#------------------------------------------------------------------------------
#$Date: 2016-04-02 22:23:21 +0300 (Sat, 02 Apr 2016) $
#$Revision: 180858 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/89/2018900.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2018900_Fobs
loop_
_publ_author_name
'Arce, Alejandro'
'De Sanctis, Ysaura'
'Galarza, Esperanza'
'Garland, Mar\'ia Teresa'
'Baggio, Ricardo'
_publ_section_title
;
 Two complexes derived from the reaction of <i>M</i>~3~(CO)~12~ clusters
 (<i>M</i> = Ru, Os) with the 9-(triphenylphosphonio)fluorenide ylide:
 tricarbonyl[9-(triphenylphosphonio)fluorenylidene]ruthenium and
 nonacarbonyl-\m~3~-fluorenylidene-\m~2~-hydrido-<i>triangulo</i>-triosmium(III)
;
_journal_coeditor_code           DT3019
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              363
_journal_page_last               366
_journal_volume                  69
_journal_year                    2013
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 103.771
_cell_angle_gamma                90.000
_cell_length_a                   9.3325
_cell_length_b                   13.9604
_cell_length_c                   17.8645
_exptl_crystal_F_000             1760.00
_reflns_d_resolution_high        0.8408
_cod_data_source_file            dt3019IIsup3.hkl
_cod_data_source_block           II
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' aa in P2(1)/n'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            644.31
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 5185.99 5894.18 375.77 o
4 0 0 59527.89 62289.40 1471.32 o
6 0 0 36.59 798.50 523.02 o
8 0 0 8228.35 7189.04 865.78 o
10 0 0 3109.12 3285.40 878.48 o
1 1 0 608.28 1250.43 205.66 o
2 1 0 6927.46 7948.19 427.81 o
3 1 0 109.33 180.27 359.26 o
4 1 0 187430.88 181668.44 4242.59 o
5 1 0 5941.09 6036.36 594.11 o
6 1 0 869.58 1070.17 556.03 o
7 1 0 15699.49 17269.96 915.29 o
8 1 0 22625.05 23180.64 1095.56 o
9 1 0 365.42 -569.99 795.96 o
10 1 0 2948.51 4058.52 905.14 o
0 2 0 251003.78 222800.75 2362.50 o
1 2 0 6775.88 7662.56 361.80 o
2 2 0 18427.88 20451.27 675.36 o
3 2 0 53722.53 48895.16 1183.15 o
4 2 0 72364.20 69041.74 1609.70 o
5 2 0 5668.55 5465.10 554.76 o
6 2 0 3956.43 2889.33 629.66 o
7 2 0 8851.01 7315.99 828.97 o
8 2 0 145.11 1021.93 752.80 o
9 2 0 10505.02 9860.02 954.65 o
10 2 0 123.52 170.11 835.32 o
1 3 0 358.66 841.66 318.64 o
2 3 0 22214.34 23349.48 773.11 o
3 3 0 920.01 368.15 377.03 o
4 3 0 5320.96 5838.32 495.10 o
5 3 0 16273.96 16237.87 704.56 o
6 3 0 19497.53 19062.46 850.55 o
7 3 0 39113.26 36126.76 1324.06 o
8 3 0 26839.70 26410.19 1157.76 o
9 3 0 2484.24 1613.50 821.35 o
10 3 0 4103.07 4342.88 911.48 o
0 4 0 2870.64 3213.04 373.23 o
1 4 0 132199.23 137514.77 2820.78 o
2 4 0 69022.02 76237.13 1701.10 o
3 4 0 22265.01 24097.20 768.03 o
4 4 0 32994.29 32360.22 1038.43 o
5 4 0 17763.57 18507.69 798.50 o
6 4 0 23838.76 24031.19 950.84 o
7 4 0 289.07 -690.60 690.60 o
8 4 0 4882.85 3874.44 809.93 o
9 4 0 960.81 1750.61 784.54 o
10 4 0 2016.14 1461.17 848.01 o
1 5 0 9120.89 9849.87 474.78 o
2 5 0 71564.80 77676.73 1848.36 o
3 5 0 82577.12 84620.77 1880.09 o
4 5 0 2010.79 1372.30 488.75 o
5 5 0 43842.51 42802.94 1317.72 o
6 5 0 9029.32 8819.05 736.30 o
7 5 0 8130.46 7520.38 812.46 o
8 5 0 6834.68 5401.62 822.62 o
9 5 0 1069.12 1943.57 770.57 o
10 5 0 2514.23 212.00 863.24 o
0 6 0 148.48 148.53 371.96 o
1 6 0 223001.86 225879.20 4336.53 o
2 6 0 8345.71 8315.07 510.33 o
3 6 0 13643.20 13772.55 636.01 o
4 6 0 1006.45 1212.35 525.56 o
5 6 0 16681.48 18110.35 808.66 o
6 6 0 17377.41 17075.73 896.25 o
7 6 0 1522.21 1844.55 688.06 o
8 6 0 848.48 199.31 746.45 o
9 6 0 4975.83 4240.05 898.79 o
10 6 0 2440.83 2452.63 924.18 o
1 7 0 561.33 775.65 425.27 o
2 7 0 26039.24 26448.27 892.44 o
3 7 0 49609.46 50508.66 1344.38 o
4 7 0 18464.24 19516.93 813.73 o
5 7 0 38486.23 38990.70 1264.40 o
6 7 0 22529.92 23980.41 1011.77 o
7 7 0 7816.98 7321.07 809.93 o
8 7 0 1348.69 2302.83 776.92 o
9 7 0 257.80 258.97 839.12 o
0 8 0 4490.76 4255.29 510.33 o
1 8 0 26825.69 28102.40 886.09 o
2 8 0 4358.74 4033.13 561.11 o
3 8 0 39501.77 41834.33 1266.94 o
4 8 0 10399.66 10592.51 746.45 o
5 8 0 938.63 736.30 666.48 o
6 8 0 7527.31 8076.41 813.73 o
7 8 0 1994.08 3664.98 768.03 o
8 8 0 12167.59 12737.92 1011.77 o
9 8 0 724.57 672.82 860.71 o
1 9 0 22294.97 24004.53 874.67 o
2 9 0 23560.26 24498.35 945.76 o
3 9 0 6773.68 8232.55 690.60 o
4 9 0 3226.75 3587.54 690.60 o
5 9 0 287.83 -349.11 708.37 o
6 9 0 22768.13 22779.48 1104.44 o
7 9 0 13026.27 14271.45 982.57 o
8 9 0 4570.75 6942.77 919.10 o
9 9 0 305.37 -661.40 855.63 o
0 10 0 11593.83 11606.82 735.03 o
1 10 0 14060.84 13297.77 783.27 o
2 10 0 5434.67 7236.02 714.72 o
3 10 0 35161.88 37326.41 1207.27 o
4 10 0 8682.23 8610.86 816.27 o
5 10 0 5279.32 5754.54 776.92 o
6 10 0 9572.35 9689.91 934.33 o
7 10 0 15898.00 14205.44 1079.05 o
8 10 0 2080.71 2809.35 888.63 o
1 11 0 31699.47 33420.24 1137.45 o
2 11 0 37458.11 36899.87 1350.72 o
3 11 0 25927.11 28865.36 1133.64 o
4 11 0 10634.72 10937.81 914.02 o
5 11 0 183.31 -482.40 699.48 o
6 11 0 103.73 -27.93 799.77 o
7 11 0 5820.54 4406.35 939.41 o
8 11 0 210.41 346.57 875.94 o
0 12 0 46974.87 49797.75 1481.48 o
1 12 0 37.68 396.08 714.72 o
2 12 0 9225.72 9941.27 858.17 o
3 12 0 12650.77 13797.94 930.53 o
4 12 0 1456.37 2480.56 785.81 o
5 12 0 12102.86 12590.67 1001.62 o
6 12 0 6360.08 8028.17 990.19 o
7 12 0 4104.93 4799.89 919.10 o
1 13 0 20262.92 20960.33 1047.32 o
2 13 0 10124.91 8645.13 905.14 o
3 13 0 1229.65 963.53 751.53 o
4 13 0 6946.09 7646.06 927.99 o
5 13 0 23667.77 22954.67 1264.40 o
6 13 0 1095.42 568.73 898.79 o
0 14 0 1545.63 883.56 790.88 o
1 14 0 4567.82 5894.18 879.75 o
2 14 0 2.86 228.51 787.08 o
3 14 0 190.78 689.33 785.81 o
4 14 0 570.01 -505.25 868.32 o
5 14 0 10054.10 12589.40 1131.10 o
1 15 0 12630.27 14210.52 1063.82 o
2 15 0 5214.79 6436.25 957.19 o
3 15 0 1022.32 3256.21 873.40 o
4 15 0 4050.12 4069.94 964.80 o
0 16 0 8526.98 5917.03 1035.89 o
1 16 0 76.09 436.70 900.06 o
2 16 0 11253.13 10624.25 1148.88 o
-9 0 1 25201.34 25588.84 1165.38 o
-7 0 1 14223.09 14588.82 840.39 o
-5 0 1 40536.07 41214.82 1124.76 o
-3 0 1 72517.65 70203.32 1544.95 o
-1 0 1 231422.94 210814.33 2205.08 o
1 0 1 158439.72 157276.70 2099.71 o
3 0 1 163802.36 162296.20 3446.63 o
5 0 1 46152.13 48920.54 1340.57 o
7 0 1 10869.31 11618.25 816.27 o
9 0 1 7818.81 8613.40 925.45 o
-10 1 1 1326.97 -656.32 844.20 o
-9 1 1 26.49 1882.63 766.76 o
-8 1 1 7165.94 7839.02 856.90 o
-7 1 1 2717.18 4001.39 685.52 o
-6 1 1 4120.44 3956.96 627.12 o
-5 1 1 152801.69 153215.67 3597.70 o
-4 1 1 0.31 -333.87 397.35 o
-3 1 1 63952.18 62393.50 1518.29 o
-2 1 1 1764.03 1947.38 311.02 o
-1 1 1 282598.47 258424.80 2405.66 o
0 1 1 3829.37 4136.48 134.72 o
1 1 1 77843.16 73045.68 1600.81 o
2 1 1 26917.18 27314.05 808.66 o
3 1 1 345.65 1039.70 383.38 o
4 1 1 21314.00 22159.98 794.69 o
5 1 1 6825.31 7585.12 606.81 o
6 1 1 11213.04 12654.14 752.80 o
7 1 1 8407.49 10671.22 851.82 o
8 1 1 2.67 25.39 707.10 o
9 1 1 710.58 1676.98 799.77 o
10 1 1 2844.01 3355.23 938.14 o
-10 2 1 6792.24 6810.74 987.65 o
-9 2 1 3942.77 3802.08 877.21 o
-8 2 1 75.49 712.18 727.41 o
-7 2 1 8760.73 9668.33 779.46 o
-6 2 1 5453.37 5518.41 627.12 o
-5 2 1 17193.46 17225.53 719.79 o
-4 2 1 12513.89 11377.05 556.03 o
-3 2 1 13020.83 13503.42 540.80 o
-2 2 1 19382.19 20594.71 677.90 o
-1 2 1 23839.06 27263.27 693.13 o
0 2 1 11971.14 13529.62 311.72 o
1 2 1 29814.37 29375.69 790.88 o
2 2 1 22810.27 21862.92 727.41 o
3 2 1 81178.55 76697.96 1824.24 o
4 2 1 2237.39 2139.07 455.74 o
5 2 1 1844.95 2271.09 516.68 o
6 2 1 38513.36 38782.50 1232.66 o
7 2 1 43518.11 44339.00 1434.51 o
8 2 1 32793.40 35366.34 1249.16 o
9 2 1 243.84 153.61 793.42 o
10 2 1 2093.89 726.14 920.37 o
-10 3 1 1244.98 1490.37 827.70 o
-9 3 1 1977.95 728.68 762.96 o
-8 3 1 24161.86 21576.02 1071.44 o
-7 3 1 47465.61 44792.21 1411.66 o
-6 3 1 4616.84 3482.17 608.08 o
-5 3 1 4426.42 5420.66 531.91 o
-4 3 1 8743.14 9121.19 526.83 o
-3 3 1 23146.19 25536.79 754.07 o
-2 3 1 938.08 811.20 335.14 o
-1 3 1 70396.20 74444.63 1562.73 o
0 3 1 37485.63 42953.27 974.96 o
1 3 1 15147.35 15132.16 571.26 o
2 3 1 49888.59 51255.11 1244.09 o
3 3 1 97872.68 96221.23 2084.48 o
4 3 1 49469.77 47402.25 1249.16 o
5 3 1 382.00 67.28 495.10 o
6 3 1 19681.11 18865.69 892.44 o
7 3 1 6542.44 6856.44 816.27 o
8 3 1 68.47 1005.43 727.41 o
9 3 1 233.64 -252.63 752.80 o
10 3 1 8230.06 5896.72 1056.20 o
-10 4 1 229.52 542.07 794.69 o
-9 4 1 0.88 1065.09 751.53 o
-8 4 1 7921.44 7208.09 850.55 o
-7 4 1 1.86 501.44 637.28 o
-6 4 1 4161.49 4193.08 625.85 o
-5 4 1 542.93 1235.20 490.02 o
-4 4 1 3013.26 3833.82 476.05 o
-3 4 1 121719.97 129072.73 2676.06 o
-2 4 1 27488.62 30423.00 818.81 o
-1 4 1 30493.95 33041.93 896.25 o
0 4 1 16649.49 18368.09 429.32 o
1 4 1 1270.58 1876.29 350.38 o
2 4 1 3793.45 4566.31 406.23 o
3 4 1 50285.09 50459.15 1239.01 o
4 4 1 54032.16 47536.81 1402.77 o
5 4 1 5362.91 4812.58 573.80 o
6 4 1 9593.80 7566.08 741.37 o
7 4 1 56353.91 52362.09 1642.70 o
8 4 1 12256.80 11718.54 957.19 o
9 4 1 940.56 799.77 799.77 o
10 4 1 1112.93 533.18 860.71 o
-10 5 1 28.82 -172.65 784.54 o
-9 5 1 533.34 -547.14 774.38 o
-8 5 1 1267.38 675.36 727.41 o
-7 5 1 35115.82 32873.09 1223.78 o
-6 5 1 17824.75 18051.96 855.63 o
-5 5 1 1200.71 1676.98 520.49 o
-4 5 1 121222.09 125332.88 2707.79 o
-3 5 1 8.43 -397.35 397.35 o
-2 5 1 2606.45 3025.16 399.89 o
-1 5 1 35486.61 39895.84 1043.51 o
0 5 1 204252.20 206910.03 2630.18 o
1 5 1 104862.66 113472.14 2384.08 o
2 5 1 16751.82 17275.04 648.70 o
3 5 1 42320.54 40566.12 1151.42 o
4 5 1 1056.40 1228.85 495.10 o
5 5 1 2116.41 1421.81 566.19 o
6 5 1 845.55 939.41 605.54 o
7 5 1 2553.19 1581.77 715.98 o
8 5 1 2544.00 2849.97 769.30 o
9 5 1 171.56 -754.07 754.07 o
10 5 1 818.41 717.25 869.59 o
-10 6 1 2062.33 2497.06 863.24 o
-9 6 1 2856.28 3224.47 835.32 o
-8 6 1 21612.55 21918.78 1106.98 o
-7 6 1 4037.76 3610.39 764.22 o
-6 6 1 1302.82 19.04 643.62 o
-5 6 1 11616.86 12659.22 759.15 o
-4 6 1 20211.86 20611.22 813.73 o
-3 6 1 50975.52 55307.28 1374.84 o
-2 6 1 74641.91 77347.93 1758.22 o
-1 6 1 7930.23 8111.95 479.86 o
0 6 1 103523.51 107839.51 1750.20 o
1 6 1 26849.54 27917.06 859.44 o
2 6 1 6384.21 6316.91 491.29 o
3 6 1 1344.19 990.19 470.98 o
4 6 1 74813.31 74222.48 1925.80 o
5 6 1 289.59 649.97 586.50 o
6 6 1 80.36 267.86 619.50 o
7 6 1 130.77 -335.14 665.21 o
8 6 1 3.49 851.82 731.22 o
9 6 1 3642.77 3804.62 855.63 o
-9 7 1 7867.24 6069.37 960.99 o
-8 7 1 423.04 1839.47 756.61 o
-7 7 1 186.75 0.00 690.60 o
-6 7 1 10309.39 10732.15 827.70 o
-5 7 1 3449.25 3224.47 670.28 o
-4 7 1 100626.39 105702.97 2483.10 o
-3 7 1 3638.50 2929.95 520.49 o
-2 7 1 2988.23 2756.03 467.17 o
-1 7 1 15629.93 16009.37 682.98 o
0 7 1 107458.98 110584.23 2295.85 o
1 7 1 2306.70 1760.76 455.74 o
2 7 1 2820.07 2923.60 487.48 o
3 7 1 10299.56 11510.34 638.55 o
4 7 1 7450.58 7350.27 658.86 o
5 7 1 64691.45 65606.54 1834.39 o
6 7 1 600.03 350.38 658.86 o
7 7 1 668.93 1954.99 698.21 o
8 7 1 4048.04 4090.25 848.01 o
9 7 1 6422.40 6550.50 950.84 o
-9 8 1 3768.85 3706.87 935.60 o
-8 8 1 5184.58 5273.41 870.86 o
-7 8 1 6803.53 6744.73 849.28 o
-6 8 1 907.13 212.00 682.98 o
-5 8 1 27132.97 28678.74 1063.82 o
-4 8 1 51.26 -393.54 545.87 o
-3 8 1 2006.47 2319.33 531.91 o
-2 8 1 908.24 1368.50 490.02 o
-1 8 1 2284.14 2688.75 488.75 o
0 8 1 27467.38 26912.36 1488.46 o
1 8 1 55683.09 56786.22 1491.63 o
2 8 1 3550.44 3468.21 554.76 o
3 8 1 2506.70 2127.64 576.34 o
4 8 1 33245.47 33481.17 1133.64 o
5 8 1 3809.02 2970.57 732.49 o
6 8 1 6845.41 6154.42 816.27 o
7 8 1 13313.99 13542.77 1004.16 o
8 8 1 2708.58 3423.78 850.55 o
9 8 1 15899.98 15485.08 1183.15 o
-9 9 1 10777.51 8990.43 1079.05 o
-8 9 1 12652.33 13282.53 1039.70 o
-7 9 1 1693.71 1676.98 779.46 o
-6 9 1 14458.56 13716.69 957.19 o
-5 9 1 79.24 680.44 643.62 o
-4 9 1 4583.94 5495.56 672.82 o
-3 9 1 235.79 798.50 590.31 o
-2 9 1 3067.28 2707.79 581.42 o
-1 9 1 39.67 562.38 502.71 o
0 9 1 4460.87 4544.49 419.60 o
1 9 1 10777.15 10960.66 704.56 o
2 9 1 81221.70 83019.95 2103.52 o
3 9 1 5165.72 4789.73 661.40 o
4 9 1 2527.79 3174.96 670.28 o
5 9 1 49951.79 50182.41 1607.16 o
6 9 1 115.39 422.74 713.45 o
7 9 1 2026.55 3385.69 797.23 o
8 9 1 3666.62 4473.64 915.29 o
-8 10 1 193.68 -192.96 821.35 o
-7 10 1 5329.08 6135.38 896.25 o
-6 10 1 4823.61 4691.98 846.74 o
-5 10 1 5709.68 5763.42 795.96 o
-4 10 1 16849.10 17000.83 927.99 o
-3 10 1 15601.08 16199.79 864.51 o
-2 10 1 111653.02 108476.76 2725.57 o
-1 10 1 13664.94 13757.32 773.11 o
0 10 1 139.85 90.03 1268.21 o
1 10 1 10132.99 11614.44 757.88 o
2 10 1 89.83 60.93 623.31 o
3 10 1 11453.35 12556.39 830.24 o
4 10 1 896.53 328.79 684.25 o
5 10 1 467.51 1173.00 686.79 o
6 10 1 25681.00 28667.32 1204.73 o
7 10 1 2936.25 2923.60 845.47 o
8 10 1 5198.17 5081.71 964.80 o
-8 11 1 5593.91 5618.70 976.23 o
-7 11 1 2980.07 2253.32 889.90 o
-6 11 1 20157.56 21144.40 1169.19 o
-5 11 1 16962.15 19155.13 1025.74 o
-4 11 1 1230.12 1266.94 727.41 o
-3 11 1 13867.17 12869.95 898.79 o
-2 11 1 4429.74 4105.49 757.88 o
-1 11 1 6255.16 6876.75 738.84 o
0 11 1 1451.90 1375.99 944.49 o
1 11 1 37011.20 39369.00 1305.02 o
2 11 1 65499.31 64914.68 1909.29 o
3 11 1 6386.26 7411.20 812.46 o
4 11 1 23.79 -50.78 694.40 o
5 11 1 3251.40 3925.22 830.24 o
6 11 1 4340.00 6071.91 889.90 o
7 11 1 9.30 966.07 823.89 o
-7 12 1 1537.87 696.94 907.68 o
-6 12 1 18777.50 18034.18 1176.80 o
-5 12 1 22.00 -766.76 766.76 o
-4 12 1 662.06 1221.24 765.49 o
-3 12 1 31551.68 29707.02 1211.08 o
-2 12 1 39053.47 40167.50 1387.54 o
-1 12 1 36935.40 36596.46 1338.03 o
0 12 1 6511.63 6854.53 570.90 o
1 12 1 2419.91 4396.20 747.72 o
2 12 1 8997.60 9583.28 873.40 o
3 12 1 5401.28 6033.82 798.50 o
4 12 1 2784.46 2114.95 782.00 o
5 12 1 7373.85 7558.46 944.49 o
6 12 1 2838.29 3983.62 892.44 o
7 12 1 1065.96 898.79 872.13 o
-6 13 1 14.96 -888.63 888.63 o
-5 13 1 8972.53 9688.64 1020.66 o
-4 13 1 5176.56 5647.90 881.02 o
-3 13 1 1316.97 705.83 788.34 o
-2 13 1 5269.56 6151.88 803.58 o
-1 13 1 4333.65 5665.67 822.62 o
0 13 1 121.77 -16.25 516.68 o
1 13 1 8941.38 9198.63 883.56 o
2 13 1 11902.14 13474.22 929.26 o
3 13 1 6804.34 7087.49 891.17 o
4 13 1 25700.37 27096.97 1237.74 o
5 13 1 366.27 -63.47 897.52 o
6 13 1 17398.32 18213.18 1236.47 o
-5 14 1 39.66 795.96 886.09 o
-4 14 1 2608.47 2500.87 900.06 o
-3 14 1 530.40 -477.32 808.66 o
-2 14 1 9174.50 10972.08 964.80 o
-1 14 1 638.15 564.92 783.27 o
0 14 1 21278.57 20617.96 789.47 o
1 14 1 25.39 313.56 792.15 o
2 14 1 16502.61 17617.79 1067.63 o
3 14 1 399.71 -59.67 826.43 o
4 14 1 2709.90 1542.41 901.33 o
5 14 1 0.78 36.81 924.18 o
-4 15 1 2160.43 2269.82 927.99 o
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