#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/88/2018838.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018838_Fobs loop_ _publ_author_name 'Gomes, Ligia R.' 'Low, John Nicolson' 'Wardell, James L.' 'Pinheiro, Alessandra C.' 'Mendon\,ca, Thais C. N. de' 'de Souza, Marcus V. N.' _publ_section_title ; Three 2-(methysulfanyl)nicotinamides ; _journal_coeditor_code SK3475 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 293 _journal_page_last 298 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.150 _cell_angle_gamma 90.000 _cell_length_a 11.4200 _cell_length_b 8.5800 _cell_length_c 23.6100 _exptl_crystal_F_000 896.00 _reflns_d_resolution_high 0.7761 _[local]_cod_data_source_file sk3475IIsup4.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2012ncs0315' _shelx_refln_list_code 4 _shelx_f_calc_maximum 172.10 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2032.00 2331.53 51.56 o 3 0 0 1239.80 1006.00 62.94 o 4 0 0 209.31 226.39 36.63 o 5 0 0 8817.01 8601.25 193.80 o 6 0 0 264.32 328.01 50.54 o 1 1 0 85.06 157.79 29.23 o 2 1 0 3336.79 3966.71 71.91 o 3 1 0 217.98 222.34 30.78 o 4 1 0 1258.93 1355.63 49.97 o 5 1 0 1396.33 1436.87 59.51 o 6 1 0 20.56 45.23 16.29 o 7 1 0 505.86 815.76 267.31 o 8 1 0 534.89 1547.33 198.00 o 9 1 0 417.10 400.18 90.43 o 10 1 0 39.20 37.40 98.10 o 0 2 0 9485.05 8144.69 141.32 o 1 2 0 34.18 52.47 15.50 o 2 2 0 231.31 240.70 47.24 o 3 2 0 49.25 54.84 17.10 o 4 2 0 4213.80 6273.37 742.15 o 5 2 0 680.40 1024.16 67.50 o 6 2 0 26.08 58.05 17.54 o 7 2 0 46.81 11.58 56.82 o 8 2 0 2.27 22.75 23.03 o 9 2 0 236.14 346.60 65.22 o 10 2 0 95.19 254.08 77.87 o 11 2 0 58.96 708.89 117.57 o 12 2 0 1.72 -9.39 105.51 o 1 3 0 20.37 1.72 14.28 o 2 3 0 5533.64 6909.74 130.12 o 3 3 0 460.93 504.32 86.90 o 4 3 0 59.49 42.66 29.48 o 5 3 0 1469.59 2167.25 150.52 o 6 3 0 379.34 620.79 58.74 o 7 3 0 1182.68 1961.56 188.28 o 8 3 0 300.13 434.46 95.29 o 9 3 0 305.34 614.85 113.79 o 10 3 0 320.13 239.04 88.77 o 11 3 0 263.02 242.80 54.00 o 12 3 0 94.41 210.52 91.62 o 13 3 0 0.07 -37.66 78.26 o 14 3 0 40.62 58.07 87.76 o 0 4 0 4163.80 4282.18 123.78 o 1 4 0 184.38 109.87 36.54 o 2 4 0 556.76 494.22 105.22 o 3 4 0 2095.80 2269.07 78.07 o 4 4 0 193.63 175.79 53.77 o 5 4 0 149.00 182.26 28.19 o 6 4 0 793.60 1148.42 107.55 o 7 4 0 1645.46 3146.57 226.24 o 8 4 0 120.61 212.80 34.83 o 9 4 0 520.25 797.18 57.32 o 10 4 0 0.68 -23.66 46.48 o 12 4 0 114.60 149.89 44.92 o 13 4 0 0.69 -41.01 55.33 o 1 5 0 12.75 -1.61 45.11 o 4 5 0 904.02 1088.50 175.95 o 5 5 0 11.84 87.59 87.86 o 6 5 0 587.87 1001.06 121.96 o 7 5 0 760.69 1488.50 92.09 o 8 5 0 339.56 638.35 73.26 o 9 5 0 171.43 414.31 73.92 o 10 5 0 8.31 -38.75 41.00 o 11 5 0 192.54 147.89 56.97 o 12 5 0 4.59 67.48 63.34 o 1 6 0 48.16 45.78 46.38 o 2 6 0 10.10 6.45 40.25 o 3 6 0 84.42 916.26 179.22 o 4 6 0 1.22 46.95 33.04 o 5 6 0 7.52 253.01 50.18 o 6 6 0 211.39 190.33 103.74 o 7 6 0 319.19 521.07 150.99 o 8 6 0 72.12 74.27 30.35 o 9 6 0 430.33 656.11 97.27 o 10 6 0 139.94 309.17 89.75 o 11 6 0 99.44 151.14 69.53 o 12 6 0 42.72 70.09 52.06 o 1 7 0 16.41 34.05 35.61 o 2 7 0 462.18 513.97 105.01 o 3 7 0 96.93 201.88 62.58 o 4 7 0 216.10 205.68 55.08 o 5 7 0 477.75 423.90 140.72 o 6 7 0 327.62 539.35 118.47 o 7 7 0 0.52 2.75 19.12 o 8 7 0 75.43 99.33 34.80 o 10 7 0 226.03 208.01 98.40 o 11 7 0 2.50 1.81 35.72 o 0 8 0 231.54 182.04 43.73 o 1 8 0 198.00 137.52 26.79 o 2 8 0 6.10 39.20 16.17 o 3 8 0 287.29 426.52 177.59 o 4 8 0 2.60 66.83 39.43 o 5 8 0 90.55 125.45 60.72 o 6 8 0 49.51 77.92 29.23 o 7 8 0 45.11 399.57 91.40 o 8 8 0 149.14 137.22 44.25 o 9 8 0 10.29 91.31 31.89 o 10 8 0 0.05 2.82 38.43 o 1 9 0 13.75 27.25 15.56 o 2 9 0 132.63 310.38 59.88 o 3 9 0 88.47 162.44 82.40 o 4 9 0 59.54 68.91 29.44 o 5 9 0 0.34 35.76 22.86 o 6 9 0 39.52 159.60 50.05 o 7 9 0 154.92 239.19 115.15 o 8 9 0 22.23 44.81 25.00 o 0 10 0 257.77 304.43 58.00 o 1 10 0 71.21 62.21 49.97 o 2 10 0 18.40 32.39 21.74 o 3 10 0 267.82 243.14 51.24 o 4 10 0 4.69 11.76 42.90 o 5 10 0 58.14 120.83 32.42 o 6 10 0 26.26 83.01 34.97 o -10 1 1 97.87 403.45 144.02 o -9 1 1 111.00 -3.37 67.29 o -8 1 1 950.81 2061.81 244.48 o -7 1 1 1701.36 2259.68 95.15 o -5 1 1 34.04 66.97 40.39 o -4 1 1 2851.38 4093.26 541.77 o -3 1 1 98.75 140.04 43.10 o -2 1 1 4028.68 4480.47 95.20 o -1 1 1 3194.32 3163.74 41.94 o 0 1 1 79.98 20.58 52.70 o 1 1 1 4548.75 5883.79 171.02 o 2 1 1 3415.71 3943.24 78.96 o 3 1 1 72.22 85.56 20.42 o 4 1 1 4671.32 6023.99 99.65 o 5 1 1 889.20 1065.60 130.21 o 6 1 1 7.94 0.41 12.37 o 7 1 1 819.60 825.18 75.21 o 8 1 1 207.93 335.40 54.51 o 9 1 1 256.01 394.73 143.74 o 10 1 1 0.12 177.95 136.85 o -13 2 1 9.33 50.86 119.90 o -12 2 1 84.29 121.63 95.79 o -10 2 1 514.25 1099.84 142.78 o -9 2 1 554.84 701.34 66.48 o -8 2 1 384.39 516.60 75.77 o -7 2 1 0.42 12.94 10.57 o -6 2 1 393.26 603.05 71.66 o -5 2 1 444.89 604.21 37.54 o -4 2 1 129.84 238.80 49.60 o -3 2 1 687.34 710.87 32.39 o -2 2 1 228.89 318.91 82.30 o -1 2 1 281.44 272.26 69.56 o 0 2 1 4720.68 4048.46 72.42 o 1 2 1 11957.75 14314.91 496.96 o 2 2 1 1018.64 1323.14 215.78 o 3 2 1 8193.30 11395.66 188.55 o 4 2 1 17.27 58.78 23.87 o 6 2 1 19.32 20.07 11.37 o 7 2 1 16.97 26.36 14.54 o 8 2 1 1151.55 1447.75 126.61 o 9 2 1 0.83 151.89 64.89 o 10 2 1 0.25 111.94 98.63 o 11 2 1 246.47 146.36 91.93 o 12 2 1 128.06 71.03 105.96 o -14 3 1 1.93 -33.05 96.27 o -13 3 1 22.78 113.11 109.97 o -12 3 1 0.61 36.40 55.76 o -10 3 1 135.42 265.52 70.04 o -9 3 1 717.00 1403.25 144.92 o -8 3 1 49.71 44.13 14.15 o -7 3 1 471.57 853.82 79.42 o -6 3 1 1201.68 2205.09 165.80 o -5 3 1 150.34 77.11 29.71 o -4 3 1 459.41 412.81 37.83 o -3 3 1 393.81 476.08 96.01 o -2 3 1 4757.75 5635.80 202.58 o -1 3 1 2368.50 2521.66 65.40 o 0 3 1 31.50 64.15 33.14 o 1 3 1 1205.50 1405.58 110.12 o 2 3 1 198.29 246.47 49.00 o 3 3 1 88.88 180.87 38.50 o 4 3 1 220.90 392.66 63.88 o 5 3 1 1923.51 3345.12 285.42 o 6 3 1 5.58 15.40 13.65 o 8 3 1 7.06 24.11 53.51 o 9 3 1 1132.94 1778.18 142.96 o 10 3 1 91.03 307.80 108.22 o 11 3 1 90.74 137.63 60.40 o 12 3 1 501.47 383.05 109.65 o 13 3 1 4.27 133.45 127.29 o -13 4 1 0.33 43.78 59.02 o -12 4 1 88.99 264.25 47.42 o -11 4 1 85.19 6.75 42.37 o -10 4 1 29.00 7.65 44.73 o -9 4 1 0.16 11.70 14.49 o -8 4 1 19.70 23.52 24.83 o -7 4 1 0.49 -17.48 20.45 o -6 4 1 744.90 1258.19 127.19 o -5 4 1 0.00 28.49 17.56 o -4 4 1 0.01 -25.79 25.79 o -3 4 1 95.56 165.61 49.39 o -2 4 1 3.21 25.24 35.97 o -1 4 1 906.23 889.46 50.82 o 0 4 1 406.53 462.96 103.52 o 1 4 1 790.31 710.57 58.33 o 2 4 1 9.92 44.11 39.60 o 3 4 1 770.58 2219.20 122.71 o 4 4 1 43.77 35.93 38.86 o 5 4 1 36.52 55.15 59.99 o 6 4 1 36.51 63.54 17.56 o 7 4 1 186.15 238.08 51.47 o 8 4 1 931.54 1553.95 163.78 o 9 4 1 36.51 36.30 32.15 o 10 4 1 52.46 229.33 85.23 o 12 4 1 3.99 54.39 49.82 o 13 4 1 31.92 41.70 62.56 o -12 5 1 6.42 102.85 71.17 o -11 5 1 18.17 39.60 47.88 o -10 5 1 295.83 564.93 180.28 o -9 5 1 473.97 781.59 58.32 o -8 5 1 2024.51 4380.55 156.91 o -7 5 1 11.61 23.67 34.57 o -6 5 1 1212.32 2097.75 155.26 o -5 5 1 0.67 -5.95 28.31 o -4 5 1 1342.05 1373.01 117.10 o -3 5 1 1124.51 1670.90 142.64 o -1 5 1 1737.96 1570.70 55.33 o 0 5 1 524.63 545.91 83.57 o 1 5 1 2002.51 2094.25 100.26 o 2 5 1 0.02 -6.20 25.23 o 3 5 1 1041.42 1449.62 186.34 o 4 5 1 29.44 1.55 28.70 o 6 5 1 81.82 97.21 38.70 o 7 5 1 75.42 74.43 48.54 o 8 5 1 710.89 1035.24 81.13 o 9 5 1 300.47 604.19 111.92 o 11 5 1 3.61 8.56 51.13 o 12 5 1 40.15 -0.39 42.76 o -12 6 1 0.10 -46.06 46.06 o -11 6 1 122.89 71.50 46.59 o -10 6 1 4.38 -6.37 36.85 o -9 6 1 43.31 28.62 40.88 o -7 6 1 147.66 72.63 62.04 o -6 6 1 80.06 138.51 55.43 o -5 6 1 418.39 278.25 74.86 o -4 6 1 255.12 264.95 73.10 o -3 6 1 662.73 801.83 109.96 o -2 6 1 291.72 234.75 48.02 o -1 6 1 77.26 61.41 28.22 o 0 6 1 1657.00 1705.45 103.74 o 1 6 1 110.17 119.62 35.65 o 2 6 1 299.20 295.94 81.51 o 3 6 1 2091.70 2340.07 207.18 o 4 6 1 159.82 138.34 67.96 o 5 6 1 983.09 1242.51 123.94 o 6 6 1 167.07 93.96 31.83 o 7 6 1 120.29 150.02 44.49 o 8 6 1 37.75 94.59 39.90 o 9 6 1 45.74 60.48 39.86 o 10 6 1 11.75 5.71 11.49 o 11 6 1 79.87 23.22 48.76 o 12 6 1 63.40 4.03 45.18 o -11 7 1 1.29 -7.50 35.55 o -10 7 1 0.86 -0.38 34.10 o -9 7 1 2.80 472.44 47.04 o -8 7 1 12.65 80.14 53.49 o -7 7 1 153.89 86.65 45.53 o -6 7 1 0.07 216.23 37.56 o -5 7 1 88.65 320.21 67.95 o -4 7 1 828.08 798.52 148.82 o -3 7 1 1256.41 1654.16 116.93 o -2 7 1 58.65 128.15 25.64 o -1 7 1 120.72 134.76 24.10 o 0 7 1 60.93 50.19 16.59 o 1 7 1 433.58 472.84 183.78 o 2 7 1 10.69 41.40 90.83 o 3 7 1 47.18 99.79 28.31 o 4 7 1 27.39 392.47 110.68 o 5 7 1 0.62 38.13 20.72 o 7 7 1 93.86 126.00 28.17 o 8 7 1 0.39 29.21 59.10 o 9 7 1 131.20 111.57 115.10 o 10 7 1 39.20 40.50 16.52 o 11 7 1 71.71 36.25 36.96 o -10 8 1 1.26 37.31 23.04 o -9 8 1 8.35 -10.09 41.66 o -8 8 1 269.20 377.59 96.74 o -7 8 1 14.88 49.13 57.93 o -6 8 1 687.61 649.83 183.96 o -5 8 1 256.45 411.31 72.57 o -4 8 1 28.46 39.60 78.29 o -3 8 1 2.05 33.16 24.40 o -2 8 1 8.43 9.06 23.90 o -1 8 1 9.17 43.20 18.64 o 0 8 1 86.73 174.44 32.06 o 1 8 1 124.96 81.04 19.30 o 2 8 1 137.72 164.52 30.75 o 3 8 1 919.78 1019.73 152.12 o 4 8 1 11.48 83.58 52.82 o 5 8 1 34.76 77.25 33.85 o 6 8 1 5.77 137.24 64.27 o 7 8 1 258.67 80.05 49.51 o 8 8 1 31.97 44.70 37.91 o 9 8 1 43.79 30.17 39.26 o -8 9 1 41.88 39.59 41.17 o -7 9 1 91.57 231.66 78.82 o -6 9 1 10.26 4.40 12.59 o -5 9 1 17.96 10.12 22.76 o -4 9 1 50.00 83.10 78.14 o -3 9 1 5.53 62.61 26.03 o -2 9 1 1141.03 686.33 136.35 o -1 9 1 103.29 140.84 31.49 o 0 9 1 51.57 53.64 15.78 o 1 9 1 96.65 87.21 54.26 o 2 9 1 416.11 455.28 82.76 o 3 9 1 443.15 390.13 87.35 o 4 9 1 2.05 91.45 20.97 o 5 9 1 152.12 176.70 31.72 o 6 9 1 127.20 124.05 54.64 o 7 9 1 127.77 69.32 37.76 o 8 9 1 17.91 62.56 27.72 o -6 10 1 126.50 136.97 43.72 o -5 10 1 5.15 -11.65 11.65 o -4 10 1 8.76 95.93 26.77 o -3 10 1 16.69 50.53 31.16 o -2 10 1 214.62 189.84 40.37 o -1 10 1 22.14 73.45 23.88 o 0 10 1 102.91 125.16 23.38 o 1 10 1 291.35 281.42 97.64 o 2 10 1 7.57 44.32 20.82 o 3 10 1 135.80 149.34 68.08 o 4 10 1 17.75 -18.76 41.10 o 5 10 1 26.58 48.69 16.56 o 6 10 1 75.94 104.98 39.68 o 0 11 1 74.87 98.70 28.14 o -7 0 2 7.06 5.03 8.36 o -6 0 2 37.98 79.98 84.26 o -5 0 2 26341.74 38721.89 143.23 o -4 0 2 286.30 220.43 54.96 o -3 0 2 5383.68 6266.84 113.61 o -2 0 2 2941.44 2631.53 91.41 o -1 0 2 5459.86 5381.66 85.85 o 0 0 2 4790.05 3619.76 59.80 o 1 0 2 14995.38 17862.66 278.34 o 2 0 2 4124.14 4557.56 170.46 o 3 0 2 2548.14 2960.48 201.00 o 4 0 2 158.55 142.85 29.11 o 5 0 2 1401.51 1195.54 115.38 o 6 0 2 695.13 574.58 29.83 o 7 0 2 0.18 -6.31 13.93 o 8 0 2 401.05 550.04 40.32 o -11 1 2 9.56 162.13 167.27 o -10 1 2 168.56 280.19 122.81 o -9 1 2 92.73 109.03 62.17 o -8 1 2 932.28 1314.66 145.27 o -7 1 2 288.29 385.30 49.18 o -6 1 2 15.67 19.14 16.47 o -5 1 2 3023.24 3925.53 96.17 o -4 1 2 413.93 462.96 40.14 o -3 1 2 988.26 1265.40 53.34 o -2 1 2 812.41 746.16 38.36 o -1 1 2 196.84 290.42 23.50 o 0 1 2 805.06 781.85 69.54 o 1 1 2 3071.12 3475.06 128.82 o 2 1 2 2386.73 2394.05 131.55 o 4 1 2 2371.66 2570.01 46.82 o 5 1 2 3.16 21.85 7.99 o 6 1 2 2583.69 2462.16 88.62 o 7 1 2 1993.29 2314.75 186.84 o 8 1 2 623.75 670.85 58.70 o 9 1 2 545.32 651.68 154.84 o -13 2 2 6.61 -26.70 101.31 o -12 2 2 16.41 26.68 94.50 o -11 2 2 62.40 220.07 95.87 o -10 2 2 554.11 895.23 165.34 o -9 2 2 15.91 148.32 46.39 o -8 2 2 106.81 100.66 66.06 o -7 2 2 1.13 1.11 10.56 o -6 2 2 376.06 399.02 51.51 o -5 2 2 96.89 90.70 41.56 o -4 2 2 366.86 737.37 52.08 o -3 2 2 461.03 416.89 29.08 o -2 2 2 349.66 229.38 21.52 o -1 2 2 20355.50 19283.43 585.73 o 0 2 2 9906.11 9851.31 209.43 o 1 2 2 585.34 647.93 30.25 o 2 2 2 23.00 27.76 25.20 o 3 2 2 368.94 469.83 51.64 o 4 2 2 2506.24 3394.31 292.89 o 5 2 2 69.08 75.44 19.98 o 7 2 2 35.44 29.95 15.20 o 8 2 2 294.37 640.79 242.78 o 9 2 2 46.19 40.28 44.60 o 10 2 2 376.93 285.39 95.90 o 11 2 2 63.57 -1.69 80.57 o 12 2 2 1.32 -1.26 110.73 o -14 3 2 95.47 54.94 96.03 o -13 3 2 103.08 37.55 63.45 o -12 3 2 143.26 135.25 80.39 o -11 3 2 20.52 52.83 46.26 o -10 3 2 129.74 221.90 72.51 o -9 3 2 32.71 85.96 47.70 o -8 3 2 216.07 249.30 36.05 o -7 3 2 0.05 59.21 93.60 o -6 3 2 7.98 18.76 34.34 o -5 3 2 3272.05 3966.49 170.62 o -4 3 2 48.08 38.85 26.19 o -3 3 2 938.44 1190.97 54.67 o -2 3 2 275.97 342.34 147.07 o -1 3 2 239.80 286.56 45.24 o 0 3 2 3772.88 3788.09 80.30 o 1 3 2 4090.12 4486.23 79.91 o 2 3 2 674.88 824.65 49.39 o 3 3 2 2262.32 3190.13 102.24 o 4 3 2 2386.43 3527.05 218.12 o 5 3 2 2.99 40.53 13.91 o 6 3 2 1322.06 1889.48 226.45 o 7 3 2 103.36 145.45 54.58 o 8 3 2 1140.14 1162.15 86.12 o 10 3 2 39.28 10.25 61.29 o 11 3 2 0.03 8.82 61.02 o 12 3 2 622.93 261.89 86.24 o 13 3 2 234.46 277.84 174.98 o -13 4 2 1.87 32.51 56.93 o -11 4 2 42.60 99.79 45.59 o -10 4 2 280.32 309.23 54.89 o -9 4 2 347.20 384.69 44.28 o -8 4 2 992.31 1935.72 72.25 o -7 4 2 13.64 -5.76 21.59 o -6 4 2 1139.83 1886.16 176.92 o -5 4 2 18.91 -11.51 25.90 o -4 4 2 495.49 533.62 161.00 o -3 4 2 8033.28 8669.22 210.73 o -2 4 2 189.29 121.79 52.97 o -1 4 2 380.53 324.42 49.45 o 0 4 2 1339.81 1052.24 91.15 o 1 4 2 43.83 58.79 17.51 o 2 4 2 126.38 71.42 30.40 o 3 4 2 5833.67 7802.18 134.38 o 4 4 2 122.69 132.57 47.21 o 5 4 2 0.45 -8.78 22.67 o 6 4 2 1107.49 1903.90 185.91 o 7 4 2 591.95 905.34 85.39 o 8 4 2 1874.89 2704.49 283.28 o 9 4 2 20.00 26.37 43.18 o 10 4 2 11.13 50.43 56.68 o 12 4 2 74.48 140.05 79.00 o 13 4 2 11.64 18.71 59.86 o -13 5 2 0.30 2.68 47.45 o -12 5 2 50.64 9.09 42.38 o -11 5 2 45.20 -29.31 45.11 o -10 5 2 12.25 1.47 33.35 o -9 5 2 6.58 26.53 22.68 o -8 5 2 25.03 119.42 46.56 o -7 5 2 1352.10 2315.19 126.18 o -5 5 2 130.33 144.08 42.67 o -4 5 2 1586.89 1816.01 151.77 o -3 5 2 49.81 58.45 24.85 o -2 5 2 62.71 49.90 17.87 o -1 5 2 305.17 386.78 78.65 o 0 5 2 15.24 -12.04 22.59 o 1 5 2 36.96 -28.10 28.10 o 2 5 2 64.58 60.71 21.30 o 3 5 2 267.27 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