#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:22:02 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180855 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/86/2018620.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018620_Fobs loop_ _publ_author_name 'Traeger, J.' 'Kelling, A.' 'Schilde, U.' 'Holdt, H.-J.' _publ_section_title ; rac-1-[(2-Methoxyethyl)sulfanyl]-2-[(2-methoxyethyl)sulfinyl]benzene and its PdCl~2~ complex ; _journal_coeditor_code FA3283 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m238 _journal_page_last m241 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.044 _cell_angle_gamma 90.000 _cell_length_a 15.6089 _cell_length_b 6.7055 _cell_length_c 14.2492 _exptl_crystal_F_000 584.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file fa3283Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TRAEG20' _shelx_refln_list_code 4 _shelx_f_calc_maximum 192.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1753.27 1625.16 17.28 o 3 0 0 9225.42 8623.75 49.37 o 4 0 0 26766.19 26332.99 185.95 o 5 0 0 50.79 59.90 3.79 o 6 0 0 2246.43 2276.17 26.62 o 7 0 0 2502.52 2670.14 41.40 o 8 0 0 212.23 148.80 4.22 o 9 0 0 802.14 845.88 8.12 o 10 0 0 3825.62 3894.02 28.84 o 11 0 0 67.02 54.41 3.62 o 12 0 0 296.08 269.63 3.72 o 13 0 0 91.64 94.83 5.19 o 14 0 0 363.20 375.68 10.08 o 15 0 0 78.85 82.82 3.49 o 16 0 0 0.90 4.39 3.64 o 17 0 0 7.60 8.36 3.98 o 1 1 0 6432.08 6350.21 29.60 o 2 1 0 1420.48 1408.66 11.54 o 3 1 0 10.71 9.53 3.31 o 4 1 0 1057.63 1075.22 5.60 o 5 1 0 35.89 24.13 2.71 o 6 1 0 56.23 59.41 2.65 o 7 1 0 269.97 295.91 3.16 o 8 1 0 237.48 280.32 3.59 o 9 1 0 530.87 443.22 4.71 o 10 1 0 10.24 23.02 3.94 o 11 1 0 4.18 2.41 2.33 o 12 1 0 11.51 12.79 2.61 o 13 1 0 776.84 733.88 4.41 o 14 1 0 1.53 -1.52 2.99 o 15 1 0 0.60 -0.14 2.51 o 16 1 0 3.73 3.61 2.47 o 17 1 0 79.10 67.05 2.95 o 0 2 0 221.46 230.41 4.75 o 1 2 0 632.79 692.44 6.06 o 2 2 0 76.22 58.88 2.13 o 3 2 0 26.84 23.90 2.48 o 4 2 0 392.11 376.72 3.15 o 5 2 0 30.65 30.59 2.36 o 6 2 0 484.03 478.60 5.59 o 7 2 0 152.90 162.74 2.93 o 8 2 0 1507.97 1493.09 11.47 o 9 2 0 23.26 25.61 2.52 o 10 2 0 1461.57 1540.61 28.22 o 11 2 0 28.79 31.09 2.55 o 12 2 0 5.01 1.71 3.17 o 13 2 0 330.51 330.40 4.16 o 14 2 0 86.59 101.60 2.80 o 15 2 0 0.03 -0.49 2.59 o 16 2 0 47.75 47.44 2.85 o 1 3 0 3432.81 3361.86 27.82 o 2 3 0 26.33 19.97 2.35 o 3 3 0 805.27 767.09 6.89 o 4 3 0 42.12 52.25 2.22 o 5 3 0 4979.50 5046.60 46.53 o 6 3 0 860.44 865.20 7.88 o 7 3 0 290.59 279.20 2.85 o 8 3 0 131.47 115.17 2.53 o 9 3 0 1912.21 1952.57 33.30 o 10 3 0 150.41 154.95 4.48 o 11 3 0 291.24 297.04 4.89 o 12 3 0 139.20 139.64 4.22 o 13 3 0 11.29 10.52 3.04 o 14 3 0 151.40 150.05 6.80 o 15 3 0 206.30 231.21 6.00 o 16 3 0 53.74 46.24 3.30 o 0 4 0 581.22 625.47 10.18 o 1 4 0 540.25 568.03 5.62 o 2 4 0 6.71 6.99 1.87 o 3 4 0 0.03 -0.76 1.89 o 4 4 0 1409.95 1454.65 12.83 o 5 4 0 3.67 4.75 2.26 o 6 4 0 397.29 411.18 3.89 o 7 4 0 25.69 26.29 2.51 o 8 4 0 422.19 386.77 3.37 o 9 4 0 351.19 356.82 3.77 o 10 4 0 202.00 193.56 2.69 o 11 4 0 420.61 426.13 8.54 o 12 4 0 13.11 16.43 2.90 o 13 4 0 182.37 179.04 4.91 o 14 4 0 45.63 47.79 2.68 o 1 5 0 692.41 689.73 3.70 o 2 5 0 102.08 104.70 2.03 o 3 5 0 60.87 67.40 1.96 o 4 5 0 236.17 236.09 2.56 o 5 5 0 674.20 622.51 3.36 o 6 5 0 134.97 139.67 2.54 o 7 5 0 26.71 26.86 2.04 o 8 5 0 16.27 16.30 2.08 o 9 5 0 104.10 105.97 2.63 o 10 5 0 138.13 138.93 2.73 o 11 5 0 194.56 204.71 2.79 o 12 5 0 162.09 162.75 4.03 o 13 5 0 2.41 8.30 2.45 o 0 6 0 579.29 601.18 7.27 o 1 6 0 96.61 98.10 1.82 o 2 6 0 125.31 127.16 1.89 o 3 6 0 3.77 2.60 1.80 o 4 6 0 442.32 449.61 3.01 o 5 6 0 96.66 86.44 2.31 o 6 6 0 144.41 141.48 2.63 o 7 6 0 0.36 2.15 2.34 o 8 6 0 266.92 261.22 5.26 o 9 6 0 54.01 49.84 3.91 o 10 6 0 287.86 304.08 3.31 o 11 6 0 131.37 129.56 2.93 o 1 7 0 214.57 224.65 3.74 o 2 7 0 76.39 78.05 1.91 o 3 7 0 137.12 139.33 2.13 o 4 7 0 381.55 375.69 7.15 o 5 7 0 158.47 168.90 3.12 o 6 7 0 93.90 90.82 2.47 o 7 7 0 2.45 0.47 2.43 o 8 7 0 159.40 146.42 2.95 o -17 1 1 22.22 19.84 2.62 o -16 1 1 78.15 74.05 3.06 o -15 1 1 194.74 193.02 3.68 o -14 1 1 736.82 722.28 8.97 o -13 1 1 128.80 124.07 2.57 o -12 1 1 6.80 8.31 2.18 o -11 1 1 0.16 -1.53 2.15 o -10 1 1 873.95 905.50 4.85 o -9 1 1 941.24 901.59 5.48 o -8 1 1 610.97 607.44 5.19 o -7 1 1 1003.20 1019.22 7.74 o -6 1 1 1004.15 947.16 6.92 o -5 1 1 280.86 256.03 3.29 o -4 1 1 35.18 30.10 2.92 o -3 1 1 1519.83 1411.51 7.41 o -2 1 1 392.93 360.29 3.88 o -1 1 1 116.67 107.61 3.52 o 0 1 1 1918.20 1963.35 9.54 o 1 1 1 2216.16 2173.14 19.60 o 2 1 1 2082.31 1988.81 43.32 o 3 1 1 6212.30 6325.41 166.79 o 4 1 1 4108.55 4156.66 77.66 o 5 1 1 103.44 88.74 3.65 o 6 1 1 1452.61 1523.71 30.81 o 7 1 1 3.30 4.75 3.09 o 8 1 1 917.87 911.42 20.17 o 9 1 1 0.09 1.40 2.72 o 10 1 1 1714.08 1685.51 23.61 o 11 1 1 4.10 3.84 2.29 o 12 1 1 4.92 5.79 2.33 o 13 1 1 274.66 262.12 3.03 o 14 1 1 758.08 782.56 4.39 o 15 1 1 8.15 7.96 2.35 o 16 1 1 0.01 1.21 2.60 o -17 2 1 0.31 -0.66 2.72 o -16 2 1 214.86 222.13 5.50 o -15 2 1 98.38 106.37 3.34 o -14 2 1 162.01 153.10 3.18 o -13 2 1 352.87 340.24 3.88 o -12 2 1 0.75 0.35 2.33 o -11 2 1 202.11 207.29 4.01 o -10 2 1 434.91 419.66 4.37 o -9 2 1 354.42 349.76 3.24 o -8 2 1 214.14 202.20 2.78 o -7 2 1 0.84 12.79 5.01 o -6 2 1 77.21 77.71 2.65 o -5 2 1 786.27 704.16 6.81 o -4 2 1 71.91 61.33 2.41 o -3 2 1 4091.35 4135.16 32.40 o -2 2 1 3535.56 3465.22 24.98 o -1 2 1 8090.59 8041.44 80.59 o 0 2 1 876.90 946.59 4.71 o 1 2 1 5339.50 5453.00 27.32 o 2 2 1 1081.98 1027.74 11.00 o 3 2 1 139.80 108.39 2.55 o 4 2 1 114.78 154.60 2.90 o 5 2 1 2693.37 2701.22 11.01 o 6 2 1 4.25 5.41 3.93 o 7 2 1 1865.35 2110.22 9.40 o 8 2 1 75.23 78.45 4.37 o 9 2 1 1934.91 1967.97 36.46 o 10 2 1 120.62 127.63 3.56 o 11 2 1 870.83 875.77 8.77 o 12 2 1 97.13 91.62 2.86 o 13 2 1 106.21 109.23 2.93 o 14 2 1 0.00 -0.23 2.74 o 15 2 1 216.27 243.59 4.02 o 16 2 1 22.83 22.58 3.66 o -16 3 1 6.11 6.37 3.21 o -15 3 1 20.83 25.79 4.52 o -14 3 1 129.44 111.36 4.97 o -13 3 1 1.49 4.90 4.26 o -12 3 1 151.63 149.36 3.17 o -11 3 1 28.81 23.37 2.75 o -10 3 1 33.13 29.19 2.21 o -9 3 1 7.11 5.23 2.28 o -8 3 1 627.41 632.39 5.11 o -7 3 1 131.23 125.51 2.27 o -6 3 1 550.38 616.54 9.58 o -5 3 1 290.13 273.81 2.58 o -4 3 1 718.56 735.82 5.69 o -3 3 1 2.36 0.95 2.23 o -2 3 1 0.88 3.60 2.35 o -1 3 1 3.82 1.72 1.85 o 0 3 1 10.38 20.43 1.90 o 1 3 1 1008.14 1081.92 7.24 o 2 3 1 869.22 925.68 8.60 o 3 3 1 88.60 107.47 2.29 o 4 3 1 18.14 21.53 1.89 o 5 3 1 14.17 15.40 2.26 o 6 3 1 361.50 393.86 5.86 o 7 3 1 23.76 21.33 2.34 o 8 3 1 351.23 340.67 9.84 o 9 3 1 32.07 35.57 2.76 o 10 3 1 340.44 329.17 3.48 o 11 3 1 382.10 380.45 4.19 o 12 3 1 178.91 179.53 3.34 o 13 3 1 33.91 36.19 5.74 o 14 3 1 5.25 3.39 3.16 o 15 3 1 214.51 215.39 4.23 o -15 4 1 199.67 204.08 3.18 o -14 4 1 289.85 293.28 3.25 o -13 4 1 376.59 410.74 16.16 o -12 4 1 13.17 14.41 4.45 o -11 4 1 767.13 812.39 5.48 o -10 4 1 14.19 17.68 2.33 o -9 4 1 1883.42 1896.08 18.58 o -8 4 1 14.46 15.31 2.04 o -7 4 1 27.37 27.93 2.12 o -6 4 1 3.09 4.40 1.98 o -5 4 1 1540.19 1509.83 7.19 o -4 4 1 1640.94 1666.53 5.65 o -3 4 1 621.55 649.13 7.52 o -2 4 1 187.79 179.10 2.65 o -1 4 1 399.60 364.68 3.81 o 0 4 1 15.16 12.79 1.81 o 1 4 1 977.48 926.78 6.92 o 2 4 1 240.30 250.64 3.68 o 3 4 1 50.48 38.50 1.98 o 4 4 1 585.40 612.67 4.37 o 5 4 1 1307.52 1231.07 12.99 o 6 4 1 339.02 354.68 3.42 o 7 4 1 1.13 0.83 2.21 o 8 4 1 302.93 307.32 2.88 o 9 4 1 1296.99 1292.11 17.30 o 10 4 1 0.20 1.58 2.34 o 11 4 1 22.08 26.00 2.45 o 12 4 1 2.57 2.61 2.41 o 13 4 1 469.75 490.33 3.54 o 14 4 1 2.47 0.00 2.70 o -13 5 1 94.04 85.48 3.36 o -12 5 1 125.25 121.52 4.72 o -11 5 1 10.41 6.51 2.47 o -10 5 1 774.89 771.10 15.83 o -9 5 1 176.38 172.58 3.80 o -8 5 1 182.20 184.52 2.90 o -7 5 1 305.04 300.86 4.69 o -6 5 1 651.60 655.28 6.81 o -5 5 1 373.91 367.76 4.77 o -4 5 1 1573.18 1554.56 7.35 o -3 5 1 867.76 887.86 7.87 o -2 5 1 137.18 137.98 2.11 o -1 5 1 3.47 3.06 1.64 o 0 5 1 1488.91 1462.43 9.83 o 1 5 1 105.94 101.76 1.98 o 2 5 1 2.34 2.65 1.83 o 3 5 1 26.14 22.07 1.89 o 4 5 1 729.96 688.42 4.37 o 5 5 1 310.23 316.83 2.86 o 6 5 1 204.51 191.75 2.27 o 7 5 1 0.26 -2.15 2.15 o 8 5 1 83.07 86.61 2.53 o 9 5 1 157.17 171.10 4.11 o 10 5 1 204.20 209.91 5.48 o 11 5 1 9.15 4.51 2.45 o 12 5 1 20.91 19.02 2.60 o 13 5 1 4.73 6.10 2.49 o -11 6 1 114.62 123.67 2.97 o -10 6 1 14.66 16.49 2.59 o -9 6 1 0.64 -2.01 2.48 o -8 6 1 109.82 117.58 2.55 o -7 6 1 68.64 71.16 2.34 o -6 6 1 3.22 1.36 2.09 o -5 6 1 49.17 45.06 2.15 o -4 6 1 3.84 13.52 3.34 o -3 6 1 181.79 166.32 1.90 o -2 6 1 88.38 87.63 1.76 o -1 6 1 186.36 173.58 1.86 o 0 6 1 59.97 66.34 1.76 o 1 6 1 257.65 249.48 3.93 o 2 6 1 0.12 -1.52 1.83 o 3 6 1 40.60 41.60 1.93 o 4 6 1 13.76 14.51 2.12 o 5 6 1 5.66 6.67 2.18 o 6 6 1 1.12 3.61 2.28 o 7 6 1 43.15 41.45 2.52 o 8 6 1 3.46 4.53 2.49 o 9 6 1 0.00 1.07 2.57 o 10 6 1 275.72 270.41 3.13 o -8 7 1 25.88 25.13 2.58 o -7 7 1 84.65 82.87 3.26 o -6 7 1 164.41 154.13 2.63 o -5 7 1 169.14 165.22 2.63 o -4 7 1 47.54 46.68 2.10 o -3 7 1 59.07 63.13 1.88 o -2 7 1 36.25 35.70 1.86 o -1 7 1 252.21 259.94 2.49 o 0 7 1 185.19 172.66 1.94 o 1 7 1 0.99 0.94 1.84 o 2 7 1 308.93 301.91 4.31 o 3 7 1 20.42 24.56 2.07 o 4 7 1 98.23 97.75 3.79 o 5 7 1 0.00 4.14 2.28 o 6 7 1 192.68 178.60 3.35 o 7 7 1 2.44 2.30 2.59 o -17 0 2 98.92 92.41 4.48 o -16 0 2 0.11 3.96 8.71 o -15 0 2 1074.23 1074.58 30.49 o -14 0 2 687.02 651.84 13.37 o -13 0 2 724.17 705.69 4.87 o -12 0 2 0.52 1.03 2.95 o -11 0 2 546.23 501.61 4.45 o -10 0 2 1066.00 995.64 5.66 o -9 0 2 1097.87 1038.47 5.68 o -8 0 2 6.66 21.19 3.34 o -7 0 2 1120.24 1206.27 19.62 o -6 0 2 477.45 429.85 5.19 o -5 0 2 6970.31 6982.26 34.54 o -4 0 2 28587.30 28424.73 148.88 o -3 0 2 15.68 18.87 4.49 o -2 0 2 2006.73 1927.85 10.49 o -1 0 2 4155.37 4077.66 51.36 o 0 0 2 4413.13 4249.20 36.07 o 1 0 2 2967.78 2903.00 14.10 o 2 0 2 10555.27 10327.39 24.98 o 3 0 2 207.90 177.00 4.95 o 4 0 2 1.89 9.22 3.57 o 5 0 2 531.81 507.58 10.39 o 6 0 2 2165.44 2262.49 14.41 o 7 0 2 91.32 107.16 5.48 o 8 0 2 471.00 505.05 5.80 o 9 0 2 37.90 44.16 3.38 o 10 0 2 1123.05 1139.92 29.94 o 11 0 2 361.46 371.00 4.35 o 12 0 2 0.80 -1.30 3.04 o 13 0 2 350.30 352.09 4.23 o 14 0 2 127.43 131.67 3.93 o 15 0 2 1.34 4.38 3.25 o 16 0 2 131.51 144.79 4.17 o -17 1 2 40.85 45.68 2.48 o -16 1 2 0.41 1.80 2.39 o -15 1 2 146.81 125.65 4.67 o -14 1 2 132.05 132.61 2.54 o -13 1 2 432.49 386.28 2.88 o -12 1 2 66.67 54.50 2.32 o -11 1 2 133.26 129.10 2.46 o -10 1 2 173.47 162.69 2.91 o -9 1 2 82.63 114.86 2.37 o -8 1 2 657.43 783.39 4.45 o -7 1 2 3.89 1.66 2.21 o -6 1 2 1865.92 1901.98 10.64 o -5 1 2 1164.57 1186.72 17.26 o -4 1 2 420.67 329.98 4.00 o -3 1 2 3008.97 2973.99 14.86 o -2 1 2 11004.93 10854.70 52.49 o -1 1 2 640.85 629.17 4.27 o 0 1 2 7525.61 7756.56 55.24 o 1 1 2 911.31 985.02 10.05 o 2 1 2 2553.43 2524.60 47.72 o 3 1 2 1217.05 1161.78 7.66 o 4 1 2 203.04 237.69 3.80 o 5 1 2 16.11 33.57 2.64 o 6 1 2 25.31 24.59 2.60 o 7 1 2 228.82 224.49 3.26 o 8 1 2 231.70 235.97 2.95 o 9 1 2 1285.21 1234.81 11.78 o 10 1 2 178.18 176.98 2.88 o 11 1 2 162.30 175.42 2.69 o 12 1 2 36.86 36.12 2.48 o 13 1 2 122.52 114.96 3.07 o 14 1 2 13.06 11.50 2.62 o 15 1 2 64.35 74.87 2.78 o 16 1 2 4.47 6.31 2.83 o -17 2 2 5.56 2.08 2.85 o -16 2 2 42.43 37.54 2.64 o -15 2 2 30.35 36.83 2.46 o -14 2 2 74.38 80.23 2.58 o -13 2 2 9.25 7.26 2.34 o -12 2 2 133.59 130.60 2.60 o -11 2 2 127.25 132.88 2.53 o -10 2 2 12.23 12.00 2.30 o -9 2 2 50.71 65.12 2.31 o -8 2 2 403.43 382.11 2.87 o -7 2 2 1.45 0.10 2.32 o -6 2 2 26.55 16.92 3.14 o -5 2 2 774.12 796.47 9.14 o -4 2 2 1302.58 1295.27 11.17 o -3 2 2 854.11 835.53 3.92 o -2 2 2 800.71 787.84 5.43 o -1 2 2 699.52 734.03 4.78 o 0 2 2 113.97 108.89 2.12 o 1 2 2 2649.30 2717.10 19.94 o 2 2 2 2210.69 2296.05 15.47 o 3 2 2 1233.32 1398.39 13.08 o 4 2 2 1123.63 1178.96 4.99 o 5 2 2 866.32 920.98 25.88 o 6 2 2 1833.85 1943.98 9.73 o 7 2 2 358.37 368.78 7.06 o 8 2 2 263.77 257.61 3.42 o 9 2 2 14.84 14.81 3.15 o 10 2 2 2.25 3.46 2.89 o 11 2 2 226.25 212.94 4.80 o 12 2 2 110.23 113.65 5.63 o 13 2 2 6.41 7.64 2.97 o 14 2 2 175.31 174.12 4.11 o 15 2 2 199.90 202.01 3.69 o -16 3 2 51.58 55.37 3.23 o -15 3 2 8.49 12.69 2.93 o -14 3 2 373.93 377.49 5.87 o -13 3 2 5.24 4.70 2.43 o -12 3 2 11.46 10.43 2.43 o -11 3 2 1.61 1.25 1.99 o -10 3 2 2637.62 2638.84 42.74 o -9 3 2 1189.53 1156.18 12.72 o -8 3 2 127.57 118.58 2.27 o -7 3 2 17.22 17.87 1.89 o -6 3 2 1719.45 1641.90 12.85 o -5 3 2 4014.86 3952.47 34.59 o -4 3 2 729.34 685.39 3.57 o -3 3 2 68.68 84.00 2.24 o -2 3 2 329.43 405.33 3.49 o -1 3 2 1809.86 1833.40 17.31 o 0 3 2 1403.24 1280.19 9.48 o 1 3 2 1075.11 1151.14 7.68 o 2 3 2 416.07 464.42 4.59 o 3 3 2 1431.48 1465.95 16.04 o 4 3 2 1803.78 1902.40 13.65 o 5 3 2 1529.31 1522.85 25.92 o 6 3 2 3.07 2.78 2.22 o 7 3 2 20.68 31.30 2.54 o 8 3 2 251.94 262.28 4.36 o 9 3 2 106.22 88.43 2.92 o 10 3 2 232.08 239.83 3.33 o 11 3 2 8.97 10.60 2.89 o 12 3 2 77.80 73.93 3.42 o 13 3 2 286.59 304.42 4.41 o 14 3 2 127.03 126.66 3.38 o 15 3 2 175.60 184.72 3.85 o -15 4 2 1.33 3.49 3.26 o -14 4 2 4.17 5.84 3.96 o -13 4 2 331.38 345.44 5.15 o -12 4 2 120.58 131.92 4.86 o -11 4 2 222.75 221.23 2.49 o -10 4 2 352.53 368.82 7.85 o -9 4 2 1494.44 1484.38 19.94 o -8 4 2 3.25 2.27 2.04 o -7 4 2 185.38 182.27 2.30 o -6 4 2 700.55 698.53 4.07 o -5 4 2 393.55 399.22 4.65 o -4 4 2 1.39 0.79 2.40 o -3 4 2 972.66 987.90 5.44 o -2 4 2 677.64 697.54 5.59 o -1 4 2 69.46 75.89 1.91 o 0 4 2 229.92 245.37 5.80 o 1 4 2 468.24 444.77 3.37 o 2 4 2 70.56 66.87 2.04 o 3 4 2 181.80 190.21 2.11 o 4 4 2 269.51 260.19 3.79 o 5 4 2 1.82 1.09 2.05 o 6 4 2 4.75 1.86 2.35 o 7 4 2 59.76 65.12 2.40 o 8 4 2 240.04 225.56 5.44 o 9 4 2 51.81 47.69 2.40 o 10 4 2 0.13 1.69 2.29 o 11 4 2 117.93 128.93 2.70 o 12 4 2 166.19 168.52 2.81 o 13 4 2 25.51 21.61 2.73 o 14 4 2 52.16 52.82 2.84 o -14 5 2 166.24 188.50 4.67 o -13 5 2 60.40 60.90 3.31 o -12 5 2 0.81 2.54 3.10 o -11 5 2 90.99 87.18 2.46 o -10 5 2 70.73 75.74 2.17 o -9 5 2 83.48 86.02 2.01 o -8 5 2 7.81 4.68 1.78 o -7 5 2 130.91 122.77 2.61 o -6 5 2 214.25 198.44 2.42 o -5 5 2 393.27 385.50 4.83 o -4 5 2 161.55 158.67 10.39 o -3 5 2 3.17 3.54 1.79 o -2 5 2 596.99 586.93 3.74 o -1 5 2 0.04 0.21 1.77 o 0 5 2 247.81 220.72 3.56 o 1 5 2 485.91 470.73 5.04 o 2 5 2 88.18 89.96 1.95 o 3 5 2 368.48 349.39 2.45 o 4 5 2 224.01 209.19 2.57 o 5 5 2 280.66 266.93 2.77 o 6 5 2 126.20 123.59 2.41 o 7 5 2 4.16 6.06 2.23 o 8 5 2 277.58 308.20 4.46 o 9 5 2 9.01 8.91 2.55 o 10 5 2 61.95 56.79 2.47 o 11 5 2 118.42 121.55 3.59 o 12 5 2 181.43 193.77 5.30 o -12 6 2 144.87 142.51 3.46 o -11 6 2 4.52 10.30 3.00 o -10 6 2 2.18 2.64 2.51 o -9 6 2 6.37 1.70 2.30 o -8 6 2 127.92 131.59 3.04 o -7 6 2 2.54 3.02 2.50 o -6 6 2 47.01 49.02 2.20 o -5 6 2 259.42 236.76 2.46 o -4 6 2 304.85 306.43 2.99 o -3 6 2 34.78 35.55 1.73 o -2 6 2 9.38 10.39 1.66 o -1 6 2 384.89 366.53 2.42 o 0 6 2 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