#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/86/2018666.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018666_Fobs loop_ _publ_author_name 'Zhang, Zhenfeng' 'Xian, Dong' 'Glidewell, Christopher' _publ_section_title ; 4,6-Diaminopyrimidine-2(1H)-thione hemihydrate: a three-dimensional hydrogen-bonded framework ; _journal_coeditor_code SK3446 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o377 _journal_page_last o380 _journal_volume 68 _journal_year 2012 _space_group_IT_number 64 _symmetry_space_group_name_Hall '-C 2ac 2' _symmetry_space_group_name_H-M 'C m c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.7274 _cell_length_b 13.2590 _cell_length_c 19.9820 _exptl_crystal_F_000 1264.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file sk3446Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' zf3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 272.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' 'x, -y, -z' '-x, y+1/2, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1, z+1/2' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1, -z+1/2' '-x, -y, -z' 'x, y-1/2, -z-1/2' '-x, y, z' 'x, -y-1/2, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, y, -z-1/2' '-x+1/2, y+1/2, z' 'x+1/2, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11197.29 11881.66 862.97 o 4 0 0 44319.87 40826.86 2913.25 o 6 0 0 2884.89 2890.22 304.83 o 8 0 0 63048.22 60668.35 6538.17 o 10 0 0 3494.27 3975.85 380.13 o 12 0 0 1164.94 1364.68 176.45 o 0 2 0 41726.05 49243.50 3453.77 o 2 2 0 37159.20 37027.16 3359.23 o 4 2 0 6477.29 7499.77 310.12 o 6 2 0 5845.28 6023.45 481.46 o 8 2 0 2962.33 3016.84 177.90 o 10 2 0 2030.27 2387.11 223.84 o 12 2 0 29.52 53.03 40.28 o 0 4 0 57294.21 59474.39 2583.90 o 2 4 0 20696.01 20800.65 1179.35 o 4 4 0 988.23 1122.13 124.59 o 6 4 0 3500.71 3513.57 158.61 o 8 4 0 2286.25 2000.49 141.02 o 10 4 0 415.06 384.02 240.80 o 12 4 0 2.19 -55.44 114.74 o 0 6 0 46998.31 49401.55 2387.73 o 2 6 0 2855.34 2389.62 105.71 o 4 6 0 41509.09 45319.62 1306.28 o 6 6 0 1877.04 1911.79 135.56 o 8 6 0 5923.88 5090.79 949.19 o 10 6 0 543.57 742.08 651.77 o 0 8 0 15951.54 15501.98 620.87 o 2 8 0 2973.89 2731.93 126.46 o 4 8 0 3070.93 3287.59 150.11 o 6 8 0 1908.95 1940.00 351.00 o 8 8 0 2299.41 2243.00 349.77 o 10 8 0 605.08 542.14 388.13 o 0 10 0 5645.42 5216.44 262.30 o 2 10 0 1.30 7.24 46.65 o 4 10 0 1446.72 1553.36 162.07 o 6 10 0 1.02 -42.47 61.62 o 8 10 0 942.39 964.32 134.50 o 10 10 0 30.62 69.37 166.33 o 0 12 0 976.34 959.27 151.43 o 2 12 0 53.78 66.78 46.97 o 4 12 0 1419.04 1402.52 115.28 o 6 12 0 1.00 30.76 130.06 o 8 12 0 201.62 310.40 101.58 o 0 14 0 725.99 856.43 151.39 o 2 14 0 1315.47 1369.46 131.11 o 4 14 0 1294.15 1378.68 175.54 o 6 14 0 665.54 690.68 184.13 o 0 16 0 414.60 265.81 113.21 o 2 16 0 1.70 53.96 64.71 o 4 16 0 18.24 45.00 60.48 o 1 1 1 1307.09 1282.95 37.01 o 3 1 1 395.31 369.82 38.71 o 5 1 1 157.49 160.89 22.78 o 7 1 1 1.36 6.19 20.17 o 9 1 1 43.87 90.18 34.33 o 11 1 1 30.12 52.04 42.46 o 0 2 1 6.01 2.57 12.77 o 2 2 1 2769.21 2886.02 74.33 o 4 2 1 2387.92 2160.11 69.82 o 6 2 1 1034.41 1056.11 61.68 o 8 2 1 19.93 43.15 28.57 o 10 2 1 215.69 203.80 123.93 o 12 2 1 78.17 164.87 44.18 o 1 3 1 2798.55 2765.90 70.61 o 3 3 1 6839.34 6575.73 410.06 o 5 3 1 3583.99 3229.70 105.82 o 7 3 1 1295.15 1235.77 76.70 o 9 3 1 342.65 477.14 113.02 o 11 3 1 423.81 639.90 160.87 o 0 4 1 4369.79 4378.42 134.18 o 2 4 1 1239.43 1299.97 46.11 o 4 4 1 276.50 477.75 62.84 o 6 4 1 394.51 322.74 35.06 o 8 4 1 67.68 94.91 34.14 o 10 4 1 85.74 115.01 105.69 o 12 4 1 3.51 30.38 45.57 o 1 5 1 3604.97 3765.60 88.91 o 3 5 1 2804.26 2869.67 102.08 o 5 5 1 1552.59 1474.04 118.15 o 7 5 1 33.65 5.87 33.99 o 9 5 1 307.16 252.29 84.86 o 11 5 1 135.75 283.74 147.03 o 0 6 1 6787.61 6506.00 196.54 o 2 6 1 213.62 192.38 26.02 o 4 6 1 4677.11 4470.69 119.89 o 6 6 1 196.48 191.96 43.35 o 8 6 1 927.19 1048.43 95.45 o 10 6 1 97.52 170.37 121.31 o 1 7 1 4847.99 4845.52 113.38 o 3 7 1 0.91 -6.60 23.10 o 5 7 1 89.36 108.23 42.35 o 7 7 1 1357.62 1232.47 293.35 o 9 7 1 534.15 568.56 208.11 o 11 7 1 52.78 83.08 98.11 o 0 8 1 963.43 1090.60 69.86 o 2 8 1 154.34 151.38 30.94 o 4 8 1 2600.57 2680.10 94.82 o 6 8 1 281.32 278.04 56.73 o 8 8 1 146.51 118.40 64.45 o 10 8 1 6.28 60.40 112.27 o 1 9 1 143.86 164.18 28.74 o 3 9 1 120.72 90.21 34.95 o 5 9 1 61.08 36.43 33.71 o 7 9 1 45.52 50.50 45.41 o 9 9 1 46.19 173.30 105.33 o 0 10 1 345.72 339.61 53.66 o 2 10 1 284.72 312.27 43.02 o 4 10 1 4728.99 4667.39 138.82 o 6 10 1 12.95 67.30 67.15 o 8 10 1 72.80 119.07 88.45 o 10 10 1 100.19 143.59 103.89 o 1 11 1 585.42 582.71 52.70 o 3 11 1 12.96 2.70 33.95 o 5 11 1 55.76 18.86 43.47 o 7 11 1 423.19 647.61 173.24 o 9 11 1 57.00 63.24 58.29 o 0 12 1 7019.91 6482.23 277.40 o 2 12 1 1014.92 939.71 64.61 o 4 12 1 1988.63 2025.75 92.35 o 6 12 1 437.03 463.02 60.98 o 8 12 1 1698.29 2111.85 533.90 o 1 13 1 73.28 47.15 41.90 o 3 13 1 380.00 446.45 52.30 o 5 13 1 221.19 193.55 63.58 o 7 13 1 69.47 119.63 67.06 o 0 14 1 211.09 258.29 80.05 o 2 14 1 84.72 67.07 41.49 o 4 14 1 211.48 232.46 46.56 o 6 14 1 29.19 71.12 47.60 o 1 15 1 1.04 35.45 45.31 o 3 15 1 149.15 192.31 48.51 o 5 15 1 105.76 143.18 46.24 o 0 16 1 322.59 208.18 72.48 o 2 16 1 25.64 0.40 40.64 o 4 16 1 512.36 437.50 64.82 o 1 17 1 834.59 811.79 81.67 o 2 0 2 1794.84 1570.22 230.01 o 4 0 2 6250.63 6078.42 559.63 o 6 0 2 954.67 1341.82 148.03 o 8 0 2 55.31 77.41 29.85 o 10 0 2 105.80 155.44 69.41 o 12 0 2 265.03 358.50 70.61 o 1 1 2 2111.90 1918.45 52.84 o 3 1 2 10887.33 10852.39 311.05 o 5 1 2 6212.27 6032.73 211.99 o 7 1 2 112.90 137.75 29.89 o 9 1 2 70.13 150.87 54.23 o 11 1 2 525.53 724.02 83.27 o 0 2 2 867.03 837.78 44.25 o 2 2 2 11199.86 10772.71 226.79 o 4 2 2 2378.66 2109.80 108.50 o 6 2 2 3046.61 3062.66 101.27 o 8 2 2 252.24 240.93 38.49 o 10 2 2 563.67 650.58 158.90 o 12 2 2 135.61 169.07 50.71 o 1 3 2 6067.33 5855.90 165.43 o 3 3 2 17158.02 18417.84 406.37 o 5 3 2 12110.13 11957.84 525.49 o 7 3 2 103.72 121.09 28.73 o 9 3 2 295.94 352.92 94.15 o 11 3 2 428.54 613.32 281.48 o 0 4 2 38566.41 40395.86 1351.82 o 2 4 2 6097.77 6609.64 148.92 o 4 4 2 4582.59 4679.02 261.26 o 6 4 2 1584.02 1663.09 70.91 o 8 4 2 3120.46 3179.23 134.71 o 10 4 2 605.14 723.63 262.74 o 12 4 2 164.77 116.13 165.72 o 1 5 2 12338.61 12612.44 246.47 o 3 5 2 395.65 333.95 28.66 o 5 5 2 226.50 267.70 39.14 o 7 5 2 2014.19 1955.11 142.19 o 9 5 2 950.89 1113.77 220.09 o 11 5 2 161.82 268.67 168.61 o 0 6 2 12603.73 13195.22 368.04 o 2 6 2 127.67 96.50 26.31 o 4 6 2 509.41 474.18 41.70 o 6 6 2 26.76 15.53 41.40 o 8 6 2 1914.22 1840.99 156.03 o 10 6 2 59.58 174.78 132.77 o 1 7 2 297.72 360.50 28.90 o 3 7 2 373.63 289.06 33.01 o 5 7 2 42.40 11.02 32.94 o 7 7 2 12.16 -16.56 34.86 o 9 7 2 69.78 91.16 127.44 o 11 7 2 21.83 -12.75 120.67 o 0 8 2 470.77 542.00 51.54 o 2 8 2 1697.92 1495.02 65.97 o 4 8 2 298.40 370.12 41.79 o 6 8 2 744.42 872.60 79.29 o 8 8 2 29.98 30.75 104.97 o 10 8 2 161.33 289.78 139.45 o 1 9 2 3252.47 2981.49 89.26 o 3 9 2 8287.20 8039.05 212.06 o 5 9 2 7453.37 7163.54 209.00 o 7 9 2 1191.72 1257.79 239.28 o 9 9 2 531.39 768.38 311.11 o 0 10 2 243.49 254.27 48.20 o 2 10 2 2181.20 2052.17 83.66 o 4 10 2 1329.49 1424.67 92.65 o 6 10 2 1107.11 1140.21 125.84 o 8 10 2 54.05 94.45 114.72 o 10 10 2 247.79 186.13 111.93 o 1 11 2 20.28 -6.21 37.00 o 3 11 2 212.31 244.65 42.41 o 5 11 2 236.29 164.70 39.06 o 7 11 2 9.03 63.25 111.10 o 9 11 2 5.28 84.60 95.85 o 0 12 2 2463.21 2314.94 154.73 o 2 12 2 0.51 -11.81 31.31 o 4 12 2 1670.06 1714.01 89.87 o 6 12 2 0.04 26.95 68.60 o 8 12 2 547.84 631.61 181.01 o 1 13 2 1.10 41.70 38.60 o 3 13 2 191.09 193.64 42.16 o 5 13 2 284.28 316.29 68.41 o 7 13 2 0.81 -44.20 82.13 o 0 14 2 12.53 43.71 57.69 o 2 14 2 11.69 -13.18 37.26 o 4 14 2 200.09 216.33 55.65 o 6 14 2 5.43 61.68 47.42 o 1 15 2 2925.05 2702.16 121.80 o 3 15 2 1881.51 1773.52 107.88 o 5 15 2 1644.08 1516.08 94.50 o 0 16 2 177.57 190.60 73.45 o 2 16 2 172.44 211.77 55.58 o 4 16 2 1.43 83.81 47.16 o 1 17 2 164.39 151.74 53.63 o 1 1 3 13259.27 13326.52 372.12 o 3 1 3 7640.22 7546.51 186.29 o 5 1 3 4545.63 4725.17 155.93 o 7 1 3 88.92 130.89 28.49 o 9 1 3 692.17 688.88 70.14 o 11 1 3 376.58 577.08 70.36 o 0 2 3 15803.45 15382.01 410.57 o 2 2 3 25057.19 24923.59 646.63 o 4 2 3 93.80 156.68 20.79 o 6 2 3 4872.63 4827.48 162.43 o 8 2 3 1726.94 1777.26 133.29 o 10 2 3 1236.77 1420.25 227.62 o 12 2 3 25.27 142.32 87.09 o 1 3 3 37424.61 40475.48 742.21 o 3 3 3 16734.53 16118.77 358.77 o 5 3 3 10217.67 9273.63 446.25 o 7 3 3 3773.76 3523.72 117.06 o 9 3 3 3795.90 3711.31 306.73 o 11 3 3 457.98 755.83 232.38 o 0 4 3 12819.40 12836.96 349.09 o 2 4 3 394.85 406.91 23.60 o 4 4 3 31.99 19.22 18.43 o 6 4 3 241.40 254.44 33.67 o 8 4 3 676.50 657.33 127.95 o 10 4 3 1.03 69.41 97.74 o 12 4 3 8.10 44.01 192.54 o 1 5 3 2934.75 2740.71 69.53 o 3 5 3 856.32 792.46 41.41 o 5 5 3 131.73 66.06 32.47 o 7 5 3 1077.78 1227.73 131.70 o 9 5 3 399.17 443.15 111.32 o 11 5 3 71.73 207.41 170.19 o 0 6 3 1.62 -19.80 23.14 o 2 6 3 740.30 784.59 40.40 o 4 6 3 48.18 33.56 27.21 o 6 6 3 171.06 209.02 61.33 o 8 6 3 33.19 53.47 37.51 o 10 6 3 39.45 120.88 101.00 o 1 7 3 4280.91 4484.38 107.14 o 3 7 3 102.75 155.06 29.23 o 5 7 3 98.46 141.45 37.96 o 7 7 3 295.85 290.36 51.88 o 9 7 3 762.47 730.16 165.33 o 11 7 3 10.94 121.85 176.99 o 0 8 3 4.42 0.80 30.83 o 2 8 3 7244.32 6707.19 158.65 o 4 8 3 4889.42 4902.69 137.20 o 6 8 3 3778.06 3366.33 145.43 o 8 8 3 54.88 85.31 54.75 o 10 8 3 553.41 851.07 240.42 o 1 9 3 36.19 11.21 26.47 o 3 9 3 2076.55 2051.22 84.83 o 5 9 3 2045.51 2297.40 103.54 o 7 9 3 11.05 -46.21 46.21 o 9 9 3 12.57 85.28 157.49 o 0 10 3 144.75 139.47 46.35 o 2 10 3 1032.26 1049.21 65.55 o 4 10 3 4434.39 4388.34 134.19 o 6 10 3 821.78 936.05 105.48 o 8 10 3 53.50 148.47 121.57 o 10 10 3 68.54 174.52 175.38 o 1 11 3 2237.57 1945.10 92.76 o 3 11 3 113.45 99.87 36.32 o 5 11 3 1.61 47.46 34.37 o 7 11 3 564.01 798.69 165.40 o 9 11 3 524.86 522.12 221.19 o 0 12 3 969.03 821.78 96.55 o 2 12 3 735.81 755.81 59.12 o 4 12 3 7.85 57.39 34.60 o 6 12 3 226.44 195.49 91.91 o 8 12 3 259.06 305.55 128.09 o 1 13 3 466.07 467.84 58.24 o 3 13 3 644.46 645.22 59.39 o 5 13 3 673.32 652.79 63.06 o 7 13 3 92.16 237.47 145.45 o 0 14 3 41.53 -22.29 49.07 o 2 14 3 153.95 201.59 47.98 o 4 14 3 130.45 220.73 44.60 o 6 14 3 111.53 134.52 62.48 o 1 15 3 21.25 98.94 45.42 o 3 15 3 150.99 185.54 50.13 o 5 15 3 134.48 164.43 45.68 o 0 16 3 538.13 795.86 110.55 o 2 16 3 727.08 758.19 76.23 o 4 16 3 553.48 486.67 65.65 o 1 17 3 143.55 232.50 56.15 o 0 0 4 39572.17 42708.59 1590.99 o 2 0 4 43312.42 39200.49 1963.88 o 4 0 4 3985.75 4567.62 318.19 o 6 0 4 5479.20 5378.24 340.35 o 8 0 4 3767.28 3767.74 251.75 o 10 0 4 1961.82 2012.89 106.84 o 12 0 4 2.67 -16.26 57.53 o 1 1 4 1422.97 1422.57 112.70 o 3 1 4 2090.36 2006.23 63.14 o 5 1 4 1335.01 1525.73 60.97 o 7 1 4 70.56 65.82 25.10 o 9 1 4 112.82 129.19 29.40 o 11 1 4 17.08 96.50 78.50 o 0 2 4 12667.99 12721.39 336.28 o 2 2 4 231.59 286.76 20.30 o 4 2 4 5169.97 4998.11 167.41 o 6 2 4 35.06 11.64 19.36 o 8 2 4 334.23 324.57 42.70 o 10 2 4 53.38 26.38 36.03 o 12 2 4 198.74 230.27 168.20 o 1 3 4 3801.82 3943.35 85.27 o 3 3 4 123.32 156.45 18.55 o 5 3 4 72.65 109.44 22.96 o 7 3 4 256.23 299.94 37.36 o 9 3 4 226.15 139.92 52.81 o 11 3 4 0.05 211.03 229.55 o 0 4 4 13750.28 14482.65 498.13 o 2 4 4 13977.21 14138.90 286.83 o 4 4 4 12.51 46.25 18.87 o 6 4 4 3765.99 3511.95 115.09 o 8 4 4 81.38 39.14 37.73 o 10 4 4 511.11 628.53 82.70 o 12 4 4 44.48 132.20 279.80 o 1 5 4 7466.52 8167.08 198.81 o 3 5 4 1037.19 1019.00 48.82 o 5 5 4 736.74 713.62 50.77 o 7 5 4 1182.46 1281.20 82.80 o 9 5 4 952.10 1064.41 183.60 o 11 5 4 75.10 238.37 275.20 o 0 6 4 1976.29 2140.92 90.27 o 2 6 4 1332.69 1278.00 48.68 o 4 6 4 433.73 476.30 42.81 o 6 6 4 488.56 477.18 54.85 o 8 6 4 419.37 304.51 49.95 o 10 6 4 90.11 280.99 144.11 o 1 7 4 4.38 -5.28 19.39 o 3 7 4 916.71 918.51 52.31 o 5 7 4 483.22 530.93 51.15 o 7 7 4 85.44 102.86 41.60 o 9 7 4 0.19 -4.92 39.12 o 11 7 4 84.71 219.99 221.70 o 0 8 4 7139.70 6722.10 214.03 o 2 8 4 2998.81 2796.04 82.39 o 4 8 4 750.58 820.41 54.96 o 6 8 4 1194.75 1043.70 134.33 o 8 8 4 716.81 678.78 141.31 o 10 8 4 156.39 266.88 248.84 o 1 9 4 65.66 99.13 30.62 o 3 9 4 1433.11 1341.96 91.65 o 5 9 4 1469.93 1455.58 90.69 o 7 9 4 6.68 -41.58 41.58 o 9 9 4 10.10 194.64 185.89 o 0 10 4 3428.18 3558.85 146.24 o 2 10 4 4394.58 4338.02 131.30 o 4 10 4 22.59 14.06 34.21 o 6 10 4 1589.48 1822.55 170.49 o 8 10 4 1040.39 1069.11 199.95 o 10 10 4 568.19 881.94 265.22 o 1 11 4 317.89 357.97 47.91 o 3 11 4 1242.48 1149.96 71.39 o 5 11 4 960.84 967.51 78.10 o 7 11 4 147.04 189.19 124.83 o 9 11 4 40.25 131.29 269.56 o 0 12 4 0.23 38.24 49.68 o 2 12 4 1193.88 1105.99 71.43 o 4 12 4 312.08 223.61 45.31 o 6 12 4 567.18 629.74 83.65 o 8 12 4 4.79 171.75 138.39 o 1 13 4 417.99 432.39 62.47 o 3 13 4 434.34 499.53 54.04 o 5 13 4 256.64 358.96 82.55 o 7 13 4 247.77 351.76 121.59 o 0 14 4 0.95 87.47 63.56 o 2 14 4 871.74 881.89 76.65 o 4 14 4 262.55 242.85 47.25 o 6 14 4 370.41 484.51 111.14 o 1 15 4 88.21 68.52 41.31 o 3 15 4 261.72 166.86 49.52 o 5 15 4 311.81 345.21 54.73 o 0 16 4 134.30 93.02 64.02 o 2 16 4 76.42 157.82 51.13 o 4 16 4 55.35 24.60 43.77 o 1 1 5 22167.06 22654.97 619.63 o 3 1 5 20166.33 20614.70 605.62 o 5 1 5 11946.40 11599.24 410.58 o 7 1 5 3649.84 3986.72 152.72 o 9 1 5 2148.50 2492.38 91.84 o 11 1 5 938.20 1049.57 138.53 o 0 2 5 74246.37 69123.87 2804.19 o 2 2 5 18070.50 16527.71 480.83 o 4 2 5 2669.45 2558.99 143.66 o 6 2 5 4476.43 4583.62 349.15 o 8 2 5 3149.01 2946.00 152.36 o 10 2 5 329.05 399.98 56.92 o 12 2 5 122.29 251.98 170.13 o 1 3 5 68.95 57.00 17.23 o 3 3 5 111.88 114.01 17.49 o 5 3 5 2.48 -17.70 17.70 o 7 3 5 37.15 25.12 27.09 o 9 3 5 8.17 -34.75 34.75 o 11 3 5 23.06 155.81 178.37 o 0 4 5 1848.34 1989.21 75.29 o 2 4 5 2625.18 2811.57 79.58 o 4 4 5 12749.27 13139.86 296.33 o 6 4 5 432.04 425.99 40.07 o 8 4 5 106.06 11.92 46.30 o 10 4 5 165.60 158.79 106.14 o 12 4 5 431.58 684.76 423.66 o 1 5 5 3637.05 3389.61 82.86 o 3 5 5 717.13 709.16 38.62 o 5 5 5 318.63 301.31 39.06 o 7 5 5 919.11 879.21 150.55 o 9 5 5 403.29 380.12 56.32 o 11 5 5 137.13 263.70 351.93 o 0 6 5 1046.91 1046.54 62.10 o 2 6 5 754.62 683.71 36.40 o 4 6 5 250.87 279.64 33.75 o 6 6 5 102.88 75.46 37.66 o 8 6 5 14.55 17.33 36.40 o 10 6 5 24.72 -20.00 73.84 o 1 7 5 28094.66 26900.75 519.85 o 3 7 5 7274.51 7184.49 165.90 o 5 7 5 5548.61 5330.22 264.88 o 7 7 5 5539.54 5284.33 324.55 o 9 7 5 4539.11 4718.44 309.77 o 11 7 5 676.57 491.61 171.08 o 0 8 5 1638.34 1824.03 95.23 o 2 8 5 3764.49 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303.37 278.98 o 2 0 24 26.64 177.90 197.98 o 4 0 24 878.74 507.86 229.59 o 1 1 24 9.85 188.25 135.87 o 3 1 24 71.06 203.05 147.92 o 0 2 24 2.59 67.04 181.90 o 2 2 24 36.78 86.24 140.46 o 4 2 24 25.95 280.97 153.63 o 1 3 24 24.74 114.99 138.10 o 3 3 24 23.88 270.36 145.18 o 0 4 24 54.78 58.90 165.70 o 2 4 24 153.92 266.35 150.35 o 1 5 24 336.62 275.82 131.98 o 3 5 24 349.89 498.06 161.09 o 0 6 24 92.40 381.01 194.03 o 1 1 25 657.91 571.03 155.68 o 3 1 25 415.56 402.25 164.37 o 0 2 25 124.39 337.73 209.23 o 2 2 25 85.25 268.49 152.31 o 1 3 25 922.38 739.89 196.09 o 0 4 25 112.37 107.72 170.63 o