#------------------------------------------------------------------------------ #$Date: 2013-03-10 17:00:37 +0200 (Sun, 10 Mar 2013) $ #$Revision: 75609 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/87/2018777.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018777_Fobs loop_ _publ_author_name 'Altaf, Muhammad' 'Stoeckli-Evans, Helen' _publ_section_title ; Chiral one- and two-dimensional silver(I)--biotin coordination polymers ; _journal_coeditor_code EG3103 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 127 _journal_page_last 137 _journal_volume 69 _journal_year 2013 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.946 _cell_angle_gamma 90.000 _cell_length_a 15.1130 _cell_length_b 9.6028 _cell_length_c 28.6670 _exptl_crystal_F_000 2256.00 _reflns_d_resolution_high 0.8212 _[local]_cod_data_source_file eg3103IVsup5.hkl _[local]_cod_data_source_block IV #BEGIN Tags that were not found in dictionaries: _shelx_title ' A5BIO' _shelx_refln_list_code 4 _shelx_f_calc_maximum 514.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 7 -9 0 424.10 431.10 85.71 o 8 -9 0 193.41 242.88 91.03 o 3 -8 0 478.49 503.41 113.78 o 4 -8 0 4189.21 4660.65 127.61 o 5 -8 0 57.29 35.94 77.63 o 6 -8 0 530.43 504.47 114.00 o 7 -8 0 97.61 -11.27 112.51 o 8 -8 0 928.62 1223.97 122.50 o 9 -8 0 1475.08 1332.65 126.12 o 10 -8 0 1227.72 1277.35 128.67 o 11 -8 0 492.09 528.51 131.44 o 12 -8 0 81.14 83.58 131.86 o 1 -7 0 110.15 123.35 71.67 o 2 -7 0 854.15 806.69 105.91 o 3 -7 0 4442.02 4090.88 97.19 o 4 -7 0 1661.46 1546.39 82.52 o 5 -7 0 546.23 323.91 74.65 o 6 -7 0 605.34 575.51 109.53 o 7 -7 0 406.42 454.50 112.51 o 8 -7 0 325.68 353.90 77.63 o 9 -7 0 1630.93 1714.41 121.44 o 10 -7 0 2242.44 1966.86 95.49 o 11 -7 0 668.73 716.30 126.76 o 12 -7 0 32.04 103.57 129.10 o 13 -7 0 120.12 119.74 134.20 o 14 -7 0 136.23 96.13 139.94 o 0 -6 0 23155.19 24965.97 198.22 o 1 -6 0 2290.03 2638.28 111.87 o 2 -6 0 14524.36 15011.10 163.76 o 3 -6 0 1264.51 1283.94 78.05 o 4 -6 0 3768.63 4088.97 119.31 o 5 -6 0 1928.18 1961.33 85.07 o 6 -6 0 3359.91 3419.88 126.12 o 7 -6 0 132.40 130.58 75.71 o 8 -6 0 5277.73 5603.46 137.60 o 9 -6 0 2290.43 2199.53 95.49 o 10 -6 0 1922.25 2040.87 126.54 o 11 -6 0 5188.38 5775.94 147.17 o 12 -6 0 211.97 264.57 122.50 o 13 -6 0 41.52 116.76 124.20 o 14 -6 0 63.37 91.24 131.22 o 15 -6 0 139.75 201.41 139.73 o 1 -5 0 1380.53 1245.36 62.41 o 2 -5 0 65.19 230.97 99.53 o 3 -5 0 650.31 714.18 100.38 o 4 -5 0 4576.98 4675.11 121.44 o 5 -5 0 11424.96 12682.69 159.72 o 6 -5 0 3586.12 3587.90 118.89 o 7 -5 0 5875.86 5759.77 133.35 o 8 -5 0 593.30 621.24 101.66 o 9 -5 0 1129.96 1158.68 112.72 o 10 -5 0 1241.38 1178.88 114.85 o 11 -5 0 2489.98 2615.95 98.26 o 12 -5 0 4572.86 4989.45 144.62 o 13 -5 0 1051.67 1213.33 128.03 o 14 -5 0 151.77 268.40 128.25 o 15 -5 0 268.66 297.96 134.41 o 16 -5 0 436.78 407.28 174.18 o 0 -4 0 21847.40 20486.95 192.69 o 1 -4 0 669.22 667.84 59.69 o 2 -4 0 6527.80 6275.10 138.03 o 3 -4 0 429.94 574.66 77.42 o 4 -4 0 13407.93 14364.35 175.25 o 5 -4 0 2761.60 2697.41 114.00 o 6 -4 0 21714.60 21455.49 205.87 o 7 -4 0 75.20 90.60 68.06 o 8 -4 0 2216.09 2242.49 89.33 o 9 -4 0 264.52 273.93 103.57 o 10 -4 0 2686.82 2915.41 124.84 o 11 -4 0 3325.44 3744.64 132.29 o 12 -4 0 4941.79 4896.72 147.39 o 13 -4 0 3062.64 3222.51 137.60 o 14 -4 0 805.75 889.42 154.41 o 15 -4 0 47.65 155.89 128.46 o 16 -4 0 254.44 288.18 168.02 o 1 -3 0 92217.84 103355.75 1666.77 o 2 -3 0 1418.54 1572.76 113.57 o 3 -3 0 47459.52 50663.13 333.27 o 4 -3 0 22595.72 21727.72 223.53 o 5 -3 0 21003.53 21512.49 211.40 o 6 -3 0 4746.54 4599.82 115.27 o 7 -3 0 38975.27 40693.91 342.73 o 8 -3 0 173.48 288.02 68.42 o 9 -3 0 17252.81 18742.49 434.53 o 10 -3 0 1833.86 1933.85 56.46 o 11 -3 0 6305.33 6611.95 100.22 o 12 -3 0 1153.93 1244.88 93.07 o 13 -3 0 2384.14 2435.87 68.76 o 14 -3 0 48.63 55.23 59.42 o 15 -3 0 82.24 136.40 70.39 o 16 -3 0 13.70 11.92 64.50 o 17 -3 0 733.81 626.13 97.27 o 0 -2 0 68828.45 77551.09 506.81 o 1 -2 0 541.01 580.96 70.36 o 2 -2 0 68952.91 69955.68 464.70 o 3 -2 0 493.37 531.06 81.88 o 4 -2 0 16595.16 16681.63 151.43 o 5 -2 0 13493.41 14330.76 187.04 o 6 -2 0 14685.91 13746.24 287.84 o 7 -2 0 202.06 281.98 50.42 o 8 -2 0 17526.83 16287.74 222.33 o 9 -2 0 113.53 119.85 44.04 o 10 -2 0 1916.35 1969.84 51.97 o 11 -2 0 3305.10 3454.24 128.00 o 12 -2 0 10006.99 9981.09 319.36 o 13 -2 0 1115.06 1167.46 60.87 o 14 -2 0 6065.39 6453.36 109.67 o 15 -2 0 83.60 107.52 62.94 o 16 -2 0 185.72 218.97 67.76 o 17 -2 0 601.58 581.36 76.57 o 18 -2 0 1101.78 1110.17 87.30 o 1 -1 0 15999.56 16348.86 309.02 o 2 -1 0 7758.38 8555.48 106.49 o 3 -1 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9758.86 144.19 o 13 2 0 1066.73 1019.47 55.32 o 14 2 0 6023.65 5923.09 122.50 o 15 2 0 77.69 145.84 58.44 o 16 2 0 141.53 209.50 80.08 o 17 2 0 621.65 521.64 69.96 o 18 2 0 1132.56 1198.85 84.87 o 1 3 0 92401.13 109241.16 937.70 o 2 3 0 1491.47 1592.08 58.68 o 3 3 0 46948.76 52603.31 1532.32 o 4 3 0 22578.59 21987.99 305.25 o 5 3 0 20989.95 21055.36 229.26 o 6 3 0 4874.20 4719.96 77.50 o 7 3 0 39240.01 40095.34 471.10 o 8 3 0 173.93 235.23 39.81 o 9 3 0 17407.08 18157.08 188.45 o 10 3 0 1885.99 1929.70 45.26 o 11 3 0 6417.09 6559.47 78.48 o 12 3 0 1166.12 1075.24 55.37 o 13 3 0 2451.48 2335.13 54.95 o 14 3 0 47.81 69.59 45.40 o 15 3 0 50.55 135.76 61.74 o 16 3 0 27.98 41.20 61.44 o 17 3 0 748.93 669.16 72.06 o 0 4 0 22212.95 22412.34 199.07 o 1 4 0 657.53 675.99 59.71 o 2 4 0 6386.32 6085.10 89.59 o 3 4 0 413.16 459.37 42.65 o 4 4 0 13146.27 13671.53 419.35 o 5 4 0 2682.51 2601.52 42.57 o 6 4 0 21836.85 20974.66 333.39 o 7 4 0 104.57 115.30 35.44 o 8 4 0 2355.00 2287.17 50.44 o 9 4 0 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483.20 81.80 o 4 -2 32 154.16 110.49 68.19 o 5 -2 32 118.32 214.27 80.04 o 6 -2 32 195.47 166.80 86.14 o -7 -1 32 65.54 72.90 100.16 o -6 -1 32 129.93 70.88 81.24 o -5 -1 32 163.74 130.32 79.78 o -4 -1 32 309.82 234.39 95.11 o -3 -1 32 127.56 241.35 77.28 o -2 -1 32 778.12 794.24 69.45 o -1 -1 32 51.30 76.36 93.60 o 0 -1 32 59.22 80.13 92.61 o 1 -1 32 170.63 227.30 77.78 o 2 -1 32 73.92 313.24 94.96 o 3 -1 32 342.95 295.09 80.22 o 4 -1 32 266.57 236.50 83.55 o 5 -1 32 155.29 159.77 72.95 o 6 -1 32 55.11 46.94 70.09 o -7 0 32 356.52 320.13 101.71 o -6 0 32 207.38 151.12 79.87 o -5 0 32 113.15 102.13 97.60 o -4 0 32 311.57 434.12 69.85 o -3 0 32 154.64 220.00 93.68 o -2 0 32 70.39 78.19 66.54 o -1 0 32 55.85 83.22 76.15 o 0 0 32 34.27 108.44 64.97 o 1 0 32 45.70 73.88 93.76 o 2 0 32 149.02 209.43 74.32 o 3 0 32 90.31 113.41 70.59 o 4 0 32 457.36 630.44 85.18 o 5 0 32 285.26 257.84 79.34 o 6 0 32 122.83 126.68 80.81 o 7 0 32 1.69 -99.53 99.53 o -7 1 32 63.81 73.15 100.98 o -6 1 32 112.88 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