#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:22:02 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180855 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/86/2018621.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018621_Fobs loop_ _publ_author_name 'Traeger, J.' 'Kelling, A.' 'Schilde, U.' 'Holdt, H.-J.' _publ_section_title ; rac-1-[(2-Methoxyethyl)sulfanyl]-2-[(2-methoxyethyl)sulfinyl]benzene and its PdCl~2~ complex ; _journal_coeditor_code FA3283 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m238 _journal_page_last m241 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.416 _cell_angle_gamma 90.000 _cell_length_a 10.6595 _cell_length_b 12.9818 _cell_length_c 12.2828 _exptl_crystal_F_000 904.00 _reflns_d_resolution_high 0.8410 _cod_data_source_file fa3283IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' TRAEG20I' _shelx_refln_list_code 4 _shelx_f_calc_maximum 304.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 54.09 48.12 38.07 o 4 0 0 894.71 801.47 36.77 o 6 0 0 22021.76 23865.15 110.72 o 8 0 0 8914.11 9214.13 98.53 o 10 0 0 212.66 217.29 31.30 o 12 0 0 599.50 597.06 54.38 o 1 1 0 7862.91 7257.05 101.07 o 2 1 0 11771.02 10752.34 144.74 o 3 1 0 23.24 24.72 24.82 o 4 1 0 292.12 264.26 26.00 o 5 1 0 413.54 373.15 23.02 o 6 1 0 5902.14 5702.24 52.72 o 7 1 0 2939.16 2982.17 37.59 o 8 1 0 2546.07 2474.66 51.75 o 9 1 0 552.48 591.97 23.61 o 10 1 0 2339.17 2371.81 38.50 o 11 1 0 143.90 151.92 23.87 o 12 1 0 1485.11 1378.04 34.02 o 0 2 0 39593.39 42034.95 219.93 o 1 2 0 10733.97 10471.34 75.08 o 2 2 0 19873.30 19388.65 247.05 o 3 2 0 106.21 139.28 25.04 o 4 2 0 138.72 140.57 20.66 o 5 2 0 1411.33 1360.25 27.96 o 6 2 0 10256.04 10306.34 95.19 o 7 2 0 10027.95 10576.62 238.74 o 8 2 0 2292.52 2342.90 30.90 o 9 2 0 330.01 368.32 22.51 o 10 2 0 1325.24 1252.75 26.82 o 11 2 0 857.14 854.20 38.07 o 12 2 0 452.44 433.98 33.93 o 1 3 0 1342.59 1229.47 27.31 o 2 3 0 1044.52 1026.80 27.59 o 3 3 0 4764.22 4623.02 44.56 o 4 3 0 2271.02 2086.80 43.35 o 5 3 0 5333.65 4803.51 60.93 o 6 3 0 40.27 16.27 25.40 o 7 3 0 2887.95 3023.06 37.51 o 8 3 0 1213.63 1271.22 29.10 o 9 3 0 701.09 733.47 27.40 o 10 3 0 86.71 61.04 25.26 o 11 3 0 2144.17 2190.52 87.58 o 12 3 0 192.88 222.44 48.58 o 0 4 0 4971.10 5190.12 55.72 o 1 4 0 11529.13 10519.04 128.30 o 2 4 0 616.47 636.93 21.73 o 3 4 0 991.53 966.57 26.40 o 4 4 0 4894.31 4974.76 62.23 o 5 4 0 1891.60 1898.93 30.25 o 6 4 0 335.90 314.66 24.97 o 7 4 0 10854.82 11367.00 236.07 o 8 4 0 528.58 576.38 25.79 o 9 4 0 2068.90 2234.77 34.12 o 10 4 0 1348.84 1261.65 31.45 o 11 4 0 0.60 13.51 29.85 o 12 4 0 22.04 34.69 31.60 o 1 5 0 8638.82 9102.67 137.28 o 2 5 0 2169.16 2106.26 26.95 o 3 5 0 6888.14 6705.77 40.43 o 4 5 0 1466.00 1414.72 24.17 o 5 5 0 6342.88 6277.68 144.06 o 6 5 0 5645.77 5596.94 41.04 o 7 5 0 723.19 781.29 27.30 o 8 5 0 125.56 133.57 28.09 o 9 5 0 77.48 43.05 22.08 o 10 5 0 1939.79 2018.16 34.19 o 11 5 0 2349.30 2317.15 37.33 o 0 6 0 603.94 669.19 27.35 o 1 6 0 1676.61 1566.38 22.78 o 2 6 0 3814.54 3676.42 30.39 o 3 6 0 3222.60 3334.65 29.74 o 4 6 0 2773.39 2969.48 28.68 o 5 6 0 1961.25 1942.40 45.56 o 6 6 0 929.03 976.37 25.85 o 7 6 0 1346.52 1399.39 28.44 o 8 6 0 2497.15 2570.30 41.74 o 9 6 0 1897.71 2007.14 30.94 o 10 6 0 0.17 -5.76 24.23 o 11 6 0 842.22 804.79 30.39 o 1 7 0 256.66 284.58 16.68 o 2 7 0 4631.15 4694.16 53.36 o 3 7 0 1927.48 1860.60 23.20 o 4 7 0 28493.60 29066.27 183.83 o 5 7 0 624.55 592.06 19.11 o 6 7 0 1087.39 1144.31 22.90 o 7 7 0 1627.28 1667.71 27.27 o 8 7 0 44.76 39.06 21.83 o 9 7 0 13.23 6.75 25.72 o 10 7 0 3196.03 3141.32 37.66 o 11 7 0 96.24 73.02 27.55 o 0 8 0 96.40 161.38 24.33 o 1 8 0 223.57 253.92 15.75 o 2 8 0 6575.35 6962.34 37.42 o 3 8 0 95.78 105.78 16.56 o 4 8 0 1610.57 1649.76 24.16 o 5 8 0 431.39 414.66 17.84 o 6 8 0 1655.01 1730.24 25.72 o 7 8 0 163.59 199.77 22.66 o 8 8 0 1150.16 1183.49 26.00 o 9 8 0 25.86 21.77 23.64 o 10 8 0 519.77 579.99 26.42 o 1 9 0 6.13 25.85 13.91 o 2 9 0 6828.50 6877.10 60.89 o 3 9 0 5660.00 5702.93 45.36 o 4 9 0 12537.02 12829.37 72.97 o 5 9 0 327.16 337.97 18.70 o 6 9 0 495.38 509.74 19.51 o 7 9 0 16.77 5.33 23.56 o 8 9 0 200.21 241.83 27.26 o 9 9 0 172.53 139.10 60.40 o 10 9 0 1857.13 1759.83 62.73 o 0 10 0 189.37 226.76 22.80 o 1 10 0 1762.52 1833.51 21.04 o 2 10 0 272.64 282.08 17.82 o 3 10 0 1535.17 1571.18 20.99 o 4 10 0 174.58 161.40 16.30 o 5 10 0 922.85 897.89 20.52 o 6 10 0 294.03 290.53 20.72 o 7 10 0 182.16 189.56 22.36 o 8 10 0 707.98 732.39 27.16 o 9 10 0 1241.72 1108.25 27.45 o 1 11 0 47.05 18.22 16.41 o 2 11 0 635.01 637.64 18.32 o 3 11 0 8712.07 9030.41 60.07 o 4 11 0 66.13 66.10 16.47 o 5 11 0 1606.74 1575.46 22.54 o 6 11 0 404.21 403.10 21.02 o 7 11 0 1.30 34.28 21.06 o 8 11 0 2.18 14.93 26.11 o 0 12 0 7.96 -7.61 25.16 o 1 12 0 1996.59 2029.42 25.00 o 2 12 0 309.11 354.99 17.55 o 3 12 0 442.72 459.98 19.15 o 4 12 0 239.11 207.00 16.70 o 5 12 0 145.51 130.73 17.86 o 6 12 0 196.43 209.04 19.34 o 7 12 0 1090.78 1011.92 25.10 o 1 13 0 343.95 322.37 16.74 o 2 13 0 472.71 465.08 19.17 o 3 13 0 2356.76 2487.26 33.42 o 4 13 0 802.91 788.51 20.40 o 5 13 0 581.84 569.20 19.27 o 6 13 0 0.87 -6.44 17.98 o 0 14 0 1615.15 1699.95 31.19 o 1 14 0 623.87 658.67 19.00 o 2 14 0 483.72 475.10 19.57 o 3 14 0 0.16 -2.32 18.41 o 4 14 0 31.77 40.22 18.90 o 5 14 0 49.88 51.54 19.24 o 1 15 0 21.46 6.79 17.67 o 2 15 0 1218.22 1126.29 21.95 o -11 0 1 29.69 36.64 34.32 o -9 0 1 396.11 427.73 32.37 o -7 0 1 53338.00 55759.34 174.13 o -5 0 1 63.03 39.59 31.60 o -3 0 1 2171.15 1820.42 53.11 o -1 0 1 31598.18 31211.41 252.37 o 1 0 1 28517.57 25684.94 652.18 o 3 0 1 98.31 92.84 40.76 o 5 0 1 2678.80 2632.40 63.47 o 7 0 1 6398.68 6063.12 105.92 o 9 0 1 3526.89 3714.44 77.08 o 11 0 1 199.11 180.76 32.92 o -12 1 1 168.81 157.14 27.50 o -11 1 1 236.63 224.91 29.70 o -10 1 1 315.88 297.11 24.04 o -9 1 1 21.35 12.08 21.72 o -8 1 1 835.42 856.10 29.52 o -7 1 1 2250.48 2220.75 30.85 o -6 1 1 5215.11 5451.57 147.92 o -5 1 1 8484.05 8355.68 114.01 o -4 1 1 106.99 74.82 21.96 o -3 1 1 1478.03 1642.32 37.26 o -2 1 1 313.74 283.69 31.42 o -1 1 1 17104.85 16037.66 221.68 o 0 1 1 803.39 727.76 35.14 o 1 1 1 21539.99 20867.44 209.95 o 2 1 1 742.65 607.67 27.87 o 3 1 1 4168.73 3811.24 42.07 o 4 1 1 1.41 10.20 19.27 o 5 1 1 4223.72 4053.57 40.48 o 6 1 1 3740.36 3806.12 33.29 o 7 1 1 58.78 79.58 19.70 o 8 1 1 11.21 13.07 21.97 o 9 1 1 1163.23 1121.68 26.54 o 10 1 1 2345.84 2294.36 44.32 o 11 1 1 5517.01 5453.84 71.55 o 12 1 1 87.37 60.42 25.67 o -12 2 1 106.39 86.96 45.91 o -11 2 1 136.32 170.35 31.01 o -10 2 1 90.00 109.07 22.63 o -9 2 1 940.46 1025.79 27.47 o -8 2 1 7770.59 8244.37 71.49 o -7 2 1 11755.79 12043.08 107.95 o -6 2 1 11924.94 12291.30 92.65 o -5 2 1 3017.77 2952.74 51.68 o -4 2 1 556.88 491.98 29.15 o -3 2 1 0.53 0.50 23.46 o -2 2 1 26746.18 26708.64 279.50 o -1 2 1 12401.16 12257.68 76.61 o 0 2 1 35891.65 37460.39 133.36 o 1 2 1 3540.32 3305.11 41.21 o 2 2 1 5832.30 5600.14 48.49 o 3 2 1 9729.93 9657.30 93.17 o 4 2 1 11438.47 12032.61 201.45 o 5 2 1 2597.23 2686.70 52.33 o 6 2 1 1664.05 1645.80 27.27 o 7 2 1 3854.69 3862.64 52.05 o 8 2 1 4561.34 4817.85 36.81 o 9 2 1 2381.41 2442.27 52.23 o 10 2 1 2.80 21.87 25.45 o 11 2 1 266.70 300.79 25.94 o 12 2 1 203.84 182.85 26.90 o -12 3 1 1864.21 1656.46 69.25 o -11 3 1 227.15 246.08 30.97 o -10 3 1 1818.63 1859.94 81.08 o -9 3 1 36.77 29.92 23.40 o -8 3 1 1262.17 1262.81 30.91 o -7 3 1 26.07 6.64 24.59 o -6 3 1 7076.31 7151.67 51.68 o -5 3 1 140.53 109.34 24.24 o -4 3 1 8474.20 8321.86 269.71 o -3 3 1 4286.19 4094.05 42.42 o -2 3 1 2331.17 2373.04 35.27 o -1 3 1 1298.32 1244.19 26.66 o 0 3 1 3632.89 3555.89 37.65 o 1 3 1 2684.28 2582.33 34.05 o 2 3 1 8374.14 7913.02 84.32 o 3 3 1 1.94 5.37 19.86 o 4 3 1 12282.35 12206.58 209.92 o 5 3 1 929.16 894.08 22.85 o 6 3 1 5438.34 5516.73 44.99 o 7 3 1 5793.17 5915.58 41.04 o 8 3 1 542.05 557.56 22.73 o 9 3 1 6.93 0.49 20.30 o 10 3 1 5232.13 5198.56 48.26 o 11 3 1 348.68 372.21 44.71 o 12 3 1 1309.38 1212.13 38.41 o -12 4 1 516.33 500.54 34.34 o -11 4 1 405.22 401.39 33.45 o -10 4 1 601.96 600.88 29.60 o -9 4 1 202.94 176.19 39.65 o -8 4 1 4147.63 4318.94 40.29 o -7 4 1 164.94 148.08 23.24 o -6 4 1 8895.16 8961.91 53.59 o -5 4 1 223.80 187.83 22.48 o -4 4 1 1317.65 1463.30 31.87 o -3 4 1 1501.28 1605.17 27.52 o -2 4 1 2615.48 2295.72 28.91 o -1 4 1 436.21 490.83 22.39 o 0 4 1 89045.53 97893.39 669.14 o 1 4 1 4477.62 4187.63 35.76 o 2 4 1 7446.70 7129.20 93.16 o 3 4 1 15624.20 15809.30 88.71 o 4 4 1 1719.25 1746.53 25.22 o 5 4 1 241.52 192.42 18.99 o 6 4 1 11096.32 11675.00 121.06 o 7 4 1 221.36 237.71 19.70 o 8 4 1 2522.34 2625.05 64.30 o 9 4 1 1132.91 1054.27 28.90 o 10 4 1 655.19 704.40 29.23 o 11 4 1 991.78 1031.77 33.80 o 12 4 1 645.20 628.21 46.48 o -11 5 1 522.12 510.98 30.76 o -10 5 1 2602.64 2471.12 44.85 o -9 5 1 309.02 291.84 26.77 o -8 5 1 455.04 412.71 25.51 o -7 5 1 472.60 501.38 26.38 o -6 5 1 2331.60 2299.50 46.35 o -5 5 1 599.30 555.31 21.33 o -4 5 1 12781.85 13057.87 156.68 o -3 5 1 584.70 566.94 23.36 o -2 5 1 15684.80 15969.25 58.14 o -1 5 1 10005.43 10109.67 148.48 o 0 5 1 5269.58 5088.03 77.93 o 1 5 1 221.84 261.36 18.25 o 2 5 1 8201.77 7979.44 41.58 o 3 5 1 8007.18 7821.14 40.84 o 4 5 1 20083.66 20712.67 153.19 o 5 5 1 504.97 476.35 19.70 o 6 5 1 75.30 71.78 21.41 o 7 5 1 6127.52 6283.12 41.83 o 8 5 1 1679.57 1749.78 30.70 o 9 5 1 745.21 783.32 31.54 o 10 5 1 1632.56 1715.26 65.09 o 11 5 1 571.91 566.17 49.25 o -11 6 1 123.27 96.08 28.06 o -10 6 1 1022.29 1031.50 54.95 o -9 6 1 1477.25 1536.89 30.27 o -8 6 1 361.18 406.85 26.27 o -7 6 1 648.30 719.88 23.95 o -6 6 1 810.52 856.76 27.23 o -5 6 1 1000.15 996.71 23.80 o -4 6 1 1862.75 1884.81 32.74 o -3 6 1 6803.27 6648.00 90.22 o -2 6 1 3595.35 3378.50 28.33 o -1 6 1 2793.87 2640.89 25.81 o 0 6 1 1870.93 1868.27 24.70 o 1 6 1 3753.50 3731.68 28.20 o 2 6 1 3093.29 2867.47 26.48 o 3 6 1 276.76 291.18 18.83 o 4 6 1 1893.10 1867.11 23.90 o 5 6 1 2970.98 2928.65 31.59 o 6 6 1 7030.86 6872.42 118.23 o 7 6 1 2164.40 2230.28 35.17 o 8 6 1 132.63 153.43 24.59 o 9 6 1 144.99 141.66 41.32 o 10 6 1 1040.30 1036.90 27.98 o 11 6 1 280.52 253.77 35.54 o -11 7 1 4499.56 4361.70 227.75 o -10 7 1 252.78 247.87 26.84 o -9 7 1 1309.88 1239.82 29.62 o -8 7 1 174.08 150.56 25.48 o -7 7 1 34.80 35.54 21.12 o -6 7 1 310.95 339.81 20.94 o -5 7 1 3485.61 3267.06 46.60 o -4 7 1 1886.97 1900.09 24.28 o -3 7 1 26635.79 27611.55 115.61 o -2 7 1 1491.10 1471.89 20.68 o -1 7 1 718.88 847.92 24.25 o 0 7 1 8072.04 8346.56 91.45 o 1 7 1 320.10 356.98 17.38 o 2 7 1 378.17 338.89 17.31 o 3 7 1 13497.37 13988.23 130.09 o 4 7 1 849.28 807.86 18.58 o 5 7 1 4805.81 4684.30 30.79 o 6 7 1 319.77 347.38 19.73 o 7 7 1 232.68 250.47 23.44 o 8 7 1 373.54 471.81 26.51 o 9 7 1 788.06 830.71 37.28 o 10 7 1 0.14 15.60 23.55 o 11 7 1 898.35 846.97 30.77 o -10 8 1 124.33 125.22 26.74 o -9 8 1 3446.70 3663.62 172.49 o -8 8 1 2.60 -10.99 22.98 o -7 8 1 15.29 34.69 21.46 o -6 8 1 98.43 105.11 20.34 o -5 8 1 1590.07 1521.01 27.44 o -4 8 1 100.32 116.47 15.27 o -3 8 1 6420.26 6415.91 33.22 o -2 8 1 914.95 906.35 21.54 o -1 8 1 2628.83 2675.68 24.01 o 0 8 1 28.23 16.14 16.55 o 1 8 1 1278.68 1178.07 20.52 o 2 8 1 262.08 281.20 17.07 o 3 8 1 1257.40 1327.39 19.64 o 4 8 1 627.29 621.50 17.66 o 5 8 1 1105.66 1095.32 19.34 o 6 8 1 6.12 9.01 17.47 o 7 8 1 5749.83 6097.34 60.40 o 8 8 1 30.80 16.90 20.77 o 9 8 1 1120.59 1106.08 28.77 o 10 8 1 16.04 3.24 23.75 o -10 9 1 1082.18 1074.27 75.88 o -9 9 1 1758.25 1706.27 30.11 o -8 9 1 113.17 113.78 20.88 o -7 9 1 8.84 17.15 19.13 o -6 9 1 2.05 12.13 21.87 o -5 9 1 3382.97 3264.57 26.22 o -4 9 1 5437.25 5522.28 45.17 o -3 9 1 10905.65 11260.93 65.16 o -2 9 1 930.75 898.30 19.14 o -1 9 1 1175.78 1246.94 19.10 o 0 9 1 4.45 18.31 14.58 o 1 9 1 1058.78 999.12 27.25 o 2 9 1 846.93 836.88 17.38 o 3 9 1 6938.20 7185.58 33.32 o 4 9 1 3352.46 3318.93 26.86 o 5 9 1 1910.54 1959.97 27.45 o 6 9 1 342.86 392.63 18.74 o 7 9 1 20.42 19.41 19.08 o 8 9 1 283.17 291.97 24.33 o 9 9 1 704.70 704.76 28.75 o 10 9 1 190.30 83.45 96.21 o -9 10 1 494.28 510.82 28.77 o -8 10 1 882.33 846.89 25.85 o -7 10 1 70.95 60.66 20.16 o -6 10 1 265.67 280.27 20.97 o -5 10 1 36.13 39.05 17.02 o -4 10 1 345.82 333.17 17.34 o -3 10 1 392.22 402.46 17.34 o -2 10 1 2633.40 2635.38 24.50 o -1 10 1 554.25 607.12 17.71 o 0 10 1 356.10 360.26 17.90 o 1 10 1 1508.91 1509.12 33.64 o 2 10 1 1447.91 1421.54 20.82 o 3 10 1 73.18 74.26 15.28 o 4 10 1 129.53 122.51 15.17 o 5 10 1 269.73 270.07 17.83 o 6 10 1 1061.75 1126.64 22.04 o 7 10 1 1252.83 1254.91 26.24 o 8 10 1 1504.99 1446.00 29.03 o 9 10 1 566.06 508.15 74.00 o -8 11 1 10.41 3.97 25.78 o -7 11 1 1.52 2.87 20.47 o -6 11 1 218.46 229.22 19.52 o -5 11 1 100.62 130.87 18.36 o -4 11 1 8062.65 8262.68 35.64 o -3 11 1 351.25 322.06 16.67 o -2 11 1 2718.13 2738.81 30.85 o -1 11 1 1126.06 1215.27 19.88 o 0 11 1 55.15 57.44 17.62 o 1 11 1 4.60 7.30 16.75 o 2 11 1 4062.55 4142.96 73.00 o 3 11 1 809.06 777.40 23.91 o 4 11 1 3815.06 3876.22 26.28 o 5 11 1 48.48 28.44 18.51 o 6 11 1 277.86 305.51 18.69 o 7 11 1 378.92 370.82 22.43 o 8 11 1 275.97 219.49 54.70 o -7 12 1 0.22 9.57 20.23 o -6 12 1 561.82 494.07 21.26 o -5 12 1 185.73 178.61 17.81 o -4 12 1 14.67 15.70 18.15 o -3 12 1 9.44 -4.46 17.95 o -2 12 1 1374.57 1476.21 28.12 o -1 12 1 225.84 209.37 18.09 o 0 12 1 1286.84 1268.15 28.90 o 1 12 1 10.41 14.12 16.35 o 2 12 1 1349.70 1401.74 20.48 o 3 12 1 1235.44 1318.61 34.72 o 4 12 1 477.02 504.41 19.04 o 5 12 1 54.13 58.38 18.06 o 6 12 1 976.59 960.78 28.85 o 7 12 1 36.09 30.60 21.72 o -6 13 1 274.95 288.62 19.48 o -5 13 1 472.58 503.71 20.40 o -4 13 1 1960.80 1969.61 49.44 o -3 13 1 905.71 963.70 38.74 o -2 13 1 701.43 726.12 20.32 o -1 13 1 7.23 17.29 15.83 o 0 13 1 418.96 453.25 19.20 o 1 13 1 803.14 811.61 19.82 o 2 13 1 2712.35 2760.95 57.87 o 3 13 1 449.65 403.53 18.31 o 4 13 1 329.16 346.13 18.80 o 5 13 1 329.92 333.92 19.47 o 6 13 1 875.09 872.72 22.58 o -5 14 1 142.24 125.08 19.57 o -4 14 1 79.12 58.53 20.54 o -3 14 1 4.37 14.24 18.77 o -2 14 1 214.38 224.34 17.97 o -1 14 1 1580.04 1559.05 42.51 o 0 14 1 580.55 599.70 17.49 o 1 14 1 2119.42 2097.13 50.64 o 2 14 1 203.72 237.43 17.64 o 3 14 1 146.02 152.29 19.59 o 4 14 1 853.48 811.08 21.73 o 5 14 1 118.14 93.37 18.63 o -2 15 1 13.68 23.73 18.72 o -1 15 1 304.78 293.63 19.69 o 0 15 1 224.63 231.20 19.28 o 1 15 1 733.87 733.37 24.09 o 2 15 1 19.09 11.10 19.33 o -12 0 2 159.80 121.18 38.41 o -10 0 2 69.09 45.47 31.52 o -8 0 2 10410.05 11022.84 104.75 o -6 0 2 18181.05 18574.38 100.33 o -4 0 2 42.45 18.10 28.86 o -2 0 2 69.80 76.62 36.65 o 0 0 2 92922.47 96063.89 989.18 o 2 0 2 14476.19 13592.03 95.88 o 4 0 2 7832.21 7902.88 107.10 o 6 0 2 3844.17 3940.89 49.44 o 8 0 2 1014.83 1008.32 32.64 o 10 0 2 801.10 949.22 35.32 o 12 0 2 763.77 713.38 37.22 o -12 1 2 2356.82 2236.86 49.46 o -11 1 2 2.17 2.17 24.08 o -10 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