#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/88/2018841.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018841_Fobs loop_ _publ_author_name 'Degtyarenko, Anna S.' 'Domasevitch, Konstantin V.' _publ_section_title ; Cadmium(II) iodide and thiocyanate complexes adopted by polycyclic 1,4-bis(pyridazin-4-yl)benzene: interplay of coordination and \p--\p stacking interactions ; _journal_coeditor_code TP3018 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 219 _journal_page_last 224 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 88.980 _cell_angle_beta 75.434 _cell_angle_gamma 87.049 _cell_length_a 5.9018 _cell_length_b 7.6619 _cell_length_c 9.2433 _exptl_crystal_F_000 228.00 _reflns_d_resolution_high 0.7400 _[local]_cod_data_source_file tp3018IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' ip305 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 147.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2396.27 2342.23 207.72 o 2 0 0 232.28 219.53 6.53 o 3 0 0 409.68 421.87 12.49 o 4 0 0 1286.16 1309.23 23.80 o 5 0 0 695.13 681.03 12.62 o 6 0 0 464.47 453.12 6.86 o 7 0 0 4.15 3.60 2.56 o -7 1 0 217.74 218.10 3.65 o -6 1 0 514.97 501.83 10.46 o -5 1 0 2317.59 2280.81 27.34 o -4 1 0 191.98 192.50 4.16 o -3 1 0 514.00 509.47 11.99 o -2 1 0 2830.94 2814.78 68.45 o -1 1 0 5585.33 5511.96 18.95 o 0 1 0 2245.05 2240.96 12.55 o 1 1 0 2755.52 2507.64 12.65 o 2 1 0 410.98 394.34 10.15 o 3 1 0 2240.60 2249.90 68.08 o 4 1 0 1504.36 1520.25 27.92 o 5 1 0 35.14 42.15 2.83 o 6 1 0 1.27 1.82 2.16 o 7 1 0 203.10 203.83 12.38 o -7 2 0 273.74 283.26 6.54 o -6 2 0 182.59 172.06 2.18 o -5 2 0 321.81 320.59 7.48 o -4 2 0 1404.47 1394.48 37.97 o -3 2 0 1845.96 1857.33 28.17 o -2 2 0 1579.25 1587.22 9.65 o -1 2 0 793.37 743.18 5.29 o 0 2 0 39.69 38.08 2.34 o 1 2 0 38.18 29.14 2.31 o 2 2 0 2392.33 2462.67 91.20 o 3 2 0 1699.67 1781.42 53.45 o 4 2 0 326.20 333.98 5.15 o 5 2 0 74.59 74.70 1.83 o 6 2 0 473.94 466.99 7.02 o 7 2 0 115.08 114.01 2.62 o -7 3 0 16.30 18.17 2.38 o -6 3 0 87.09 86.50 2.19 o -5 3 0 683.01 666.47 8.89 o -4 3 0 416.12 410.25 6.01 o -3 3 0 338.60 360.08 9.86 o -2 3 0 476.92 486.27 15.86 o -1 3 0 1552.89 1586.34 18.79 o 0 3 0 720.02 709.24 9.05 o 1 3 0 2705.50 2981.23 88.56 o 2 3 0 26.05 41.24 2.00 o 3 3 0 421.18 465.86 17.46 o 4 3 0 639.41 674.13 13.02 o 5 3 0 569.10 548.60 13.71 o 6 3 0 148.66 155.73 2.79 o 7 3 0 145.29 147.08 3.34 o -6 4 0 514.17 548.44 9.35 o -5 4 0 149.78 149.22 3.19 o -4 4 0 142.75 136.63 1.93 o -3 4 0 112.15 103.16 2.87 o -2 4 0 1281.04 1265.04 36.83 o -1 4 0 3504.11 3755.53 103.79 o 0 4 0 767.72 815.15 16.58 o 1 4 0 9.22 10.74 1.88 o 2 4 0 906.39 1027.76 13.28 o 3 4 0 232.84 235.71 3.97 o 4 4 0 480.28 470.58 7.08 o 5 4 0 139.93 144.64 2.07 o 6 4 0 0.42 -0.34 2.46 o 7 4 0 32.14 30.68 3.07 o -6 5 0 354.27 374.06 4.23 o -5 5 0 8.62 9.67 2.20 o -4 5 0 39.49 40.42 2.26 o -3 5 0 1032.91 1036.17 23.18 o -2 5 0 718.00 698.39 22.02 o -1 5 0 240.54 245.13 3.28 o 0 5 0 105.84 111.95 4.20 o 1 5 0 103.39 105.78 2.57 o 2 5 0 901.74 918.62 4.41 o 3 5 0 581.10 601.96 15.29 o 4 5 0 5.18 4.37 1.62 o 5 5 0 0.24 0.51 2.10 o 6 5 0 86.98 90.75 2.21 o -6 6 0 14.22 14.59 3.08 o -5 6 0 188.14 189.59 2.54 o -4 6 0 413.25 407.74 8.71 o -3 6 0 497.33 494.92 14.13 o -2 6 0 148.32 144.99 2.36 o -1 6 0 3.48 4.06 2.12 o 0 6 0 162.78 162.35 2.87 o 1 6 0 553.03 546.46 20.28 o 2 6 0 359.16 364.90 6.65 o 3 6 0 2.68 2.56 2.06 o 4 6 0 115.63 119.50 3.37 o 5 6 0 172.42 172.40 4.99 o 6 6 0 159.66 164.61 2.53 o -5 7 0 147.59 150.25 2.97 o -4 7 0 67.63 69.19 2.73 o -3 7 0 98.21 97.21 2.27 o -2 7 0 11.70 10.42 2.63 o -1 7 0 502.57 501.25 3.91 o 0 7 0 402.98 407.96 6.04 o 1 7 0 88.43 95.65 4.24 o 2 7 0 29.21 32.22 2.60 o 3 7 0 319.23 351.79 19.64 o 4 7 0 119.91 123.80 3.84 o 5 7 0 182.66 188.27 2.99 o -4 8 0 3.65 4.82 3.06 o -3 8 0 138.69 146.78 3.56 o -2 8 0 482.78 514.68 4.62 o -1 8 0 100.39 98.50 5.71 o 0 8 0 77.49 76.92 2.49 o 1 8 0 160.93 163.77 7.35 o 2 8 0 142.09 153.87 3.17 o 3 8 0 398.36 389.24 16.65 o 4 8 0 120.63 116.54 3.87 o 5 8 0 0.41 0.38 2.92 o -3 9 0 147.48 160.74 4.23 o -2 9 0 171.78 183.01 5.99 o -1 9 0 55.39 55.31 7.03 o 0 9 0 53.09 59.40 3.52 o 1 9 0 158.38 170.89 3.70 o 2 9 0 174.46 183.07 5.50 o 3 9 0 19.94 20.53 2.26 o 4 9 0 9.06 9.41 2.91 o -1 10 0 81.89 86.32 4.27 o 0 10 0 168.30 178.83 4.43 o 1 10 0 25.70 27.53 3.72 o 2 10 0 3.60 3.99 3.58 o -2 -10 1 44.15 36.80 4.39 o -1 -10 1 109.83 109.89 4.03 o 0 -10 1 154.59 163.34 4.21 o 1 -10 1 6.93 6.08 3.73 o -3 -9 1 19.65 17.66 2.94 o -2 -9 1 67.98 71.30 2.77 o -1 -9 1 288.77 298.24 5.41 o 0 -9 1 72.82 73.48 2.78 o 1 -9 1 1.13 2.61 2.16 o 2 -9 1 71.26 77.37 3.44 o 3 -9 1 150.05 150.27 3.53 o -4 -8 1 31.51 34.10 2.02 o -3 -8 1 148.89 155.09 5.85 o -2 -8 1 75.89 75.15 2.66 o -1 -8 1 11.17 9.46 2.12 o 0 -8 1 62.20 59.91 2.84 o 1 -8 1 295.33 299.73 4.26 o 2 -8 1 447.25 434.15 5.26 o 3 -8 1 166.56 164.33 9.12 o 4 -8 1 54.11 56.20 3.08 o -5 -7 1 127.20 129.02 3.19 o -4 -7 1 189.97 198.89 2.45 o -3 -7 1 118.28 122.54 3.00 o -2 -7 1 26.31 26.30 1.91 o -1 -7 1 329.07 342.21 14.92 o 0 -7 1 476.18 506.61 8.59 o 1 -7 1 577.46 599.35 25.60 o 2 -7 1 137.26 140.37 2.96 o 3 -7 1 242.46 247.51 3.67 o 4 -7 1 186.90 181.33 3.34 o 5 -7 1 538.53 579.93 7.42 o -6 -6 1 206.44 203.92 2.62 o -5 -6 1 85.10 86.33 2.00 o -4 -6 1 34.41 32.19 1.91 o -3 -6 1 150.48 162.59 3.02 o -2 -6 1 957.49 989.94 5.87 o -1 -6 1 709.72 773.99 15.35 o 0 -6 1 957.16 978.64 4.59 o 1 -6 1 130.41 131.13 5.19 o 2 -6 1 105.13 108.61 2.17 o 3 -6 1 816.80 840.42 11.20 o 4 -6 1 524.58 513.41 3.64 o 5 -6 1 60.15 54.29 2.16 o 6 -6 1 26.87 22.29 2.44 o -6 -5 1 63.44 64.22 2.15 o -5 -5 1 95.12 94.09 1.91 o -4 -5 1 228.32 239.48 2.61 o -3 -5 1 459.85 472.56 6.02 o -2 -5 1 1642.90 1698.19 26.24 o -1 -5 1 269.71 275.39 3.65 o 0 -5 1 57.06 64.14 2.33 o 1 -5 1 637.66 647.38 21.86 o 2 -5 1 981.51 936.63 9.44 o 3 -5 1 380.74 388.03 5.13 o 4 -5 1 209.35 211.82 2.79 o 5 -5 1 21.69 20.63 1.96 o 6 -5 1 107.55 100.84 2.41 o -7 -4 1 123.21 126.91 5.89 o -6 -4 1 31.59 30.07 2.22 o -5 -4 1 243.20 246.86 7.64 o -4 -4 1 827.72 811.43 18.63 o -3 -4 1 496.56 509.65 18.98 o -2 -4 1 18.11 16.34 1.82 o -1 -4 1 426.93 455.91 4.64 o 0 -4 1 953.28 1007.30 4.94 o 1 -4 1 527.28 500.54 5.19 o 2 -4 1 408.92 387.78 10.82 o 3 -4 1 68.50 64.60 2.17 o 4 -4 1 464.78 467.77 3.41 o 5 -4 1 497.99 491.54 11.01 o 6 -4 1 452.00 456.48 7.48 o 7 -4 1 48.55 48.02 2.70 o -7 -3 1 25.34 25.88 3.04 o -6 -3 1 254.78 250.24 2.40 o -5 -3 1 458.29 453.99 10.76 o -4 -3 1 28.20 24.18 1.82 o -3 -3 1 19.36 16.92 1.40 o -2 -3 1 374.62 386.49 9.85 o -1 -3 1 2775.97 2944.26 219.78 o 0 -3 1 947.03 952.11 6.04 o 1 -3 1 467.39 471.28 7.09 o 2 -3 1 48.28 40.53 1.78 o 3 -3 1 727.18 699.94 8.80 o 4 -3 1 1413.18 1377.02 16.44 o 5 -3 1 284.30 279.88 8.36 o 6 -3 1 24.33 24.78 2.56 o 7 -3 1 176.79 189.02 4.18 o -7 -2 1 246.08 240.80 4.16 o -6 -2 1 237.73 248.76 3.00 o -5 -2 1 8.49 10.69 2.07 o -4 -2 1 75.98 81.31 7.50 o -3 -2 1 549.17 527.32 11.19 o -2 -2 1 1209.42 1177.95 22.77 o -1 -2 1 3840.73 3481.61 15.49 o 0 -2 1 20.90 41.97 12.06 o 1 -2 1 373.01 368.34 13.81 o 2 -2 1 5120.51 5097.85 16.26 o 3 -2 1 2185.89 2204.94 40.94 o 4 -2 1 1.13 2.41 1.85 o 5 -2 1 33.50 33.88 1.94 o 6 -2 1 34.59 34.37 1.97 o 7 -2 1 454.77 470.89 10.69 o -7 -1 1 10.21 9.90 2.57 o -6 -1 1 220.85 220.01 5.34 o -5 -1 1 69.49 70.21 2.24 o -4 -1 1 1014.17 998.60 35.56 o -3 -1 1 2693.56 2768.89 101.71 o -2 -1 1 1071.88 1094.19 25.22 o -1 -1 1 492.95 483.17 4.69 o 0 -1 1 2003.33 1820.40 9.09 o 1 -1 1 1262.50 1317.14 33.00 o 2 -1 1 3452.18 3483.36 66.09 o 3 -1 1 1047.58 1062.82 29.19 o 4 -1 1 4.74 20.25 4.31 o 5 -1 1 251.06 236.59 2.75 o 6 -1 1 711.06 690.96 17.87 o 7 -1 1 198.47 206.06 4.24 o -7 0 1 53.22 55.15 3.08 o -6 0 1 105.49 105.79 2.88 o -5 0 1 1004.14 972.19 33.89 o -4 0 1 497.52 507.75 9.90 o -3 0 1 609.89 656.46 19.75 o -2 0 1 2170.61 2232.70 52.73 o -1 0 1 1092.22 1057.84 23.92 o 0 0 1 632.40 577.87 6.36 o 1 0 1 769.24 801.11 15.48 o 2 0 1 455.78 403.24 9.34 o 3 0 1 391.63 394.96 10.07 o 4 0 1 1599.98 1587.45 54.08 o 5 0 1 1438.88 1439.39 38.01 o 6 0 1 429.17 421.21 6.88 o 7 0 1 60.45 57.12 2.27 o -7 1 1 516.72 517.13 22.52 o -6 1 1 449.13 416.40 9.14 o -5 1 1 30.11 30.63 2.26 o -4 1 1 21.03 24.92 1.46 o -3 1 1 1018.97 1095.81 29.41 o -2 1 1 3066.32 3102.20 88.87 o -1 1 1 2373.49 2322.61 9.78 o 0 1 1 3251.26 3204.88 10.59 o 1 1 1 777.86 770.71 31.62 o 2 1 1 2602.05 2580.26 75.86 o 3 1 1 2161.09 2145.97 52.15 o 4 1 1 832.42 801.88 16.79 o 5 1 1 216.27 222.56 2.99 o 6 1 1 839.20 816.92 10.15 o 7 1 1 196.28 189.43 7.21 o -7 2 1 302.10 292.44 3.40 o -6 2 1 25.51 24.10 1.85 o -5 2 1 303.39 289.67 6.45 o -4 2 1 451.95 458.73 8.72 o -3 2 1 2292.87 2253.02 48.04 o -2 2 1 1122.13 1136.77 20.25 o -1 2 1 167.19 157.48 3.13 o 0 2 1 1229.28 1217.32 8.37 o 1 2 1 21898.22 20790.16 85.81 o 2 2 1 2252.83 2279.77 46.23 o 3 2 1 510.91 503.41 11.96 o 4 2 1 149.40 147.51 1.72 o 5 2 1 236.34 227.59 8.30 o 6 2 1 421.31 418.78 3.70 o 7 2 1 378.18 382.84 4.05 o -7 3 1 32.78 30.28 2.24 o -6 3 1 82.24 77.12 2.19 o -5 3 1 612.45 608.23 10.46 o -4 3 1 3549.11 3445.86 56.73 o -3 3 1 391.65 387.63 5.57 o -2 3 1 158.34 154.98 6.56 o -1 3 1 1199.68 1159.37 34.10 o 0 3 1 2886.55 2894.37 14.05 o 1 3 1 3176.97 3453.67 15.69 o 2 3 1 1277.73 1381.00 48.71 o 3 3 1 20.87 22.58 1.58 o 4 3 1 611.59 608.52 13.87 o 5 3 1 991.92 988.37 21.66 o 6 3 1 59.21 57.76 2.36 o 7 3 1 0.23 0.54 2.62 o -6 4 1 414.29 428.54 3.11 o -5 4 1 384.67 389.85 10.55 o -4 4 1 373.69 360.26 5.85 o -3 4 1 713.02 691.70 8.34 o -2 4 1 747.64 740.24 4.19 o -1 4 1 1700.48 1671.45 6.87 o 0 4 1 1156.02 1215.22 41.51 o 1 4 1 2.38 5.86 2.92 o 2 4 1 0.83 3.20 2.26 o 3 4 1 1038.19 1045.14 17.51 o 4 4 1 928.08 973.96 19.89 o 5 4 1 253.82 253.99 2.22 o 6 4 1 9.97 10.15 1.77 o 7 4 1 91.91 91.75 4.08 o -6 5 1 70.35 77.37 2.82 o -5 5 1 45.17 42.13 2.10 o -4 5 1 233.51 231.18 4.46 o -3 5 1 223.76 220.69 4.44 o -2 5 1 799.47 769.87 12.32 o -1 5 1 336.72 358.96 13.27 o 0 5 1 376.98 376.60 6.30 o 1 5 1 138.48 133.94 3.15 o 2 5 1 1061.43 1066.31 47.15 o 3 5 1 53.59 51.12 1.96 o 4 5 1 228.84 241.25 4.36 o 5 5 1 77.31 80.28 3.30 o 6 5 1 124.81 130.17 2.83 o 7 5 1 107.71 109.73 6.56 o -5 6 1 246.06 259.07 2.88 o -4 6 1 182.21 183.40 2.85 o -3 6 1 271.24 267.58 5.15 o -2 6 1 83.87 79.46 2.41 o -1 6 1 352.54 366.95 11.99 o 0 6 1 1056.16 1098.61 24.79 o 1 6 1 523.57 523.28 4.28 o 2 6 1 119.55 126.36 4.82 o 3 6 1 184.72 191.03 2.28 o 4 6 1 5.84 7.31 1.50 o 5 6 1 147.29 150.36 2.21 o 6 6 1 107.21 117.65 3.23 o -5 7 1 388.57 407.54 5.91 o -4 7 1 21.65 23.78 2.07 o -3 7 1 3.13 4.12 2.62 o -2 7 1 315.31 320.20 7.97 o -1 7 1 280.64 275.23 3.45 o 0 7 1 293.84 312.57 13.90 o 1 7 1 68.54 71.87 2.82 o 2 7 1 0.24 0.68 2.03 o 3 7 1 160.11 170.67 2.68 o 4 7 1 265.09 272.23 6.77 o 5 7 1 8.24 9.53 2.57 o 6 7 1 0.56 3.19 2.56 o -4 8 1 38.20 39.15 3.22 o -3 8 1 115.50 121.52 3.55 o -2 8 1 297.26 296.10 16.95 o -1 8 1 218.36 220.10 3.65 o 0 8 1 11.68 10.20 2.65 o 1 8 1 11.18 13.23 2.19 o 2 8 1 123.67 123.71 3.14 o 3 8 1 162.43 175.27 3.01 o 4 8 1 0.30 -0.02 2.49 o 5 8 1 32.35 26.36 2.65 o -3 9 1 80.36 81.82 3.47 o -2 9 1 67.28 73.62 4.00 o -1 9 1 8.53 7.16 3.22 o 0 9 1 120.88 125.35 5.17 o 1 9 1 114.95 121.27 3.60 o 2 9 1 81.49 80.13 2.88 o 3 9 1 14.04 14.98 2.85 o 4 9 1 37.96 34.06 2.62 o -1 10 1 119.34 124.88 4.42 o 0 10 1 43.94 45.33 4.01 o 1 10 1 71.57 72.27 4.31 o 2 10 1 31.38 31.08 3.72 o -1 -10 2 4.81 7.91 3.63 o 0 -10 2 20.58 20.63 3.04 o 1 -10 2 43.90 46.34 3.80 o -3 -9 2 72.45 70.51 3.35 o -2 -9 2 117.05 116.35 2.62 o -1 -9 2 35.81 35.97 2.60 o 0 -9 2 12.52 12.73 2.50 o 1 -9 2 1.01 0.69 2.16 o 2 -9 2 183.33 186.80 2.88 o 3 -9 2 115.73 120.27 3.36 o -4 -8 2 33.16 32.30 2.93 o -3 -8 2 284.83 288.18 3.93 o -2 -8 2 21.03 21.55 2.48 o -1 -8 2 85.10 89.82 2.85 o 0 -8 2 145.53 146.67 2.37 o 1 -8 2 433.66 442.11 6.97 o 2 -8 2 85.90 89.22 3.44 o 3 -8 2 42.11 46.04 3.19 o 4 -8 2 0.28 1.32 2.94 o -5 -7 2 160.63 162.68 3.79 o -4 -7 2 204.60 208.36 2.66 o -3 -7 2 10.35 9.74 2.17 o -2 -7 2 11.46 11.24 2.12 o -1 -7 2 133.13 137.07 2.63 o 0 -7 2 983.80 1011.51 37.77 o 1 -7 2 403.10 418.89 3.69 o 2 -7 2 14.81 16.99 1.83 o 3 -7 2 38.78 42.04 2.71 o 4 -7 2 210.14 219.22 8.95 o 5 -7 2 268.52 262.51 12.24 o -6 -6 2 114.39 107.80 4.02 o -5 -6 2 240.97 234.47 2.37 o -4 -6 2 93.86 96.85 2.66 o -3 -6 2 35.10 34.48 1.92 o -2 -6 2 351.32 362.57 3.64 o -1 -6 2 482.81 475.59 3.13 o 0 -6 2 188.38 178.88 5.53 o 1 -6 2 160.67 162.79 2.13 o 2 -6 2 217.68 215.20 3.64 o 3 -6 2 1052.91 1029.16 23.99 o 4 -6 2 563.39 562.51 3.94 o 5 -6 2 148.69 156.07 4.02 o 6 -6 2 44.76 46.40 2.21 o -6 -5 2 33.84 29.73 2.13 o -5 -5 2 18.41 17.12 1.78 o -4 -5 2 300.85 296.74 3.68 o -3 -5 2 463.42 475.78 8.19 o -2 -5 2 958.41 959.11 4.07 o -1 -5 2 150.85 152.79 2.17 o 0 -5 2 397.10 435.03 3.38 o 1 -5 2 709.53 718.72 13.59 o 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313.10 10.76 o 1 -1 9 569.47 520.58 3.56 o 2 -1 9 122.24 123.22 2.50 o 3 -1 9 273.42 271.83 3.27 o 4 -1 9 371.65 358.12 3.21 o 5 -1 9 257.68 254.17 4.97 o 6 -1 9 59.33 60.66 3.12 o -3 0 9 242.47 238.50 3.15 o -2 0 9 308.16 322.66 3.03 o -1 0 9 265.36 263.71 2.78 o 0 0 9 49.28 47.59 2.68 o 1 0 9 304.37 303.93 5.96 o 2 0 9 985.70 936.25 4.33 o 3 0 9 431.78 440.89 7.98 o 4 0 9 77.85 78.51 2.46 o 5 0 9 115.99 120.66 3.35 o 6 0 9 98.03 98.34 2.28 o -3 1 9 481.79 520.70 10.21 o -2 1 9 73.83 74.74 2.36 o -1 1 9 5.73 5.78 2.13 o 0 1 9 359.96 366.55 3.79 o 1 1 9 543.91 538.49 29.04 o 2 1 9 314.08 320.51 12.29 o 3 1 9 200.14 190.10 3.35 o 4 1 9 141.13 145.23 3.15 o 5 1 9 706.86 728.47 20.26 o 6 1 9 327.80 325.15 2.81 o -3 2 9 23.87 23.86 2.63 o -2 2 9 136.89 147.52 4.75 o -1 2 9 309.02 329.82 6.14 o 0 2 9 889.28 913.82 5.62 o 1 2 9 196.66 200.25 9.19 o 2 2 9 56.24 55.93 2.89 o 3 2 9 63.53 71.22 2.97 o 4 2 9 797.61 777.62 4.78 o 5 2 9 652.27 653.64 13.37 o 6 2 9 154.37 162.46 3.28 o -3 3 9 71.85 76.45 3.32 o -2 3 9 138.12 145.97 3.08 o -1 3 9 471.89 495.07 9.66 o 0 3 9 527.96 531.15 4.71 o 1 3 9 119.76 128.17 4.13 o 2 3 9 194.14 203.37 14.50 o 3 3 9 450.00 471.10 6.75 o 4 3 9 189.52 188.24 9.69 o 5 3 9 15.62 15.88 2.61 o 6 3 9 68.22 72.09 3.37 o -2 4 9 98.43 105.31 5.29 o -1 4 9 42.31 39.96 4.42 o 0 4 9 80.94 74.18 4.60 o 1 4 9 529.15 494.30 8.86 o 2 4 9 149.50 146.25 5.42 o 3 4 9 152.12 161.96 12.95 o 4 4 9 60.49 66.66 3.45 o 5 4 9 1.05 1.64 2.81 o 6 4 9 36.65 42.06 3.88 o -2 5 9 29.68 28.26 5.88 o -1 5 9 160.22 146.52 6.03 o 0 5 9 47.06 42.55 4.97 o 1 5 9 31.13 28.29 3.96 o 2 5 9 17.21 15.66 3.85 o 3 5 9 54.40 48.39 4.56 o 4 5 9 120.87 109.81 5.02 o 5 5 9 155.72 173.49 5.55 o -1 6 9 136.24 134.14 4.34 o 0 6 9 40.67 37.84 3.78 o 1 6 9 4.01 3.45 3.28 o 2 6 9 5.34 4.20 3.76 o 3 6 9 147.36 136.42 5.23 o 4 6 9 113.15 104.55 4.21 o 1 7 9 39.33 36.30 3.42 o 2 7 9 227.52 220.18 6.02 o 3 7 9 8.12 7.22 3.74 o 1 -6 10 305.85 291.52 12.03 o 2 -6 10 110.35 102.88 6.46 o -1 -5 10 116.03 113.28 2.85 o 0 -5 10 266.21 255.38 6.95 o 1 -5 10 197.05 192.76 3.87 o 2 -5 10 153.03 159.78 3.82 o 3 -5 10 168.69 175.56 8.30 o -1 -4 10 202.56 191.45 3.31 o 0 -4 10 96.68 91.59 3.93 o 1 -4 10 81.44 78.24 2.65 o 2 -4 10 190.59 193.11 6.85 o 3 -4 10 900.67 926.11 37.14 o 4 -4 10 347.35 362.91 3.78 o -2 -3 10 464.18 479.29 4.64 o -1 -3 10 54.83 53.00 2.68 o 0 -3 10 165.96 155.13 2.86 o 1 -3 10 272.17 269.31 8.47 o 2 -3 10 623.60 630.22 23.80 o 3 -3 10 121.11 108.59 2.45 o 4 -3 10 193.95 199.31 3.07 o 5 -3 10 29.98 31.01 3.09 o -2 -2 10 32.81 33.90 3.63 o -1 -2 10 261.52 260.94 3.24 o 0 -2 10 270.41 284.86 7.91 o 1 -2 10 454.11 466.29 3.56 o 2 -2 10 69.50 71.72 2.30 o 3 -2 10 28.86 27.71 2.57 o 4 -2 10 139.88 136.56 3.43 o 5 -2 10 268.08 270.76 6.33 o -2 -1 10 103.72 106.53 3.52 o -1 -1 10 323.71 310.38 3.35 o 0 -1 10 132.85 135.13 2.51 o 1 -1 10 10.15 14.83 2.16 o 2 -1 10 66.65 72.46 2.78 o 3 -1 10 228.59 234.83 3.58 o 4 -1 10 517.31 544.19 8.77 o 5 -1 10 100.01 93.56 4.70 o 6 -1 10 35.86 30.91 3.77 o -3 0 10 143.90 135.67 7.08 o -2 0 10 98.99 101.29 2.69 o -1 0 10 162.65 161.82 8.32 o 0 0 10 4.94 4.03 2.07 o 1 0 10 162.08 173.93 4.03 o 2 0 10 353.40 361.07 5.11 o 3 0 10 556.63 567.75 4.42 o 4 0 10 19.15 17.33 3.16 o 5 0 10 133.00 124.07 5.14 o 6 0 10 88.85 89.79 3.89 o -2 1 10 93.79 90.12 2.74 o -1 1 10 12.89 13.94 2.46 o 0 1 10 410.79 440.20 5.61 o 1 1 10 324.39 329.32 3.74 o 2 1 10 576.62 565.60 8.23 o 3 1 10 78.04 81.24 3.32 o 4 1 10 46.17 45.89 2.69 o 5 1 10 115.06 114.74 6.36 o 6 1 10 251.15 258.26 2.84 o -2 2 10 103.85 100.99 2.92 o -1 2 10 214.77 227.82 3.24 o 0 2 10 251.42 260.72 3.98 o 1 2 10 104.33 106.67 3.44 o 2 2 10 106.61 107.92 4.30 o 3 2 10 311.09 298.28 25.08 o 4 2 10 217.55 230.14 5.23 o 5 2 10 122.19 129.26 3.31 o 6 2 10 49.95 51.58 2.76 o -2 3 10 400.01 442.93 5.14 o -1 3 10 85.27 88.64 2.98 o 0 3 10 18.84 17.79 2.65 o 1 3 10 51.24 50.79 4.16 o 2 3 10 221.93 239.97 10.07 o 3 3 10 207.15 227.79 4.10 o 4 3 10 208.09 214.65 3.40 o 5 3 10 35.93 37.89 3.14 o -1 4 10 74.09 73.16 5.39 o 0 4 10 47.92 43.79 4.08 o 1 4 10 518.13 485.20 8.23 o 2 4 10 138.76 128.24 4.51 o 3 4 10 45.98 41.29 4.93 o 4 4 10 6.89 8.28 3.27 o 5 4 10 233.05 242.44 4.09 o -1 5 10 43.37 40.78 3.30 o 0 5 10 319.34 305.20 8.03 o 1 5 10 312.07 296.24 7.22 o 2 5 10 66.48 61.19 4.05 o 3 5 10 20.80 20.01 3.26 o 4 5 10 113.83 114.42 4.13 o 1 6 10 29.98 27.93 3.69 o 2 6 10 88.27 82.38 4.35 o 3 6 10 72.17 66.61 4.69 o 0 -4 11 176.96 168.99 3.35 o 1 -4 11 173.68 177.36 5.49 o 2 -4 11 201.32 190.85 3.04 o 3 -4 11 188.33 169.30 4.85 o -1 -3 11 37.59 33.03 2.64 o 0 -3 11 106.11 108.98 3.20 o 1 -3 11 199.55 195.60 3.37 o 2 -3 11 447.53 463.60 11.53 o 3 -3 11 239.55 257.46 3.54 o 4 -3 11 125.25 127.56 3.34 o -1 -2 11 158.35 163.98 3.96 o 0 -2 11 241.33 249.21 3.44 o 1 -2 11 288.46 277.20 13.38 o 2 -2 11 97.88 97.50 2.77 o 3 -2 11 101.52 103.95 4.95 o 4 -2 11 603.81 644.54 16.10 o -1 -1 11 667.12 691.02 4.35 o 0 -1 11 135.27 136.68 3.41 o 1 -1 11 104.30 95.05 3.28 o 2 -1 11 166.09 172.31 6.96 o 3 -1 11 385.44 394.07 11.53 o 4 -1 11 204.41 209.12 3.55 o 5 -1 11 225.32 233.85 10.93 o -1 0 11 60.07 63.79 3.68 o 0 0 11 152.17 158.86 4.20 o 1 0 11 140.13 151.09 3.46 o 2 0 11 309.28 322.22 5.38 o 3 0 11 213.29 224.54 5.20 o 4 0 11 17.87 18.26 3.04 o 5 0 11 33.18 32.61 3.15 o -1 1 11 31.61 32.83 2.39 o 0 1 11 176.55 170.21 3.94 o 1 1 11 181.73 194.68 11.39 o 2 1 11 49.14 52.63 2.74 o 3 1 11 12.60 13.15 3.19 o 4 1 11 69.10 71.30 3.36 o 5 1 11 278.49 285.42 4.02 o -1 2 11 77.05 83.58 3.27 o 0 2 11 257.33 271.10 3.77 o 1 2 11 5.29 4.40 3.09 o 2 2 11 38.45 40.16 3.62 o 3 2 11 123.79 120.42 10.24 o 4 2 11 310.91 322.97 9.19 o 5 2 11 46.64 47.14 3.22 o -1 3 11 106.85 100.88 4.00 o 0 3 11 3.32 4.01 3.23 o 1 3 11 152.23 158.33 5.97 o 2 3 11 134.85 140.27 5.04 o 3 3 11 353.76 376.68 5.96 o 4 3 11 95.75 101.69 3.90 o 0 4 11 47.42 44.11 3.41 o 1 4 11 118.36 119.52 4.93 o 2 4 11 128.58 117.80 4.33 o 3 4 11 58.84 53.98 4.01 o 4 4 11 56.15 42.90 5.66 o 1 -2 12 235.33 243.31 4.18 o 2 -2 12 240.48 251.34 3.63 o 3 -2 12 49.78 48.63 2.77 o 0 -1 12 72.38 71.00 3.34 o 1 -1 12 83.73 85.84 4.09 o 2 -1 12 50.60 50.78 3.75 o 3 -1 12 472.63 484.45 4.91 o 0 0 12 69.84 67.89 3.25 o 1 0 12 135.23 141.85 3.05 o 2 0 12 334.94 347.07 6.98 o 3 0 12 116.52 123.51 4.07 o 4 0 12 85.96 91.67 4.38 o 0 1 12 489.99 501.73 29.90 o 1 1 12 175.41 168.33 4.64 o 2 1 12 99.13 99.09 4.00 o 3 1 12 100.14 106.52 4.13 o 4 1 12 89.87 86.98 4.45 o 1 2 12 99.01 105.57 4.54 o 2 2 12 38.96 39.65 3.94 o 3 2 12 84.14 91.10 4.23 o 2 3 12 95.66 85.49 34.05 o