#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:22:23 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180856 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/87/2018797.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018797_Fobs loop_ _publ_author_name 'Gomes, Ligia R.' 'Low, John Nicolson' 'Wardell, James L.' 'de Cardoso, Laura N.' 'De Souza, Marcus V. N.' _publ_section_title ; Substituted 4-alkoxy-7-Cl-quinolines exhibiting \p--\p stacking ; _journal_coeditor_code SK3473 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 191 _journal_page_last 194 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.560 _cell_angle_gamma 90.000 _cell_length_a 3.9320 _cell_length_b 11.9800 _cell_length_c 20.8600 _exptl_crystal_F_000 432.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file sk3473IIIsup4.hkl _cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2012ncs0570' _shelx_refln_list_code 4 _shelx_f_calc_maximum 190.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3062.08 3118.84 420.06 o 4 0 0 5.12 8.80 64.66 o 1 1 0 9630.44 10803.93 775.62 o 2 1 0 553.51 609.81 50.27 o 3 1 0 95.63 96.14 23.01 o 4 1 0 58.26 41.79 30.10 o 0 2 0 138.30 94.25 34.99 o 1 2 0 398.23 466.76 34.32 o 2 2 0 4.93 5.67 9.36 o 3 2 0 10.60 12.64 10.33 o 4 2 0 0.87 18.03 34.14 o 1 3 0 149.52 146.24 21.94 o 2 3 0 1.50 -3.12 12.37 o 3 3 0 75.20 97.75 26.90 o 4 3 0 7.37 40.91 40.70 o 0 4 0 2130.86 1396.06 186.36 o 1 4 0 146.12 100.89 30.64 o 2 4 0 1877.80 2990.61 192.38 o 3 4 0 37.23 22.07 11.91 o 4 4 0 38.32 25.54 33.98 o 1 5 0 2631.99 2879.00 903.34 o 2 5 0 144.80 163.22 33.04 o 3 5 0 367.55 757.15 231.51 o 4 5 0 29.16 31.75 38.67 o 0 6 0 451.02 300.09 129.82 o 1 6 0 51.58 53.84 26.34 o 2 6 0 13.91 12.31 8.78 o 3 6 0 7.10 20.94 33.03 o 4 6 0 58.71 85.87 44.48 o 1 7 0 16.81 120.91 64.11 o 2 7 0 16.22 29.57 11.99 o 3 7 0 0.90 3.05 24.45 o 4 7 0 0.89 26.27 31.76 o 0 8 0 137.24 18.22 33.55 o 1 8 0 0.23 21.28 31.58 o 2 8 0 106.12 192.80 54.34 o 3 8 0 3.35 17.66 29.43 o 1 9 0 122.55 0.74 39.34 o 2 9 0 13.25 34.10 22.67 o 3 9 0 40.86 34.16 36.97 o 0 10 0 118.57 72.19 110.13 o 1 10 0 52.56 17.92 41.36 o 2 10 0 21.70 41.72 21.00 o 3 10 0 8.23 37.70 43.11 o 1 11 0 15.53 3.76 23.93 o 2 11 0 0.24 17.93 23.23 o 0 12 0 1.40 2.94 42.03 o 1 12 0 4.85 10.79 31.36 o 2 12 0 1.72 16.07 16.66 o 1 13 0 14.50 78.59 48.02 o -3 0 1 9.09 4.57 13.79 o -1 0 1 1127.32 1149.80 81.16 o 1 0 1 1556.38 1627.32 50.05 o 3 0 1 136.90 170.89 55.15 o -4 1 1 66.81 56.42 36.91 o -3 1 1 51.70 66.18 29.04 o -2 1 1 881.86 1032.29 53.60 o -1 1 1 4718.84 4699.40 299.06 o 1 1 1 54.29 33.14 11.51 o 2 1 1 350.26 394.22 27.35 o 3 1 1 109.54 119.16 26.68 o 4 1 1 136.84 92.78 61.42 o -4 2 1 26.36 22.81 29.64 o -3 2 1 103.43 113.26 37.38 o -2 2 1 11.14 11.59 9.39 o -1 2 1 1477.94 1594.87 62.40 o 0 2 1 87.78 70.93 17.76 o 1 2 1 411.42 517.79 36.39 o 2 2 1 207.30 258.61 25.90 o 3 2 1 20.31 10.52 5.90 o 4 2 1 6.14 23.70 27.86 o -4 3 1 91.03 116.94 91.46 o -3 3 1 7.15 7.79 8.81 o -2 3 1 0.03 2.52 11.21 o -1 3 1 49.57 23.67 11.22 o 0 3 1 495.32 318.03 40.77 o 1 3 1 68.61 64.90 17.72 o 2 3 1 206.59 224.23 29.41 o 3 3 1 43.16 29.41 18.85 o 4 3 1 23.62 28.32 28.45 o -4 4 1 22.92 36.50 37.12 o -3 4 1 77.34 64.52 25.95 o -2 4 1 640.05 790.76 122.18 o -1 4 1 441.83 400.84 52.51 o 0 4 1 238.23 214.10 35.93 o 1 4 1 368.45 354.73 46.06 o 2 4 1 168.77 423.81 201.49 o 3 4 1 423.42 319.40 296.97 o 4 4 1 3.74 3.82 17.57 o -4 5 1 25.59 51.10 41.14 o -3 5 1 58.33 62.44 33.45 o -2 5 1 325.00 376.31 59.64 o -1 5 1 1138.60 1520.99 132.90 o 0 5 1 454.43 396.58 42.27 o 1 5 1 235.27 287.00 76.54 o 2 5 1 408.65 594.31 107.16 o 3 5 1 29.01 121.25 103.85 o 4 5 1 38.01 60.17 42.25 o -4 6 1 2.14 11.93 22.56 o -3 6 1 114.37 209.53 119.26 o -2 6 1 37.95 41.05 14.59 o -1 6 1 148.23 119.86 42.34 o 0 6 1 105.11 93.06 49.87 o 1 6 1 267.30 344.65 96.91 o 2 6 1 0.07 9.82 6.89 o 3 6 1 20.50 20.67 27.23 o 4 6 1 0.06 26.98 24.58 o -4 7 1 7.86 9.26 20.93 o -3 7 1 10.85 21.00 34.52 o -2 7 1 36.87 36.74 18.60 o -1 7 1 125.78 173.45 65.35 o 0 7 1 1.45 45.44 23.19 o 1 7 1 34.74 23.38 30.53 o 2 7 1 2.36 5.28 6.94 o 3 7 1 0.14 9.71 22.78 o 4 7 1 6.90 21.09 28.93 o -3 8 1 23.40 50.75 44.58 o -2 8 1 63.10 86.04 27.71 o -1 8 1 68.59 68.69 117.49 o 0 8 1 230.28 118.16 122.03 o 1 8 1 116.56 59.95 99.91 o 2 8 1 0.89 13.39 11.70 o 3 8 1 22.80 30.56 33.56 o -3 9 1 4.36 11.96 26.41 o -2 9 1 63.85 126.91 61.50 o -1 9 1 30.22 70.36 143.91 o 0 9 1 639.03 874.44 206.38 o 1 9 1 52.42 12.68 53.24 o 2 9 1 124.59 137.77 71.68 o 3 9 1 9.06 23.47 30.22 o -3 10 1 31.75 67.20 41.73 o -2 10 1 3.60 23.55 20.34 o -1 10 1 277.49 3.82 37.99 o 0 10 1 36.98 212.06 124.38 o 1 10 1 88.65 32.66 53.02 o 2 10 1 19.28 35.17 25.85 o 3 10 1 29.01 29.95 28.86 o -2 11 1 10.68 33.38 30.39 o -1 11 1 48.15 17.29 25.47 o 1 11 1 4.31 26.66 27.52 o 2 11 1 0.01 4.53 21.56 o -2 12 1 3.99 29.81 19.44 o -1 12 1 5.82 46.72 43.93 o 0 12 1 0.24 8.52 32.31 o 2 12 1 1.40 17.88 20.88 o -1 13 1 2.81 31.19 50.43 o 0 13 1 19.12 41.84 50.79 o 1 13 1 0.38 22.49 26.13 o 0 14 1 0.09 6.81 33.80 o -4 0 2 123.35 273.11 110.16 o -2 0 2 815.24 958.69 67.53 o 2 0 2 25.20 15.63 13.94 o 4 0 2 16.69 2.22 57.40 o -4 1 2 0.03 5.32 17.85 o -3 1 2 330.50 377.65 86.85 o -2 1 2 16.36 8.61 15.73 o -1 1 2 0.22 -2.13 10.14 o 0 1 2 982.12 289.70 55.36 o 1 1 2 5000.35 4847.16 671.72 o 2 1 2 846.96 1199.29 57.28 o 3 1 2 83.60 84.38 25.91 o 4 1 2 0.05 -1.36 37.19 o -4 2 2 76.95 71.61 62.64 o -3 2 2 213.55 232.60 57.48 o -2 2 2 1.18 0.93 6.51 o -1 2 2 452.95 407.78 33.60 o 0 2 2 724.77 624.00 40.62 o 1 2 2 1429.49 1513.94 118.62 o 2 2 2 54.41 50.72 18.08 o 3 2 2 261.19 374.23 96.34 o 4 2 2 24.64 28.70 30.73 o -4 3 2 86.52 83.58 62.43 o -3 3 2 9.38 8.95 7.73 o -2 3 2 485.55 464.61 75.13 o -1 3 2 64.21 67.11 17.75 o 0 3 2 653.00 471.70 43.38 o 1 3 2 14.20 13.88 13.63 o 2 3 2 347.61 314.19 42.74 o 3 3 2 52.82 37.69 22.53 o 4 3 2 66.63 52.83 44.44 o -4 4 2 86.81 89.62 74.25 o -3 4 2 38.75 35.81 17.34 o -2 4 2 296.49 324.53 78.22 o -1 4 2 2.72 17.74 10.55 o 0 4 2 567.32 505.57 42.87 o 1 4 2 18.08 24.38 13.85 o 2 4 2 12.06 33.74 28.34 o 3 4 2 29.90 52.94 33.68 o 4 4 2 0.17 6.75 21.71 o -4 5 2 65.82 58.26 28.43 o -3 5 2 19.94 29.72 24.54 o -2 5 2 447.22 769.15 100.33 o -1 5 2 208.64 449.37 140.77 o 0 5 2 172.58 194.81 24.65 o 1 5 2 111.59 98.61 23.14 o 2 5 2 344.73 524.32 161.38 o 3 5 2 47.57 52.27 39.59 o 4 5 2 7.97 13.59 22.14 o -4 6 2 0.43 8.15 22.25 o -3 6 2 98.89 160.99 80.47 o -2 6 2 124.42 134.87 31.24 o -1 6 2 436.49 569.41 75.71 o 0 6 2 8.13 1.85 23.39 o 1 6 2 109.82 73.53 24.49 o 2 6 2 122.36 157.55 36.67 o 3 6 2 133.84 169.89 94.29 o 4 6 2 34.69 39.03 28.85 o -4 7 2 6.64 12.45 24.74 o -3 7 2 17.17 18.04 21.15 o -2 7 2 134.78 99.69 29.00 o -1 7 2 0.15 16.60 27.84 o 0 7 2 506.80 900.09 83.95 o 1 7 2 29.24 30.20 42.20 o 2 7 2 95.68 125.15 34.81 o 3 7 2 48.14 44.75 38.20 o 4 7 2 32.61 64.51 43.32 o -3 8 2 91.52 175.60 75.57 o -2 8 2 24.14 36.79 16.30 o -1 8 2 398.27 479.39 175.01 o 0 8 2 5.59 30.95 47.49 o 1 8 2 58.07 4.58 38.75 o 2 8 2 31.44 25.48 17.74 o 3 8 2 1.50 22.02 22.16 o -3 9 2 0.73 16.85 23.11 o -2 9 2 54.00 94.44 43.03 o -1 9 2 63.75 112.32 56.51 o 1 9 2 470.94 54.52 336.13 o 2 9 2 0.20 18.82 40.62 o 3 9 2 22.90 37.23 41.51 o -3 10 2 0.03 8.69 21.94 o -2 10 2 1.36 11.17 16.01 o -1 10 2 102.37 -6.14 35.51 o 0 10 2 83.79 42.83 104.63 o 1 10 2 122.41 214.61 271.65 o 2 10 2 71.91 -0.12 41.55 o 3 10 2 4.56 11.27 24.31 o -2 11 2 23.79 75.59 41.01 o -1 11 2 0.86 11.72 25.57 o 0 11 2 88.95 6.38 96.61 o 1 11 2 27.51 66.71 65.59 o 2 11 2 212.01 -3.15 46.63 o -2 12 2 4.88 7.35 13.67 o -1 12 2 17.94 59.40 62.48 o 0 12 2 3.49 29.65 58.25 o 1 12 2 55.10 34.50 60.01 o 2 12 2 4.50 10.29 19.70 o -1 13 2 13.12 21.07 30.81 o 0 13 2 9.99 20.14 35.91 o 1 13 2 8.32 53.01 34.18 o 0 14 2 14.57 51.99 52.26 o -3 0 3 523.80 646.41 199.71 o -1 0 3 9.17 2.82 10.74 o 1 0 3 36306.15 42847.73 1770.68 o 3 0 3 523.09 952.82 268.25 o -4 1 3 30.83 20.97 23.85 o -3 1 3 315.62 352.96 69.77 o -2 1 3 25.39 18.08 20.61 o -1 1 3 6183.09 6085.27 437.32 o 0 1 3 4170.23 3642.70 68.52 o 1 1 3 14225.68 14693.75 1307.94 o 2 1 3 1274.77 2028.83 145.87 o 3 1 3 51.68 80.54 21.66 o 4 1 3 1.26 -4.73 36.54 o -4 2 3 134.00 116.24 76.98 o -3 2 3 0.81 5.09 8.49 o -2 2 3 942.72 1015.93 54.89 o -1 2 3 222.31 184.74 21.12 o 0 2 3 1528.44 1457.33 70.85 o 1 2 3 89.18 84.15 21.57 o 2 2 3 2058.55 2586.57 222.42 o 3 2 3 19.88 15.02 14.85 o 4 2 3 42.64 46.54 47.77 o -4 3 3 0.17 4.81 25.52 o -3 3 3 232.26 241.56 57.08 o -2 3 3 45.03 34.94 18.94 o -1 3 3 2175.78 2572.27 141.51 o 0 3 3 59.51 52.41 15.21 o 1 3 3 846.14 995.92 58.13 o 2 3 3 3.21 22.27 21.41 o 3 3 3 336.32 351.98 114.36 o 4 3 3 0.37 4.20 14.97 o -4 4 3 66.70 45.28 42.89 o -3 4 3 71.85 74.00 35.62 o -2 4 3 192.09 202.54 55.42 o -1 4 3 207.69 263.78 24.46 o 0 4 3 68.22 23.09 13.81 o 1 4 3 162.81 169.26 22.14 o 2 4 3 424.21 296.54 96.11 o 3 4 3 98.67 79.90 50.07 o 4 4 3 0.91 7.92 18.02 o -4 5 3 28.62 25.69 32.83 o -3 5 3 99.28 79.84 33.30 o -2 5 3 17.50 21.91 11.90 o -1 5 3 2350.05 3329.22 183.48 o 0 5 3 671.69 852.42 76.37 o 1 5 3 89.36 82.82 16.33 o 2 5 3 160.11 122.65 51.49 o 3 5 3 39.42 48.92 35.19 o 4 5 3 45.42 38.62 27.15 o -4 6 3 19.73 33.37 32.14 o -3 6 3 71.38 148.51 80.95 o -2 6 3 629.50 1027.00 100.46 o -1 6 3 18.88 24.44 15.81 o 0 6 3 1728.21 2055.30 364.81 o 1 6 3 47.06 41.04 21.21 o 2 6 3 176.25 152.85 80.91 o 3 6 3 3.27 34.89 48.14 o 4 6 3 46.89 63.92 38.48 o -4 7 3 1.50 29.48 44.03 o -3 7 3 126.18 209.91 100.87 o -2 7 3 4.55 16.54 20.17 o -1 7 3 194.52 224.51 38.50 o 0 7 3 5.25 23.22 60.80 o 1 7 3 481.69 321.20 129.71 o 2 7 3 0.09 6.32 7.08 o 3 7 3 133.39 151.54 108.73 o 4 7 3 1.50 7.10 46.63 o -3 8 3 9.81 36.22 38.93 o -2 8 3 104.85 95.25 36.92 o -1 8 3 17.26 30.58 18.99 o 0 8 3 109.91 126.62 66.10 o 1 8 3 12.09 130.72 116.09 o 2 8 3 62.91 51.23 24.91 o 3 8 3 3.15 11.73 18.85 o -3 9 3 0.24 8.42 28.63 o -2 9 3 3.70 22.35 23.46 o -1 9 3 15.91 20.61 18.72 o 0 9 3 30.12 24.16 31.91 o 1 9 3 134.17 -4.84 39.09 o 2 9 3 1.63 8.37 22.50 o 3 9 3 1.59 5.46 24.86 o -3 10 3 16.22 17.54 27.52 o -2 10 3 26.77 52.12 25.43 o -1 10 3 1.28 3.85 37.18 o 0 10 3 357.29 327.32 230.46 o 1 10 3 149.66 10.73 34.38 o 2 10 3 18.31 42.30 34.52 o 3 10 3 1.27 9.04 15.76 o -2 11 3 19.56 29.04 22.06 o -1 11 3 44.30 46.96 25.07 o 0 11 3 11.89 81.22 105.18 o 1 11 3 17.70 15.50 24.55 o 2 11 3 15.30 16.79 37.11 o -2 12 3 20.49 44.37 28.36 o -1 12 3 0.70 26.13 43.27 o 0 12 3 62.53 361.10 97.88 o 1 12 3 3.71 7.66 22.37 o 2 12 3 7.40 24.41 20.99 o -1 13 3 15.68 13.95 31.61 o 0 13 3 0.13 16.32 32.52 o 1 13 3 14.84 91.21 54.48 o 0 14 3 0.02 16.77 30.27 o -4 0 4 0.90 6.33 19.56 o -2 0 4 1358.79 1739.43 143.90 o 0 0 4 7248.78 6451.62 582.09 o 2 0 4 217.63 295.20 29.59 o 4 0 4 53.64 24.88 64.39 o -4 1 4 4.97 9.02 14.77 o -3 1 4 71.65 75.57 36.80 o -2 1 4 67.38 48.61 19.05 o -1 1 4 2.59 11.77 6.55 o 0 1 4 1135.77 1056.13 63.82 o 1 1 4 293.48 327.63 28.49 o 2 1 4 641.56 819.35 58.78 o 3 1 4 3.58 4.74 6.95 o 4 1 4 32.58 13.13 35.76 o -4 2 4 16.30 14.69 39.01 o -3 2 4 361.16 480.06 96.59 o -2 2 4 23.81 9.63 14.09 o -1 2 4 1270.49 1197.98 71.01 o 0 2 4 2268.87 1956.39 79.98 o 1 2 4 1025.19 964.49 43.92 o 2 2 4 62.63 26.74 13.74 o 3 2 4 531.55 511.61 189.48 o 4 2 4 0.86 22.75 41.79 o -4 3 4 61.67 82.85 74.14 o -3 3 4 40.38 16.73 23.10 o -2 3 4 240.10 239.33 48.49 o -1 3 4 74.78 66.33 20.30 o 0 3 4 2860.29 2471.07 95.64 o 1 3 4 32.13 22.52 10.94 o 2 3 4 87.52 84.66 20.80 o 3 3 4 27.41 18.01 20.67 o 4 3 4 137.67 38.11 93.78 o -4 4 4 2.11 20.37 42.58 o -3 4 4 49.11 49.72 32.27 o -2 4 4 0.97 6.49 13.24 o -1 4 4 1713.70 2264.00 126.24 o 0 4 4 143.65 119.40 20.52 o 1 4 4 214.81 212.05 21.85 o 2 4 4 49.63 31.58 18.35 o 3 4 4 86.33 38.78 39.19 o 4 4 4 24.85 13.78 22.59 o -4 5 4 18.68 24.02 29.24 o -3 5 4 48.83 49.72 30.18 o -2 5 4 99.60 116.42 39.22 o -1 5 4 1.13 -1.58 11.28 o 0 5 4 838.56 1116.67 67.61 o 1 5 4 34.96 29.75 13.88 o 2 5 4 12.98 11.91 8.90 o 3 5 4 0.36 16.91 23.88 o 4 5 4 0.84 7.03 16.50 o -4 6 4 5.96 17.70 25.70 o -3 6 4 75.87 75.69 53.27 o -2 6 4 1.37 26.02 29.90 o -1 6 4 2.38 6.53 10.61 o 0 6 4 292.58 356.76 76.25 o 1 6 4 341.56 348.92 60.94 o 2 6 4 2.95 9.31 9.11 o 3 6 4 50.09 38.42 32.38 o 4 6 4 24.89 23.50 32.77 o -4 7 4 64.46 2.13 46.32 o -3 7 4 3.28 17.52 29.17 o -2 7 4 170.61 270.94 63.78 o -1 7 4 45.84 36.94 17.48 o 0 7 4 325.34 300.95 97.77 o 1 7 4 9.02 10.14 30.58 o 2 7 4 341.96 412.19 180.43 o 3 7 4 0.20 37.54 47.62 o -3 8 4 3.74 15.50 35.99 o -2 8 4 6.66 18.44 17.08 o -1 8 4 130.42 143.81 30.63 o 0 8 4 36.37 64.90 134.27 o 2 8 4 0.00 13.92 14.60 o 3 8 4 16.62 18.88 24.98 o -3 9 4 0.01 9.23 35.43 o -2 9 4 5.97 34.22 22.90 o -1 9 4 14.08 6.45 6.95 o 0 9 4 91.55 140.40 127.30 o 1 9 4 28.38 54.94 58.62 o 2 9 4 30.78 30.63 30.81 o 3 9 4 0.96 9.80 22.24 o -3 10 4 15.34 34.09 43.61 o -2 10 4 0.03 14.83 18.13 o -1 10 4 29.68 13.45 70.13 o 0 10 4 43.17 161.34 236.16 o 1 10 4 0.18 11.28 31.10 o 2 10 4 5.53 22.36 25.58 o 3 10 4 2.57 9.51 32.37 o -2 11 4 97.49 170.08 85.50 o -1 11 4 0.67 8.45 24.33 o 0 11 4 8.92 28.00 22.01 o 1 11 4 4.55 5.68 20.09 o 2 11 4 0.47 21.97 25.94 o -2 12 4 0.94 5.18 12.22 o -1 12 4 39.24 107.53 126.18 o 0 12 4 4.57 32.27 46.96 o 1 12 4 4.06 26.68 40.99 o 2 12 4 0.23 -0.74 16.78 o -1 13 4 4.00 12.79 22.11 o 0 13 4 3.63 12.64 24.87 o 1 13 4 0.10 26.68 29.56 o 0 14 4 4.46 10.45 25.46 o -3 0 5 51.79 73.56 62.21 o -1 0 5 0.35 3.15 8.80 o 1 0 5 4558.24 5348.94 165.36 o 3 0 5 80.26 160.93 64.19 o -4 1 5 12.84 14.13 26.18 o -3 1 5 0.11 -1.72 19.46 o -2 1 5 94.18 76.89 22.91 o -1 1 5 412.55 462.31 33.47 o 0 1 5 1199.66 1236.47 70.78 o 1 1 5 106.01 87.63 23.26 o 2 1 5 3991.45 6381.00 116.75 o 3 1 5 119.82 99.84 31.27 o 4 1 5 30.97 8.44 22.91 o -4 2 5 13.36 16.16 25.94 o -3 2 5 4.47 6.96 17.38 o -2 2 5 346.56 305.41 54.82 o -1 2 5 26.99 22.18 13.27 o 0 2 5 209.80 179.62 22.05 o 1 2 5 271.48 285.50 21.71 o 2 2 5 30.21 21.14 14.04 o 3 2 5 412.82 468.33 110.95 o 4 2 5 27.66 16.14 33.84 o -4 3 5 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