#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/86/2018615.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018615_Fobs loop_ _publ_author_name 'Granifo, Juan' 'Gavi\~no, Rub\'en' 'Freire, Eleonora' 'Baggio, Ricardo' _publ_section_title ; Monodentate and bridging behaviour of the sulfur-containing ligand 4'-[4-(methylsulfanyl)phenyl]-4,2':6',4''-terpyridine in two discrete zinc(II) complexes with acetylacetonate ; _journal_coeditor_code FA3281 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m269 _journal_page_last m274 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.187 _cell_angle_gamma 90.000 _cell_length_a 26.6479 _cell_length_b 10.7706 _cell_length_c 16.4983 _exptl_crystal_F_000 2032.00 _reflns_d_resolution_high 0.7357 _[local]_cod_data_source_file fa3281Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' exp_667 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 884.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 16677.22 17434.58 124.42 o 8 0 0 801.22 1152.75 38.14 o 10 0 0 7274.89 6562.61 92.18 o 12 0 0 3068.14 3008.87 53.11 o 14 0 0 6337.01 6064.04 78.96 o 16 0 0 4040.25 3619.02 67.88 o 18 0 0 1923.05 1946.26 58.87 o 20 0 0 39.79 49.53 41.12 o 22 0 0 7351.56 7227.60 114.49 o 24 0 0 277.38 289.35 50.33 o 26 0 0 1946.33 1907.04 89.24 o 28 0 0 105.00 184.68 50.35 o 30 0 0 746.35 621.87 82.86 o 32 0 0 21.59 3.45 69.71 o 34 0 0 41.87 34.66 73.37 o 5 1 0 43172.70 42997.64 106.86 o 7 1 0 2259.06 2011.87 34.61 o 9 1 0 1050.55 1256.57 32.69 o 11 1 0 862.80 928.74 23.17 o 13 1 0 458.34 489.77 22.69 o 15 1 0 116.16 130.04 20.98 o 17 1 0 339.45 379.64 26.62 o 19 1 0 337.72 312.74 31.30 o 21 1 0 4137.02 3997.40 61.12 o 23 1 0 3316.09 3358.06 70.98 o 25 1 0 510.73 454.68 41.86 o 27 1 0 231.50 235.42 45.98 o 29 1 0 429.82 311.07 47.67 o 31 1 0 18.13 53.32 42.87 o 33 1 0 83.98 50.52 48.12 o 35 1 0 102.15 146.17 68.22 o 0 2 0 604.64 776.29 17.59 o 2 2 0 99102.05 93336.43 641.10 o 4 2 0 10237.98 10189.51 171.81 o 6 2 0 29916.25 29603.72 174.38 o 8 2 0 39347.06 36695.36 214.84 o 10 2 0 2106.83 1666.12 41.19 o 12 2 0 11476.18 11659.59 83.50 o 14 2 0 125.60 60.60 23.05 o 16 2 0 4101.44 4203.66 65.31 o 18 2 0 1114.30 946.28 41.14 o 20 2 0 682.21 758.18 42.12 o 22 2 0 2352.86 2331.67 60.18 o 24 2 0 577.46 630.45 44.73 o 26 2 0 116.43 110.99 43.49 o 28 2 0 266.83 298.50 47.75 o 30 2 0 154.34 215.06 53.95 o 32 2 0 32.19 6.71 61.93 o 34 2 0 14.86 30.21 58.74 o 1 3 0 7.15 20.07 6.12 o 3 3 0 3240.65 3015.75 34.73 o 5 3 0 109.18 88.92 22.42 o 7 3 0 7265.25 7443.90 59.62 o 9 3 0 668.26 761.59 49.73 o 11 3 0 4605.84 5647.85 110.54 o 13 3 0 19.16 52.04 28.54 o 15 3 0 395.12 442.11 38.94 o 17 3 0 594.21 674.77 48.95 o 19 3 0 57.42 118.00 45.23 o 21 3 0 30.57 10.65 46.92 o 23 3 0 137.71 204.80 52.51 o 25 3 0 150.74 165.33 51.43 o 27 3 0 106.81 128.97 50.95 o 29 3 0 56.20 75.67 53.87 o 31 3 0 307.33 218.70 61.43 o 33 3 0 22.31 76.81 66.91 o 35 3 0 84.47 87.26 102.25 o 0 4 0 30650.18 30220.30 97.06 o 2 4 0 42319.95 42508.76 136.09 o 4 4 0 2055.04 1822.85 29.15 o 6 4 0 16890.95 16382.11 165.39 o 8 4 0 29743.28 30722.36 135.44 o 10 4 0 11955.01 11510.59 85.54 o 12 4 0 84.04 169.25 22.07 o 14 4 0 20.68 31.80 50.85 o 16 4 0 4294.14 4503.74 87.03 o 18 4 0 4631.16 4668.74 119.95 o 20 4 0 2484.45 2386.63 74.26 o 22 4 0 582.40 640.50 55.60 o 24 4 0 591.58 535.20 60.86 o 26 4 0 36.79 33.71 55.52 o 28 4 0 7.19 8.44 50.78 o 30 4 0 112.13 125.52 55.70 o 32 4 0 46.95 94.05 62.46 o 34 4 0 314.28 257.48 105.46 o 1 5 0 14366.77 16546.06 55.49 o 3 5 0 133.84 135.79 17.33 o 5 5 0 485.29 553.81 22.92 o 7 5 0 35.68 55.25 46.82 o 9 5 0 1192.20 1203.17 70.62 o 11 5 0 3528.54 3821.40 105.70 o 13 5 0 101.42 53.15 55.76 o 15 5 0 321.81 232.15 56.58 o 17 5 0 2.55 12.19 63.21 o 19 5 0 599.01 585.02 55.48 o 21 5 0 0.18 38.73 48.17 o 23 5 0 665.06 659.84 63.41 o 25 5 0 249.47 236.53 55.34 o 27 5 0 1.33 -20.97 56.44 o 29 5 0 1.63 47.10 62.56 o 31 5 0 0.60 -4.91 55.74 o 33 5 0 57.15 30.96 92.18 o 0 6 0 3759.04 3002.57 46.85 o 2 6 0 26489.87 26539.85 256.49 o 4 6 0 24357.30 23579.62 116.00 o 6 6 0 18455.56 18062.70 91.95 o 8 6 0 17427.88 17347.20 212.13 o 10 6 0 1151.00 1161.21 78.74 o 12 6 0 1730.07 1646.42 89.42 o 14 6 0 496.08 510.54 74.78 o 16 6 0 120.99 54.40 72.44 o 18 6 0 188.61 210.17 74.36 o 20 6 0 70.98 47.84 53.37 o 22 6 0 1860.49 1590.57 77.47 o 24 6 0 336.35 299.84 75.19 o 26 6 0 203.70 179.64 58.44 o 28 6 0 6.24 1.70 56.88 o 30 6 0 28.58 25.26 61.40 o 32 6 0 173.82 171.13 94.50 o 1 7 0 1.43 14.26 14.85 o 3 7 0 3131.48 3288.53 49.74 o 5 7 0 0.02 2.15 20.57 o 7 7 0 40.19 35.65 23.69 o 9 7 0 295.66 262.98 30.57 o 11 7 0 8675.30 8641.24 174.76 o 13 7 0 998.42 963.15 96.38 o 15 7 0 1183.10 1227.76 96.49 o 17 7 0 1029.55 917.18 83.73 o 19 7 0 38.12 78.23 83.20 o 21 7 0 49.04 30.92 61.73 o 23 7 0 3.57 62.92 60.18 o 25 7 0 8.18 50.17 57.45 o 27 7 0 84.48 49.98 59.35 o 29 7 0 0.06 -23.18 71.17 o 31 7 0 46.81 39.43 107.86 o 0 8 0 6657.91 6445.35 173.87 o 2 8 0 6759.81 6671.93 65.52 o 4 8 0 7640.86 7905.82 77.82 o 6 8 0 7493.33 7395.75 137.37 o 8 8 0 804.21 812.68 37.83 o 10 8 0 15908.30 16381.56 289.74 o 12 8 0 8983.01 8942.40 191.77 o 14 8 0 1979.00 1928.13 106.42 o 16 8 0 2070.87 2333.24 125.90 o 18 8 0 1366.16 1475.76 103.91 o 20 8 0 2528.72 2364.03 128.12 o 22 8 0 799.19 781.04 67.82 o 24 8 0 254.87 221.99 58.29 o 26 8 0 25.54 25.62 65.60 o 28 8 0 19.17 19.08 92.91 o 1 9 0 184.28 196.00 24.96 o 3 9 0 47.64 20.51 41.65 o 5 9 0 63.16 42.30 51.64 o 7 9 0 3124.42 2834.86 126.34 o 9 9 0 4.55 20.62 85.93 o 11 9 0 10685.20 9995.91 208.31 o 13 9 0 14.20 62.96 87.75 o 15 9 0 43.59 6.97 67.07 o 17 9 0 2.50 34.06 81.53 o 19 9 0 5.23 16.93 88.84 o 21 9 0 86.32 56.60 91.28 o 23 9 0 41.27 76.28 61.01 o 25 9 0 33.73 68.92 58.60 o 27 9 0 16.42 -16.77 84.90 o 0 10 0 3164.05 3322.52 123.31 o 2 10 0 7872.21 7606.58 248.74 o 4 10 0 1646.14 1875.64 69.69 o 6 10 0 3143.45 3235.08 94.65 o 8 10 0 1002.77 1005.65 106.71 o 10 10 0 44.28 22.46 86.49 o 12 10 0 3409.00 3429.34 141.52 o 14 10 0 1111.59 1067.58 100.60 o 16 10 0 438.94 496.93 93.93 o 18 10 0 149.94 170.99 85.41 o 20 10 0 28.61 69.88 78.47 o 22 10 0 139.13 188.86 95.30 o 24 10 0 343.86 358.46 108.31 o 1 11 0 200.11 167.85 53.76 o 3 11 0 312.00 271.54 55.86 o 5 11 0 33.31 3.28 40.93 o 7 11 0 37.95 32.80 56.44 o 9 11 0 363.51 357.13 62.28 o 11 11 0 322.33 326.56 85.05 o 13 11 0 47.28 14.83 83.17 o 15 11 0 96.20 101.34 92.46 o 17 11 0 0.04 12.92 98.72 o 19 11 0 51.30 51.68 97.64 o 0 12 0 5820.60 5371.78 163.56 o 2 12 0 1547.98 1484.12 75.42 o 4 12 0 1230.64 1314.22 64.72 o 6 12 0 720.63 716.63 67.15 o 8 12 0 732.85 912.01 78.40 o 10 12 0 147.87 165.22 68.91 o 12 12 0 556.57 530.72 73.89 o 14 12 0 234.34 197.66 71.37 o 1 13 0 300.79 284.69 56.80 o 3 13 0 123.69 43.65 51.50 o 5 13 0 133.11 49.91 59.87 o 7 13 0 107.73 94.56 54.78 o 9 13 0 190.64 269.12 101.94 o 0 14 0 394.96 379.61 87.92 o 2 14 0 342.68 397.69 100.29 o 4 14 0 475.89 532.63 101.90 o -35 1 1 479.21 387.56 67.77 o -33 1 1 2064.36 2286.35 97.36 o -31 1 1 2487.57 2471.11 73.53 o -29 1 1 1931.09 1957.80 67.34 o -27 1 1 6199.86 6313.06 106.54 o -25 1 1 729.80 749.90 45.72 o -23 1 1 4377.84 4470.84 67.87 o -21 1 1 2450.53 2477.80 50.82 o -19 1 1 1338.33 1333.74 38.55 o -17 1 1 304.16 330.05 25.95 o -15 1 1 224.70 257.48 22.34 o -13 1 1 29.87 51.26 25.69 o -11 1 1 19.66 33.10 18.88 o -9 1 1 4269.31 4590.57 85.12 o -7 1 1 1077.91 1147.02 34.57 o -5 1 1 5935.50 5737.17 119.29 o 5 1 1 97.93 136.24 55.42 o 7 1 1 41942.58 40844.61 169.27 o 9 1 1 30047.01 30103.01 127.37 o 11 1 1 1932.10 1689.29 34.07 o 13 1 1 23472.47 22474.35 152.42 o 15 1 1 14033.76 13247.35 121.12 o 17 1 1 15472.52 14926.90 110.70 o 19 1 1 28085.97 26207.21 255.09 o 21 1 1 1312.29 1160.75 48.50 o 23 1 1 898.57 891.71 46.61 o 25 1 1 674.81 624.80 49.00 o 27 1 1 3686.40 3567.32 79.04 o 29 1 1 24.35 46.77 43.31 o 31 1 1 129.34 130.12 44.48 o 33 1 1 262.70 294.41 69.78 o -34 2 1 397.47 385.28 63.86 o -32 2 1 365.31 297.99 67.70 o -30 2 1 17.57 46.43 54.93 o -28 2 1 0.34 -18.05 41.95 o -26 2 1 26.19 22.93 42.87 o -24 2 1 23.86 15.03 38.55 o -22 2 1 197.23 239.21 38.61 o -20 2 1 33.87 28.02 32.51 o -18 2 1 21.87 17.67 29.15 o -16 2 1 63.58 95.90 27.02 o -14 2 1 174.35 251.74 24.69 o -12 2 1 2150.72 2353.86 70.95 o -10 2 1 5392.40 5662.29 92.28 o -8 2 1 1988.68 2011.09 54.24 o -6 2 1 8474.65 8664.69 79.78 o -4 2 1 20986.94 20679.20 123.31 o -2 2 1 2675.28 2610.33 40.68 o 0 2 1 28441.99 27896.00 114.33 o 2 2 1 0.15 10.21 17.92 o 4 2 1 19198.70 19866.28 135.59 o 6 2 1 835.85 859.83 40.22 o 8 2 1 3683.29 3928.38 78.93 o 10 2 1 209.65 150.80 19.32 o 12 2 1 36503.76 39971.58 339.32 o 14 2 1 2713.21 3258.68 52.61 o 16 2 1 1037.67 1039.39 38.66 o 18 2 1 149.28 139.10 32.05 o 20 2 1 2770.68 2764.79 66.94 o 22 2 1 3447.56 3282.07 69.58 o 24 2 1 47.08 71.05 39.58 o 26 2 1 461.51 400.86 45.18 o 28 2 1 20.78 55.90 46.63 o 30 2 1 151.25 147.61 49.16 o 32 2 1 58.53 57.99 55.97 o 34 2 1 1469.09 1588.92 128.33 o -35 3 1 1422.23 1752.66 144.68 o -33 3 1 85.64 -4.02 65.11 o -31 3 1 2014.33 2251.14 113.40 o -29 3 1 2336.35 2377.98 91.49 o -27 3 1 2821.19 2931.92 96.94 o -25 3 1 3040.69 3210.78 177.03 o -23 3 1 3368.37 3304.78 161.39 o -21 3 1 3593.75 3687.06 87.12 o -19 3 1 5455.79 5722.73 99.32 o -17 3 1 343.50 394.53 39.12 o -15 3 1 1274.89 1494.52 52.76 o -13 3 1 182.49 248.03 32.65 o -11 3 1 272.87 684.02 52.73 o -9 3 1 3221.11 3435.34 51.20 o -7 3 1 1718.72 1959.83 58.11 o -5 3 1 5596.52 5508.17 61.27 o -3 3 1 558.28 595.38 11.63 o -1 3 1 10451.86 10221.69 29.70 o 1 3 1 3699.50 3523.42 27.45 o 3 3 1 2974.91 2698.99 58.84 o 5 3 1 1181.74 1173.17 28.12 o 7 3 1 5961.32 5591.26 94.15 o 9 3 1 585.60 486.92 46.18 o 11 3 1 68253.41 71069.94 368.13 o 13 3 1 187.76 38.54 30.32 o 15 3 1 28419.05 28303.26 382.17 o 17 3 1 19674.44 18434.45 160.25 o 19 3 1 15536.49 15525.00 155.92 o 21 3 1 5520.71 5771.55 106.76 o 23 3 1 4109.24 4170.60 98.29 o 25 3 1 3990.47 4006.31 101.54 o 27 3 1 1584.93 1588.18 78.00 o 29 3 1 470.01 550.43 65.27 o 31 3 1 24.55 42.02 54.85 o 33 3 1 277.27 367.04 63.10 o -34 4 1 291.56 335.19 71.95 o -32 4 1 147.43 123.83 63.30 o -30 4 1 5.90 -29.55 60.12 o -28 4 1 0.10 -6.63 54.34 o -26 4 1 167.27 168.30 55.73 o -24 4 1 534.69 432.38 56.87 o -22 4 1 72.18 62.03 51.19 o -20 4 1 1.85 29.62 47.48 o -18 4 1 150.30 199.49 43.33 o -16 4 1 199.84 224.58 19.37 o -14 4 1 307.45 367.87 25.95 o -12 4 1 282.82 234.70 18.02 o -10 4 1 3934.54 4093.76 96.18 o -8 4 1 394.67 575.75 51.11 o -6 4 1 769.14 950.47 28.59 o -4 4 1 88.61 110.65 10.06 o -2 4 1 7965.13 8547.86 58.84 o 0 4 1 2891.32 2962.97 24.39 o 2 4 1 1723.50 1862.74 24.90 o 4 4 1 1507.39 1655.55 28.07 o 6 4 1 1629.61 1937.19 68.40 o 8 4 1 55.55 115.00 39.30 o 10 4 1 182.62 163.62 51.83 o 12 4 1 782.94 813.82 65.95 o 14 4 1 879.79 852.27 71.62 o 16 4 1 169.72 174.91 39.81 o 18 4 1 86.00 127.83 44.15 o 20 4 1 392.98 348.16 52.97 o 22 4 1 503.37 440.90 52.14 o 24 4 1 42.15 42.39 53.57 o 26 4 1 106.66 156.30 58.99 o 28 4 1 40.70 9.80 53.96 o 30 4 1 270.28 262.16 61.78 o 32 4 1 69.74 119.16 67.80 o -33 5 1 652.54 722.81 79.76 o -31 5 1 522.90 487.24 68.43 o -29 5 1 2180.36 2089.32 92.19 o -27 5 1 703.64 813.98 95.77 o -25 5 1 4061.68 3847.63 105.63 o -23 5 1 781.65 849.79 64.78 o -21 5 1 2620.05 2367.11 145.78 o -19 5 1 80.18 148.41 48.84 o -17 5 1 15.94 12.59 53.24 o -15 5 1 54.79 37.79 52.77 o -13 5 1 24.25 47.88 51.14 o -11 5 1 20.84 34.83 41.85 o -9 5 1 270.49 273.54 50.92 o -7 5 1 3167.71 3120.25 93.81 o -5 5 1 4810.27 5090.69 48.71 o -3 5 1 14151.30 14620.47 62.42 o -1 5 1 156.73 80.88 10.61 o 1 5 1 63723.66 66101.80 379.41 o 3 5 1 2871.56 2487.25 41.14 o 5 5 1 16171.51 16403.65 104.71 o 7 5 1 717.83 628.21 57.34 o 9 5 1 9072.22 9290.25 150.91 o 11 5 1 8717.22 8265.19 150.26 o 13 5 1 4873.51 4969.49 127.30 o 15 5 1 6234.88 6086.91 143.85 o 17 5 1 10001.67 10472.42 193.44 o 19 5 1 5325.77 5435.52 106.18 o 21 5 1 10375.57 9962.29 348.52 o 23 5 1 156.47 186.30 53.42 o 25 5 1 1592.65 1510.44 90.62 o 27 5 1 100.60 117.53 59.25 o 29 5 1 104.86 98.20 64.83 o 31 5 1 53.44 39.37 62.31 o -32 6 1 0.03 -31.85 104.70 o -30 6 1 70.73 5.68 62.75 o -28 6 1 9.25 -25.64 60.88 o -26 6 1 178.19 214.27 62.16 o -24 6 1 59.52 79.82 60.34 o -22 6 1 10.70 32.33 57.84 o -20 6 1 151.84 145.46 49.62 o -18 6 1 84.67 88.32 71.51 o -16 6 1 1056.60 1123.25 86.98 o -14 6 1 148.34 85.63 67.44 o -12 6 1 57.95 61.66 54.88 o -10 6 1 303.08 203.15 54.73 o -8 6 1 109.86 107.08 29.80 o -6 6 1 449.28 501.15 21.95 o -4 6 1 3021.73 3312.38 35.05 o -2 6 1 306.11 347.40 17.30 o 0 6 1 9116.83 10200.97 62.63 o 2 6 1 2985.17 3091.28 49.64 o 4 6 1 72.94 28.90 22.36 o 6 6 1 789.73 896.19 35.95 o 8 6 1 227.89 186.00 59.05 o 10 6 1 546.18 473.20 69.84 o 12 6 1 378.49 311.36 60.88 o 14 6 1 6.35 -18.59 55.70 o 16 6 1 22.46 -2.76 70.11 o 18 6 1 189.55 153.08 64.17 o 20 6 1 194.56 177.80 49.18 o 22 6 1 1258.61 993.28 67.42 o 24 6 1 556.24 511.28 65.06 o 26 6 1 47.27 20.61 54.15 o 28 6 1 0.09 18.27 61.26 o 30 6 1 13.58 -4.62 62.58 o -31 7 1 48.17 23.10 105.51 o -29 7 1 1227.48 1453.09 99.10 o -27 7 1 1070.19 1192.78 81.77 o -25 7 1 1574.21 1483.64 87.91 o -23 7 1 3157.98 3330.87 106.72 o -21 7 1 2158.16 2240.41 88.73 o -19 7 1 789.75 844.01 90.49 o -17 7 1 1185.66 1301.13 97.48 o -15 7 1 1040.97 942.16 93.35 o -13 7 1 203.67 119.43 71.32 o -11 7 1 768.29 697.09 74.72 o -9 7 1 3610.84 3807.38 55.57 o -7 7 1 7400.77 7337.54 59.10 o -5 7 1 2235.99 2269.57 37.01 o -3 7 1 2027.40 2093.36 29.52 o -1 7 1 3391.36 3567.67 76.67 o 1 7 1 74.12 200.33 26.75 o 3 7 1 6561.15 6446.55 83.05 o 5 7 1 11629.27 11398.04 84.28 o 7 7 1 1155.11 1219.26 41.49 o 9 7 1 25780.56 24815.24 154.90 o 11 7 1 2878.16 2878.80 114.47 o 13 7 1 5845.98 5709.37 154.90 o 15 7 1 18.54 48.58 75.10 o 17 7 1 9803.15 10112.84 207.56 o 19 7 1 1576.98 1691.01 107.85 o 21 7 1 2447.30 2663.76 99.91 o 23 7 1 5109.52 5204.20 144.78 o 25 7 1 684.04 743.54 76.82 o 27 7 1 89.38 191.08 63.72 o 29 7 1 311.17 300.83 75.14 o 31 7 1 15.96 -39.36 95.87 o -28 8 1 0.52 -51.90 71.90 o -26 8 1 1.48 -6.46 65.44 o -24 8 1 72.19 142.90 61.86 o -22 8 1 13.89 -2.41 58.99 o -20 8 1 24.23 23.81 87.92 o -18 8 1 245.12 297.73 89.14 o -16 8 1 65.68 12.39 75.42 o -14 8 1 1749.40 1742.07 101.93 o -12 8 1 215.16 225.10 77.69 o -10 8 1 2.89 128.92 73.17 o -8 8 1 71.00 80.94 37.55 o -6 8 1 57.45 50.24 18.38 o -4 8 1 397.64 352.83 21.08 o -2 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