#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:22:02 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180855 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/86/2018634.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018634_Fobs loop_ _publ_author_name 'Bojarska, Joanna' 'Maniukiewicz, Waldemar' 'Siero\'n, Les\/law' 'Kopczacki, Piotr' 'Walczy\'nski, Krzysztof' 'Remko, Milan' _publ_section_title ; Perindoprilat monohydrate ; _journal_coeditor_code FG3275 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o443 _journal_page_last o446 _journal_volume 68 _journal_year 2012 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.1645 _cell_length_b 10.0136 _cell_length_c 23.2429 _exptl_crystal_F_000 776.00 _reflns_d_resolution_high 0.8439 _cod_data_source_file fg3275Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Pelat_h2o_lt_0m in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 115.37 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1930.66 1926.20 52.71 o 4 0 0 141.41 156.40 5.15 o 6 0 0 0.00 2.44 0.66 o 8 0 0 330.90 350.37 6.35 o 1 1 0 794.83 686.44 16.12 o 2 1 0 392.53 358.85 7.47 o 3 1 0 157.16 164.37 3.50 o 4 1 0 680.03 688.66 8.39 o 5 1 0 2048.55 2168.82 26.95 o 6 1 0 220.25 213.18 3.65 o 7 1 0 881.85 833.83 15.05 o 8 1 0 341.43 348.87 3.91 o 9 1 0 11.94 11.73 0.52 o 0 2 0 3333.82 2983.93 114.64 o 1 2 0 7518.08 6878.49 144.44 o 2 2 0 339.31 362.09 8.42 o 3 2 0 2339.91 2440.51 50.23 o 4 2 0 560.86 642.55 7.63 o 5 2 0 995.74 1013.98 12.38 o 6 2 0 281.57 271.77 4.56 o 7 2 0 951.41 894.03 16.07 o 8 2 0 205.09 192.72 2.87 o 9 2 0 10.81 16.55 0.56 o 1 3 0 363.45 354.68 7.54 o 2 3 0 0.38 0.58 0.30 o 3 3 0 200.43 235.67 5.39 o 4 3 0 69.19 55.05 0.87 o 5 3 0 18.82 21.08 0.61 o 6 3 0 57.66 53.05 1.11 o 7 3 0 150.21 134.68 2.65 o 8 3 0 68.32 61.15 1.08 o 9 3 0 224.79 218.90 3.11 o 0 4 0 930.03 1054.06 35.11 o 1 4 0 616.12 664.21 13.99 o 2 4 0 1614.67 1726.39 27.02 o 3 4 0 436.31 400.90 8.19 o 4 4 0 4.76 6.71 0.55 o 5 4 0 17.84 22.82 0.74 o 6 4 0 85.87 92.88 3.21 o 7 4 0 80.37 67.08 1.00 o 8 4 0 0.05 0.75 0.35 o 9 4 0 186.64 193.93 2.48 o 1 5 0 321.03 363.67 4.86 o 2 5 0 91.98 106.29 1.69 o 3 5 0 356.26 377.02 5.55 o 4 5 0 19.67 24.39 1.07 o 5 5 0 37.79 44.55 1.32 o 6 5 0 113.48 117.11 2.72 o 7 5 0 1098.52 1102.33 13.49 o 8 5 0 92.38 92.26 1.38 o 0 6 0 2818.21 2915.33 48.53 o 1 6 0 482.73 472.65 6.34 o 2 6 0 1676.62 1748.13 29.19 o 3 6 0 144.10 132.56 3.32 o 4 6 0 71.44 79.87 2.77 o 5 6 0 270.89 277.36 5.77 o 6 6 0 113.24 106.50 2.62 o 7 6 0 159.80 167.66 2.29 o 8 6 0 29.76 35.28 1.04 o 1 7 0 96.50 92.45 1.76 o 2 7 0 8.72 7.91 0.56 o 3 7 0 64.38 70.67 1.66 o 4 7 0 364.43 371.94 9.15 o 5 7 0 10.77 13.00 0.51 o 6 7 0 496.41 487.67 8.10 o 7 7 0 5.18 5.30 0.44 o 0 8 0 182.20 198.56 7.03 o 1 8 0 0.37 0.07 0.47 o 2 8 0 1333.01 1337.21 26.45 o 3 8 0 73.76 66.92 2.08 o 4 8 0 30.89 31.06 1.44 o 5 8 0 68.19 63.72 1.53 o 6 8 0 101.56 101.97 1.78 o 7 8 0 84.61 88.34 1.94 o 1 9 0 3.46 5.92 0.64 o 2 9 0 32.58 32.98 0.83 o 3 9 0 1568.78 1574.72 19.88 o 4 9 0 76.96 78.11 1.50 o 5 9 0 165.63 165.86 3.10 o 6 9 0 13.72 11.50 0.59 o 0 10 0 119.85 122.48 2.52 o 1 10 0 54.87 60.49 1.08 o 2 10 0 75.46 62.19 2.14 o 3 10 0 1.62 2.87 0.43 o 4 10 0 108.29 120.79 1.98 o 5 10 0 1.57 1.13 0.50 o 1 11 0 126.55 140.96 2.18 o 2 11 0 19.67 20.07 1.26 o 3 11 0 5.84 10.26 0.50 o 1 0 1 8651.24 7631.22 160.15 o 2 0 1 54.14 48.55 1.14 o 3 0 1 7389.91 7206.81 164.06 o 4 0 1 1314.99 1286.11 17.53 o 5 0 1 2.83 3.25 0.34 o 6 0 1 182.00 174.67 3.40 o 7 0 1 851.20 816.44 14.67 o 8 0 1 5.60 7.14 0.33 o 9 0 1 0.47 0.58 0.30 o -9 1 1 32.35 36.19 0.85 o -8 1 1 238.28 236.88 2.84 o -7 1 1 497.55 461.87 8.50 o -6 1 1 1161.16 1205.22 19.16 o -5 1 1 541.04 523.06 6.68 o -4 1 1 0.22 1.48 0.39 o -3 1 1 2202.74 2348.35 48.31 o -2 1 1 4408.83 4038.32 85.57 o -1 1 1 1284.57 1177.15 27.76 o 0 1 1 12519.01 10517.26 304.62 o 1 1 1 1279.22 1211.12 24.99 o 2 1 1 4385.68 4277.15 88.14 o 3 1 1 2192.36 2358.44 48.64 o 4 1 1 0.19 1.41 0.21 o 5 1 1 540.90 520.70 6.90 o 6 1 1 1159.74 1177.71 17.64 o 7 1 1 493.16 459.64 8.42 o 8 1 1 237.03 239.86 2.88 o 9 1 1 31.76 37.04 0.80 o -9 2 1 43.81 40.63 0.82 o -8 2 1 466.02 450.00 6.27 o -7 2 1 156.61 156.16 2.82 o -6 2 1 844.09 833.66 13.37 o -5 2 1 265.87 259.24 3.39 o -4 2 1 28.41 41.09 0.91 o -3 2 1 1329.82 1440.78 29.69 o -2 2 1 80.82 87.83 2.16 o -1 2 1 6483.42 5948.50 125.06 o 0 2 1 3240.91 3049.93 58.43 o 1 2 1 6496.63 6080.20 129.60 o 2 2 1 79.87 90.91 2.21 o 3 2 1 1315.67 1430.55 29.45 o 4 2 1 29.15 42.03 0.92 o 5 2 1 267.33 260.06 3.29 o 6 2 1 838.01 823.50 12.41 o 7 2 1 153.79 154.65 2.99 o 8 2 1 465.26 448.78 6.26 o 9 2 1 44.23 40.14 0.81 o -9 3 1 55.78 55.60 1.00 o -8 3 1 57.42 72.21 1.20 o -7 3 1 584.70 530.77 9.32 o -6 3 1 120.89 122.53 2.35 o -5 3 1 339.32 333.38 4.06 o -4 3 1 631.41 625.15 8.06 o -3 3 1 1661.33 1779.77 26.26 o -2 3 1 503.63 531.90 14.38 o -1 3 1 4325.07 4458.92 104.82 o 0 3 1 1297.51 1247.28 23.66 o 1 3 1 4332.42 4360.43 82.80 o 2 3 1 505.71 516.83 13.18 o 3 3 1 1663.17 1771.23 26.20 o 4 3 1 632.15 629.84 7.76 o 5 3 1 336.94 326.38 4.28 o 6 3 1 119.27 119.52 2.81 o 7 3 1 580.28 553.38 8.70 o 8 3 1 59.74 74.16 1.22 o 9 3 1 55.76 56.79 1.11 o -9 4 1 112.82 117.22 1.58 o -8 4 1 1.64 1.27 0.36 o -7 4 1 117.66 100.51 1.52 o -6 4 1 197.62 189.30 3.66 o -5 4 1 378.42 372.43 5.93 o -4 4 1 317.25 315.89 4.59 o -3 4 1 2140.20 2238.67 32.01 o -2 4 1 472.23 496.83 7.45 o -1 4 1 979.60 1110.11 26.14 o 0 4 1 1246.30 1293.40 30.40 o 1 4 1 981.50 1093.38 22.87 o 2 4 1 465.35 483.79 7.69 o 3 4 1 2145.02 2193.69 31.77 o 4 4 1 316.31 308.77 4.47 o 5 4 1 380.44 377.18 7.62 o 6 4 1 197.26 193.03 3.50 o 7 4 1 118.63 101.81 1.51 o 8 4 1 1.58 1.13 0.39 o 9 4 1 111.74 116.95 1.70 o -8 5 1 23.91 20.84 0.59 o -7 5 1 63.45 74.48 1.13 o -6 5 1 1466.41 1315.21 30.31 o -5 5 1 70.75 72.01 1.82 o -4 5 1 12.65 13.83 0.54 o -3 5 1 103.10 115.52 1.85 o -2 5 1 910.97 933.30 13.50 o -1 5 1 327.28 352.17 4.56 o 0 5 1 773.29 758.58 10.17 o 1 5 1 327.51 342.39 4.83 o 2 5 1 906.13 924.43 13.30 o 3 5 1 102.88 118.19 2.39 o 4 5 1 13.07 13.56 0.52 o 5 5 1 71.29 74.46 1.85 o 6 5 1 1462.35 1344.88 59.26 o 7 5 1 63.92 73.15 1.19 o 8 5 1 24.13 21.53 0.67 o -8 6 1 105.56 109.98 1.53 o -7 6 1 33.65 38.85 0.83 o -6 6 1 81.27 70.91 1.21 o -5 6 1 149.27 146.00 3.27 o -4 6 1 263.71 266.89 5.11 o -3 6 1 1116.23 1117.40 16.92 o -2 6 1 350.10 329.45 5.35 o -1 6 1 610.20 625.97 8.00 o 0 6 1 45.64 58.16 0.99 o 1 6 1 612.55 619.67 8.26 o 2 6 1 351.02 331.76 5.74 o 3 6 1 1109.13 1084.64 15.50 o 4 6 1 261.35 266.78 5.57 o 5 6 1 148.71 143.24 3.20 o 6 6 1 81.41 71.65 1.05 o 7 6 1 33.06 38.84 0.89 o 8 6 1 104.21 109.34 1.64 o -7 7 1 4.02 2.85 0.39 o -6 7 1 35.48 36.46 0.86 o -5 7 1 221.30 206.76 2.51 o -4 7 1 59.35 62.47 2.10 o -3 7 1 68.77 66.19 1.71 o -2 7 1 93.78 91.85 1.98 o -1 7 1 30.30 31.83 1.09 o 0 7 1 429.29 416.00 6.11 o 1 7 1 31.19 32.95 1.24 o 2 7 1 95.36 93.76 1.99 o 3 7 1 70.54 67.75 2.28 o 4 7 1 60.51 61.63 2.07 o 5 7 1 220.98 208.66 3.07 o 6 7 1 34.86 36.43 1.11 o 7 7 1 3.72 2.70 0.40 o -7 8 1 10.77 11.79 0.60 o -6 8 1 152.00 150.41 2.25 o -5 8 1 21.73 20.75 0.83 o -4 8 1 231.19 226.23 2.91 o -3 8 1 501.29 469.84 10.54 o -2 8 1 411.27 409.22 8.24 o -1 8 1 135.35 138.96 3.42 o 0 8 1 0.71 0.15 0.51 o 1 8 1 134.82 138.15 3.12 o 2 8 1 409.91 408.59 8.34 o 3 8 1 499.29 459.99 18.63 o 4 8 1 231.00 226.63 3.88 o 5 8 1 21.57 20.00 0.90 o 6 8 1 154.39 152.98 2.51 o 7 8 1 10.53 10.89 0.51 o -6 9 1 113.31 129.84 2.42 o -5 9 1 4.73 6.80 0.42 o -4 9 1 509.20 523.88 6.56 o -3 9 1 31.85 33.34 0.97 o -2 9 1 96.10 99.41 2.00 o -1 9 1 204.71 204.38 4.46 o 0 9 1 279.72 277.54 5.87 o 1 9 1 204.86 202.14 4.41 o 2 9 1 95.78 101.13 2.36 o 3 9 1 31.23 33.54 1.47 o 4 9 1 513.27 528.96 7.77 o 5 9 1 4.53 6.32 0.66 o 6 9 1 112.87 126.20 2.38 o -5 10 1 62.90 61.70 1.45 o -4 10 1 59.50 58.24 1.25 o -3 10 1 48.91 55.37 1.07 o -2 10 1 1.75 1.66 0.37 o -1 10 1 28.74 24.80 0.75 o 0 10 1 52.28 42.32 0.95 o 1 10 1 29.00 25.24 0.97 o 2 10 1 1.47 1.55 0.47 o 3 10 1 48.82 55.35 1.15 o 4 10 1 59.58 58.81 1.13 o 5 10 1 63.07 62.89 1.57 o -3 11 1 215.77 232.28 4.02 o -2 11 1 76.69 94.81 1.35 o -1 11 1 62.71 70.36 1.46 o 0 11 1 1.59 1.93 0.35 o 1 11 1 62.85 71.20 1.87 o 2 11 1 75.66 96.97 1.63 o 3 11 1 215.27 231.59 3.47 o 0 0 2 5371.70 4983.97 177.67 o 1 0 2 798.10 797.74 15.14 o 2 0 2 4117.61 3800.96 71.90 o 3 0 2 684.59 743.46 17.01 o 4 0 2 80.89 68.67 1.00 o 5 0 2 584.42 572.30 7.28 o 6 0 2 108.41 98.00 1.93 o 7 0 2 121.14 119.62 2.51 o 8 0 2 26.89 26.48 1.51 o 9 0 2 165.16 170.87 2.51 o -9 1 2 3.18 3.73 0.34 o -8 1 2 454.08 417.57 5.29 o -7 1 2 565.09 545.90 9.95 o -6 1 2 185.22 188.50 3.10 o -5 1 2 295.61 279.00 4.19 o -4 1 2 1314.50 1438.29 19.71 o -3 1 2 2756.85 2872.93 65.82 o -2 1 2 73.60 79.31 1.93 o -1 1 2 3440.86 3127.50 60.83 o 0 1 2 238.09 200.92 3.86 o 1 1 2 3430.31 3200.94 74.12 o 2 1 2 76.28 87.21 1.75 o 3 1 2 2746.61 2810.15 57.98 o 4 1 2 1316.71 1425.88 15.62 o 5 1 2 292.17 275.92 3.78 o 6 1 2 189.95 191.95 3.11 o 7 1 2 565.38 548.79 10.99 o 8 1 2 454.94 414.51 4.76 o 9 1 2 3.41 3.40 0.34 o -9 2 2 7.27 5.28 0.34 o -8 2 2 65.15 74.85 1.37 o -7 2 2 229.03 233.50 4.02 o -6 2 2 410.31 373.91 6.17 o -5 2 2 166.58 168.80 2.39 o -4 2 2 468.05 466.33 6.02 o -3 2 2 528.98 539.71 11.21 o -2 2 2 21.15 20.35 0.80 o -1 2 2 6902.10 6409.59 134.49 o 0 2 2 6042.17 5712.04 108.82 o 1 2 2 6869.47 6517.42 136.96 o 2 2 2 20.65 19.30 0.87 o 3 2 2 528.10 539.82 12.59 o 4 2 2 473.09 465.05 5.35 o 5 2 2 166.38 167.41 2.20 o 6 2 2 406.62 373.28 6.22 o 7 2 2 229.57 230.30 4.26 o 8 2 2 64.41 74.63 1.38 o 9 2 2 7.11 5.13 0.40 o -9 3 2 73.36 76.16 1.25 o -8 3 2 9.65 15.58 0.58 o -7 3 2 41.05 41.16 0.76 o -6 3 2 1644.29 1657.40 30.66 o -5 3 2 5.77 6.16 0.33 o -4 3 2 282.70 272.99 3.61 o -3 3 2 5488.89 5579.28 85.48 o -2 3 2 531.96 597.96 20.04 o -1 3 2 496.47 458.93 13.43 o 0 3 2 577.96 594.61 11.31 o 1 3 2 494.81 459.06 8.78 o 2 3 2 538.81 606.91 14.11 o 3 3 2 5509.08 5623.33 75.19 o 4 3 2 288.42 277.64 3.66 o 5 3 2 5.53 5.97 0.36 o 6 3 2 1636.03 1613.31 26.55 o 7 3 2 41.27 40.95 0.92 o 8 3 2 9.31 15.66 0.63 o 9 3 2 72.88 78.27 1.89 o -9 4 2 127.70 134.26 1.77 o -8 4 2 117.15 126.42 1.81 o -7 4 2 171.62 164.41 1.99 o -6 4 2 156.01 159.72 3.34 o -5 4 2 343.12 351.47 5.32 o -4 4 2 379.39 408.07 5.89 o -3 4 2 927.10 997.72 14.37 o -2 4 2 1159.68 1127.53 15.46 o -1 4 2 4624.18 4750.90 111.65 o 0 4 2 4327.67 4711.44 111.40 o 1 4 2 4621.57 4521.12 96.22 o 2 4 2 1164.55 1127.16 17.71 o 3 4 2 931.05 968.49 14.50 o 4 4 2 378.52 400.54 5.51 o 5 4 2 339.90 350.36 7.10 o 6 4 2 157.48 160.11 3.51 o 7 4 2 171.75 164.55 2.97 o 8 4 2 117.00 127.36 1.97 o 9 4 2 128.40 141.28 2.02 o -8 5 2 164.62 174.31 2.33 o -7 5 2 42.19 46.20 0.94 o -6 5 2 384.87 372.56 8.37 o -5 5 2 658.73 646.96 10.90 o -4 5 2 281.66 271.70 4.73 o -3 5 2 434.25 448.96 6.59 o -2 5 2 342.80 320.06 4.74 o -1 5 2 2714.55 2835.09 35.71 o 0 5 2 74.94 74.72 2.36 o 1 5 2 2713.25 2745.34 37.70 o 2 5 2 343.58 323.60 5.22 o 3 5 2 431.96 439.50 6.75 o 4 5 2 282.64 271.85 6.96 o 5 5 2 656.87 655.54 13.00 o 6 5 2 387.05 389.36 7.92 o 7 5 2 42.19 45.40 1.00 o 8 5 2 162.33 177.03 2.55 o -8 6 2 222.57 240.38 3.07 o -7 6 2 310.39 311.15 4.51 o -6 6 2 206.49 205.91 2.79 o -5 6 2 221.48 214.49 4.55 o -4 6 2 152.43 140.49 2.89 o -3 6 2 720.07 712.48 11.51 o -2 6 2 349.07 345.26 5.62 o -1 6 2 1399.45 1465.88 19.22 o 0 6 2 844.03 880.48 11.64 o 1 6 2 1396.56 1399.18 21.94 o 2 6 2 342.77 332.28 5.74 o 3 6 2 721.61 687.82 13.69 o 4 6 2 154.75 143.91 3.81 o 5 6 2 217.69 216.86 4.63 o 6 6 2 206.38 204.64 3.39 o 7 6 2 314.18 314.94 4.35 o 8 6 2 220.71 239.69 3.30 o -7 7 2 52.73 59.39 1.12 o -6 7 2 275.22 269.42 3.71 o -5 7 2 66.27 63.67 1.05 o -4 7 2 1422.27 1378.52 28.78 o -3 7 2 750.60 778.29 15.33 o -2 7 2 203.57 218.86 4.57 o -1 7 2 125.49 128.46 2.20 o 0 7 2 969.91 947.00 13.20 o 1 7 2 123.97 126.92 2.47 o 2 7 2 200.35 217.93 4.59 o 3 7 2 745.82 752.67 25.26 o 4 7 2 1420.37 1361.04 38.11 o 5 7 2 64.86 62.54 1.28 o 6 7 2 274.47 271.57 4.22 o 7 7 2 52.07 57.48 1.13 o -7 8 2 30.37 32.77 0.80 o -6 8 2 65.92 74.69 1.29 o -5 8 2 82.22 84.06 1.40 o -4 8 2 573.13 538.91 6.29 o -3 8 2 12.97 12.74 0.77 o -2 8 2 130.47 129.36 2.91 o -1 8 2 122.11 131.59 2.60 o 0 8 2 223.83 251.43 4.89 o 1 8 2 122.84 131.25 3.23 o 2 8 2 130.81 131.75 3.32 o 3 8 2 14.32 12.35 0.91 o 4 8 2 575.23 548.37 9.13 o 5 8 2 82.72 88.47 1.90 o 6 8 2 67.19 75.85 1.40 o 7 8 2 31.14 34.49 0.74 o -6 9 2 9.24 9.66 0.48 o -5 9 2 7.37 8.38 0.49 o -4 9 2 64.55 57.01 1.02 o -3 9 2 328.49 314.88 3.86 o -2 9 2 131.10 129.75 1.88 o -1 9 2 549.74 550.96 8.74 o 0 9 2 17.04 18.71 0.88 o 1 9 2 549.78 540.10 15.55 o 2 9 2 130.63 126.31 2.77 o 3 9 2 327.61 317.99 4.03 o 4 9 2 64.55 57.49 1.20 o 5 9 2 7.63 8.19 0.69 o 6 9 2 9.61 10.38 0.75 o -5 10 2 9.10 10.60 0.82 o -4 10 2 111.21 112.34 1.70 o -3 10 2 1.07 1.85 0.33 o -2 10 2 79.35 96.37 1.65 o -1 10 2 138.24 135.22 2.10 o 0 10 2 9.27 11.90 0.55 o 1 10 2 138.13 140.15 3.29 o 2 10 2 80.91 101.40 1.79 o 3 10 2 0.91 2.03 0.43 o 4 10 2 111.01 111.56 1.84 o 5 10 2 9.68 11.76 0.66 o -3 11 2 70.57 75.09 1.18 o -2 11 2 7.21 7.12 0.38 o -1 11 2 8.89 8.81 0.57 o 0 11 2 14.15 12.48 0.55 o 1 11 2 8.81 8.55 0.48 o 2 11 2 6.71 7.13 0.55 o 3 11 2 70.52 75.23 1.30 o 1 0 3 1304.59 1147.25 21.79 o 2 0 3 1.66 0.80 0.18 o 3 0 3 96.98 82.77 1.84 o 4 0 3 1753.49 1752.15 21.68 o 5 0 3 208.03 197.71 2.61 o 6 0 3 187.86 180.69 3.29 o 7 0 3 248.87 230.02 4.41 o 8 0 3 17.67 14.51 0.55 o 9 0 3 0.06 0.19 0.30 o -9 1 3 99.78 99.34 1.40 o -8 1 3 432.78 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