11865.14 265.74 o 7 13 0 8354.00 8457.27 209.34 o 9 13 0 7838.12 7437.07 155.11 o 0 14 0 659.84 797.12 59.56 o 2 14 0 1203.86 1254.27 32.50 o 4 14 0 980.38 922.72 34.99 o 6 14 0 1026.37 1059.38 59.82 o 1 15 0 1231.08 1390.04 44.64 o 3 15 0 2931.76 3295.85 71.02 o 5 15 0 754.02 745.32 94.68 o 1 1 1 17.27 40.23 16.85 o 3 1 1 30.45 48.35 27.41 o 5 1 1 38.97 45.78 31.86 o 7 1 1 43.81 49.78 27.29 o 9 1 1 0.50 19.40 33.65 o 11 1 1 14.85 11.42 31.89 o 13 1 1 0.03 20.67 33.11 o 15 1 1 20.33 38.80 44.86 o 0 2 1 59.36 84.58 22.06 o 2 2 1 47.03 54.14 14.99 o 4 2 1 284.89 348.16 20.87 o 6 2 1 73.80 73.09 26.88 o 8 2 1 134.96 122.71 24.04 o 10 2 1 64.92 72.69 31.58 o 12 2 1 58.74 51.03 34.81 o 14 2 1 61.31 88.52 48.82 o 1 3 1 1026.75 1129.21 17.49 o 3 3 1 1392.00 1392.96 17.77 o 5 3 1 456.31 480.93 21.55 o 7 3 1 568.25 584.86 25.65 o 9 3 1 159.92 111.74 29.92 o 11 3 1 400.65 363.03 31.76 o 13 3 1 135.66 120.39 38.15 o 15 3 1 227.57 298.02 52.74 o 0 4 1 3920.89 3767.12 41.07 o 2 4 1 1186.51 1277.13 16.74 o 4 4 1 1745.85 1760.40 22.39 o 6 4 1 1405.01 1569.91 24.47 o 8 4 1 1651.88 1557.02 26.55 o 10 4 1 801.67 645.00 29.66 o 12 4 1 376.70 277.41 32.73 o 14 4 1 377.97 384.05 46.32 o 1 5 1 3035.29 3168.03 22.80 o 3 5 1 3780.93 4061.46 35.43 o 5 5 1 2584.81 2612.02 22.00 o 7 5 1 981.46 1034.85 20.91 o 9 5 1 763.92 751.73 26.89 o 11 5 1 1081.37 860.27 31.67 o 13 5 1 753.85 726.34 36.93 o 0 6 1 2823.00 2949.91 64.71 o 2 6 1 2220.34 2265.98 31.69 o 4 6 1 1543.47 1468.47 18.18 o 6 6 1 2267.90 2365.48 24.44 o 8 6 1 2268.90 2406.33 28.09 o 10 6 1 1148.01 1126.03 30.66 o 12 6 1 586.76 487.35 37.25 o 14 6 1 473.81 383.41 48.54 o 1 7 1 2619.17 2586.45 34.92 o 3 7 1 2451.74 2543.16 31.08 o 5 7 1 1867.45 1846.10 20.19 o 7 7 1 841.90 899.44 22.80 o 9 7 1 879.95 923.02 22.73 o 11 7 1 768.22 687.33 31.67 o 13 7 1 944.10 787.05 44.12 o 0 8 1 1083.15 1134.48 26.67 o 2 8 1 2236.10 2194.95 27.62 o 4 8 1 1769.58 1634.64 23.59 o 6 8 1 2016.72 1969.35 22.60 o 8 8 1 1502.98 1584.85 23.91 o 10 8 1 1280.28 1357.28 29.10 o 12 8 1 987.18 996.35 40.15 o 1 9 1 3998.45 3894.52 62.48 o 3 9 1 2076.19 2045.90 35.74 o 5 9 1 1808.86 1806.90 24.64 o 7 9 1 1708.92 1698.28 24.78 o 9 9 1 1576.86 1662.59 28.13 o 11 9 1 676.59 708.92 33.73 o 0 10 1 1574.55 1553.25 41.71 o 2 10 1 2918.32 2855.14 62.80 o 4 10 1 3880.68 3629.18 51.97 o 6 10 1 2869.88 2766.52 27.61 o 8 10 1 1670.38 1649.50 28.09 o 10 10 1 2003.25 2230.19 39.22 o 12 10 1 1730.80 1583.30 143.02 o 1 11 1 4906.65 4972.71 85.79 o 3 11 1 2641.87 2441.49 42.97 o 5 11 1 1994.12 1921.36 29.66 o 7 11 1 2377.62 2353.10 42.44 o 9 11 1 1896.08 1998.18 34.37 o 11 11 1 1025.06 1092.92 51.11 o 0 12 1 1765.67 1741.16 45.23 o 2 12 1 2192.70 2256.37 34.37 o 4 12 1 2922.88 2766.52 51.84 o 6 12 1 2534.75 2524.27 49.30 o 8 12 1 1899.46 1813.57 44.02 o 10 12 1 1792.42 2006.32 122.88 o 1 13 1 2391.21 2444.52 52.13 o 3 13 1 2339.34 2382.66 46.48 o 5 13 1 1550.98 1472.08 39.90 o 7 13 1 1241.52 1249.03 43.72 o 9 13 1 901.16 821.86 112.80 o 0 14 1 1872.83 1971.73 65.46 o 2 14 1 1250.12 1290.50 32.12 o 4 14 1 1131.56 1088.02 29.64 o 6 14 1 1656.37 1566.16 37.40 o 1 15 1 1460.09 1574.13 34.52 o 3 15 1 2319.89 2552.66 63.60 o 5 15 1 1653.18 1551.07 134.96 o 0 0 2 29875.51 28930.44 147.05 o 2 0 2 22281.33 20531.17 2580.70 o 4 0 2 1502.55 1509.76 50.11 o 6 0 2 7259.26 7931.04 117.46 o 8 0 2 123.50 171.51 40.65 o 10 0 2 546.81 529.77 46.50 o 12 0 2 131.71 100.59 46.65 o 14 0 2 321.27 199.61 62.12 o 1 1 2 750.99 702.62 24.42 o 3 1 2 1619.81 1794.93 35.57 o 5 1 2 8359.51 8913.48 175.78 o 7 1 2 822.35 881.11 30.74 o 9 1 2 1151.90 1254.93 36.96 o 11 1 2 4495.57 4511.65 59.96 o 13 1 2 669.24 784.69 45.37 o 15 1 2 1484.95 1478.97 51.65 o 0 2 2 135231.17 131186.09 290.07 o 2 2 2 45191.50 49295.54 503.00 o 4 2 2 55096.86 61896.25 591.86 o 6 2 2 28920.77 27303.31 529.86 o 8 2 2 21790.27 21245.62 55.70 o 10 2 2 15958.78 15510.73 358.98 o 12 2 2 8830.38 9446.10 93.05 o 14 2 2 8739.68 9367.35 137.24 o 1 3 2 130504.68 128120.21 298.13 o 3 3 2 81806.81 85950.47 1347.67 o 5 3 2 95663.93 106863.23 823.74 o 7 3 2 58063.26 55886.44 824.87 o 9 3 2 49608.63 47870.91 73.82 o 11 3 2 25075.63 22608.54 420.86 o 13 3 2 13136.03 13658.72 156.94 o 15 3 2 9991.41 9628.71 163.16 o 0 4 2 54282.93 56177.32 988.41 o 2 4 2 79933.70 88384.25 1660.85 o 4 4 2 55251.32 57683.04 544.42 o 6 4 2 46007.66 48432.95 293.81 o 8 4 2 10787.49 10603.40 68.66 o 10 4 2 24121.60 23765.16 49.71 o 12 4 2 10749.96 10646.57 46.78 o 14 4 2 10988.80 11841.37 105.21 o 1 5 2 5834.84 6327.31 58.09 o 3 5 2 13.80 56.87 15.92 o 5 5 2 5291.31 5627.80 40.56 o 7 5 2 3136.59 3314.85 43.47 o 9 5 2 7696.13 7145.78 64.42 o 11 5 2 616.33 587.55 42.94 o 13 5 2 1068.75 1008.15 37.63 o 0 6 2 6108.35 5847.00 114.11 o 2 6 2 992.61 833.67 15.92 o 4 6 2 2388.15 2151.34 24.84 o 6 6 2 593.60 528.76 17.16 o 8 6 2 6848.53 7179.86 36.02 o 10 6 2 160.44 162.12 28.03 o 12 6 2 83.65 69.89 33.10 o 14 6 2 687.87 740.16 50.76 o 1 7 2 295.33 313.47 39.98 o 3 7 2 1812.68 1869.17 24.15 o 5 7 2 223.91 251.34 14.42 o 7 7 2 39.19 54.93 21.56 o 9 7 2 819.84 895.33 30.23 o 11 7 2 81.40 61.02 33.11 o 13 7 2 93.33 74.98 42.87 o 0 8 2 24965.66 23867.49 276.74 o 2 8 2 11816.63 11206.15 91.12 o 4 8 2 12812.34 12565.68 146.38 o 6 8 2 8693.31 8734.68 91.32 o 8 8 2 5614.36 5803.04 69.90 o 10 8 2 5906.62 6206.91 54.32 o 12 8 2 2809.86 2750.68 46.00 o 1 9 2 34050.29 34513.78 378.38 o 3 9 2 36475.27 34416.87 400.63 o 5 9 2 37561.43 35116.03 369.25 o 7 9 2 21219.19 21289.60 229.68 o 9 9 2 15883.51 16437.88 158.60 o 11 9 2 15195.13 16696.34 152.21 o 0 10 2 48619.01 48769.58 917.52 o 2 10 2 16726.90 16221.72 269.91 o 4 10 2 22879.69 21024.06 270.94 o 6 10 2 12125.56 11621.83 155.86 o 8 10 2 15801.52 16016.75 151.28 o 10 10 2 7137.57 7597.10 111.41 o 1 11 2 524.42 518.15 16.13 o 3 11 2 1493.30 1492.86 24.87 o 5 11 2 2847.40 2534.40 43.11 o 7 11 2 895.15 902.31 30.00 o 9 11 2 825.98 814.46 34.09 o 11 11 2 2277.72 2314.52 128.92 o 0 12 2 298.19 319.21 25.12 o 2 12 2 3589.28 3551.55 66.06 o 4 12 2 1188.92 1155.08 22.52 o 6 12 2 1973.63 1898.85 27.75 o 8 12 2 619.64 679.70 35.67 o 10 12 2 339.69 358.56 120.86 o 1 13 2 1647.03 1749.07 31.16 o 3 13 2 2234.01 2395.69 39.36 o 5 13 2 490.30 519.33 28.15 o 7 13 2 591.92 572.89 34.13 o 0 14 2 870.31 866.46 38.86 o 2 14 2 1395.25 1397.93 24.26 o 4 14 2 1154.35 1118.21 28.99 o 6 14 2 1152.05 1133.59 39.05 o 1 15 2 8458.05 8655.19 172.52 o 3 15 2 4620.60 4732.98 76.68 o 1 1 3 1383.90 1345.85 53.68 o 3 1 3 1214.95 1241.75 42.27 o 5 1 3 514.42 520.96 28.68 o 7 1 3 724.22 671.11 34.83 o 9 1 3 295.72 320.62 33.84 o 11 1 3 262.68 321.07 36.52 o 13 1 3 97.86 85.60 39.00 o 15 1 3 114.93 104.75 112.80 o 0 2 3 1884.74 1835.33 36.03 o 2 2 3 1610.46 1641.72 32.43 o 4 2 3 1929.62 2031.93 33.10 o 6 2 3 1129.88 1087.71 36.07 o 8 2 3 896.21 805.58 32.37 o 10 2 3 557.68 537.88 31.95 o 12 2 3 351.46 344.59 36.83 o 14 2 3 243.11 261.46 48.87 o 1 3 3 983.21 1073.73 20.80 o 3 3 3 1142.95 1169.40 21.25 o 5 3 3 495.22 513.99 21.82 o 7 3 3 544.66 536.20 23.24 o 9 3 3 205.27 141.17 31.36 o 11 3 3 368.38 366.93 35.58 o 13 3 3 148.55 120.96 44.22 o 0 4 3 461.42 443.78 23.05 o 2 4 3 20.40 42.07 17.13 o 4 4 3 141.20 128.44 17.08 o 6 4 3 166.96 199.03 17.99 o 8 4 3 345.03 341.67 29.21 o 10 4 3 164.93 132.91 31.50 o 12 4 3 68.41 70.34 36.55 o 14 4 3 119.31 91.64 42.67 o 1 5 3 258.37 265.11 16.68 o 3 5 3 513.31 563.24 15.45 o 5 5 3 327.79 318.86 18.22 o 7 5 3 49.02 55.88 25.35 o 9 5 3 64.00 37.38 22.53 o 11 5 3 272.96 249.05 29.33 o 13 5 3 242.84 229.97 44.62 o 0 6 3 1516.63 1551.19 27.04 o 2 6 3 1174.32 1181.02 18.21 o 4 6 3 859.48 826.57 16.10 o 6 6 3 1334.33 1391.05 25.05 o 8 6 3 1470.54 1525.46 24.83 o 10 6 3 752.75 713.13 28.62 o 12 6 3 399.10 298.18 37.44 o 1 7 3 4240.14 4071.59 26.36 o 3 7 3 3951.13 3791.83 41.40 o 5 7 3 3066.90 3013.11 39.91 o 7 7 3 1673.94 1742.73 22.51 o 9 7 3 1467.88 1569.56 31.22 o 11 7 3 1197.75 1171.03 40.97 o 13 7 3 1204.65 1084.77 53.73 o 0 8 3 3282.17 3167.13 76.57 o 2 8 3 4403.76 4285.66 29.01 o 4 8 3 3785.03 3653.64 51.13 o 6 8 3 3636.72 3534.92 40.17 o 8 8 3 2779.67 2931.16 31.36 o 10 8 3 2103.84 2252.19 35.18 o 12 8 3 1504.98 1500.59 44.47 o 1 9 3 4093.72 4084.20 41.20 o 3 9 3 2419.77 2274.34 21.68 o 5 9 3 2052.11 1982.29 28.88 o 7 9 3 1859.67 1862.56 29.41 o 9 9 3 1641.09 1754.77 31.86 o 11 9 3 797.75 868.02 40.34 o 0 10 3 500.55 496.06 24.32 o 2 10 3 1193.27 1193.77 19.34 o 4 10 3 1851.58 1685.30 23.24 o 6 10 3 1409.34 1353.15 23.93 o 8 10 3 835.53 830.64 32.55 o 10 10 3 1141.40 1274.55 44.20 o 1 11 3 1809.99 1843.60 21.10 o 3 11 3 766.32 729.43 20.83 o 5 11 3 557.71 529.82 24.89 o 7 11 3 865.90 829.21 27.34 o 9 11 3 768.94 777.84 36.93 o 0 12 3 904.77 911.73 28.66 o 2 12 3 1228.34 1206.87 19.90 o 4 12 3 1741.71 1693.56 31.52 o 6 12 3 1596.75 1594.12 33.14 o 8 12 3 1222.19 1187.01 36.86 o 1 13 3 2921.56 3066.86 47.78 o 3 13 3 2774.77 2855.15 44.80 o 5 13 3 1933.91 1937.97 36.23 o 7 13 3 1530.32 1516.61 38.52 o 0 14 3 2939.25 3335.74 67.56 o 2 14 3 2262.74 2366.34 37.68 o 4 14 3 2036.65 2002.34 56.98 o 6 14 3 2485.34 2294.37 70.50 o 1 15 3 1846.65 2012.99 38.24 o 3 15 3 2581.81 2391.06 76.55 o 0 0 4 186785.84 170589.27 338.41 o 2 0 4 62181.50 58638.42 261.87 o 4 0 4 76078.63 79352.59 3173.53 o 6 0 4 39779.25 36220.46 1272.32 o 8 0 4 44471.19 45480.80 3052.58 o 10 0 4 21911.59 24629.88 1035.07 o 12 0 4 13585.69 13316.55 90.29 o 14 0 4 11015.50 11789.40 301.80 o 1 1 4 32832.86 36840.77 2118.73 o 3 1 4 40601.27 40908.00 1354.18 o 5 1 4 46453.19 47814.72 989.05 o 7 1 4 22691.60 22634.18 1021.75 o 9 1 4 17025.34 17260.79 981.30 o 11 1 4 17384.63 17989.07 576.64 o 13 1 4 6276.68 6259.22 52.20 o 0 2 4 11911.60 11862.40 89.43 o 2 2 4 748.26 838.56 26.16 o 4 2 4 2895.71 2878.02 61.11 o 6 2 4 883.72 858.76 25.53 o 8 2 4 1049.44 1065.62 50.44 o 10 2 4 1395.96 1560.82 121.25 o 12 2 4 876.03 988.59 46.20 o 14 2 4 2010.09 2037.60 56.53 o 1 3 4 2629.62 2641.01 32.23 o 3 3 4 5342.04 5326.19 74.05 o 5 3 4 461.54 442.07 20.87 o 7 3 4 587.95 520.49 28.38 o 9 3 4 144.00 125.70 26.51 o 11 3 4 39.57 24.02 33.27 o 13 3 4 21.41 23.35 42.11 o 0 4 4 48.91 60.71 23.00 o 2 4 4 894.97 937.79 19.34 o 4 4 4 347.37 378.64 17.78 o 6 4 4 698.68 694.99 23.78 o 8 4 4 824.75 754.28 27.08 o 10 4 4 1329.06 1191.88 35.99 o 12 4 4 391.48 322.38 40.69 o 14 4 4 1678.88 1679.99 157.12 o 1 5 4 25221.33 25208.53 277.77 o 3 5 4 10404.02 10102.85 97.76 o 5 5 4 20412.28 20589.88 241.86 o 7 5 4 14210.33 14219.38 202.11 o 9 5 4 16867.72 16058.08 567.62 o 11 5 4 4695.91 4263.65 103.44 o 13 5 4 3797.80 3266.68 139.55 o 0 6 4 48511.31 48624.47 423.48 o 2 6 4 58503.67 57353.36 383.94 o 4 6 4 43173.00 44300.25 464.90 o 6 6 4 37121.21 37754.82 424.79 o 8 6 4 12380.62 13061.46 82.91 o 10 6 4 21128.64 20215.65 750.53 o 12 6 4 9800.19 8928.30 239.03 o 1 7 4 29118.30 28863.48 331.66 o 3 7 4 20252.34 19672.91 191.48 o 5 7 4 27118.71 26927.56 389.27 o 7 7 4 17387.63 16725.78 291.28 o 9 7 4 16875.97 17050.32 234.05 o 11 7 4 8184.12 8044.36 312.70 o 0 8 4 5023.43 4961.82 56.69 o 2 8 4 1290.87 1199.16 18.86 o 4 8 4 1842.75 1821.93 22.68 o 6 8 4 1146.67 1156.15 24.89 o 8 8 4 720.98 735.16 28.49 o 10 8 4 1364.50 1376.55 35.07 o 12 8 4 616.60 568.05 122.88 o 1 9 4 3564.57 3389.30 31.28 o 3 9 4 1895.55 1806.74 23.59 o 5 9 4 408.57 394.17 24.05 o 7 9 4 911.75 954.40 24.30 o 9 9 4 284.02 331.34 35.96 o 11 9 4 118.70 92.88 45.23 o 0 10 4 536.44 583.39 21.46 o 2 10 4 1958.50 1905.34 27.53 o 4 10 4 307.45 335.85 22.88 o 6 10 4 974.39 938.80 27.48 o 8 10 4 33.95 52.16 28.88 o 10 10 4 101.50 121.84 38.11 o 1 11 4 2141.11 2069.11 24.97 o 3 11 4 3245.39 2986.60 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5 280.10 268.06 40.88 o 1 9 5 1467.46 1485.18 22.73 o 3 9 5 822.29 809.00 23.13 o 5 9 5 693.93 690.24 27.26 o 7 9 5 677.33 679.21 29.22 o 9 9 5 658.41 708.78 40.19 o 0 10 5 1843.18 1806.24 38.79 o 2 10 5 2585.63 2561.83 29.48 o 4 10 5 3123.78 2962.92 41.24 o 6 10 5 2485.07 2571.96 48.16 o 8 10 5 1679.19 1813.09 55.95 o 1 11 5 4694.64 4733.01 49.15 o 3 11 5 3110.96 3264.90 42.71 o 5 11 5 2426.58 2430.95 51.72 o 7 11 5 2413.09 2474.19 59.77 o 0 12 5 1497.99 1595.78 34.65 o 2 12 5 1836.23 1839.09 23.01 o 4 12 5 2194.23 2146.78 34.05 o 6 12 5 2007.45 1974.05 42.55 o 1 13 5 977.84 974.76 26.74 o 3 13 5 914.86 928.51 29.93 o 5 13 5 612.21 564.02 52.37 o 0 14 5 395.78 366.62 54.39 o 0 0 6 1013.73 1019.27 132.95 o 2 0 6 2995.88 2683.13 151.46 o 4 0 6 630.93 626.52 44.73 o 6 0 6 1631.89 1753.89 42.21 o 8 0 6 64.67 90.63 52.66 o 10 0 6 120.34 105.77 71.55 o 12 0 6 21.75 76.27 76.15 o 1 1 6 30.34 38.27 94.68 o 3 1 6 459.31 412.19 40.74 o 5 1 6 2026.86 2052.04 45.29 o 7 1 6 548.53 512.61 31.39 o 9 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27.81 o 8 6 6 1930.59 2069.08 35.53 o 10 6 6 73.47 71.84 40.59 o 1 7 6 135.20 133.31 18.21 o 3 7 6 426.57 410.83 27.37 o 5 7 6 102.79 111.10 26.45 o 7 7 6 36.37 47.06 31.56 o 9 7 6 449.29 357.66 40.54 o 11 7 6 125.24 116.83 58.42 o 0 8 6 9552.11 9539.20 159.71 o 2 8 6 5375.12 4949.69 67.40 o 4 8 6 5444.06 5330.24 71.53 o 6 8 6 3881.46 3837.59 86.48 o 8 8 6 2632.11 2800.15 49.45 o 10 8 6 2856.40 2896.67 118.85 o 1 9 6 14519.35 14099.51 171.66 o 3 9 6 15230.36 14649.92 189.73 o 5 9 6 16086.87 16616.25 224.17 o 7 9 6 9966.02 10146.94 322.13 o 9 9 6 7846.23 8199.91 257.20 o 0 10 6 18799.86 19019.64 308.69 o 2 10 6 8262.21 8447.83 117.97 o 4 10 6 9914.67 9920.02 172.11 o 6 10 6 5863.60 6524.19 134.76 o 8 10 6 6641.87 7049.62 202.74 o 1 11 6 331.65 394.50 25.12 o 3 11 6 681.04 658.26 26.85 o 5 11 6 1337.89 1343.12 37.61 o 7 11 6 567.07 517.69 72.52 o 0 12 6 150.39 221.75 41.95 o 2 12 6 1193.10 1154.60 28.30 o 4 12 6 446.45 521.27 34.51 o 1 13 6 639.87 584.17 84.60 o 1 1 7 1380.77 1222.72 138.99 o 3 1 7 1183.28 1162.65 50.50 o 5 1 7 856.53 894.42 41.46 o 7 1 7 752.94 755.24 34.72 o 9 1 7 462.85 485.00 44.44 o 11 1 7 304.07 275.98 52.08 o 0 2 7 1624.65 1462.44 145.03 o 2 2 7 1693.35 1765.75 90.01 o 4 2 7 1570.80 1557.87 40.62 o 6 2 7 1254.13 1264.17 35.42 o 8 2 7 835.54 892.65 38.85 o 10 2 7 626.60 666.86 52.84 o 1 3 7 395.51 358.43 60.37 o 3 3 7 357.06 332.09 44.06 o 5 3 7 229.69 222.62 33.20 o 7 3 7 219.64 217.80 31.22 o 9 3 7 135.28 146.41 39.17 o 11 3 7 148.89 157.72 56.03 o 0 4 7 71.40 72.40 50.91 o 2 4 7 102.51 84.59 35.44 o 4 4 7 58.14 55.67 33.31 o 6 4 7 13.76 18.25 30.76 o 8 4 7 3.45 14.40 35.36 o 10 4 7 3.84 29.43 44.99 o 1 5 7 71.63 69.97 33.20 o 3 5 7 31.62 29.09 33.77 o 5 5 7 33.16 50.55 28.17 o 7 5 7 55.36 61.22 36.84 o 9 5 7 20.59 33.96 42.59 o 0 6 7 331.20 313.81 38.23 o 2 6 7 243.60 262.28 28.30 o 4 6 7 234.85 238.25 29.92 o 6 6 7 351.69 338.23 33.83 o 8 6 7 458.36 400.76 42.44 o 10 6 7 264.22 235.68 98.70 o 1 7 7 2518.41 2583.99 48.18 o 3 7 7 2386.62 2366.94 31.14 o 5 7 7 1891.55 1860.52 49.80 o 7 7 7 1217.28 1172.00 49.95 o 9 7 7 980.90 1031.13 48.18 o 0 8 7 2746.94 2715.14 53.16 o 2 8 7 2832.90 2961.73 46.20 o 4 8 7 2744.45 2903.81 64.38 o 6 8 7 2453.72 2439.42 91.32 o 8 8 7 2068.21 2058.36 72.13 o 1 9 7 1891.71 1905.30 42.40 o 3 9 7 1352.98 1365.76 31.57 o 5 9 7 1104.95 1144.70 36.80 o 7 9 7 950.37 1008.20 53.33 o 0 10 7 64.26 59.51 33.60 o 2 10 7 183.87 178.12 30.86 o 4 10 7 364.02 338.16 34.89 o 6 10 7 336.17 314.24 110.79 o 1 11 7 226.82 189.40 31.80 o 3 11 7 69.98 78.00 34.26 o 0 12 7 236.48 213.52 72.52 o 0 0 8 32625.56 31956.03 179.28 o 2 0 8 18018.07 15792.69 145.03 o 4 0 8 18633.25 18495.96 1370.73 o 6 0 8 12029.21 13165.94 459.12 o 8 0 8 11561.96 11951.27 463.11 o 10 0 8 7181.59 6437.94 134.96 o 1 1 8 8799.27 8023.25 141.01 o 3 1 8 9766.65 9429.28 128.92 o 5 1 8 11303.52 10954.30 321.10 o 7 1 8 7153.46 7323.61 220.57 o 9 1 8 5936.09 6318.12 75.78 o 0 2 8 2042.36 2153.37 106.76 o 2 2 8 474.50 394.82 96.69 o 4 2 8 770.11 753.90 66.40 o 6 2 8 370.84 414.70 47.58 o 8 2 8 368.60 309.60 45.02 o 10 2 8 611.21 560.00 80.57 o 1 3 8 673.09 590.21 98.70 o 3 3 8 888.45 989.63 74.00 o 5 3 8 89.83 89.25 46.48 o 7 3 8 63.50 79.51 39.02 o 9 3 8 118.58 126.12 45.63 o 0 4 8 95.25 54.39 98.70 o 2 4 8 233.27 181.01 65.18 o 4 4 8 159.45 167.61 55.48 o 6 4 8 184.08 151.24 42.12 o 8 4 8 39.20 12.95 46.67 o 1 5 8 6073.81 5633.80 298.97 o 3 5 8 3699.40 4115.30 127.59 o 5 5 8 5824.50 5768.27 90.52 o 7 5 8 4607.96 4615.56 206.43 o 9 5 8 5117.81 4749.89 116.83 o 0 6 8 14424.17 15393.74 209.36 o 2 6 8 15299.43 15072.87 586.27 o 4 6 8 12331.65 12493.50 276.76 o 6 6 8 10267.82 9845.00 334.54 o 8 6 8 4619.55 4516.23 261.87 o 1 7 8 7896.46 8308.58 168.18 o 3 7 8 6311.07 6725.88 183.03 o 5 7 8 7951.64 8282.28 106.64 o 7 7 8 5702.81 5403.47 165.98 o 0 8 8 1521.94 1699.02 54.50 o 2 8 8 596.00 545.40 43.05 o 4 8 8 678.74 708.82 39.08 o 6 8 8 458.06 422.55 51.53 o 1 9 8 767.65 788.55 39.40 o 3 9 8 432.74 484.29 36.97 o 5 9 8 74.19 64.46 78.56 o 0 10 8 137.82 310.46 58.84 o 2 10 8 258.86 239.71 76.55 o 1 1 9 494.41 441.15 104.75 o 3 1 9 475.82 394.82 96.69 o 5 1 9 411.09 370.64 94.68 o 7 1 9 258.28 257.96 49.74 o 0 2 9 537.88 479.42 106.76 o 2 2 9 426.13 376.69 102.73 o 4 2 9 335.21 286.04 102.73 o 6 2 9 226.85 255.80 62.27 o 8 2 9 173.72 159.14 74.53 o 1 3 9 63.89 52.37 94.68 o 3 3 9 50.48 44.32 92.66 o 5 3 9 31.29 45.29 113.62 o 7 3 9 35.75 22.74 74.72 o 0 4 9 1237.73 1168.34 116.83 o 2 4 9 1173.12 1182.44 102.73 o 4 4 9 1071.21 1299.00 103.04 o 6 4 9 982.62 956.68 76.71 o 1 5 9 1857.60 1835.09 112.80 o 3 5 9 1782.22 2098.84 115.20 o 5 5 9 1411.96 1557.12 76.32 o 0 6 9 549.07 532.84 181.48 o 2 6 9 467.80 501.72 88.09 o 4 6 9 452.88 466.32 62.54 o 1 7 9 12.53 19.02 76.34 o 3 7 9 16.72 14.37 71.33 o 0 8 9 31.68 30.22 58.42 o 2 8 9 23.27 22.16 58.42 o