#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/89/2018920.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018920_Fobs loop_ _publ_author_name 'Schmidt, Horst' 'Hennings, Erik' 'Z\"urner, Philipp' 'Voigt, Wolfgang' _publ_section_title ; Fe~2~(SO~4~)~3~·H~2~SO~4~·28H~2~O, a low-temperature water-rich iron(III) sulfate ; _journal_coeditor_code OV3022 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 330 _journal_page_last 333 _journal_volume 69 _journal_year 2013 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.0802 _cell_length_b 12.7630 _cell_length_c 12.8324 _exptl_crystal_F_000 1052.00 _reflns_d_resolution_high 0.8414 _[local]_cod_data_source_file ov3022I_200Ksup5.hkl _[local]_cod_data_source_block I_200K #BEGIN Tags that were not found in dictionaries: _shelx_title ' feso4_h2so4_h2o_200K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 252.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 55.36 45.62 49.37 o 4 0 0 53637.16 46100.96 124.49 o 6 0 0 30093.99 26938.49 86.06 o 8 0 0 1300.87 1333.34 39.68 o 10 0 0 3303.94 3489.01 42.31 o 12 0 0 10432.44 10787.25 55.37 o 14 0 0 4.58 -51.84 34.56 o 2 1 0 4735.66 5082.39 76.74 o 4 1 0 10162.29 8543.71 60.62 o 6 1 0 5178.40 5244.20 47.81 o 8 1 0 980.13 1073.61 35.75 o 10 1 0 1457.57 1457.77 39.25 o 12 1 0 3912.50 3892.17 43.31 o 14 1 0 201.59 323.35 36.43 o 0 2 0 28.27 18.50 68.18 o 2 2 0 38500.37 31687.10 128.43 o 4 2 0 12070.39 11306.02 66.43 o 6 2 0 3085.37 2967.79 43.31 o 8 2 0 11312.02 12227.77 56.06 o 10 2 0 2178.25 2155.22 37.31 o 12 2 0 373.66 402.53 36.18 o 14 2 0 3565.68 3840.04 43.62 o 2 3 0 5016.76 4896.47 64.62 o 4 3 0 120.11 106.99 35.62 o 6 3 0 1318.39 1263.85 38.81 o 8 3 0 47.17 54.06 37.37 o 10 3 0 1931.38 2127.29 40.25 o 12 3 0 366.80 369.85 35.12 o 14 3 0 315.21 272.23 34.31 o 0 4 0 63758.50 62495.57 158.80 o 2 4 0 3752.21 4288.83 54.18 o 4 4 0 2151.75 2013.23 43.43 o 6 4 0 25021.40 23429.05 73.99 o 8 4 0 246.62 173.36 32.00 o 10 4 0 2696.89 2394.90 33.44 o 12 4 0 3560.58 3197.09 38.87 o 2 5 0 633.46 633.96 43.68 o 4 5 0 1063.91 1301.91 40.68 o 6 5 0 1165.17 1305.85 37.56 o 8 5 0 128.54 92.62 33.87 o 10 5 0 472.09 459.66 32.00 o 12 5 0 0.56 -49.50 33.00 o 0 6 0 26846.22 27007.43 93.49 o 2 6 0 41704.58 45440.76 112.49 o 4 6 0 3988.26 3804.80 44.43 o 6 6 0 15629.49 17075.55 65.06 o 8 6 0 31.22 11.94 35.69 o 10 6 0 5656.43 5441.12 43.25 o 12 6 0 1065.68 983.99 32.50 o 2 7 0 1444.99 1448.96 41.31 o 4 7 0 883.13 855.82 37.12 o 6 7 0 2071.37 2146.60 39.18 o 8 7 0 109.45 122.74 31.31 o 10 7 0 103.09 179.61 34.50 o 12 7 0 1206.27 1215.98 35.93 o 0 8 0 2127.69 2338.52 41.25 o 2 8 0 3650.54 3759.86 42.56 o 4 8 0 7356.10 7438.29 51.31 o 6 8 0 4683.69 4905.41 46.62 o 8 8 0 11332.44 12216.46 54.43 o 10 8 0 17.71 59.87 32.87 o 12 8 0 1539.62 1534.39 38.87 o 2 9 0 2768.25 3012.41 39.50 o 4 9 0 459.24 494.59 40.43 o 6 9 0 552.04 553.15 32.81 o 8 9 0 31.99 -14.00 35.62 o 10 9 0 2032.32 2259.90 38.37 o 0 10 0 6063.66 6759.53 51.06 o 2 10 0 114.29 120.18 34.56 o 4 10 0 1533.23 1461.71 33.62 o 6 10 0 5693.29 5705.91 47.37 o 8 10 0 454.48 438.34 32.75 o 10 10 0 1957.44 2186.53 38.25 o 2 11 0 253.25 326.29 31.37 o 4 11 0 70.03 55.87 33.69 o 6 11 0 1336.65 1210.23 38.18 o 8 11 0 109.25 109.74 31.19 o 0 12 0 3276.49 3758.42 43.75 o 2 12 0 5577.88 6059.20 49.06 o 4 12 0 4058.00 4102.21 41.56 o 6 12 0 768.47 720.89 32.31 o 8 12 0 3856.10 3792.73 45.62 o 2 13 0 357.24 282.86 35.50 o 4 13 0 499.63 442.72 32.62 o 6 13 0 175.10 153.30 33.19 o 0 14 0 688.79 742.95 33.69 o 2 14 0 3643.63 3385.95 38.68 o 4 14 0 1393.34 1348.09 37.56 o 2 15 0 1200.57 1175.42 34.62 o 1 1 1 13399.79 12414.32 121.12 o 2 1 1 3029.08 2996.54 69.50 o 3 1 1 14587.03 13131.58 85.99 o 4 1 1 7779.65 7022.95 58.43 o 5 1 1 13469.57 12413.95 64.93 o 6 1 1 1282.28 1361.09 40.93 o 7 1 1 19237.71 18348.15 67.68 o 8 1 1 561.94 515.15 38.50 o 9 1 1 3170.91 3268.71 42.43 o 10 1 1 64.01 89.18 33.31 o 11 1 1 2208.30 2405.64 39.68 o 12 1 1 79.29 78.68 33.75 o 13 1 1 2309.79 2495.39 40.25 o 14 1 1 0.11 -26.56 35.19 o 0 2 1 4817.92 5070.08 88.31 o 1 2 1 1194.12 1342.78 67.25 o 2 2 1 8564.46 7802.33 78.74 o 3 2 1 7237.79 6716.28 66.81 o 4 2 1 15.75 128.49 41.68 o 5 2 1 735.32 776.76 41.87 o 6 2 1 28.71 12.81 39.00 o 7 2 1 84.43 127.49 34.31 o 8 2 1 282.10 286.35 36.31 o 9 2 1 504.35 540.71 37.00 o 10 2 1 366.48 427.78 32.06 o 11 2 1 19.60 -10.75 33.94 o 12 2 1 721.61 766.20 36.06 o 13 2 1 11.99 6.19 35.06 o 14 2 1 175.46 170.99 33.31 o 1 3 1 10929.29 11268.77 85.24 o 2 3 1 18044.92 17673.95 92.68 o 3 3 1 772.93 720.01 40.06 o 4 3 1 1402.70 1011.87 38.81 o 5 3 1 9473.93 7999.07 58.31 o 6 3 1 5411.80 5097.77 46.06 o 7 3 1 6774.01 6033.02 47.50 o 8 3 1 317.03 327.60 36.93 o 9 3 1 8.00 8.25 38.43 o 10 3 1 3607.81 4096.84 41.93 o 11 3 1 2346.30 2581.69 40.62 o 12 3 1 338.25 403.60 34.37 o 13 3 1 811.97 797.69 35.06 o 14 3 1 1299.88 1322.97 36.50 o 0 4 1 7306.67 6843.83 67.12 o 1 4 1 714.28 790.44 45.43 o 2 4 1 2516.36 2194.22 47.50 o 3 4 1 1609.62 1538.95 44.43 o 4 4 1 4488.27 5150.26 50.81 o 5 4 1 555.05 511.53 39.06 o 6 4 1 2730.72 2567.82 40.75 o 7 4 1 1.70 -25.37 34.12 o 8 4 1 10073.36 8997.00 51.50 o 9 4 1 948.54 786.32 34.69 o 10 4 1 2919.67 2585.69 34.62 o 11 4 1 0.37 17.25 31.37 o 12 4 1 29.77 42.06 32.56 o 13 4 1 15.36 75.56 31.12 o 1 5 1 11134.54 11057.73 67.93 o 2 5 1 4682.82 4808.41 53.93 o 3 5 1 19835.49 20208.59 80.74 o 4 5 1 133.34 145.30 36.93 o 5 5 1 3199.76 3444.13 42.87 o 6 5 1 2104.79 2164.91 40.31 o 7 5 1 6303.07 6115.32 48.75 o 8 5 1 35.75 29.56 35.62 o 9 5 1 3627.04 3425.76 40.56 o 10 5 1 1296.92 1132.80 34.31 o 11 5 1 683.34 616.39 31.12 o 12 5 1 1692.92 1606.51 33.44 o 13 5 1 2134.87 1941.55 34.62 o 0 6 1 3713.25 3827.29 55.43 o 1 6 1 805.67 822.13 44.18 o 2 6 1 1169.87 1425.71 44.43 o 3 6 1 1220.45 1328.53 40.18 o 4 6 1 903.24 936.87 36.56 o 5 6 1 225.78 260.48 33.00 o 6 6 1 3655.28 4142.40 44.25 o 7 6 1 979.19 1087.67 38.93 o 8 6 1 3728.52 4088.53 42.06 o 9 6 1 310.60 313.10 30.56 o 10 6 1 455.19 488.84 35.00 o 11 6 1 424.84 493.40 34.44 o 12 6 1 6.36 48.06 32.12 o 13 6 1 34.28 57.81 31.44 o 1 7 1 24864.38 26706.13 83.87 o 2 7 1 159.47 171.30 33.87 o 3 7 1 920.33 978.99 36.81 o 4 7 1 4332.62 4445.75 45.68 o 5 7 1 13916.85 13767.35 60.75 o 6 7 1 25.18 54.18 34.31 o 7 7 1 6799.34 7482.23 49.25 o 8 7 1 345.49 337.29 31.44 o 9 7 1 674.33 675.70 35.31 o 10 7 1 624.34 655.08 34.75 o 11 7 1 3851.39 4057.22 40.68 o 12 7 1 555.15 624.02 35.25 o 0 8 1 3771.71 4092.34 44.12 o 1 8 1 405.70 400.10 37.25 o 2 8 1 1220.89 1405.34 39.75 o 3 8 1 111.13 96.62 33.00 o 4 8 1 7.00 -8.50 36.12 o 5 8 1 2274.19 2195.66 40.43 o 6 8 1 185.98 198.24 35.25 o 7 8 1 96.67 120.37 32.06 o 8 8 1 1231.95 1373.78 36.50 o 9 8 1 70.52 101.93 35.44 o 10 8 1 3.56 -15.37 32.56 o 11 8 1 229.36 270.23 32.69 o 12 8 1 115.65 137.62 33.94 o 1 9 1 2941.85 3234.52 42.50 o 2 9 1 733.21 799.13 36.68 o 3 9 1 3171.96 3490.19 41.87 o 4 9 1 498.85 570.84 36.81 o 5 9 1 835.74 755.95 36.18 o 6 9 1 42.93 28.69 31.06 o 7 9 1 350.74 401.28 35.12 o 8 9 1 40.72 62.25 34.00 o 9 9 1 935.94 1024.74 33.50 o 10 9 1 223.35 222.61 34.37 o 11 9 1 601.19 685.64 35.37 o 0 10 1 2068.31 2141.98 43.50 o 1 10 1 34.75 39.75 37.50 o 2 10 1 1482.36 1568.33 36.87 o 3 10 1 16.60 26.37 31.94 o 4 10 1 89.44 58.37 32.50 o 5 10 1 0.05 17.56 31.94 o 6 10 1 839.41 810.94 34.81 o 7 10 1 27.45 12.94 34.06 o 8 10 1 386.93 376.04 36.06 o 9 10 1 8.87 31.62 33.87 o 10 10 1 5.83 40.81 35.12 o 1 11 1 4459.53 4982.71 42.25 o 2 11 1 1314.95 1430.09 35.44 o 3 11 1 559.45 660.27 31.62 o 4 11 1 943.13 902.19 34.06 o 5 11 1 1710.39 1749.32 35.00 o 6 11 1 715.83 622.14 34.00 o 7 11 1 1563.95 1565.77 39.12 o 8 11 1 64.08 25.81 34.00 o 9 11 1 210.29 220.11 35.87 o 0 12 1 7647.25 7887.89 50.87 o 1 12 1 1476.26 1573.95 38.18 o 2 12 1 147.62 161.86 36.81 o 3 12 1 0.01 -5.37 34.12 o 4 12 1 856.32 760.26 34.12 o 5 12 1 78.80 30.81 33.19 o 6 12 1 13.65 8.06 32.19 o 7 12 1 562.39 576.02 34.25 o 8 12 1 393.02 458.53 36.18 o 1 13 1 3543.47 3737.05 41.56 o 2 13 1 438.42 417.85 33.69 o 3 13 1 1769.41 1961.86 39.31 o 4 13 1 1354.48 1367.53 35.25 o 5 13 1 3354.71 2995.04 38.12 o 6 13 1 30.12 36.81 33.44 o 7 13 1 1130.19 1031.55 36.31 o 0 14 1 987.98 1017.37 36.31 o 1 14 1 1.14 19.50 32.50 o 2 14 1 808.49 793.76 35.31 o 3 14 1 0.01 19.37 34.94 o 4 14 1 5.30 16.62 35.12 o 5 14 1 3.88 29.87 32.81 o 1 15 1 1041.31 975.06 35.81 o 0 0 2 248.70 70.25 78.93 o 1 0 2 5851.68 5384.56 80.93 o 2 0 2 34090.95 28536.32 137.74 o 3 0 2 41.73 61.50 49.87 o 4 0 2 376.78 517.21 43.18 o 5 0 2 6.33 42.18 38.31 o 6 0 2 39035.98 37851.79 94.68 o 7 0 2 409.36 395.16 36.87 o 8 0 2 7279.31 6822.15 50.87 o 9 0 2 1555.01 1635.76 39.31 o 10 0 2 2044.21 2125.41 36.50 o 11 0 2 493.22 524.59 33.94 o 12 0 2 3573.94 3831.04 39.81 o 13 0 2 212.73 226.86 35.87 o 14 0 2 3061.55 3241.84 40.81 o 1 1 2 2465.88 2510.70 82.31 o 2 1 2 11365.14 10082.92 92.43 o 3 1 2 16033.38 14513.23 88.18 o 4 1 2 6861.15 5634.61 55.50 o 5 1 2 5492.14 5414.50 53.00 o 6 1 2 302.28 278.11 37.37 o 7 1 2 18.02 -17.37 37.37 o 8 1 2 453.58 490.97 35.87 o 9 1 2 1214.61 1210.42 39.50 o 10 1 2 2627.35 2622.19 39.68 o 11 1 2 2048.47 2131.23 37.93 o 12 1 2 63.50 92.68 35.19 o 13 1 2 265.52 312.60 36.62 o 14 1 2 29.44 14.06 34.75 o 0 2 2 45954.88 48211.38 182.74 o 1 2 2 7101.41 7094.25 84.81 o 2 2 2 2031.82 1773.31 58.37 o 3 2 2 629.35 574.46 46.12 o 4 2 2 4074.59 3715.74 49.50 o 5 2 2 22.08 60.81 43.00 o 6 2 2 363.45 255.86 36.43 o 7 2 2 6560.37 6459.99 47.06 o 8 2 2 51.31 93.18 39.43 o 9 2 2 1711.37 1701.13 43.18 o 10 2 2 1487.47 1566.27 37.12 o 11 2 2 1881.02 2014.11 39.50 o 12 2 2 2563.97 2615.63 40.06 o 13 2 2 141.29 159.93 35.62 o 14 2 2 272.51 314.73 34.56 o 1 3 2 9030.46 9140.99 79.37 o 2 3 2 205.56 190.36 45.25 o 3 3 2 8715.68 8643.90 62.93 o 4 3 2 1060.54 904.56 43.00 o 5 3 2 5486.55 4670.86 47.37 o 6 3 2 78.88 56.87 33.75 o 7 3 2 256.74 263.73 36.18 o 8 3 2 116.84 81.81 34.44 o 9 3 2 1039.35 1051.74 38.31 o 10 3 2 45.62 38.37 31.06 o 11 3 2 993.19 923.69 39.25 o 12 3 2 49.78 104.49 32.75 o 13 3 2 221.09 245.42 34.56 o 0 4 2 19997.76 19199.53 90.43 o 1 4 2 1240.21 1268.16 47.87 o 2 4 2 1954.45 2105.42 46.37 o 3 4 2 70.46 65.06 36.87 o 4 4 2 160.07 271.17 41.81 o 5 4 2 3171.52 3278.58 44.93 o 6 4 2 5301.47 4872.47 45.75 o 7 4 2 18.57 16.69 34.56 o 8 4 2 19.56 7.12 34.12 o 9 4 2 1115.00 1057.74 35.62 o 10 4 2 10.52 10.69 28.50 o 11 4 2 51.76 -6.87 33.87 o 12 4 2 1864.65 1715.76 37.31 o 13 4 2 2.03 17.44 31.69 o 1 5 2 533.11 559.27 44.43 o 2 5 2 3159.17 3129.84 46.62 o 3 5 2 630.07 707.45 41.68 o 4 5 2 711.52 762.13 39.75 o 5 5 2 143.16 154.74 35.56 o 6 5 2 1326.76 1479.96 39.31 o 7 5 2 171.91 206.42 33.12 o 8 5 2 822.08 851.13 37.87 o 9 5 2 421.94 392.16 31.12 o 10 5 2 372.34 319.42 33.37 o 11 5 2 54.70 91.93 30.37 o 12 5 2 60.94 63.12 31.25 o 13 5 2 0.05 4.44 34.94 o 0 6 2 1709.39 1749.75 48.43 o 1 6 2 134.80 181.86 40.18 o 2 6 2 393.56 315.35 39.75 o 3 6 2 390.12 427.28 36.12 o 4 6 2 13554.93 13790.79 63.31 o 5 6 2 431.75 432.09 36.12 o 6 6 2 3010.25 3206.59 43.00 o 7 6 2 64.83 66.43 34.31 o 8 6 2 16218.91 17123.55 62.37 o 9 6 2 225.88 231.61 30.31 o 10 6 2 626.48 587.15 37.43 o 11 6 2 66.21 107.37 31.81 o 12 6 2 2461.87 2446.14 39.25 o 13 6 2 45.65 84.37 33.87 o 1 7 2 672.80 690.01 38.43 o 2 7 2 5068.86 5349.00 48.56 o 3 7 2 54.81 54.06 34.81 o 4 7 2 1066.41 1026.93 41.00 o 5 7 2 246.82 269.17 34.00 o 6 7 2 934.52 924.19 36.56 o 7 7 2 1.06 -36.75 34.44 o 8 7 2 107.51 106.43 32.44 o 9 7 2 15.19 41.50 33.94 o 10 7 2 2423.37 2486.33 37.75 o 11 7 2 24.75 69.06 32.94 o 12 7 2 243.16 239.61 32.37 o 0 8 2 14467.09 14566.29 66.68 o 1 8 2 642.65 684.83 37.50 o 2 8 2 451.26 460.84 37.37 o 3 8 2 12.11 13.69 32.69 o 4 8 2 424.83 372.35 35.06 o 5 8 2 71.28 37.81 34.25 o 6 8 2 10302.88 10531.83 53.18 o 7 8 2 449.68 494.03 32.31 o 8 8 2 129.73 147.24 35.12 o 9 8 2 172.78 234.80 35.25 o 10 8 2 3838.38 3962.10 41.25 o 11 8 2 103.13 121.55 31.50 o 12 8 2 1879.97 1850.18 35.93 o 1 9 2 1301.56 1353.59 39.06 o 2 9 2 1747.29 1827.06 38.87 o 3 9 2 688.27 715.51 37.31 o 4 9 2 66.77 97.74 37.12 o 5 9 2 1847.69 1782.00 36.62 o 6 9 2 2123.53 2099.73 37.50 o 7 9 2 402.05 413.28 34.06 o 8 9 2 0.02 -15.56 34.75 o 9 9 2 17.17 111.24 33.00 o 10 9 2 377.07 418.10 32.19 o 11 9 2 247.94 257.36 34.12 o 0 10 2 5.69 -23.44 38.18 o 1 10 2 1179.02 1277.72 38.81 o 2 10 2 4095.31 4451.44 43.87 o 3 10 2 1675.53 1737.19 38.87 o 4 10 2 612.05 635.08 31.37 o 5 10 2 103.31 105.74 30.06 o 6 10 2 466.04 419.78 36.12 o 7 10 2 1.03 34.06 36.56 o 8 10 2 2428.04 2399.02 40.31 o 9 10 2 353.25 376.22 33.87 o 10 10 2 73.11 46.37 35.31 o 1 11 2 62.84 64.62 32.56 o 2 11 2 2044.36 2172.85 37.93 o 3 11 2 241.54 276.42 33.37 o 4 11 2 1134.75 1146.92 37.06 o 5 11 2 73.59 86.43 34.50 o 6 11 2 1046.00 960.18 36.50 o 7 11 2 101.35 134.80 35.25 o 8 11 2 746.67 727.51 34.94 o 9 11 2 248.07 272.92 34.37 o 0 12 2 2128.30 2305.90 41.93 o 1 12 2 138.45 129.93 37.00 o 2 12 2 869.21 978.12 36.93 o 3 12 2 63.56 57.62 35.06 o 4 12 2 1846.64 1890.18 37.87 o 5 12 2 0.63 -11.56 33.75 o 6 12 2 5556.25 5110.58 41.87 o 7 12 2 7.60 -1.25 33.56 o 8 12 2 579.14 563.90 36.62 o 1 13 2 75.02 66.06 35.75 o 2 13 2 30.51 1.75 36.25 o 3 13 2 3.09 21.56 34.62 o 4 13 2 145.12 171.99 32.94 o 5 13 2 237.69 236.67 33.56 o 6 13 2 0.84 39.00 35.44 o 7 13 2 125.47 184.05 35.06 o 0 14 2 3491.61 3401.70 40.50 o 1 14 2 50.46 31.06 32.06 o 2 14 2 668.47 708.20 34.56 o 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46.43 o 4 3 3 3889.69 3856.04 51.06 o 5 3 3 295.13 269.48 38.56 o 6 3 3 2055.14 1995.67 41.50 o 7 3 3 3527.43 3363.58 44.06 o 8 3 3 25.07 33.87 35.75 o 9 3 3 1376.89 1355.91 36.62 o 10 3 3 739.53 732.26 33.69 o 11 3 3 22.87 45.81 36.43 o 12 3 3 35.58 45.25 33.25 o 13 3 3 2721.83 2719.62 38.43 o 0 4 3 949.31 940.68 45.62 o 1 4 3 1316.29 1128.67 44.75 o 2 4 3 456.25 585.77 40.25 o 3 4 3 3.97 63.68 43.50 o 4 4 3 370.20 394.66 37.43 o 5 4 3 4193.21 4383.51 47.06 o 6 4 3 296.32 243.73 33.37 o 7 4 3 4682.24 4155.33 43.37 o 8 4 3 681.01 562.52 37.00 o 9 4 3 493.66 445.16 32.56 o 10 4 3 1244.53 1056.30 32.87 o 11 4 3 153.03 145.49 32.37 o 12 4 3 2.92 77.68 34.75 o 13 4 3 859.99 744.82 35.00 o 1 5 3 11174.75 10709.50 67.93 o 2 5 3 5614.94 5745.41 56.12 o 3 5 3 868.55 912.62 39.75 o 4 5 3 869.44 860.50 38.56 o 5 5 3 12397.94 13114.21 62.12 o 6 5 3 492.74 505.78 36.06 o 7 5 3 386.91 402.41 35.62 o 8 5 3 14.70 29.50 34.87 o 9 5 3 140.86 155.99 30.56 o 10 5 3 1303.08 1161.92 35.93 o 11 5 3 5422.26 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1 8 747.57 745.76 40.87 o 7 1 8 669.38 661.02 34.87 o 8 1 8 3.11 40.50 36.93 o 9 1 8 121.45 89.43 39.31 o 10 1 8 448.95 462.72 38.37 o 11 1 8 834.27 779.51 40.56 o 12 1 8 969.73 989.68 40.81 o 0 2 8 10534.99 10063.11 74.12 o 1 2 8 1718.36 1751.00 51.81 o 2 2 8 156.71 162.18 43.75 o 3 2 8 1230.21 1186.54 43.00 o 4 2 8 217.89 193.42 46.18 o 5 2 8 2015.17 2083.29 48.00 o 6 2 8 19177.71 19687.06 88.18 o 7 2 8 1553.20 1527.39 41.93 o 8 2 8 212.83 190.36 40.00 o 9 2 8 1069.66 978.31 39.81 o 10 2 8 3084.14 3084.97 43.93 o 11 2 8 962.95 927.69 41.00 o 12 2 8 887.72 922.62 40.43 o 1 3 8 77.75 117.93 45.43 o 2 3 8 137.08 103.43 41.43 o 3 3 8 102.54 112.99 44.68 o 4 3 8 386.12 352.73 41.06 o 5 3 8 121.85 130.43 40.62 o 6 3 8 595.58 571.59 41.18 o 7 3 8 17.41 60.81 37.50 o 8 3 8 72.07 72.74 35.75 o 9 3 8 60.03 61.31 34.37 o 10 3 8 120.32 103.18 38.00 o 11 3 8 146.07 156.99 34.44 o 0 4 8 4766.09 5301.38 63.25 o 1 4 8 92.27 112.49 44.93 o 2 4 8 99.27 111.30 43.56 o 3 4 8 137.45 137.30 41.37 o 4 4 8 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786.94 38.37 o 4 11 9 490.35 406.16 38.50 o 5 11 9 940.52 922.44 36.68 o 0 12 9 115.09 153.43 34.87 o 1 12 9 17.87 -31.69 35.12 o 2 12 9 1435.81 1385.22 37.68 o 0 0 10 5793.00 6740.84 72.68 o 1 0 10 976.18 962.00 63.93 o 2 0 10 5.70 42.18 46.06 o 3 0 10 5511.60 6218.50 57.81 o 4 0 10 2667.15 2981.42 41.31 o 5 0 10 409.86 411.03 45.12 o 6 0 10 7537.56 7747.33 60.50 o 7 0 10 256.91 280.67 41.50 o 8 0 10 30.52 42.43 35.93 o 9 0 10 90.48 44.25 36.81 o 10 0 10 2445.78 2321.71 42.93 o 1 1 10 44.75 39.62 52.00 o 2 1 10 2630.23 2787.87 52.81 o 3 1 10 1045.99 1103.05 39.81 o 4 1 10 5422.55 6003.83 48.62 o 5 1 10 388.60 317.10 38.56 o 6 1 10 799.47 838.50 47.68 o 7 1 10 175.26 148.24 36.56 o 8 1 10 464.10 485.22 36.37 o 9 1 10 386.89 420.66 35.37 o 10 1 10 1003.79 979.93 38.56 o 0 2 10 20.00 20.87 47.25 o 1 2 10 1408.33 1382.78 54.18 o 2 2 10 2215.73 2516.95 49.00 o 3 2 10 228.75 180.86 37.37 o 4 2 10 596.05 567.71 37.68 o 5 2 10 530.55 516.84 34.69 o 6 2 10 6.32 7.87 44.62 o 7 2 10 318.59 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43.43 o 5 6 12 1082.30 1015.99 40.06 o 6 6 12 971.23 903.94 40.06 o 1 7 12 359.40 322.10 41.75 o 2 7 12 135.59 169.99 40.00 o 3 7 12 160.69 141.93 38.37 o 4 7 12 1581.74 1593.89 45.68 o 5 7 12 1560.82 1535.08 42.12 o 0 8 12 4539.34 4296.14 46.43 o 1 8 12 99.44 114.62 39.68 o 2 8 12 388.84 357.60 39.81 o 3 8 12 151.56 106.31 39.25 o 4 8 12 1247.85 1087.05 41.00 o 1 9 12 134.88 141.05 38.25 o 2 9 12 214.37 242.36 36.37 o 1 1 13 3524.82 4026.53 64.31 o 2 1 13 92.70 94.99 43.75 o 3 1 13 1335.73 1448.84 48.93 o 4 1 13 10.19 14.94 39.31 o 5 1 13 2735.55 2900.61 46.06 o 6 1 13 0.81 -12.81 35.00 o 7 1 13 1864.20 2033.42 39.87 o 0 2 13 0.13 44.18 46.06 o 1 2 13 622.24 637.46 49.37 o 2 2 13 12.43 20.37 41.31 o 3 2 13 410.99 457.59 47.25 o 4 2 13 93.01 110.87 38.06 o 5 2 13 5.52 37.06 36.00 o 6 2 13 252.17 259.98 35.56 o 7 2 13 316.55 330.23 36.18 o 1 3 13 2634.77 2799.18 55.81 o 2 3 13 26.01 40.68 39.18 o 3 3 13 7328.58 7965.82 68.68 o 4 3 13 31.64 81.31 39.18 o 5 3 13 4.69 2.00 36.50 o 6 3 13 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