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Information card for entry 2018663
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| Coordinates | 2018663.cif |
|---|---|
| Structure factors | 2018663.hkl |
| Original IUCr paper | HTML |
| Chemical name | bis(<i>N</i>,<i>N</i>'-dimethylethylenediamine- κ^2^<i>N</i>,<i>N</i>')bis(perchlorato-κ<i>O</i>)copper(II)] |
|---|---|
| Formula | C8 H24 Cl2 Cu N4 O8 |
| Calculated formula | C8 H24 Cl2 Cu N4 O8 |
| Title of publication | The weakly coordinating perchlorate group in bis(<i>N</i>,<i>N</i>'-dimethylethylenediamine-κ^2^<i>N</i>,<i>N</i>')bis(perchlorato-κ<i>O</i>)copper(II) studied at 100, 250 and 400K |
| Authors of publication | Schnitzler, Silvia; Şerb, Mihaela-Diana; Englert, Ulli |
| Journal of publication | Acta Crystallographica Section C |
| Year of publication | 2012 |
| Journal volume | 68 |
| Journal issue | 9 |
| Pages of publication | m251 - m254 |
| a | 8.731 ± 0.003 Å |
| b | 13.824 ± 0.005 Å |
| c | 15.314 ± 0.006 Å |
| α | 90° |
| β | 94.866 ± 0.009° |
| γ | 90° |
| Cell volume | 1841.7 ± 1.2 Å3 |
| Cell temperature | 400 ± 2 K |
| Ambient diffraction temperature | 400 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 9 |
| Hermann-Mauguin space group symbol | C 1 c 1 |
| Hall space group symbol | C -2yc |
| Residual factor for all reflections | 0.125 |
| Residual factor for significantly intense reflections | 0.0753 |
| Weighted residual factors for significantly intense reflections | 0.1765 |
| Weighted residual factors for all reflections included in the refinement | 0.2065 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.012 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 180855 (current) | 2016-04-02 | cif/2/01/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/01/86. |
2018663.cif 2018663.hkl |
| 176760 | 2016-02-20 | cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/01. |
2018663.cif 2018663.hkl |
| 125873 | 2014-10-25 | cod/ (saulius@koala.ibt.lt) Adding DOIs to 1887 Acta Cryst. CIFs, their DOIs fetched using ACCE codes. |
2018663.cif 2018663.hkl |
| 88064 | 2013-08-29 | Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet. | 2018663.cif 2018663.hkl |
| 74188 | 2013-02-22 | hkl/ Adding the rest of the Fobs data for the structures publishe din the IUCr journals in 2012 and in January of 2013. |
2018663.cif 2018663.hkl |
| 70212 | 2012-12-21 | cif/ Adding structures of 2018661, 2018662, 2018663 via cif-deposit CGI script. |
2018663.cif |
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