#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:22:02 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180855 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/86/2018609.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018609_Fobs loop_ _publ_author_name 'Wilk, Magdalena' 'Janczak, Jan' 'Videnova-Adrabinska, Veneta' _publ_section_title ; The supramolecular architecture of tris(naphthalene-1,5-diaminium) bis(5-aminonaphthalen-1-aminium) octakis[hydrogen (5-carboxypyridin-3-yl)phosphonate] ; _journal_coeditor_code EM3051 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o351 _journal_page_last o354 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.260 _cell_angle_gamma 90.000 _cell_length_a 14.3060 _cell_length_b 26.6750 _cell_length_c 14.4360 _exptl_crystal_F_000 2504.00 _reflns_d_resolution_high 0.7222 _cod_data_source_file em3051Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title '3,5pyPC-diamine in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 563.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2.42 8.68 41.31 o 3 0 0 1005.20 1060.46 40.05 o 4 0 0 282403.75 294323.66 431.87 o 5 0 0 11.25 21.39 39.21 o 6 0 0 750.57 701.71 52.39 o 7 0 0 2071.09 2108.66 72.06 o 8 0 0 29256.88 31238.15 180.98 o 9 0 0 886.58 901.97 71.11 o 10 0 0 0.57 -2.04 63.19 o 11 0 0 1837.58 1882.27 95.26 o 12 0 0 11650.60 10747.54 187.38 o 13 0 0 1935.20 1955.20 109.01 o 14 0 0 21.09 53.30 84.53 o 15 0 0 0.13 19.82 97.38 o 16 0 0 236.90 92.13 153.36 o 17 0 0 1034.74 941.89 168.62 o 18 0 0 397.29 530.78 269.03 o 2 1 0 106.54 169.09 22.60 o 3 1 0 262.00 266.94 23.16 o 4 1 0 294535.44 305852.84 321.03 o 5 1 0 6.84 95.23 30.19 o 6 1 0 358.28 384.07 27.20 o 7 1 0 3.97 26.90 26.09 o 8 1 0 88028.02 90656.19 192.98 o 9 1 0 2026.04 1952.10 59.35 o 10 1 0 862.84 908.16 53.30 o 11 1 0 43.51 81.56 48.29 o 12 1 0 562.96 718.00 63.30 o 13 1 0 0.03 87.65 54.79 o 14 1 0 67.65 136.56 56.63 o 15 1 0 33.71 47.62 75.06 o 16 1 0 274.47 164.46 92.90 o 17 1 0 191.06 302.52 110.93 o 18 1 0 3.40 91.19 290.90 o 2 2 0 10.11 23.67 16.07 o 3 2 0 539.11 561.98 24.98 o 4 2 0 112225.84 107192.09 152.16 o 5 2 0 2171.80 2303.79 41.40 o 6 2 0 36.36 73.18 25.81 o 7 2 0 141.99 141.94 28.91 o 8 2 0 5098.35 5411.25 73.36 o 9 2 0 1805.66 1810.92 50.05 o 10 2 0 83.56 112.78 45.11 o 11 2 0 751.24 712.58 56.41 o 12 2 0 1107.00 1110.92 67.65 o 13 2 0 211.80 269.24 60.18 o 14 2 0 18.18 70.71 68.04 o 15 2 0 5.37 103.12 75.88 o 16 2 0 862.62 847.71 101.40 o 17 2 0 53.35 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15 4 0 15.84 36.63 74.10 o 16 4 0 344.95 286.24 92.56 o 17 4 0 87.18 56.26 108.76 o 18 4 0 18.34 256.71 176.99 o 1 5 0 2.55 25.12 23.83 o 2 5 0 27.76 34.90 27.46 o 3 5 0 23.00 46.37 29.23 o 4 5 0 28055.74 27879.32 176.01 o 5 5 0 111.40 90.63 29.04 o 6 5 0 358.54 392.56 34.57 o 7 5 0 57.41 59.71 31.93 o 8 5 0 18310.21 18483.45 305.73 o 9 5 0 117.83 120.07 38.68 o 10 5 0 411.53 351.37 47.84 o 11 5 0 29.55 100.35 51.82 o 12 5 0 1036.01 991.53 66.74 o 13 5 0 1572.87 1419.18 83.12 o 14 5 0 4.28 -0.64 63.86 o 15 5 0 580.19 553.81 77.69 o 16 5 0 34.56 41.83 88.65 o 17 5 0 97.00 184.18 109.60 o 18 5 0 2.22 36.40 175.98 o 0 6 0 317865.47 335920.88 2406.53 o 1 6 0 154.39 137.48 24.52 o 2 6 0 743.18 759.45 27.57 o 3 6 0 890.24 880.75 34.08 o 4 6 0 37831.27 37501.23 382.35 o 5 6 0 3179.23 3247.88 71.30 o 6 6 0 1.95 8.94 31.22 o 7 6 0 307.51 309.38 35.91 o 8 6 0 5451.73 5543.61 84.45 o 9 6 0 192.55 199.79 41.80 o 10 6 0 155.26 163.50 44.81 o 11 6 0 899.10 944.51 69.19 o 12 6 0 0.00 18.17 60.21 o 13 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11 8 0 32.91 5.21 58.97 o 12 8 0 787.01 918.85 71.49 o 13 8 0 208.63 223.09 65.35 o 14 8 0 171.35 168.27 65.35 o 15 8 0 145.65 100.16 82.12 o 16 8 0 7.83 28.24 86.66 o 17 8 0 9.12 273.39 105.88 o 18 8 0 6.15 150.86 185.91 o 1 9 0 4662.51 4813.33 54.80 o 2 9 0 516.65 453.53 29.09 o 3 9 0 109.94 138.45 25.71 o 4 9 0 11163.91 10749.35 104.97 o 5 9 0 4066.41 4245.43 58.89 o 6 9 0 3950.78 4069.57 51.96 o 7 9 0 124.35 129.13 33.28 o 8 9 0 1222.64 1097.47 52.80 o 9 9 0 1688.43 1654.00 62.21 o 10 9 0 1008.94 1028.55 59.33 o 11 9 0 306.24 312.24 61.68 o 12 9 0 3390.18 3238.44 99.21 o 13 9 0 20.59 29.71 62.05 o 14 9 0 25.04 67.43 73.65 o 15 9 0 27.38 -40.51 79.43 o 16 9 0 12.81 116.45 85.94 o 17 9 0 664.47 842.52 107.98 o 18 9 0 61.49 27.88 160.93 o 0 10 0 2421.17 2169.73 70.32 o 1 10 0 973.54 960.70 35.08 o 2 10 0 327.67 340.15 28.61 o 3 10 0 64.52 72.66 25.53 o 4 10 0 14217.46 14995.84 142.80 o 5 10 0 11486.60 11424.50 130.45 o 6 10 0 966.38 993.97 33.37 o 7 10 0 5.64 -9.64 37.00 o 8 10 0 1768.69 1816.92 62.64 o 9 10 0 656.03 615.42 52.67 o 10 10 0 330.25 380.05 53.77 o 11 10 0 585.65 648.12 58.66 o 12 10 0 986.29 890.92 72.42 o 13 10 0 114.13 102.90 66.56 o 14 10 0 6.65 46.93 76.91 o 15 10 0 28.25 124.61 78.68 o 16 10 0 776.75 790.27 98.95 o 17 10 0 191.71 323.13 119.56 o 18 10 0 57.92 15.99 197.52 o 1 11 0 4378.73 4410.53 73.18 o 2 11 0 5.36 19.83 27.92 o 3 11 0 1.80 4.96 27.17 o 4 11 0 21144.69 22201.29 194.83 o 5 11 0 1820.48 1898.49 46.04 o 6 11 0 2942.57 3064.92 56.68 o 7 11 0 0.50 13.61 39.50 o 8 11 0 12308.68 12558.08 131.43 o 9 11 0 0.24 -45.36 46.63 o 10 11 0 606.75 568.46 56.23 o 11 11 0 79.78 102.81 52.84 o 12 11 0 2.32 -32.59 63.60 o 13 11 0 149.13 130.72 69.28 o 14 11 0 39.33 41.19 77.24 o 15 11 0 0.34 99.91 81.24 o 16 11 0 228.14 227.12 97.38 o 17 11 0 76.24 121.17 96.58 o 18 11 0 12.72 294.37 219.74 o 0 12 0 142573.30 151844.44 849.89 o 1 12 0 1294.60 1373.89 43.23 o 2 12 0 2071.90 2109.84 47.96 o 3 12 0 499.99 572.44 34.10 o 4 12 0 486.76 560.57 36.05 o 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