#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/88/2018849.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018849_Fobs loop_ _publ_author_name 'Y\'epes, Andr\'es F.' 'Palma, Alirio' 'Cobo, Justo' 'Glidewell, Christopher' _publ_section_title ; Three closely related thienyl-substituted 1,4-epoxynaphtho[1,2-b]azepines: hydrogen-bonded assembly in one, two and three dimensions ; _journal_coeditor_code YF3025 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 307 _journal_page_last 312 _journal_volume 69 _journal_year 2013 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.3160 _cell_length_b 9.9230 _cell_length_c 20.2250 _exptl_crystal_F_000 1504.00 _reflns_d_resolution_high 0.7698 _[local]_cod_data_source_file yf3025IIIsup4.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' AF176' _shelx_refln_list_code 4 _shelx_f_calc_maximum 433.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x+1/2, y+1/2, z+1/2' 'x+1/2, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 0 -26 135.69 108.12 92.39 o 2 0 -26 2037.25 2011.81 134.39 o 1 1 -26 335.45 351.77 58.76 o 2 1 -26 686.11 636.16 69.53 o 2 0 -25 1402.22 1415.97 144.00 o 4 0 -25 2727.29 2714.34 154.53 o 6 0 -25 1872.47 1736.26 143.97 o 0 1 -25 482.73 391.43 71.01 o 1 1 -25 1342.36 1286.42 63.07 o 2 1 -25 1502.46 1516.20 76.15 o 3 1 -25 401.58 452.07 88.85 o 4 1 -25 103.17 61.87 69.09 o 5 1 -25 183.60 102.89 73.05 o 1 2 -25 349.45 414.86 77.39 o 2 2 -25 56.55 43.35 59.78 o 3 2 -25 2968.41 2737.60 95.75 o 4 2 -25 763.17 473.74 72.39 o 5 2 -25 1570.49 1499.61 95.54 o 0 3 -25 3317.97 3338.11 163.68 o 1 3 -25 880.10 743.45 65.70 o 2 3 -25 438.26 474.27 66.47 o 3 3 -25 29.02 1.58 62.14 o 4 3 -25 33.50 50.95 67.19 o 0 0 -24 705.77 774.83 187.31 o 2 0 -24 2957.09 3089.19 121.63 o 4 0 -24 26.77 -15.50 92.80 o 6 0 -24 3134.45 3343.01 187.98 o 8 0 -24 46.67 -57.25 113.96 o 1 1 -24 1094.39 1146.30 60.20 o 2 1 -24 41.51 38.84 42.80 o 3 1 -24 762.37 784.70 64.95 o 4 1 -24 1240.06 1121.48 69.37 o 5 1 -24 498.44 543.04 87.01 o 6 1 -24 38.35 25.60 83.65 o 7 1 -24 610.79 698.00 88.49 o 0 2 -24 2211.61 2071.03 103.45 o 1 2 -24 1129.63 1076.10 59.63 o 2 2 -24 667.25 657.76 63.96 o 3 2 -24 1437.55 1355.49 74.89 o 4 2 -24 67.32 59.82 61.06 o 5 2 -24 585.19 622.32 64.79 o 6 2 -24 686.28 648.64 90.95 o 7 2 -24 1008.83 1196.45 106.99 o 1 3 -24 628.52 627.78 61.63 o 2 3 -24 4728.45 4706.81 120.46 o 3 3 -24 361.99 247.49 62.88 o 4 3 -24 250.81 170.55 65.52 o 5 3 -24 406.44 423.29 69.95 o 6 3 -24 1827.03 1693.42 90.90 o 0 4 -24 2354.79 2286.28 140.49 o 1 4 -24 353.85 367.99 60.18 o 2 4 -24 573.57 544.96 79.80 o 3 4 -24 68.27 9.98 77.74 o 4 4 -24 14.76 3.47 83.80 o 5 4 -24 16.17 32.43 69.86 o 1 5 -24 536.24 546.39 93.08 o 2 5 -24 1788.81 1530.72 116.15 o 2 0 -23 1010.67 1066.72 81.58 o 4 0 -23 15187.34 15769.56 588.63 o 6 0 -23 926.43 1001.34 123.53 o 8 0 -23 130.18 136.26 105.49 o 0 1 -23 137.33 216.88 63.96 o 1 1 -23 1079.72 1151.17 59.12 o 2 1 -23 210.42 138.37 46.72 o 3 1 -23 482.78 455.36 52.04 o 4 1 -23 22.97 20.45 54.08 o 5 1 -23 997.17 854.34 63.67 o 6 1 -23 52.08 40.04 69.30 o 7 1 -23 1360.36 1326.81 106.81 o 8 1 -23 556.87 527.36 112.23 o 9 1 -23 370.25 437.98 105.83 o 1 2 -23 1180.67 1198.90 59.95 o 2 2 -23 308.66 354.81 51.63 o 3 2 -23 835.63 769.75 62.77 o 4 2 -23 697.89 781.18 66.37 o 5 2 -23 889.95 912.47 73.06 o 6 2 -23 36.35 0.38 55.70 o 7 2 -23 1333.42 1185.80 105.78 o 8 2 -23 1.23 42.84 103.08 o 9 2 -23 829.83 824.37 114.93 o 0 3 -23 3767.75 3938.54 155.58 o 1 3 -23 343.01 380.63 48.79 o 2 3 -23 484.25 521.37 63.48 o 3 3 -23 344.11 393.12 76.46 o 4 3 -23 19.73 12.96 62.48 o 5 3 -23 1118.56 1116.41 79.64 o 6 3 -23 827.73 879.29 75.69 o 7 3 -23 493.83 467.55 70.01 o 8 3 -23 6132.80 6225.14 195.01 o 1 4 -23 115.14 139.74 61.90 o 2 4 -23 69.78 102.18 59.54 o 3 4 -23 388.37 324.63 66.83 o 4 4 -23 864.36 916.77 86.24 o 5 4 -23 90.49 110.51 76.41 o 6 4 -23 958.18 976.37 94.17 o 7 4 -23 321.37 310.60 82.66 o 0 5 -23 3246.48 3467.55 226.82 o 1 5 -23 900.37 1046.47 137.59 o 2 5 -23 17.39 35.42 84.27 o 3 5 -23 307.36 170.36 86.56 o 4 5 -23 114.81 96.29 89.29 o 5 5 -23 1309.05 1266.84 113.96 o 1 6 -23 792.84 806.34 106.94 o 2 6 -23 1164.82 1257.07 113.34 o 0 0 -22 4638.94 5002.00 212.24 o 2 0 -22 216.69 300.86 75.81 o 4 0 -22 43.08 6.43 74.27 o 6 0 -22 457.17 968.73 168.90 o 8 0 -22 1549.81 1672.94 196.70 o 10 0 -22 222.08 60.85 152.74 o 1 1 -22 2502.70 2488.68 76.68 o 2 1 -22 2780.69 2866.88 80.85 o 3 1 -22 162.96 168.70 41.61 o 4 1 -22 3448.54 3486.28 101.11 o 5 1 -22 638.86 762.17 70.44 o 6 1 -22 2036.45 2050.30 116.28 o 7 1 -22 1205.17 1356.00 106.13 o 8 1 -22 19.25 22.43 86.98 o 9 1 -22 758.40 799.96 110.51 o 10 1 -22 293.41 293.00 101.08 o 0 2 -22 355.14 343.86 64.76 o 1 2 -22 1019.28 1034.42 56.97 o 2 2 -22 2309.31 2318.91 72.16 o 3 2 -22 2483.26 2723.85 90.91 o 4 2 -22 50.17 107.65 67.40 o 5 2 -22 2418.34 2441.65 104.69 o 6 2 -22 1119.65 1039.35 74.75 o 7 2 -22 14.33 -5.91 63.54 o 8 2 -22 174.94 139.99 88.34 o 9 2 -22 596.53 613.32 103.09 o 10 2 -22 5.40 23.78 95.83 o 1 3 -22 1320.85 1277.85 59.47 o 2 3 -22 1967.40 1828.00 70.62 o 3 3 -22 98.61 57.14 58.50 o 4 3 -22 4260.52 4526.31 163.03 o 5 3 -22 362.48 276.49 61.32 o 6 3 -22 50.09 120.71 95.26 o 7 3 -22 574.96 545.96 71.22 o 8 3 -22 156.93 225.29 74.21 o 9 3 -22 185.15 254.20 94.55 o 0 4 -22 7907.51 8140.35 201.96 o 1 4 -22 23.76 -44.56 49.77 o 2 4 -22 2312.51 2280.44 96.03 o 3 4 -22 176.66 279.02 64.02 o 4 4 -22 121.84 67.18 65.38 o 5 4 -22 204.08 93.72 61.02 o 6 4 -22 360.85 288.60 72.51 o 7 4 -22 67.69 161.64 84.36 o 8 4 -22 3141.75 3009.65 170.86 o 1 5 -22 2633.34 2613.74 133.18 o 2 5 -22 706.78 686.62 79.99 o 3 5 -22 361.73 264.84 106.94 o 4 5 -22 36.40 73.11 79.72 o 5 5 -22 683.53 592.06 80.85 o 6 5 -22 1252.24 994.02 93.11 o 7 5 -22 878.78 866.82 91.73 o 0 6 -22 401.99 652.35 183.53 o 1 6 -22 326.46 466.07 97.11 o 2 6 -22 158.45 253.03 123.01 o 3 6 -22 1872.38 1906.47 126.43 o 4 6 -22 216.37 311.23 93.91 o 5 6 -22 1291.35 1158.03 123.08 o 1 7 -22 35.50 23.33 91.86 o 2 0 -21 1713.68 1843.23 94.18 o 4 0 -21 136.17 211.74 53.85 o 6 0 -21 2970.27 2682.04 155.84 o 8 0 -21 842.28 637.88 223.93 o 10 0 -21 237.20 297.81 180.14 o 0 1 -21 7835.18 7763.05 224.06 o 1 1 -21 1645.44 1742.16 64.71 o 2 1 -21 1090.50 1072.02 56.11 o 3 1 -21 2324.72 2312.65 79.29 o 4 1 -21 39.61 54.12 57.43 o 5 1 -21 1501.03 1380.10 76.06 o 6 1 -21 1011.27 1020.18 73.60 o 7 1 -21 596.42 552.32 107.81 o 8 1 -21 4449.45 4457.56 166.66 o 9 1 -21 866.20 841.63 104.89 o 10 1 -21 1121.75 1379.80 123.44 o 11 1 -21 925.19 843.49 144.42 o 1 2 -21 2451.50 2433.33 74.24 o 2 2 -21 80.15 103.14 41.68 o 3 2 -21 1636.47 1541.19 64.05 o 4 2 -21 2158.87 2364.79 95.07 o 5 2 -21 754.49 706.07 67.31 o 6 2 -21 11.63 -35.52 61.39 o 7 2 -21 2426.33 2478.12 98.55 o 8 2 -21 114.14 112.93 84.01 o 9 2 -21 2061.19 1999.79 256.63 o 10 2 -21 198.51 340.55 99.90 o 11 2 -21 848.65 687.94 132.17 o 0 3 -21 693.85 834.80 97.37 o 1 3 -21 527.93 596.25 54.24 o 2 3 -21 1838.55 1779.45 77.09 o 3 3 -21 993.57 906.19 72.25 o 4 3 -21 122.32 35.68 56.36 o 5 3 -21 272.71 287.69 101.67 o 6 3 -21 158.10 231.15 62.35 o 7 3 -21 445.60 484.64 74.24 o 8 3 -21 479.56 564.10 70.14 o 9 3 -21 270.89 368.05 66.97 o 10 3 -21 35.15 -92.97 92.97 o 11 3 -21 98.30 -96.15 162.41 o 1 4 -21 104.21 88.91 45.99 o 2 4 -21 1072.37 1241.28 70.88 o 3 4 -21 110.46 36.25 59.12 o 4 4 -21 10352.42 10361.10 209.55 o 5 4 -21 89.77 175.74 61.82 o 6 4 -21 1195.11 1174.62 83.18 o 7 4 -21 348.78 337.04 95.75 o 8 4 -21 108.79 169.16 71.60 o 9 4 -21 10.72 -102.33 157.04 o 10 4 -21 1254.72 1096.96 158.31 o 0 5 -21 664.93 648.47 92.45 o 1 5 -21 362.93 334.99 73.27 o 2 5 -21 848.43 879.54 98.76 o 3 5 -21 1505.46 1570.45 140.34 o 4 5 -21 578.97 701.07 104.27 o 5 5 -21 2849.85 2625.83 138.53 o 6 5 -21 36.15 169.14 70.25 o 7 5 -21 474.15 504.33 104.24 o 8 5 -21 84.39 -60.76 89.14 o 9 5 -21 704.95 604.60 104.52 o 1 6 -21 553.36 567.47 130.05 o 2 6 -21 16.13 180.55 116.85 o 3 6 -21 997.84 1126.00 106.54 o 4 6 -21 137.35 274.78 115.49 o 5 6 -21 550.90 467.61 98.38 o 6 6 -21 41.09 114.17 87.56 o 7 6 -21 1102.12 1092.87 116.46 o 0 7 -21 3124.24 3187.17 214.78 o 1 7 -21 707.40 602.65 118.06 o 2 7 -21 777.05 922.88 121.22 o 3 7 -21 25.52 -137.56 137.56 o 4 7 -21 45.68 -15.30 88.53 o 5 7 -21 200.90 242.44 98.79 o 0 0 -20 4234.64 4312.49 277.48 o 2 0 -20 3144.47 3394.85 117.37 o 4 0 -20 382.64 424.68 149.59 o 6 0 -20 3025.83 2880.53 159.41 o 8 0 -20 3461.28 3848.46 251.69 o 10 0 -20 3198.89 3693.85 266.00 o 12 0 -20 51.53 135.00 162.92 o 1 1 -20 706.09 763.52 49.81 o 2 1 -20 7516.28 7985.86 136.39 o 3 1 -20 4117.27 4103.12 92.04 o 4 1 -20 15.35 -14.66 40.40 o 5 1 -20 3135.46 2908.09 100.37 o 6 1 -20 3026.57 3242.02 129.26 o 7 1 -20 359.36 270.16 48.96 o 8 1 -20 193.95 301.44 142.27 o 9 1 -20 632.96 768.05 101.44 o 10 1 -20 2333.54 2313.87 165.18 o 11 1 -20 1578.19 1487.37 147.06 o 12 1 -20 18.83 143.18 142.95 o 0 2 -20 241.46 266.95 63.37 o 1 2 -20 5475.79 5592.32 109.46 o 2 2 -20 64.34 102.01 41.44 o 3 2 -20 611.06 629.71 52.44 o 4 2 -20 726.09 758.72 68.31 o 5 2 -20 289.39 278.90 58.38 o 6 2 -20 332.98 371.67 59.08 o 7 2 -20 4456.77 4279.43 126.44 o 8 2 -20 419.40 370.77 60.68 o 9 2 -20 1757.12 1873.40 124.64 o 10 2 -20 435.24 438.50 192.01 o 11 2 -20 191.26 121.42 196.26 o 12 2 -20 23.28 59.61 122.43 o 1 3 -20 320.76 303.93 47.89 o 2 3 -20 2699.19 2657.75 80.47 o 3 3 -20 1863.79 1620.12 97.16 o 4 3 -20 3052.32 3033.38 105.75 o 5 3 -20 1291.47 1180.03 77.76 o 6 3 -20 2537.47 2560.50 119.00 o 7 3 -20 148.48 182.07 95.37 o 8 3 -20 45.46 76.75 74.27 o 9 3 -20 337.60 263.58 64.30 o 10 3 -20 169.95 26.10 59.07 o 11 3 -20 175.80 -156.27 156.27 o 12 3 -20 1381.50 1385.97 151.99 o 0 4 -20 481.42 247.72 102.60 o 1 4 -20 32.99 45.63 60.61 o 2 4 -20 4274.64 4272.44 104.34 o 3 4 -20 554.53 542.01 63.93 o 4 4 -20 232.41 173.77 59.33 o 5 4 -20 246.53 224.08 81.84 o 6 4 -20 4995.76 4827.52 137.89 o 7 4 -20 193.72 266.54 64.58 o 8 4 -20 6.52 33.10 71.45 o 9 4 -20 454.17 460.77 91.02 o 10 4 -20 4659.66 4466.58 232.69 o 11 4 -20 74.25 84.17 78.21 o 1 5 -20 972.68 869.04 69.46 o 2 5 -20 267.51 223.57 68.71 o 3 5 -20 942.21 1024.21 72.82 o 4 5 -20 71.55 157.86 68.72 o 5 5 -20 2439.61 2692.12 118.81 o 6 5 -20 25.19 57.75 83.05 o 7 5 -20 184.82 264.69 75.30 o 8 5 -20 21.23 -84.14 84.14 o 9 5 -20 763.96 736.59 100.65 o 10 5 -20 149.90 74.53 94.04 o 0 6 -20 2400.74 2464.09 183.89 o 1 6 -20 1802.86 1802.49 116.67 o 2 6 -20 167.88 252.71 84.94 o 3 6 -20 380.79 273.37 95.97 o 4 6 -20 113.07 35.79 105.41 o 5 6 -20 670.82 644.88 107.08 o 6 6 -20 313.32 109.20 112.28 o 7 6 -20 2189.61 1862.52 131.67 o 8 6 -20 1900.25 1636.44 131.67 o 1 7 -20 294.34 211.78 136.67 o 2 7 -20 1446.46 1283.24 111.99 o 3 7 -20 492.82 485.83 95.61 o 4 7 -20 73.29 -74.51 90.80 o 5 7 -20 267.09 180.87 186.18 o 6 7 -20 1834.87 1724.08 131.24 o 7 7 -20 474.83 488.07 103.38 o 0 8 -20 543.58 556.75 145.25 o 1 8 -20 435.65 468.57 113.71 o 2 8 -20 389.33 499.85 111.79 o 3 8 -20 107.58 150.78 96.87 o 2 0 -19 5252.13 5480.01 151.49 o 4 0 -19 29.25 116.17 48.84 o 6 0 -19 4897.71 5594.55 278.37 o 8 0 -19 711.82 377.65 299.37 o 10 0 -19 4119.12 4132.82 308.23 o 12 0 -19 351.73 153.97 312.61 o 0 1 -19 1830.82 2099.26 126.52 o 1 1 -19 2051.82 2138.95 67.86 o 2 1 -19 478.91 479.25 43.94 o 3 1 -19 1579.90 1467.16 62.00 o 4 1 -19 11.04 32.19 61.59 o 5 1 -19 2503.29 2356.87 90.55 o 6 1 -19 384.57 264.04 51.08 o 7 1 -19 2937.13 3015.05 98.09 o 8 1 -19 1134.93 1134.99 129.98 o 9 1 -19 637.22 553.78 90.27 o 10 1 -19 411.81 416.60 114.80 o 11 1 -19 95.23 113.49 106.47 o 12 1 -19 469.49 486.60 132.80 o 13 1 -19 514.97 730.92 221.94 o 1 2 -19 3264.55 3238.82 87.21 o 2 2 -19 36.32 53.02 40.35 o 3 2 -19 2068.20 2163.10 69.43 o 4 2 -19 401.65 434.21 56.63 o 5 2 -19 1905.09 1719.25 104.16 o 6 2 -19 495.91 417.19 57.74 o 7 2 -19 641.27 575.44 63.56 o 8 2 -19 50.97 76.82 50.33 o 9 2 -19 453.58 508.31 126.47 o 10 2 -19 415.21 513.08 101.47 o 11 2 -19 2151.48 2194.38 139.37 o 12 2 -19 298.25 875.84 188.70 o 13 2 -19 912.79 785.67 145.79 o 0 3 -19 1940.36 1989.72 118.07 o 1 3 -19 1373.63 1350.58 62.65 o 2 3 -19 8553.86 9290.39 163.26 o 3 3 -19 687.67 653.82 61.55 o 4 3 -19 262.73 176.82 70.30 o 5 3 -19 439.46 440.80 76.29 o 6 3 -19 2625.91 2822.41 103.94 o 7 3 -19 672.21 624.62 73.96 o 8 3 -19 12.24 93.55 84.55 o 9 3 -19 256.62 370.55 112.51 o 10 3 -19 3851.29 4141.23 144.54 o 11 3 -19 12.09 76.13 67.79 o 12 3 -19 314.01 298.32 139.04 o 1 4 -19 261.59 279.01 55.38 o 2 4 -19 464.45 452.25 49.34 o 3 4 -19 2001.03 1990.97 86.96 o 4 4 -19 2349.42 2333.18 102.74 o 5 4 -19 792.60 787.86 70.91 o 6 4 -19 2201.70 2256.14 109.22 o 7 4 -19 31.14 -28.52 59.48 o 8 4 -19 659.98 633.40 81.77 o 9 4 -19 429.60 479.43 78.56 o 10 4 -19 178.37 156.50 73.91 o 11 4 -19 124.55 104.92 93.87 o 12 4 -19 278.78 304.62 239.49 o 0 5 -19 263.44 212.34 80.10 o 1 5 -19 2310.91 2247.08 90.69 o 2 5 -19 1730.55 1780.09 82.04 o 3 5 -19 13.10 54.67 56.61 o 4 5 -19 326.11 342.87 59.10 o 5 5 -19 292.00 347.47 78.87 o 6 5 -19 1134.14 1020.44 91.89 o 7 5 -19 1036.61 961.01 103.68 o 8 5 -19 232.39 230.65 84.52 o 9 5 -19 859.01 725.23 100.55 o 10 5 -19 624.18 681.32 103.36 o 11 5 -19 164.85 112.99 94.38 o 1 6 -19 1220.57 1240.69 104.38 o 2 6 -19 3236.23 3303.11 144.70 o 3 6 -19 3172.18 2877.91 140.22 o 4 6 -19 1601.37 1548.18 122.33 o 5 6 -19 943.26 1008.92 88.20 o 6 6 -19 1427.19 1481.26 120.31 o 7 6 -19 740.36 742.50 100.87 o 8 6 -19 35.94 30.45 91.06 o 9 6 -19 25.78 -29.17 90.52 o 10 6 -19 534.79 333.09 108.31 o 0 7 -19 549.14 676.23 129.53 o 1 7 -19 41.20 -82.09 82.09 o 2 7 -19 555.49 482.56 89.52 o 3 7 -19 429.85 428.62 113.66 o 4 7 -19 46.03 268.64 88.20 o 5 7 -19 246.95 284.20 85.96 o 6 7 -19 527.50 392.61 97.07 o 7 7 -19 82.48 230.78 112.60 o 8 7 -19 35.64 233.08 99.76 o 1 8 -19 653.83 641.26 113.93 o 2 8 -19 2239.45 2446.71 140.00 o 3 8 -19 381.45 452.55 97.76 o 4 8 -19 173.49 69.94 115.82 o 5 8 -19 93.44 -30.22 96.93 o 6 8 -19 2449.20 2344.34 179.02 o 0 0 -18 11594.90 12679.59 364.34 o 2 0 -18 1146.54 1095.87 80.35 o 4 0 -18 44.77 9.30 52.02 o 6 0 -18 1822.81 1938.30 311.12 o 8 0 -18 8389.16 8637.32 370.60 o 10 0 -18 2179.58 2481.08 226.87 o 12 0 -18 399.61 243.84 178.35 o 1 1 -18 1737.18 1780.84 56.34 o 2 1 -18 36.93 43.93 30.84 o 3 1 -18 1214.51 1234.29 55.88 o 4 1 -18 2432.74 2297.50 76.51 o 5 1 -18 628.09 638.77 61.57 o 6 1 -18 1178.44 1240.21 85.92 o 7 1 -18 1350.40 1508.99 92.00 o 8 1 -18 337.92 351.68 82.37 o 9 1 -18 1911.97 2220.73 149.25 o 10 1 -18 6.32 74.97 159.77 o 11 1 -18 931.53 1140.12 136.24 o 12 1 -18 196.55 146.10 167.20 o 13 1 -18 293.02 259.36 188.30 o 0 2 -18 395.93 473.27 61.90 o 1 2 -18 1145.54 1079.06 51.22 o 2 2 -18 467.27 483.48 48.34 o 3 2 -18 709.40 739.37 47.69 o 4 2 -18 152.61 185.80 57.40 o 5 2 -18 2758.43 2701.88 129.27 o 6 2 -18 602.80 617.79 76.75 o 7 2 -18 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1 13 2491.34 2540.30 70.25 o 4 1 13 677.50 652.25 38.75 o 5 1 13 2936.74 2891.96 115.34 o 6 1 13 4754.76 4836.85 111.50 o 7 1 13 1920.69 1840.63 67.52 o 8 1 13 159.29 158.08 35.52 o 9 1 13 904.80 998.21 81.91 o 10 1 13 2230.82 2257.40 133.09 o 11 1 13 1356.94 1319.28 91.82 o 12 1 13 48.28 52.00 69.59 o 13 1 13 1427.61 1364.45 99.93 o 14 1 13 1430.05 1547.74 104.98 o 15 1 13 1800.34 1756.43 114.11 o 16 1 13 86.50 181.29 84.18 o 17 1 13 404.46 494.38 146.37 o 1 2 13 3718.00 3581.58 77.62 o 2 2 13 980.42 952.73 49.79 o 3 2 13 9567.39 9396.29 187.73 o 4 2 13 3699.57 3694.70 98.31 o 5 2 13 5509.89 5451.62 152.73 o 6 2 13 20.13 33.41 51.99 o 7 2 13 1604.99 1487.47 82.88 o 8 2 13 1528.65 1517.83 85.02 o 9 2 13 4752.75 4824.60 145.42 o 10 2 13 891.42 744.56 74.81 o 11 2 13 4249.22 4142.90 143.39 o 12 2 13 987.91 958.89 91.21 o 13 2 13 1546.57 1672.22 152.36 o 14 2 13 38.44 152.66 77.29 o 15 2 13 716.40 689.99 93.87 o 16 2 13 229.59 104.81 84.01 o 17 2 13 510.47 545.97 99.81 o 0 3 13 11929.46 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7643.74 8097.16 237.63 o 1 5 13 4631.54 4590.27 108.06 o 2 5 13 2759.26 2701.22 77.95 o 3 5 13 2383.92 2125.11 66.52 o 4 5 13 1012.87 1008.39 62.86 o 5 5 13 983.60 923.93 84.90 o 6 5 13 24.10 60.43 47.60 o 7 5 13 6611.94 6587.10 179.71 o 8 5 13 6414.35 6426.17 252.72 o 9 5 13 1174.55 1172.92 121.67 o 10 5 13 646.45 572.70 111.01 o 11 5 13 402.85 290.42 162.63 o 12 5 13 5.00 -73.44 103.40 o 13 5 13 1107.99 981.98 135.26 o 14 5 13 187.65 263.49 119.24 o 15 5 13 379.88 562.42 197.26 o 1 6 13 2139.62 2110.69 79.43 o 2 6 13 122.94 161.39 51.94 o 3 6 13 569.50 598.40 68.53 o 4 6 13 269.90 202.66 57.60 o 5 6 13 1960.61 1933.82 137.94 o 6 6 13 1313.97 1403.49 85.70 o 7 6 13 827.22 811.10 266.33 o 8 6 13 170.34 240.24 94.30 o 9 6 13 1197.51 917.72 121.11 o 10 6 13 119.72 213.23 101.19 o 11 6 13 1533.43 1880.64 224.53 o 12 6 13 1059.19 1041.42 143.19 o 13 6 13 431.00 646.72 181.54 o 14 6 13 305.99 371.53 134.35 o 0 7 13 153.69 256.58 111.47 o 1 7 13 620.36 433.57 69.88 o 2 7 13 5395.18 5671.38 175.37 o 3 7 13 24.94 73.83 59.04 o 4 7 13 530.74 421.83 68.90 o 5 7 13 64.54 59.32 59.63 o 6 7 13 2698.33 2702.39 122.45 o 7 7 13 186.61 157.14 136.75 o 8 7 13 135.88 122.88 226.02 o 9 7 13 224.09 37.08 103.07 o 10 7 13 2830.23 3297.69 196.91 o 11 7 13 23.48 71.52 111.67 o 12 7 13 454.64 385.36 173.37 o 13 7 13 226.53 80.34 156.36 o 1 8 13 574.13 572.49 114.06 o 2 8 13 352.23 569.78 99.33 o 3 8 13 486.94 625.25 98.46 o 4 8 13 4984.53 4876.83 210.22 o 5 8 13 1494.50 1513.90 101.55 o 6 8 13 1186.61 1280.09 178.35 o 7 8 13 190.98 144.20 98.60 o 8 8 13 31.39 15.85 299.87 o 9 8 13 89.37 259.36 150.88 o 10 8 13 56.35 55.71 116.38 o 11 8 13 867.26 890.14 194.37 o 12 8 13 920.89 872.25 216.17 o 0 9 13 659.51 432.34 152.08 o 1 9 13 1267.82 1352.85 135.35 o 2 9 13 30.46 -94.38 94.38 o 3 9 13 1277.45 1195.79 127.70 o 4 9 13 232.64 228.47 126.70 o 5 9 13 1600.64 1639.39 145.54 o 6 9 13 127.59 70.27 167.60 o 7 9 13 1012.92 1322.10 214.18 o 9 9 13 209.22 479.91 171.98 o 10 9 13 93.31 19.87 147.00 o 1 10 13 36.74 42.91 104.45 o 2 10 13 335.35 608.35 117.97 o 3 10 13 675.62 865.29 128.44 o 4 10 13 164.48 154.10 336.40 o 5 10 13 395.98 260.76 182.93 o 6 10 13 500.00 554.96 187.11 o 7 10 13 100.38 -17.91 166.41 o 0 11 13 3058.83 3105.21 293.40 o 1 11 13 438.68 386.06 138.54 o 2 11 13 135.84 40.80 152.47 o 3 11 13 34.67 123.53 133.96 o 0 0 14 4167.05 4190.84 208.01 o 2 0 14 37106.30 39519.17 709.61 o 4 0 14 1897.58 1943.83 115.32 o 6 0 14 20335.90 21401.22 534.97 o 8 0 14 973.71 1064.35 112.02 o 10 0 14 4606.01 5118.24 218.80 o 12 0 14 589.01 304.98 235.18 o 14 0 14 1366.55 1575.61 207.81 o 16 0 14 222.69 157.25 181.14 o 1 1 14 1327.28 1325.09 51.75 o 2 1 14 270.20 291.50 34.00 o 3 1 14 7111.41 7098.94 137.46 o 4 1 14 64.44 114.21 28.65 o 5 1 14 2682.50 2628.70 96.89 o 6 1 14 802.87 854.88 69.00 o 7 1 14 320.42 235.58 51.11 o 8 1 14 73.63 127.96 57.47 o 9 1 14 167.91 193.97 62.04 o 10 1 14 36.42 86.96 93.03 o 11 1 14 4667.20 4532.24 166.01 o 12 1 14 12.68 68.46 81.48 o 13 1 14 1280.71 1261.36 95.67 o 14 1 14 2466.19 2412.90 124.97 o 15 1 14 172.27 220.05 84.21 o 16 1 14 101.28 43.97 86.39 o 0 2 14 84.05 88.98 37.38 o 1 2 14 10726.94 10651.03 179.99 o 2 2 14 320.47 307.19 44.58 o 3 2 14 1512.76 1442.26 67.32 o 4 2 14 81.30 79.42 52.87 o 5 2 14 3990.00 3766.21 119.57 o 6 2 14 174.15 184.21 107.80 o 7 2 14 6033.59 6013.63 161.39 o 8 2 14 56.39 47.64 102.68 o 9 2 14 3675.63 3496.34 126.95 o 10 2 14 107.74 133.71 66.69 o 11 2 14 106.26 73.39 66.46 o 12 2 14 13.29 128.22 70.72 o 13 2 14 1014.83 1057.85 96.58 o 14 2 14 419.02 580.37 128.07 o 15 2 14 2490.79 2302.58 143.70 o 16 2 14 249.58 300.84 89.25 o 1 3 14 473.00 431.96 39.19 o 2 3 14 12606.37 12576.84 277.90 o 3 3 14 5351.33 5369.80 129.45 o 4 3 14 2497.26 2606.35 84.09 o 5 3 14 2000.95 1944.60 71.85 o 6 3 14 19844.91 20792.05 432.60 o 7 3 14 270.46 233.40 70.19 o 8 3 14 87.45 52.92 85.40 o 9 3 14 665.71 635.22 85.56 o 10 3 14 5828.47 5969.20 172.90 o 11 3 14 850.68 731.63 103.72 o 12 3 14 344.33 203.71 76.79 o 13 3 14 362.02 460.13 80.79 o 14 3 14 3477.25 3450.31 145.98 o 15 3 14 94.80 237.21 100.95 o 16 3 14 144.88 181.99 90.24 o 0 4 14 605.85 638.69 64.49 o 1 4 14 2065.58 2131.40 69.22 o 2 4 14 3346.22 3517.47 90.69 o 3 4 14 70.78 49.79 29.62 o 4 4 14 1098.38 1181.25 75.61 o 5 4 14 263.15 234.67 88.91 o 6 4 14 1653.00 1629.64 69.60 o 7 4 14 801.97 791.92 79.62 o 8 4 14 37.53 24.11 103.87 o 9 4 14 1411.60 1425.81 158.44 o 10 4 14 4840.54 5035.51 184.87 o 11 4 14 147.47 133.92 85.34 o 12 4 14 74.53 92.99 88.27 o 13 4 14 139.98 142.99 102.06 o 14 4 14 24.18 -16.61 97.89 o 15 4 14 1129.03 1195.48 221.55 o 1 5 14 1103.10 1067.21 82.72 o 2 5 14 8516.90 8405.34 234.58 o 3 5 14 8020.02 7822.15 336.87 o 4 5 14 125.36 119.04 47.93 o 5 5 14 1549.44 1486.02 81.64 o 6 5 14 2347.30 2193.71 97.83 o 7 5 14 278.74 439.71 125.40 o 8 5 14 34.64 189.21 93.39 o 9 5 14 981.29 1138.93 127.31 o 10 5 14 2273.92 2346.97 164.81 o 11 5 14 2104.76 2235.78 165.01 o 12 5 14 11.16 133.37 146.60 o 13 5 14 351.64 353.31 122.71 o 14 5 14 616.38 650.78 143.86 o 0 6 14 1362.62 1344.99 150.48 o 1 6 14 4607.46 4741.26 219.33 o 2 6 14 8945.64 9375.72 232.26 o 3 6 14 220.05 294.77 62.25 o 4 6 14 58.76 126.81 56.15 o 5 6 14 321.36 324.13 59.71 o 6 6 14 5670.73 5714.51 233.52 o 7 6 14 3858.50 3886.02 372.63 o 8 6 14 588.27 605.96 113.47 o 9 6 14 1622.84 1503.84 139.32 o 10 6 14 1620.97 1639.36 267.23 o 11 6 14 39.52 192.48 175.76 o 12 6 14 316.97 237.89 121.74 o 13 6 14 214.30 119.08 119.71 o 14 6 14 1022.62 989.48 320.18 o 1 7 14 473.94 473.02 86.74 o 2 7 14 1063.84 989.84 103.53 o 3 7 14 22.17 11.55 115.65 o 4 7 14 262.54 339.53 74.12 o 5 7 14 215.85 132.58 63.48 o 6 7 14 2389.12 2725.46 279.77 o 7 7 14 128.55 -79.21 99.25 o 8 7 14 8.74 141.15 123.91 o 9 7 14 180.89 43.18 101.03 o 10 7 14 71.93 -24.66 189.40 o 11 7 14 41.00 182.71 119.45 o 12 7 14 37.31 181.33 125.63 o 0 8 14 11.80 -128.39 128.39 o 1 8 14 240.27 258.04 90.64 o 2 8 14 3781.99 4026.95 193.93 o 3 8 14 280.46 452.84 150.09 o 4 8 14 7.66 108.72 179.54 o 5 8 14 658.92 817.90 181.14 o 6 8 14 1586.97 2291.69 243.44 o 7 8 14 34.89 61.71 141.53 o 8 8 14 145.41 -86.50 108.24 o 9 8 14 273.80 374.64 238.46 o 10 8 14 1786.18 2059.14 179.92 o 11 8 14 368.87 544.57 328.44 o 1 9 14 300.31 323.30 149.69 o 2 9 14 241.78 110.27 96.24 o 3 9 14 3183.29 3045.38 388.85 o 4 9 14 175.44 234.93 126.40 o 5 9 14 1669.53 1721.60 236.87 o 7 9 14 232.81 255.18 176.76 o 8 9 14 163.23 191.29 166.61 o 9 9 14 481.59 410.25 175.36 o 0 10 14 379.79 201.24 158.25 o 1 10 14 179.22 629.91 121.72 o 2 10 14 32.22 -40.61 157.65 o 3 10 14 19.93 234.65 113.15 o 4 10 14 70.51 197.46 169.39 o 5 10 14 245.79 -32.64 178.95 o 6 10 14 186.23 282.85 190.69 o 2 0 15 6421.96 6673.16 168.72 o 4 0 15 25431.77 26174.47 622.35 o 6 0 15 4652.94 4713.35 197.02 o 8 0 15 371.23 444.52 104.50 o 10 0 15 1545.96 1567.98 292.71 o 12 0 15 9388.26 9236.78 424.58 o 14 0 15 476.46 755.94 138.95 o 16 0 15 42.03 20.29 118.94 o 0 1 15 437.21 350.89 57.98 o 1 1 15 4055.24 4272.50 100.49 o 2 1 15 3508.48 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