#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:22:23 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180856 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/87/2018713.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018713_Fobs loop_ _publ_author_name 'Szafranowska, Barbara' '\'Slepokura, Katarzyna' 'Lis, Tadeusz' _publ_section_title ; Potassium salts of hypodiphosphoric acid ; _journal_coeditor_code FN3115 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i71 _journal_page_last i82 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.820 _cell_angle_gamma 90.000 _cell_length_a 9.7430 _cell_length_b 15.7250 _cell_length_c 14.4180 _exptl_crystal_F_000 1408.00 _reflns_d_resolution_high 0.5692 _cod_data_source_file fn3115Vsup6.hkl _cod_data_source_block V #BEGIN Tags that were not found in dictionaries: _shelx_title ' szafr32 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 591.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 109999.33 100985.42 1341.28 o 4 0 0 74974.66 68551.91 443.34 o 5 0 0 7401.49 6902.12 160.25 o 6 0 0 51955.67 50718.37 467.24 o 7 0 0 1572.10 1479.91 125.30 o 8 0 0 2160.69 2205.56 161.22 o 9 0 0 8728.23 8419.91 173.67 o 10 0 0 3450.08 3443.05 298.36 o 11 0 0 1735.11 1738.86 201.16 o 12 0 0 4249.38 4293.80 253.95 o 13 0 0 4033.78 4496.93 191.38 o 14 0 0 487.45 703.03 214.32 o 15 0 0 406.36 441.37 198.90 o 16 0 0 1047.41 1238.33 252.80 o 2 1 0 4.35 30.73 28.36 o 3 1 0 287.36 311.06 26.27 o 4 1 0 17.14 18.52 17.99 o 5 1 0 0.42 14.34 34.85 o 6 1 0 288.79 323.77 60.80 o 7 1 0 17.71 26.43 53.57 o 8 1 0 120.15 131.72 74.57 o 9 1 0 190.38 146.15 69.39 o 10 1 0 4.15 33.53 79.67 o 11 1 0 44.44 41.05 103.62 o 12 1 0 180.36 153.27 126.86 o 13 1 0 40.23 68.51 100.48 o 14 1 0 70.58 216.48 128.35 o 15 1 0 22.46 86.38 133.60 o 16 1 0 67.14 16.65 138.79 o 2 2 0 37468.90 39001.25 214.78 o 3 2 0 48856.35 46457.10 564.77 o 4 2 0 58385.64 58836.00 212.61 o 5 2 0 953.91 1009.53 17.20 o 6 2 0 1568.62 1546.44 20.78 o 7 2 0 1397.79 1305.86 75.03 o 8 2 0 27422.43 26490.87 303.18 o 9 2 0 6188.13 6175.90 128.88 o 10 2 0 1194.57 1085.33 109.69 o 11 2 0 5003.55 4808.98 143.28 o 12 2 0 697.18 703.64 105.85 o 13 2 0 57.17 127.19 95.35 o 14 2 0 1002.09 862.60 116.27 o 15 2 0 89.22 97.97 128.64 o 16 2 0 114.69 70.88 156.07 o 1 3 0 0.54 15.61 9.64 o 2 3 0 187.40 177.96 10.66 o 3 3 0 124.43 152.39 13.19 o 4 3 0 89.40 73.94 13.87 o 5 3 0 143.82 142.01 16.51 o 6 3 0 152.12 139.23 17.73 o 7 3 0 271.99 249.31 18.76 o 8 3 0 384.75 406.86 81.55 o 9 3 0 0.39 45.75 76.55 o 10 3 0 237.32 207.61 96.21 o 11 3 0 142.91 48.37 97.02 o 12 3 0 6.86 34.26 87.40 o 13 3 0 164.06 178.00 91.16 o 14 3 0 16.89 68.95 101.84 o 15 3 0 47.86 95.96 127.95 o 16 3 0 15.20 0.44 142.96 o 0 4 0 1906.62 2843.52 90.24 o 1 4 0 16316.25 16558.53 63.56 o 2 4 0 679.43 604.52 12.25 o 3 4 0 1221.07 1530.94 29.49 o 4 4 0 5812.14 5968.68 44.27 o 5 4 0 46532.12 49526.27 317.93 o 6 4 0 1992.43 2027.46 29.42 o 7 4 0 13546.93 13474.92 164.29 o 8 4 0 2845.23 2807.67 101.45 o 9 4 0 662.14 620.90 105.72 o 10 4 0 2173.50 2241.50 139.67 o 11 4 0 3668.70 3623.26 105.21 o 12 4 0 732.25 609.98 92.37 o 13 4 0 3812.13 3668.87 140.72 o 14 4 0 187.18 156.20 120.72 o 15 4 0 1812.33 1733.48 169.54 o 16 4 0 1019.38 1116.02 186.21 o 1 5 0 66.48 106.30 12.91 o 2 5 0 325.13 341.35 13.95 o 3 5 0 7.63 16.03 11.10 o 4 5 0 1.86 28.55 17.92 o 5 5 0 14.81 25.98 17.93 o 6 5 0 339.02 335.85 26.95 o 7 5 0 195.89 199.50 24.06 o 8 5 0 1.69 10.08 34.92 o 9 5 0 97.40 100.45 56.31 o 10 5 0 17.08 19.27 60.35 o 11 5 0 7.32 31.90 69.62 o 12 5 0 29.33 68.66 84.18 o 13 5 0 94.77 76.30 111.10 o 14 5 0 71.39 54.88 107.51 o 15 5 0 270.80 341.57 139.93 o 16 5 0 171.64 209.72 159.78 o 0 6 0 21805.99 24040.78 286.90 o 1 6 0 53758.68 56536.98 315.44 o 2 6 0 29613.80 30559.26 248.79 o 3 6 0 16719.16 17709.70 93.40 o 4 6 0 21.06 42.67 17.77 o 5 6 0 3728.23 3642.60 40.14 o 6 6 0 1552.34 1637.82 34.31 o 7 6 0 1968.81 1909.85 34.18 o 8 6 0 4762.59 4611.52 77.01 o 9 6 0 2276.10 2289.47 88.70 o 10 6 0 4257.29 4323.29 109.15 o 11 6 0 1367.68 1472.67 105.34 o 12 6 0 3854.04 3576.43 188.92 o 13 6 0 3229.04 3183.99 169.14 o 14 6 0 399.19 502.02 123.73 o 15 6 0 5334.34 5391.71 252.44 o 16 6 0 805.47 832.95 178.23 o 1 7 0 22.66 33.50 10.15 o 2 7 0 18.65 30.10 12.41 o 3 7 0 323.35 340.84 19.37 o 4 7 0 18.97 31.13 16.67 o 5 7 0 12.22 34.90 19.51 o 6 7 0 0.05 14.04 20.73 o 7 7 0 1.67 18.56 21.80 o 8 7 0 162.83 185.08 37.22 o 9 7 0 29.58 19.96 52.27 o 10 7 0 406.65 423.96 82.42 o 11 7 0 104.26 109.55 77.42 o 12 7 0 158.85 187.61 103.20 o 13 7 0 79.79 203.01 140.43 o 14 7 0 0.49 62.12 115.25 o 15 7 0 331.46 402.99 160.14 o 16 7 0 83.84 59.15 134.36 o 0 8 0 575.13 565.25 40.19 o 1 8 0 6723.12 6691.09 37.67 o 2 8 0 6748.69 6482.06 55.54 o 3 8 0 23.85 30.03 15.58 o 4 8 0 11.76 30.84 19.03 o 5 8 0 7801.92 7578.29 56.76 o 6 8 0 183.71 175.14 27.67 o 7 8 0 4499.65 4447.82 48.79 o 8 8 0 3371.74 3323.16 57.05 o 9 8 0 1656.69 1697.66 88.69 o 10 8 0 6089.07 5823.39 111.91 o 11 8 0 2771.80 2792.61 120.72 o 12 8 0 1442.78 1468.39 151.51 o 13 8 0 1259.79 1133.13 198.24 o 14 8 0 255.44 208.41 127.18 o 15 8 0 2307.98 2383.26 171.72 o 16 8 0 668.30 688.61 204.75 o 1 9 0 8.57 18.82 12.76 o 2 9 0 1.07 14.59 14.26 o 3 9 0 1.53 12.61 16.11 o 4 9 0 81.90 83.16 21.89 o 5 9 0 49.96 55.45 23.96 o 6 9 0 149.25 104.81 25.06 o 7 9 0 410.11 395.52 35.54 o 8 9 0 104.18 96.52 39.56 o 9 9 0 28.84 55.09 63.96 o 10 9 0 31.80 46.94 69.48 o 11 9 0 93.49 114.88 94.70 o 12 9 0 188.55 202.89 127.47 o 13 9 0 9.50 64.73 152.03 o 14 9 0 30.57 83.64 120.40 o 15 9 0 37.88 20.89 113.22 o 16 9 0 1.33 -11.37 186.44 o 0 10 0 42524.48 44260.91 244.29 o 1 10 0 11622.04 11972.98 112.48 o 2 10 0 1813.26 2093.26 43.33 o 3 10 0 4492.93 4298.49 59.22 o 4 10 0 15.32 29.59 20.89 o 5 10 0 714.85 701.21 30.87 o 6 10 0 232.05 204.45 30.75 o 7 10 0 8825.75 8736.69 70.39 o 8 10 0 0.54 22.71 42.45 o 9 10 0 560.72 546.95 67.30 o 10 10 0 5346.37 4867.06 196.86 o 11 10 0 61.76 79.72 84.95 o 12 10 0 13.60 10.09 122.54 o 13 10 0 1027.05 940.88 179.89 o 14 10 0 37.01 19.89 122.11 o 15 10 0 163.52 134.25 132.64 o 1 11 0 170.36 199.14 37.60 o 2 11 0 353.98 317.69 20.56 o 3 11 0 135.84 146.35 23.20 o 4 11 0 365.26 345.22 27.23 o 5 11 0 154.85 121.66 26.72 o 6 11 0 75.60 85.92 30.15 o 7 11 0 8.48 11.23 29.62 o 8 11 0 679.16 650.31 60.63 o 9 11 0 61.45 79.65 86.04 o 10 11 0 7.84 38.88 95.39 o 11 11 0 25.91 19.10 104.31 o 12 11 0 33.72 87.08 141.19 o 13 11 0 43.13 -15.34 146.40 o 14 11 0 72.85 138.23 170.92 o 15 11 0 2.79 44.71 175.21 o 0 12 0 2207.13 2552.88 76.61 o 1 12 0 197.89 208.49 37.37 o 2 12 0 11289.38 11078.04 97.93 o 3 12 0 9261.30 9503.15 92.08 o 4 12 0 15390.82 15049.77 186.03 o 5 12 0 136.99 159.41 31.42 o 6 12 0 21.65 56.23 31.88 o 7 12 0 363.71 323.31 40.57 o 8 12 0 10136.31 10324.49 245.77 o 9 12 0 530.47 476.56 107.30 o 10 12 0 328.79 281.03 94.37 o 11 12 0 1545.80 1185.45 349.20 o 14 12 0 6.60 43.55 173.54 o 15 12 0 43.51 43.06 199.15 o 1 13 0 30.68 53.96 39.84 o 2 13 0 130.78 116.20 40.07 o 3 13 0 49.97 76.85 37.76 o 4 13 0 373.64 372.95 51.30 o 5 13 0 131.93 130.00 45.58 o 6 13 0 17.99 34.51 46.17 o 7 13 0 21.39 7.98 57.12 o 8 13 0 49.21 56.16 85.16 o 9 13 0 40.93 173.44 270.90 o 10 13 0 366.85 320.79 282.33 o 13 13 0 11.30 5.32 150.71 o 14 13 0 16.60 141.80 185.02 o 0 14 0 46620.39 48676.30 309.52 o 1 14 0 1278.29 1233.92 55.05 o 2 14 0 1521.56 1291.41 57.45 o 3 14 0 19378.00 19396.54 175.68 o 4 14 0 4406.48 4253.04 89.89 o 5 14 0 8093.46 8237.57 114.26 o 6 14 0 16848.54 17281.01 161.02 o 7 14 0 816.83 807.52 83.91 o 8 14 0 536.92 514.49 108.56 o 9 14 0 1265.84 1507.58 403.30 o 10 14 0 3927.45 3517.01 426.36 o 13 14 0 230.73 187.14 182.28 o 1 15 0 11.08 16.75 46.42 o 2 15 0 41.07 56.55 43.14 o 3 15 0 28.45 41.28 50.39 o 4 15 0 250.49 218.23 60.64 o 5 15 0 78.57 93.02 55.47 o 6 15 0 15.58 10.72 52.73 o 7 15 0 669.72 725.78 79.49 o 8 15 0 287.39 272.78 103.28 o 9 15 0 112.58 8.08 305.73 o 0 16 0 86.91 112.61 66.12 o 1 16 0 1000.91 1011.08 62.63 o 2 16 0 3105.49 2923.95 173.32 o 3 16 0 17511.21 17829.68 170.45 o 4 16 0 2264.76 2027.70 78.06 o 5 16 0 937.55 948.60 91.03 o 6 16 0 714.09 665.96 81.51 o 7 16 0 387.00 435.95 78.68 o 8 16 0 4516.58 4010.57 291.69 o 9 16 0 3475.90 3664.38 404.00 o 1 17 0 3.57 41.01 60.00 o 2 17 0 3.99 34.58 55.58 o 3 17 0 160.79 184.67 69.58 o 4 17 0 225.13 241.99 74.75 o 5 17 0 652.11 577.34 76.31 o 6 17 0 6.39 3.97 68.87 o 7 17 0 4.49 20.88 69.86 o 8 17 0 32.91 56.26 113.01 o 0 18 0 430.83 365.63 116.38 o 1 18 0 8608.40 8722.21 177.53 o 2 18 0 895.97 924.02 86.31 o 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259.91 341.66 122.49 o 4 22 0 10.65 62.66 121.72 o 5 22 0 1913.31 1893.72 150.92 o 6 22 0 523.89 504.19 136.01 o 7 22 0 167.12 180.23 167.21 o 8 22 0 597.02 481.07 241.36 o 1 23 0 260.23 376.34 128.24 o 2 23 0 2.37 76.94 108.79 o 3 23 0 72.91 29.76 104.93 o 4 23 0 106.93 117.54 118.34 o 5 23 0 0.09 53.18 109.48 o 6 23 0 82.50 134.61 121.57 o 7 23 0 332.21 210.38 205.02 o 8 23 0 0.01 27.53 190.81 o 0 24 0 199.84 234.54 188.73 o 1 24 0 770.68 762.49 139.53 o 2 24 0 131.41 152.32 117.97 o 3 24 0 712.43 861.70 142.01 o 4 24 0 179.53 169.82 122.74 o 5 24 0 534.08 644.68 167.82 o 6 24 0 519.11 533.31 157.75 o 7 24 0 739.52 593.75 236.08 o 1 25 0 30.34 45.15 127.26 o 2 25 0 27.05 92.98 138.41 o 3 25 0 63.30 68.83 145.65 o 4 25 0 35.34 56.53 154.94 o 5 25 0 5.95 63.55 142.75 o 6 25 0 34.57 32.50 134.92 o 7 25 0 35.62 75.01 186.23 o 0 26 0 286.22 335.93 227.29 o 1 26 0 17.96 33.93 134.54 o 2 26 0 348.30 368.77 162.54 o 3 26 0 485.84 459.27 166.27 o 4 26 0 336.74 158.74 162.51 o 5 26 0 100.18 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541.69 556.30 109.03 o -13 2 1 488.50 422.33 85.14 o -12 2 1 655.52 685.88 102.78 o -11 2 1 847.65 956.78 91.85 o -10 2 1 36.61 68.76 78.74 o -9 2 1 2737.24 2649.88 103.80 o -8 2 1 31.05 -8.62 63.48 o -7 2 1 924.30 986.15 32.37 o -6 2 1 1986.48 2021.11 27.55 o -5 2 1 1259.33 1222.21 52.63 o -4 2 1 14323.12 15672.57 132.94 o -3 2 1 2732.02 2918.13 24.96 o -2 2 1 82.15 121.69 8.53 o 2 2 1 10.42 34.21 10.25 o 3 2 1 588.57 526.37 18.87 o 4 2 1 4612.57 4949.91 103.44 o 5 2 1 10601.94 11004.78 189.47 o 6 2 1 197.40 165.87 16.76 o 7 2 1 107.63 123.34 61.98 o 8 2 1 0.41 22.70 61.02 o 9 2 1 1115.51 1132.73 104.12 o 10 2 1 164.45 216.03 115.72 o 11 2 1 2303.65 2227.15 150.04 o 12 2 1 840.92 786.77 130.02 o 13 2 1 113.34 120.97 97.89 o 14 2 1 60.58 22.53 142.18 o 15 2 1 497.60 515.63 149.46 o 16 2 1 173.84 94.56 138.83 o -16 3 1 6.52 70.65 136.47 o -15 3 1 327.36 283.21 143.10 o -14 3 1 2838.74 3064.18 163.97 o -13 3 1 99.88 127.53 81.46 o -12 3 1 120.07 113.34 95.14 o -11 3 1 14.73 53.14 74.12 o 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