#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/88/2018823.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018823_Fobs loop_ _publ_author_name 'Boer\'e, Ren\'e T.' 'Bender, Christopher O.' _publ_section_title ; A tetrabromo-1,4-ethanonaphthalene and related dibromo-1,4-ethenonaphthalene ; _journal_coeditor_code GZ3227 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 247 _journal_page_last 250 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.826 _cell_angle_gamma 90.000 _cell_length_a 9.5198 _cell_length_b 6.5032 _cell_length_c 17.1242 _exptl_crystal_F_000 600.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file gz3227IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' RB08037_0m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 236.28 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8812.21 9337.97 130.79 o 4 0 0 338.33 388.52 10.95 o 6 0 0 6777.04 6772.47 96.90 o 8 0 0 2888.49 2886.92 49.40 o 10 0 0 586.65 596.64 19.00 o 12 0 0 134.51 137.64 16.34 o 1 1 0 285.98 290.14 3.89 o 2 1 0 1998.92 2103.38 22.53 o 3 1 0 6703.65 6745.76 70.84 o 5 1 0 6297.26 6276.32 63.32 o 6 1 0 21.25 17.39 2.99 o 7 1 0 100.24 105.24 4.34 o 8 1 0 258.10 249.29 7.43 o 9 1 0 2259.76 2131.71 29.21 o 10 1 0 21.95 16.82 5.51 o 11 1 0 3276.27 3273.75 46.89 o 12 1 0 0.37 10.67 13.19 o 0 2 0 55827.50 49921.82 1604.80 o 1 2 0 120.08 125.29 2.71 o 2 2 0 22243.79 21702.62 263.76 o 3 2 0 1462.53 1578.13 16.84 o 4 2 0 374.56 410.29 6.25 o 5 2 0 14.92 15.58 2.44 o 6 2 0 5118.29 5016.31 54.23 o 7 2 0 5.23 7.45 3.51 o 8 2 0 2020.19 1946.12 31.30 o 9 2 0 123.76 135.49 6.55 o 10 2 0 98.80 110.68 7.17 o 11 2 0 21.64 25.08 7.69 o 1 3 0 460.84 496.34 6.26 o 2 3 0 1215.27 1259.03 13.83 o 3 3 0 2878.83 2828.22 29.40 o 4 3 0 198.87 221.95 7.71 o 5 3 0 5337.78 5186.71 55.88 o 6 3 0 53.45 52.24 4.58 o 7 3 0 34.70 49.77 4.35 o 8 3 0 127.76 136.58 6.01 o 9 3 0 729.88 730.41 13.88 o 10 3 0 3.35 -5.79 5.79 o 11 3 0 2636.10 2687.24 40.41 o 0 4 0 17800.61 17084.51 366.89 o 1 4 0 1040.48 1100.84 12.68 o 2 4 0 8831.45 8434.10 89.59 o 3 4 0 2001.98 2000.20 21.64 o 4 4 0 0.12 4.36 2.95 o 5 4 0 30.11 32.90 3.59 o 6 4 0 2139.18 2107.00 28.41 o 7 4 0 27.00 28.44 4.85 o 8 4 0 986.50 1006.96 16.74 o 9 4 0 307.78 298.57 12.93 o 10 4 0 40.34 40.39 8.10 o 1 5 0 326.79 322.24 7.72 o 2 5 0 670.94 677.53 10.68 o 3 5 0 589.97 580.80 14.59 o 4 5 0 565.32 550.37 13.23 o 5 5 0 4080.86 3904.92 49.42 o 6 5 0 42.85 50.19 5.22 o 7 5 0 470.69 428.98 10.59 o 8 5 0 113.49 110.19 7.12 o 9 5 0 1045.73 1097.05 19.13 o 0 6 0 6946.77 6934.98 113.22 o 1 6 0 183.24 179.32 6.96 o 2 6 0 1693.47 1741.88 24.55 o 3 6 0 1102.74 1161.48 19.48 o 4 6 0 66.67 68.65 6.22 o 5 6 0 97.73 113.02 7.01 o 6 6 0 910.70 949.24 18.02 o 7 6 0 103.79 106.53 9.03 o 8 6 0 238.54 266.79 12.65 o 1 7 0 212.08 209.83 10.65 o 2 7 0 356.29 382.23 13.95 o 3 7 0 1020.60 977.07 22.98 o 4 7 0 361.23 371.43 14.82 o 5 7 0 523.52 474.53 16.48 o 6 7 0 13.52 8.40 9.55 o 0 8 0 1352.58 1319.26 41.73 o 1 8 0 34.34 33.30 11.84 o 2 8 0 701.91 768.00 24.66 o 3 8 0 622.55 662.59 23.76 o -11 0 1 513.21 531.56 18.83 o -9 0 1 3436.23 3371.01 57.59 o -7 0 1 291.21 287.68 12.82 o -5 0 1 9739.54 9827.64 138.98 o -3 0 1 36610.33 38096.48 1470.05 o -1 0 1 24959.38 27487.72 1494.25 o 1 0 1 2493.94 2603.58 42.02 o 3 0 1 13652.16 14121.12 271.77 o 5 0 1 7453.85 7404.93 105.34 o 7 0 1 180.83 206.81 16.46 o 9 0 1 8.67 5.78 6.18 o 11 0 1 164.87 184.32 12.89 o -12 1 1 945.12 888.93 20.36 o -11 1 1 62.08 68.36 7.50 o -10 1 1 214.21 219.54 8.64 o -9 1 1 18.66 20.57 6.29 o -8 1 1 4431.58 4254.70 53.03 o -7 1 1 86.47 85.59 3.94 o -6 1 1 7438.25 7281.24 77.30 o -5 1 1 101.67 96.84 3.85 o -4 1 1 68.71 74.81 2.91 o -3 1 1 1.15 -1.43 1.43 o -2 1 1 1991.01 2095.65 22.91 o -1 1 1 3323.59 3522.20 39.31 o 0 1 1 761.92 768.78 8.62 o 1 1 1 691.91 754.89 8.22 o 2 1 1 23696.64 23381.25 425.76 o 3 1 1 5.87 7.93 1.24 o 4 1 1 2737.93 2770.15 28.62 o 6 1 1 1008.81 1002.39 13.72 o 7 1 1 106.02 113.69 4.54 o 8 1 1 6598.14 6502.98 74.32 o 9 1 1 1.00 -4.53 4.53 o 10 1 1 4360.80 4346.98 64.41 o 11 1 1 9.74 15.91 8.06 o -11 2 1 209.16 232.13 9.85 o -10 2 1 23.15 28.12 5.95 o -9 2 1 1861.44 1833.72 26.03 o -8 2 1 36.01 42.94 4.89 o -7 2 1 276.84 276.84 8.56 o -6 2 1 801.56 800.78 11.00 o -5 2 1 3775.21 3555.59 38.76 o -4 2 1 35.56 32.52 2.23 o -3 2 1 27549.62 26635.52 371.00 o -2 2 1 64.30 51.50 2.48 o -1 2 1 24528.19 24251.19 251.59 o 0 2 1 714.49 702.00 7.83 o 1 2 1 3.57 5.83 1.41 o 2 2 1 689.82 693.04 8.00 o 3 2 1 5237.29 5072.81 51.12 o 4 2 1 523.49 581.59 7.45 o 5 2 1 7459.24 7337.93 77.79 o 6 2 1 93.65 88.25 3.78 o 7 2 1 909.02 905.01 12.58 o 8 2 1 1053.31 1018.24 21.86 o 9 2 1 2.26 5.09 4.68 o 10 2 1 0.51 5.28 5.60 o 11 2 1 98.81 100.20 8.92 o -11 3 1 103.39 118.39 8.17 o -10 3 1 59.12 73.31 6.85 o -9 3 1 201.85 202.19 9.69 o -8 3 1 1732.03 1675.04 22.39 o -7 3 1 168.35 165.85 7.04 o -6 3 1 4600.19 4432.02 51.31 o -5 3 1 65.79 62.42 3.57 o -4 3 1 263.12 242.31 4.87 o -3 3 1 90.91 107.75 3.37 o -2 3 1 328.32 366.35 5.63 o -1 3 1 450.94 460.51 8.53 o 0 3 1 1042.04 925.34 11.01 o 1 3 1 6.31 8.49 1.56 o 2 3 1 8389.70 8399.94 83.95 o 3 3 1 65.20 68.36 2.65 o 4 3 1 2572.85 2514.03 27.99 o 5 3 1 129.73 133.61 4.51 o 6 3 1 1151.24 1144.13 15.66 o 7 3 1 125.92 128.01 5.39 o 8 3 1 5391.59 5273.99 61.39 o 9 3 1 0.22 5.10 5.19 o 10 3 1 2338.21 2342.29 39.04 o 11 3 1 208.49 205.47 11.35 o -10 4 1 93.44 96.33 8.07 o -9 4 1 951.29 978.40 17.08 o -8 4 1 262.13 237.71 8.20 o -7 4 1 35.47 55.99 4.76 o -6 4 1 1219.27 1212.09 16.79 o -5 4 1 2121.66 2041.56 25.27 o -4 4 1 410.46 400.48 7.04 o -3 4 1 16039.90 16075.67 168.77 o -2 4 1 231.68 233.19 4.70 o -1 4 1 13540.46 13422.71 139.90 o 0 4 1 1555.45 1614.92 17.65 o 1 4 1 149.54 148.54 4.05 o 2 4 1 585.96 563.05 7.63 o 3 4 1 2734.03 2668.99 29.91 o 4 4 1 493.99 492.51 9.33 o 5 4 1 3487.98 3402.78 43.03 o 6 4 1 1027.74 983.14 15.51 o 7 4 1 158.36 170.47 10.68 o 8 4 1 263.44 257.53 8.64 o 9 4 1 232.00 229.30 9.87 o 10 4 1 48.10 43.87 8.17 o -9 5 1 85.17 97.07 7.54 o -8 5 1 898.05 877.55 16.54 o -7 5 1 183.16 188.58 8.02 o -6 5 1 1249.09 1197.47 19.19 o -5 5 1 9.42 8.90 4.13 o -4 5 1 63.42 58.97 5.60 o -3 5 1 506.71 498.55 10.34 o -2 5 1 23.40 25.49 3.64 o -1 5 1 1277.20 1259.88 26.06 o 0 5 1 2092.95 2104.92 26.15 o 1 5 1 64.30 72.09 3.53 o 2 5 1 2846.34 2827.27 34.14 o 3 5 1 49.19 53.36 5.73 o 4 5 1 839.53 791.37 13.11 o 5 5 1 913.85 922.24 14.99 o 6 5 1 1350.39 1309.00 19.82 o 7 5 1 39.37 44.15 5.80 o 8 5 1 3005.75 2909.75 39.22 o 9 5 1 0.54 -2.70 6.48 o -8 6 1 1.19 1.23 7.99 o -7 6 1 28.18 40.70 7.90 o -6 6 1 669.92 676.23 16.50 o -5 6 1 1326.88 1280.94 23.99 o -4 6 1 875.38 904.96 18.59 o -3 6 1 6513.84 6530.85 96.07 o -2 6 1 26.95 25.47 5.11 o -1 6 1 4506.32 4561.94 62.71 o 0 6 1 483.01 512.54 10.69 o 1 6 1 245.93 237.14 7.75 o 2 6 1 710.71 715.07 13.99 o 3 6 1 618.83 652.35 14.53 o 4 6 1 7.18 7.94 5.62 o 5 6 1 1593.34 1618.48 28.57 o 6 6 1 444.91 449.22 14.51 o 7 6 1 179.51 183.40 10.21 o 8 6 1 412.64 410.54 19.54 o -6 7 1 610.60 600.99 21.83 o -5 7 1 156.47 147.91 10.79 o -4 7 1 246.46 234.43 12.76 o -3 7 1 2.44 -6.48 7.65 o -2 7 1 188.22 199.53 11.32 o -1 7 1 513.27 493.78 14.04 o 0 7 1 127.11 125.50 9.35 o 1 7 1 206.54 205.73 11.39 o 2 7 1 700.35 717.99 18.81 o 3 7 1 7.99 0.20 7.57 o 4 7 1 63.58 67.95 9.32 o 5 7 1 274.60 316.20 14.50 o 6 7 1 411.20 434.82 16.85 o -3 8 1 1674.66 1731.57 36.43 o -2 8 1 19.57 34.51 10.49 o -1 8 1 1396.45 1422.61 35.06 o 0 8 1 331.12 378.76 15.66 o 1 8 1 107.67 135.04 12.57 o 2 8 1 422.80 481.82 19.56 o 3 8 1 226.38 258.18 16.82 o -12 0 2 271.29 299.18 16.70 o -10 0 2 686.93 635.50 20.07 o -8 0 2 9627.74 9456.51 150.38 o -6 0 2 12747.43 12708.19 179.57 o -4 0 2 35151.64 36298.48 897.53 o -2 0 2 1503.87 1552.05 25.43 o 0 0 2 3561.10 3684.08 68.22 o 2 0 2 51759.93 52307.03 1565.23 o 4 0 2 35.55 39.82 2.74 o 6 0 2 593.26 619.03 12.02 o 8 0 2 628.80 590.02 14.86 o 10 0 2 528.01 548.51 16.30 o -12 1 2 181.70 197.44 10.29 o -11 1 2 981.78 969.44 18.92 o -10 1 2 133.59 135.87 7.03 o -9 1 2 2895.54 2799.48 36.85 o -8 1 2 122.49 128.38 8.60 o -7 1 2 701.19 683.73 10.06 o -6 1 2 41.17 34.62 2.83 o -5 1 2 4.52 1.59 2.02 o -4 1 2 154.19 165.00 3.94 o -3 1 2 916.04 901.68 11.15 o -2 1 2 577.69 624.47 7.63 o -1 1 2 3055.12 3091.10 32.73 o 0 1 2 10166.65 10783.28 221.73 o 1 1 2 10748.44 11082.41 120.35 o 2 1 2 522.74 526.42 6.18 o 3 1 2 2771.21 2906.68 29.74 o 4 1 2 839.46 920.36 10.59 o 5 1 2 17341.14 17227.17 170.90 o 6 1 2 82.83 100.85 3.92 o 7 1 2 9417.47 9396.55 105.36 o 8 1 2 6.21 4.66 4.55 o 9 1 2 1480.27 1466.85 20.41 o 10 1 2 10.01 5.08 6.41 o 11 1 2 316.11 299.97 12.46 o -11 2 2 3.47 4.22 6.33 o -10 2 2 113.50 109.47 6.99 o -9 2 2 26.01 36.23 5.41 o -8 2 2 1610.15 1585.91 29.21 o -7 2 2 162.50 154.03 7.39 o -6 2 2 17435.51 17289.21 190.98 o -5 2 2 107.31 109.72 4.37 o -4 2 2 34016.34 33572.63 498.28 o -3 2 2 4.60 1.90 1.30 o -2 2 2 1297.06 1328.36 15.06 o -1 2 2 1015.92 995.41 10.75 o 0 2 2 9365.80 9369.66 98.10 o 1 2 2 6.82 11.31 1.35 o 2 2 2 16836.88 16317.23 161.25 o 3 2 2 839.76 889.46 10.18 o 4 2 2 5536.44 5755.63 58.17 o 5 2 2 24.41 22.00 2.66 o 6 2 2 9.54 12.91 3.28 o 7 2 2 98.40 95.39 4.34 o 8 2 2 34.61 32.48 4.75 o 9 2 2 64.63 61.67 5.70 o 10 2 2 645.37 618.73 16.94 o 11 2 2 41.07 33.88 9.09 o -11 3 2 595.08 580.11 19.72 o -10 3 2 82.95 91.34 6.57 o -9 3 2 2543.96 2409.60 32.87 o -8 3 2 104.75 100.07 5.47 o -7 3 2 653.71 640.75 10.89 o -6 3 2 1.09 -0.36 3.13 o -5 3 2 29.69 33.34 4.12 o -4 3 2 440.72 452.78 8.15 o -3 3 2 958.85 1000.51 12.15 o -2 3 2 2279.36 2517.51 26.17 o -1 3 2 2928.09 2832.05 29.17 o 0 3 2 610.96 702.42 8.22 o 1 3 2 7148.95 7420.32 74.12 o 3 3 2 2814.00 2911.74 31.71 o 4 3 2 414.96 416.64 6.42 o 5 3 2 8892.13 8482.99 89.85 o 6 3 2 17.45 14.75 3.25 o 7 3 2 9785.64 9433.11 106.17 o 8 3 2 16.53 22.98 4.63 o 9 3 2 649.37 638.92 15.11 o 10 3 2 130.47 139.97 9.00 o 11 3 2 108.00 127.85 11.36 o -10 4 2 91.57 94.00 7.88 o -9 4 2 365.42 366.53 10.42 o -8 4 2 885.48 874.68 14.25 o -7 4 2 129.65 143.02 6.11 o -6 4 2 9136.96 8952.42 100.82 o -5 4 2 170.64 175.19 5.77 o -4 4 2 12499.07 12154.29 134.79 o -3 4 2 15.92 13.43 2.57 o -2 4 2 900.66 837.00 10.85 o -1 4 2 1019.79 975.04 12.20 o 0 4 2 3347.86 3318.79 38.87 o 1 4 2 22.41 25.76 2.42 o 2 4 2 5646.87 5606.74 60.25 o 3 4 2 922.14 920.87 12.05 o 4 4 2 3470.04 3375.04 39.73 o 5 4 2 10.55 12.06 3.74 o 6 4 2 46.52 62.85 4.84 o 7 4 2 52.50 38.90 5.70 o 8 4 2 136.21 141.79 7.56 o 9 4 2 26.11 30.83 7.70 o 10 4 2 316.41 271.88 12.42 o -9 5 2 1010.15 965.88 19.21 o -8 5 2 150.51 136.82 7.32 o -7 5 2 847.17 827.38 16.15 o -6 5 2 0.07 -2.50 4.86 o -5 5 2 19.03 12.34 4.60 o -4 5 2 575.21 596.17 12.54 o -3 5 2 1156.23 1093.00 17.57 o -2 5 2 1869.20 1838.60 24.85 o -1 5 2 3797.72 3758.96 44.24 o 0 5 2 118.53 138.75 4.93 o 1 5 2 224.90 212.38 6.05 o 2 5 2 35.28 37.14 3.42 o 3 5 2 1029.16 1022.68 14.50 o 4 5 2 600.97 586.38 10.89 o 5 5 2 3879.15 3785.06 48.08 o 6 5 2 4.65 3.29 4.89 o 7 5 2 4220.41 4163.35 53.35 o 8 5 2 301.73 324.93 10.93 o 9 5 2 402.65 350.93 12.03 o -8 6 2 467.61 463.96 15.38 o -7 6 2 1539.95 1532.54 28.66 o -6 6 2 2115.07 2122.09 36.18 o -5 6 2 0.32 2.25 6.28 o -4 6 2 5372.57 5382.92 80.54 o -3 6 2 510.56 504.53 14.04 o -2 6 2 151.32 157.12 7.82 o -1 6 2 1212.83 1230.02 22.14 o 0 6 2 632.88 650.78 23.66 o 1 6 2 122.41 118.22 6.02 o 2 6 2 2461.07 2427.88 35.48 o 3 6 2 54.31 61.03 6.21 o 4 6 2 774.44 812.72 17.18 o 5 6 2 922.04 923.68 19.08 o 6 6 2 147.31 158.72 9.23 o 7 6 2 17.11 9.75 8.42 o 8 6 2 53.35 59.06 9.88 o -6 7 2 4.49 5.10 8.37 o -5 7 2 148.04 156.30 9.97 o -4 7 2 395.19 399.30 13.49 o -3 7 2 162.64 194.24 12.65 o -2 7 2 885.66 856.51 20.19 o -1 7 2 421.31 420.16 13.77 o 0 7 2 3.98 3.42 6.19 o 1 7 2 547.35 526.94 13.89 o 2 7 2 119.85 134.24 10.14 o 3 7 2 123.26 151.83 8.79 o 4 7 2 256.39 273.27 11.71 o 5 7 2 2096.19 2174.15 42.52 o 6 7 2 11.58 4.54 10.87 o -3 8 2 84.03 106.30 10.68 o -2 8 2 213.64 227.15 15.46 o -1 8 2 340.21 346.16 22.19 o 0 8 2 259.61 309.75 14.73 o 1 8 2 3.18 7.79 9.86 o 2 8 2 466.55 506.84 19.55 o 3 8 2 248.74 260.63 17.17 o -11 0 3 19.40 28.24 9.63 o -9 0 3 4132.43 3957.25 86.94 o -7 0 3 11839.46 11589.19 182.47 o -5 0 3 4755.70 4726.50 68.28 o -3 0 3 7641.95 7813.29 102.82 o -1 0 3 2167.55 2199.12 31.34 o 1 0 3 16105.20 15898.18 427.70 o 3 0 3 524.25 524.73 10.32 o 5 0 3 16.28 35.39 3.18 o 7 0 3 1261.65 1234.44 23.56 o 9 0 3 681.65 708.15 22.39 o 11 0 3 0.62 1.15 13.26 o -12 1 3 949.99 1008.58 20.37 o -11 1 3 2.34 -1.39 6.52 o -10 1 3 1216.73 1140.09 20.08 o -9 1 3 279.87 261.85 8.28 o -8 1 3 221.01 215.79 7.11 o -7 1 3 318.12 333.60 7.26 o -6 1 3 488.32 486.80 7.69 o -5 1 3 451.22 512.94 7.50 o -4 1 3 3080.15 3050.32 31.46 o -3 1 3 30.25 30.53 1.58 o -2 1 3 17931.62 18871.95 215.87 o -1 1 3 3286.79 3455.85 38.70 o 0 1 3 21.81 34.31 1.36 o 1 1 3 5.64 2.72 0.86 o 2 1 3 22958.41 23071.36 228.65 o 3 1 3 1491.38 1628.70 17.26 o 4 1 3 30343.89 30616.56 317.09 o 5 1 3 404.26 438.56 7.13 o 6 1 3 7035.46 6969.91 74.30 o 7 1 3 234.29 226.16 6.54 o 8 1 3 32.62 29.12 4.13 o 9 1 3 0.66 -0.46 4.75 o 10 1 3 1462.09 1440.15 28.63 o 11 1 3 17.93 24.26 8.17 o -11 2 3 230.80 244.10 10.29 o -10 2 3 266.73 272.54 9.53 o -9 2 3 4790.77 4684.95 58.82 o -8 2 3 117.56 126.35 8.43 o -7 2 3 10611.24 10339.53 115.78 o -6 2 3 158.89 171.51 7.76 o -5 2 3 3865.63 3848.98 41.77 o -4 2 3 3.33 8.76 1.87 o -3 2 3 5438.39 5633.18 59.56 o -2 2 3 360.49 369.79 5.18 o -1 2 3 18117.17 18189.20 180.22 o 0 2 3 3032.88 3224.79 34.51 o 1 2 3 5271.03 5203.99 55.07 o 2 2 3 11.07 5.12 1.56 o 3 2 3 56.17 82.33 2.84 o 4 2 3 63.51 66.69 2.78 o 5 2 3 117.87 117.90 4.21 o 6 2 3 38.51 41.11 3.34 o 7 2 3 1034.73 1006.64 15.64 o 8 2 3 25.54 22.71 4.77 o 9 2 3 586.59 591.38 13.22 o 10 2 3 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