#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/89/2018918.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018918_Fobs loop_ _publ_author_name 'Walha, Siwar' 'Bouchaala, Mahmoud' 'Ben Salah, Abdelhamid' _publ_section_title ; The interpenetrated three-dimensional framework of a new mixed lithium/ammonium perchlorate grown in a gel medium ; _journal_coeditor_code OV3020 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 315 _journal_page_last 318 _journal_volume 69 _journal_year 2013 _space_group_IT_number 122 _symmetry_space_group_name_Hall 'I -4 2bw' _symmetry_space_group_name_H-M 'I -4 2 d' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.4946 _cell_length_b 7.4946 _cell_length_c 7.5457 _exptl_crystal_F_000 226.82 _reflns_d_resolution_high 0.6133 _[local]_cod_data_source_file ov3020Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Li0.41(NH4)0.59ClO4 in I-42d' _shelx_refln_list_code 4 _shelx_f_calc_maximum 87.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'y, -x, -z' '-y, x, -z' '-x+1/2, y, -z+3/4' 'x+1/2, -y, -z+3/4' '-y+1/2, -x, z+3/4' 'y+1/2, x, z+3/4' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' '-x+1, y+1/2, -z+5/4' 'x+1, -y+1/2, -z+5/4' '-y+1, -x+1/2, z+5/4' 'y+1, x+1/2, z+5/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 7635.58 7254.23 45.80 o 2 2 0 2623.40 2641.81 24.53 o 1 3 0 634.02 654.15 4.92 o 0 4 0 4.28 -0.56 0.63 o 2 4 0 1184.60 1223.14 9.95 o 4 4 0 2583.63 2571.77 22.84 o 1 5 0 441.48 511.03 4.47 o 3 5 0 559.63 568.88 5.54 o 0 6 0 714.70 736.72 8.79 o 2 6 0 1607.96 1611.90 10.91 o 4 6 0 980.90 1005.55 13.20 o 6 6 0 36.35 33.42 3.16 o 1 7 0 56.49 56.40 1.98 o 3 7 0 13.41 14.27 1.38 o 5 7 0 30.73 30.84 1.90 o 0 8 0 522.77 481.05 9.22 o 2 8 0 625.42 632.22 7.00 o 4 8 0 430.68 448.67 6.08 o 6 8 0 102.23 107.56 3.54 o 8 8 0 59.76 57.07 6.27 o 1 9 0 114.69 125.16 3.95 o 3 9 0 98.23 94.58 4.63 o 5 9 0 12.77 14.92 1.69 o 7 9 0 2.29 2.09 1.88 o 0 10 0 159.54 179.33 7.68 o 2 10 0 103.64 108.44 4.16 o 4 10 0 174.60 179.48 8.06 o 6 10 0 309.94 334.83 9.29 o 1 11 0 0.02 1.94 1.34 o 3 11 0 4.25 10.57 2.13 o 5 11 0 6.89 5.07 2.22 o 0 12 0 206.71 196.16 12.62 o 2 12 0 62.76 58.37 5.47 o 0 1 1 4128.75 3081.20 30.15 o -1 2 1 1722.22 1268.53 9.20 o 1 2 1 1755.14 1311.75 7.65 o -2 3 1 1083.22 1185.01 10.16 o 0 3 1 230.00 711.03 4.56 o 2 3 1 1132.58 1206.65 7.44 o -3 4 1 1007.58 876.14 7.60 o -1 4 1 148.91 115.87 1.96 o 1 4 1 135.23 103.85 1.83 o 3 4 1 990.67 862.27 8.13 o -4 5 1 231.19 214.69 3.44 o -2 5 1 336.35 327.83 4.10 o 0 5 1 160.52 100.80 1.72 o 2 5 1 350.54 324.93 3.62 o 4 5 1 228.16 207.49 3.13 o -5 6 1 157.90 160.63 3.42 o -3 6 1 829.39 792.42 7.56 o -1 6 1 50.80 50.66 1.60 o 1 6 1 43.94 41.03 1.47 o 3 6 1 817.55 782.13 7.07 o 5 6 1 153.28 146.43 3.22 o -6 7 1 6.39 10.92 1.65 o -4 7 1 37.46 44.03 2.39 o -2 7 1 401.20 375.19 4.68 o 0 7 1 643.80 605.97 6.15 o 2 7 1 392.55 367.11 4.68 o 4 7 1 40.60 46.92 2.17 o 6 7 1 8.82 8.95 1.28 o -7 8 1 24.91 27.18 3.89 o -5 8 1 96.05 97.37 4.96 o -3 8 1 250.02 252.88 4.64 o -1 8 1 81.09 77.84 2.83 o 1 8 1 86.76 81.68 2.58 o 3 8 1 258.23 256.58 4.44 o 5 8 1 97.98 99.36 3.66 o 7 8 1 22.75 19.77 2.31 o -8 9 1 38.71 26.84 4.16 o -6 9 1 93.88 111.14 5.51 o -4 9 1 100.41 109.74 4.08 o -2 9 1 124.16 126.12 3.96 o 0 9 1 33.45 36.66 2.28 o 2 9 1 116.74 114.38 3.67 o 4 9 1 103.20 109.32 4.00 o 6 9 1 96.86 101.44 5.02 o 8 9 1 36.51 42.61 9.67 o -5 10 1 42.46 45.47 3.47 o -3 10 1 12.68 12.83 2.19 o -1 10 1 85.01 86.81 4.34 o 1 10 1 85.65 89.15 4.76 o 3 10 1 13.73 14.62 2.94 o 5 10 1 43.09 41.46 3.87 o -4 11 1 42.75 40.32 4.02 o -2 11 1 16.42 15.72 4.81 o 0 11 1 5.65 9.90 2.13 o 2 11 1 15.20 15.12 4.33 o 4 11 1 43.34 47.07 4.40 o -1 12 1 67.09 67.31 4.70 o 1 12 1 65.68 68.84 5.86 o -1 1 2 6841.91 7219.21 41.54 o 1 1 2 6925.45 7219.50 51.26 o 0 2 2 1146.20 1303.30 6.97 o -3 3 2 2130.20 2249.65 17.59 o -1 3 2 3169.13 3341.97 14.19 o 1 3 2 3239.28 3382.29 13.62 o 3 3 2 2170.00 2225.37 15.59 o -2 4 2 261.59 270.32 2.81 o 0 4 2 122.83 180.23 1.99 o 2 4 2 261.60 267.23 2.66 o -5 5 2 700.22 730.16 12.66 o -3 5 2 1274.44 1268.97 11.71 o -1 5 2 1176.98 1224.47 7.88 o 1 5 2 1172.05 1205.35 7.27 o 3 5 2 1251.33 1230.74 8.01 o 5 5 2 682.45 669.61 8.64 o -4 6 2 249.14 252.88 6.06 o -2 6 2 0.50 -0.13 0.52 o 0 6 2 787.58 782.82 6.12 o 2 6 2 0.50 0.15 0.59 o 4 6 2 249.12 249.48 3.58 o -7 7 2 193.90 194.78 8.80 o -5 7 2 327.67 353.72 7.85 o -3 7 2 547.84 563.02 7.17 o -1 7 2 688.78 691.20 6.88 o 1 7 2 681.96 690.24 6.55 o 3 7 2 547.62 549.99 5.94 o 5 7 2 333.82 341.36 5.24 o 7 7 2 191.11 188.48 11.62 o -6 8 2 2.83 0.04 1.50 o -4 8 2 24.95 27.62 2.48 o -2 8 2 10.81 7.50 1.18 o 0 8 2 89.24 90.72 2.83 o 2 8 2 10.81 10.34 1.55 o 4 8 2 24.95 24.24 2.68 o 6 8 2 2.83 2.34 1.37 o -7 9 2 139.46 136.07 7.73 o -5 9 2 287.42 283.16 7.67 o -3 9 2 254.08 263.69 6.02 o -1 9 2 290.84 287.96 5.84 o 1 9 2 287.46 288.70 5.78 o 3 9 2 258.52 249.47 6.36 o 5 9 2 296.72 291.53 7.02 o 7 9 2 136.91 151.44 6.15 o -6 10 2 4.60 3.69 2.11 o -4 10 2 30.84 24.48 3.34 o -2 10 2 2.61 2.39 1.61 o 0 10 2 100.42 101.54 5.52 o 2 10 2 2.61 3.28 1.93 o 4 10 2 30.84 22.01 2.62 o 6 10 2 4.60 0.09 1.68 o -3 11 2 113.62 112.17 6.30 o -1 11 2 154.27 158.67 6.49 o 1 11 2 151.10 157.91 7.75 o 3 11 2 110.01 117.97 6.47 o 0 12 2 17.74 16.26 2.82 o 0 1 3 16.68 35.58 0.84 o -1 2 3 494.43 578.31 3.91 o 1 2 3 525.81 593.59 4.12 o -2 3 3 1387.21 1323.77 7.79 o 0 3 3 1765.94 1622.28 8.84 o 2 3 3 1421.75 1328.65 7.43 o -3 4 3 127.41 111.66 1.87 o -1 4 3 468.34 408.14 3.16 o 1 4 3 463.93 394.31 3.45 o 3 4 3 115.58 103.74 1.88 o -4 5 3 208.22 201.30 3.37 o -2 5 3 274.90 263.15 3.34 o 0 5 3 138.87 123.34 2.04 o 2 5 3 280.19 266.25 3.16 o 4 5 3 202.82 193.42 3.11 o -5 6 3 49.70 49.98 2.81 o -3 6 3 88.01 75.30 2.89 o -1 6 3 634.99 609.03 5.92 o 1 6 3 627.92 597.59 5.91 o 3 6 3 78.10 73.42 2.24 o 5 6 3 46.97 47.46 2.98 o -6 7 3 194.83 183.65 8.70 o -4 7 3 238.11 245.19 6.00 o -2 7 3 53.55 49.90 2.56 o 0 7 3 4.08 5.62 1.04 o 2 7 3 49.38 46.13 2.38 o 4 7 3 242.03 231.52 4.63 o 6 7 3 196.57 194.40 4.50 o -7 8 3 86.95 98.23 7.67 o -5 8 3 59.28 64.36 3.93 o -3 8 3 71.30 75.95 3.27 o -1 8 3 142.37 140.55 5.37 o 1 8 3 144.47 143.20 3.74 o 3 8 3 77.36 78.75 4.47 o 5 8 3 62.60 66.19 3.40 o 7 8 3 84.48 97.58 4.69 o -6 9 3 29.33 31.32 4.30 o -4 9 3 33.89 32.77 3.77 o -2 9 3 115.17 116.72 5.72 o 0 9 3 142.03 147.46 4.20 o 2 9 3 110.00 116.03 3.93 o 4 9 3 36.68 37.14 2.89 o 6 9 3 31.66 31.03 3.54 o -5 10 3 39.96 45.44 4.91 o -3 10 3 87.27 88.52 5.43 o -1 10 3 11.53 12.57 2.20 o 1 10 3 11.62 11.61 1.91 o 3 10 3 88.21 84.87 4.19 o 5 10 3 40.95 38.76 3.35 o -4 11 3 5.97 9.33 2.46 o -2 11 3 57.14 59.71 4.90 o 0 11 3 110.01 104.67 5.62 o 2 11 3 55.02 58.12 4.08 o 4 11 3 5.74 6.33 2.07 o 0 0 4 211.86 346.04 9.38 o -2 2 4 2029.14 2098.61 15.04 o 0 2 4 1229.23 1332.18 6.99 o 2 2 4 2050.37 2065.15 15.02 o -1 3 4 205.39 206.63 2.79 o 1 3 4 205.30 201.68 2.40 o -4 4 4 248.26 263.66 5.29 o -2 4 4 1318.96 1353.22 10.70 o 0 4 4 3517.59 3581.20 17.56 o 2 4 4 1318.65 1329.88 10.30 o 4 4 4 241.38 249.57 5.52 o -3 5 4 257.70 250.22 3.65 o -1 5 4 182.01 196.26 3.63 o 1 5 4 181.93 183.64 3.22 o 3 5 4 257.68 238.78 3.72 o -6 6 4 730.69 749.99 19.92 o -4 6 4 262.04 278.23 5.42 o -2 6 4 303.02 319.86 6.07 o 0 6 4 837.79 839.67 8.59 o 2 6 4 300.16 316.15 4.66 o 4 6 4 262.30 258.59 4.26 o 6 6 4 731.38 723.21 11.36 o -5 7 4 17.48 19.65 2.58 o -3 7 4 9.65 8.54 1.49 o -1 7 4 31.41 33.45 2.19 o 1 7 4 31.41 28.84 2.12 o 3 7 4 9.65 9.73 1.35 o 5 7 4 17.48 11.95 1.56 o -8 8 4 159.90 178.15 17.86 o -6 8 4 278.85 252.95 14.15 o -4 8 4 199.38 191.77 5.81 o -2 8 4 209.82 223.52 6.01 o 0 8 4 314.65 326.31 5.85 o 2 8 4 210.15 215.43 4.69 o 4 8 4 203.06 210.71 4.91 o 6 8 4 278.83 270.06 6.89 o 8 8 4 157.53 155.66 8.58 o -7 9 4 2.21 -1.15 2.22 o -5 9 4 9.58 8.88 2.76 o -3 9 4 66.43 61.34 5.08 o -1 9 4 75.32 76.04 3.86 o 1 9 4 75.31 80.09 3.86 o 3 9 4 66.43 63.73 4.23 o 5 9 4 9.59 9.09 1.94 o 7 9 4 2.21 1.51 1.95 o -4 10 4 102.97 91.69 5.66 o -2 10 4 234.08 232.01 6.95 o 0 10 4 213.21 206.27 7.31 o 2 10 4 232.70 238.02 8.43 o 4 10 4 102.88 100.72 4.69 o -3 11 4 3.97 4.29 2.24 o -1 11 4 0.86 -0.58 1.49 o 1 11 4 0.86 3.01 1.87 o 3 11 4 3.97 4.79 2.17 o 0 1 5 11.95 39.19 1.08 o -1 2 5 131.90 115.70 1.76 o 1 2 5 126.92 111.88 1.86 o -2 3 5 591.01 565.71 4.91 o 0 3 5 929.71 916.84 6.60 o 2 3 5 573.89 556.38 5.22 o -3 4 5 51.46 60.17 2.11 o -1 4 5 389.23 363.65 4.30 o 1 4 5 396.60 369.54 4.30 o 3 4 5 57.87 61.39 2.11 o -4 5 5 43.39 52.11 2.37 o -2 5 5 193.89 191.76 3.47 o 0 5 5 316.77 309.51 4.29 o 2 5 5 184.15 185.48 3.48 o 4 5 5 42.81 48.26 2.18 o -5 6 5 99.68 98.91 6.91 o -3 6 5 37.08 45.00 2.50 o -1 6 5 163.71 161.86 3.46 o 1 6 5 166.03 172.01 3.61 o 3 6 5 42.81 42.64 2.27 o 5 6 5 102.90 99.56 3.19 o -6 7 5 179.03 170.57 7.25 o -4 7 5 100.10 103.19 4.63 o -2 7 5 46.97 47.44 3.39 o 0 7 5 5.13 5.69 1.28 o 2 7 5 52.24 55.00 2.70 o 4 7 5 99.77 104.51 3.53 o 6 7 5 177.50 183.02 5.44 o -7 8 5 44.27 50.97 4.92 o -5 8 5 24.41 22.58 3.36 o -3 8 5 53.91 55.41 3.44 o -1 8 5 132.26 138.77 4.81 o 1 8 5 127.99 136.41 4.21 o 3 8 5 49.50 42.82 2.73 o 5 8 5 24.49 22.29 2.41 o 7 8 5 44.85 46.91 3.54 o -6 9 5 18.18 16.13 3.24 o -4 9 5 29.63 27.05 3.16 o -2 9 5 93.46 92.50 4.76 o 0 9 5 50.33 50.50 3.48 o 2 9 5 98.04 104.17 5.65 o 4 9 5 28.57 30.80 2.80 o 6 9 5 16.25 18.71 2.51 o -3 10 5 49.94 46.11 4.25 o -1 10 5 32.71 34.61 3.54 o 1 10 5 31.80 27.77 3.07 o 3 10 5 49.02 51.63 3.58 o 0 11 5 36.20 34.23 3.59 o -1 1 6 671.12 728.93 7.83 o 1 1 6 653.25 720.68 7.30 o 0 2 6 103.35 98.47 1.75 o -3 3 6 577.75 589.68 7.81 o -1 3 6 1139.77 1115.87 7.81 o 1 3 6 1121.85 1128.87 7.80 o 3 3 6 565.49 567.62 12.08 o -2 4 6 75.68 64.13 2.14 o 0 4 6 18.16 16.18 1.18 o 2 4 6 75.67 64.44 2.17 o -5 5 6 378.58 408.13 15.89 o -3 5 6 298.70 316.75 5.16 o -1 5 6 513.35 509.69 5.69 o 1 5 6 514.59 524.90 5.78 o 3 5 6 306.52 313.04 4.90 o 5 5 6 385.96 405.81 15.66 o -4 6 6 70.92 71.43 3.39 o -2 6 6 0.48 2.28 1.01 o 0 6 6 184.32 195.83 4.22 o 2 6 6 0.48 0.77 0.95 o 4 6 6 70.91 65.55 2.89 o -7 7 6 144.42 99.05 9.09 o -5 7 6 243.50 244.76 9.65 o -3 7 6 191.30 196.79 5.28 o -1 7 6 234.34 246.50 7.40 o 1 7 6 237.07 250.08 5.14 o 3 7 6 192.18 202.72 4.63 o 5 7 6 241.15 247.79 5.63 o 7 7 6 145.01 134.14 6.47 o -6 8 6 3.21 5.04 2.10 o -4 8 6 13.32 13.75 2.14 o -2 8 6 27.01 26.09 2.68 o 0 8 6 41.32 47.94 3.52 o 2 8 6 27.01 24.75 2.36 o 4 8 6 13.32 13.25 1.97 o 6 8 6 3.21 2.02 1.54 o -5 9 6 89.32 79.69 6.01 o -3 9 6 142.25 148.58 6.99 o -1 9 6 169.90 170.92 6.55 o 1 9 6 171.23 163.92 7.67 o 3 9 6 140.13 136.93 5.43 o 5 9 6 84.87 83.99 4.48 o -2 10 6 1.69 2.97 1.73 o 0 10 6 35.05 36.36 3.35 o 2 10 6 1.69 1.44 1.80 o 0 1 7 152.49 167.99 2.95 o -1 2 7 295.30 289.30 3.91 o 1 2 7 286.81 281.26 3.32 o -2 3 7 105.94 100.39 2.45 o 0 3 7 3.53 2.02 0.75 o 2 3 7 97.64 100.82 2.53 o -3 4 7 115.29 121.15 3.24 o -1 4 7 69.82 69.43 2.22 o 1 4 7 69.14 70.81 2.27 o 3 4 7 117.81 120.69 3.16 o -4 5 7 37.06 44.81 2.47 o -2 5 7 26.47 31.87 1.89 o 0 5 7 100.74 90.93 2.78 o 2 5 7 26.32 32.24 2.25 o 4 5 7 39.83 41.32 2.28 o -5 6 7 85.87 85.76 4.63 o -3 6 7 169.21 167.73 5.76 o -1 6 7 11.25 11.28 1.55 o 1 6 7 14.01 12.69 1.50 o 3 6 7 172.87 184.80 4.36 o 5 6 7 86.66 83.08 3.65 o -6 7 7 4.84 5.15 2.76 o -4 7 7 11.32 11.50 2.00 o -2 7 7 63.47 68.31 3.57 o 0 7 7 186.38 185.14 5.13 o 2 7 7 63.82 67.89 3.40 o 4 7 7 9.67 8.70 1.74 o 6 7 7 4.22 3.61 1.54 o -5 8 7 35.50 32.72 3.91 o -3 8 7 60.42 67.93 3.85 o -1 8 7 16.50 16.32 2.33 o 1 8 7 16.71 21.15 2.54 o 3 8 7 58.55 61.52 4.00 o 5 8 7 33.50 32.63 3.01 o -4 9 7 33.38 33.10 3.64 o -2 9 7 25.61 27.93 2.78 o 0 9 7 5.80 5.32 1.96 o 2 9 7 27.14 28.98 3.52 o 4 9 7 32.14 28.62 3.08 o -1 10 7 41.34 43.43 4.70 o 1 10 7 41.36 34.86 4.19 o 0 0 8 1233.93 1282.55 23.26 o -2 2 8 339.13 341.25 7.37 o 0 2 8 455.94 468.67 6.41 o 2 2 8 331.24 332.49 6.86 o -1 3 8 23.03 16.64 1.36 o 1 3 8 23.02 22.82 1.49 o -4 4 8 360.57 352.23 8.68 o -2 4 8 193.28 195.58 4.40 o 0 4 8 67.99 69.11 2.34 o 2 4 8 193.51 203.86 3.90 o 4 4 8 364.17 374.05 11.77 o -3 5 8 48.44 47.93 2.70 o -1 5 8 31.66 36.02 2.02 o 1 5 8 31.65 35.02 2.01 o 3 5 8 48.44 49.66 2.51 o -6 6 8 26.03 29.31 6.51 o -4 6 8 199.79 196.11 4.96 o -2 6 8 241.42 237.40 5.70 o 0 6 8 133.94 132.15 4.01 o 2 6 8 243.11 245.42 6.81 o 4 6 8 199.78 206.80 5.37 o 6 6 8 25.46 33.70 4.19 o -5 7 8 4.62 3.60 2.08 o -3 7 8 4.09 0.54 1.31 o -1 7 8 9.63 6.78 1.51 o 1 7 8 9.63 4.67 1.49 o 3 7 8 4.09 6.63 1.85 o 5 7 8 4.62 1.04 1.62 o -4 8 8 98.41 101.58 5.55 o -2 8 8 130.18 125.17 4.91 o 0 8 8 110.74 105.86 5.02 o 2 8 8 130.01 136.21 5.98 o 4 8 8 96.03 98.68 5.18 o -1 9 8 23.76 20.50 3.13 o 1 9 8 23.76 19.00 2.65 o 0 1 9 162.13 160.70 5.24 o -1 2 9 41.44 45.21 3.01 o 1 2 9 41.22 47.90 3.12 o -2 3 9 28.22 31.76 2.11 o 0 3 9 0.45 1.15 1.12 o 2 3 9 31.07 31.99 2.22 o -3 4 9 52.19 47.94 2.79 o -1 4 9 13.85 13.50 1.66 o 1 4 9 12.03 14.62 2.16 o 3 4 9 51.08 56.81 3.27 o -4 5 9 42.92 41.30 2.79 o -2 5 9 49.82 47.46 2.91 o 0 5 9 0.39 2.81 1.27 o 2 5 9 52.83 50.15 3.39 o 4 5 9 43.57 44.35 2.86 o -5 6 9 10.06 7.77 2.03 o -3 6 9 54.16 57.93 3.31 o -1 6 9 20.24 18.19 1.94 o 1 6 9 19.77 20.88 2.27 o 3 6 9 52.67 56.78 3.39 o 5 6 9 9.00 14.47 2.06 o -4 7 9 8.38 7.58 2.39 o -2 7 9 45.89 43.59 3.10 o 0 7 9 35.31 41.44 3.32 o 2 7 9 44.48 45.71 3.46 o 4 7 9 8.02 8.10 2.08 o -1 8 9 11.83 4.92 1.72 o 1 8 9 13.21 13.23 2.20 o -1 1 10 241.61 216.64 8.75 o 1 1 10 243.85 238.87 9.24 o 0 2 10 6.61 5.88 1.74 o -3 3 10 142.42 128.89 10.73 o -1 3 10 89.74 105.20 4.80 o 1 3 10 92.48 94.51 5.10 o 3 3 10 144.86 136.14 11.34 o -2 4 10 16.05 12.83 2.78 o 0 4 10 3.10 3.15 1.79 o 2 4 10 16.04 11.71 2.84 o -5 5 10 54.29 61.95 8.58 o -3 5 10 132.48 127.68 9.37 o -1 5 10 82.14 85.21 4.79 o 1 5 10 82.11 92.82 5.38 o 3 5 10 131.17 120.84 8.88 o 5 5 10 52.57 45.94 15.52 o -2 6 10 0.12 0.86 1.74 o 0 6 10 18.52 21.40 3.96 o 2 6 10 0.12 -0.69 1.60 o -1 7 10 74.00 69.34 4.62 o 1 7 10 73.44 67.36 10.05 o 0 1 11 12.93 11.84 2.41 o -1 2 11 10.70 8.55 2.16 o 1 2 11 12.20 5.45 2.00 o -2 3 11 25.28 25.98 3.16 o 0 3 11 23.56 24.79 3.26 o 2 3 11 26.57 27.56 3.86 o -3 4 11 5.24 6.88 3.12 o -1 4 11 5.62 8.80 2.62 o 1 4 11 6.10 5.22 2.70 o 3 4 11 5.04 4.03 2.93 o -2 5 11 14.77 16.85 3.84 o 0 5 11 2.62 2.24 2.75 o 2 5 11 14.54 11.41 5.01 o 0 0 12 16.30 9.02 4.84 o 0 2 12 43.46 34.74 5.93 o