#------------------------------------------------------------------------------
#$Date: 2016-04-02 22:23:21 +0300 (Sat, 02 Apr 2016) $
#$Revision: 180858 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/89/2018931.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2018931_Fobs
loop_
_publ_author_name
'Suarez, Sebasti\'an'
'Doctorovich, Fabio'
'Harvey, Miguel Angel'
'Baggio, Ricardo'
_publ_section_title
;
Tetraaqua(4,4'-dimethyl-2,2'-bipyridine-\k^2^N,N')nickel(II)
sulfate monohydrate: a simple molecule with an extremely complex
hydrogen-bonding scheme
;
_journal_coeditor_code SK3478
_journal_issue 4
_journal_name_full 'Acta Crystallographica Section C'
_journal_page_first 351
_journal_page_last 355
_journal_volume 69
_journal_year 2013
_space_group_IT_number 14
_symmetry_space_group_name_Hall '-P 2yn'
_symmetry_space_group_name_H-M 'P 1 21/n 1'
_cell_angle_alpha 90.000
_cell_angle_beta 113.530
_cell_angle_gamma 90.000
_cell_length_a 11.8007
_cell_length_b 11.7095
_cell_length_c 13.6967
_exptl_crystal_F_000 896.00
_reflns_d_resolution_high 0.7622
_cod_data_source_file sk3478IIasup2.hkl
_cod_data_source_block IIa
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' AIMAH03ab1 in P2(1)/n'
_shelx_refln_list_code 4
_shelx_f_calc_maximum 410.07
_shelx_f_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 26558.43 26260.04 332.80 o
4 0 0 440.82 346.15 5.36 o
6 0 0 1085.45 1232.58 13.77 o
8 0 0 2479.17 2467.80 24.54 o
10 0 0 85.14 73.21 5.58 o
12 0 0 2291.16 2510.34 54.91 o
1 1 0 18957.91 18650.18 99.58 o
2 1 0 2035.22 2198.72 12.04 o
3 1 0 2385.23 2521.36 14.14 o
4 1 0 6939.46 7219.91 36.78 o
5 1 0 906.52 778.82 6.78 o
6 1 0 2275.31 2413.75 15.68 o
7 1 0 1463.28 1408.31 11.26 o
8 1 0 1292.30 1370.08 11.63 o
9 1 0 2406.62 2461.75 22.99 o
10 1 0 0.42 1.47 1.48 o
11 1 0 53.90 49.79 4.49 o
12 1 0 10.89 8.66 2.72 o
13 1 0 174.40 176.08 9.71 o
14 1 0 87.48 79.70 10.75 o
0 2 0 764.27 891.68 7.97 o
1 2 0 857.63 901.27 5.79 o
2 2 0 1845.01 1945.19 11.18 o
3 2 0 438.73 415.78 3.68 o
4 2 0 1688.57 1514.82 12.05 o
5 2 0 4.27 4.96 1.11 o
6 2 0 118.44 105.83 2.63 o
7 2 0 20.15 18.10 1.48 o
8 2 0 2830.18 2846.68 19.32 o
9 2 0 36.32 21.46 2.53 o
10 2 0 139.81 136.95 6.00 o
11 2 0 58.44 53.08 4.55 o
12 2 0 392.74 400.27 11.05 o
13 2 0 69.59 74.88 7.23 o
1 3 0 14109.20 14898.24 71.70 o
2 3 0 5.30 -0.61 0.61 o
3 3 0 98.10 96.30 1.86 o
4 3 0 890.15 914.25 6.82 o
5 3 0 11671.54 12310.16 71.06 o
6 3 0 3456.13 3748.18 22.47 o
7 3 0 1247.75 1125.83 11.50 o
8 3 0 1719.09 1737.61 13.85 o
9 3 0 1883.86 1820.30 18.94 o
10 3 0 11.69 14.73 2.67 o
11 3 0 10.26 15.49 2.90 o
12 3 0 37.73 32.78 5.01 o
13 3 0 2681.37 3053.85 45.64 o
0 4 0 10102.56 10523.28 108.29 o
1 4 0 2863.08 3002.03 16.89 o
2 4 0 5523.69 5569.33 35.92 o
3 4 0 13.73 7.41 0.82 o
4 4 0 2934.08 3040.86 16.90 o
5 4 0 800.49 811.08 11.17 o
6 4 0 849.03 915.91 8.52 o
7 4 0 3.68 2.24 1.03 o
8 4 0 4488.59 4547.12 28.00 o
9 4 0 609.01 607.52 11.98 o
10 4 0 42.26 43.54 5.19 o
11 4 0 7.44 9.13 3.80 o
12 4 0 731.09 842.85 20.95 o
13 4 0 23.22 28.21 6.71 o
1 5 0 1359.73 1609.51 10.78 o
2 5 0 20.56 24.07 1.33 o
3 5 0 4059.28 4137.87 25.51 o
4 5 0 1537.24 1716.12 12.18 o
5 5 0 4148.82 4273.30 23.20 o
6 5 0 8.90 10.59 1.30 o
7 5 0 2575.13 2638.23 18.33 o
8 5 0 358.39 338.47 7.05 o
9 5 0 1081.73 1106.21 35.30 o
10 5 0 3.82 5.40 5.12 o
11 5 0 43.67 37.39 5.32 o
12 5 0 93.11 89.06 12.52 o
13 5 0 263.36 240.24 15.81 o
0 6 0 10246.44 10521.86 75.26 o
1 6 0 440.75 529.89 5.47 o
2 6 0 20.57 18.22 3.63 o
3 6 0 472.48 496.58 6.20 o
4 6 0 4905.28 4926.86 30.58 o
5 6 0 927.48 914.86 11.96 o
6 6 0 1081.64 1007.08 9.80 o
7 6 0 1441.97 1364.39 15.41 o
8 6 0 2047.55 2088.33 20.89 o
9 6 0 445.26 462.43 13.93 o
10 6 0 266.70 282.60 16.13 o
11 6 0 13.50 14.21 4.05 o
12 6 0 1013.35 990.81 23.88 o
1 7 0 9284.20 9689.63 50.16 o
2 7 0 122.93 104.90 3.10 o
3 7 0 293.58 256.76 5.60 o
4 7 0 171.38 174.16 4.17 o
5 7 0 2450.93 2448.95 19.32 o
6 7 0 736.28 757.87 10.76 o
7 7 0 457.92 439.62 8.45 o
8 7 0 803.70 788.26 13.04 o
9 7 0 1875.15 1950.59 32.89 o
10 7 0 420.77 404.56 13.94 o
11 7 0 417.22 419.62 14.79 o
12 7 0 8.32 9.24 4.68 o
0 8 0 9709.94 10395.44 95.36 o
1 8 0 0.37 0.79 1.03 o
2 8 0 259.71 257.29 5.43 o
3 8 0 178.19 159.06 4.28 o
4 8 0 787.39 777.90 9.56 o
5 8 0 3972.35 4134.60 33.29 o
6 8 0 8.43 7.48 1.56 o
7 8 0 481.62 461.93 8.03 o
8 8 0 1801.53 1862.96 21.89 o
9 8 0 310.70 294.48 11.99 o
10 8 0 315.28 321.93 13.06 o
11 8 0 0.59 1.71 2.55 o
1 9 0 1479.86 1487.78 16.20 o
2 9 0 239.04 219.10 5.74 o
3 9 0 1326.02 1318.90 13.50 o
4 9 0 1250.26 1237.36 14.98 o
5 9 0 10.40 11.25 2.04 o
6 9 0 289.62 282.66 6.38 o
7 9 0 793.19 787.11 11.20 o
8 9 0 47.39 42.60 4.84 o
9 9 0 1469.80 1494.01 29.16 o
10 9 0 0.31 1.58 2.24 o
0 10 0 3877.37 3942.03 61.55 o
1 10 0 646.19 625.25 12.19 o
2 10 0 158.73 179.39 5.52 o
3 10 0 253.53 234.65 7.73 o
4 10 0 159.25 151.33 6.98 o
5 10 0 201.82 201.51 8.18 o
6 10 0 119.76 104.17 4.37 o
7 10 0 636.02 652.46 10.52 o
8 10 0 2740.11 2809.09 28.68 o
9 10 0 2.69 4.34 4.55 o
10 10 0 134.03 143.84 13.66 o
1 11 0 3124.85 3153.62 28.80 o
2 11 0 3.10 0.81 1.53 o
3 11 0 163.62 135.85 8.53 o
4 11 0 424.68 416.19 10.63 o
5 11 0 1302.27 1282.09 20.40 o
6 11 0 45.50 37.17 3.57 o
7 11 0 586.86 607.95 14.44 o
8 11 0 162.17 161.21 9.10 o
9 11 0 657.12 726.17 28.09 o
0 12 0 357.71 369.50 12.32 o
1 12 0 592.79 576.74 10.90 o
2 12 0 27.99 27.03 3.63 o
3 12 0 26.97 18.67 4.91 o
4 12 0 2666.25 2816.55 33.09 o
5 12 0 150.73 142.26 6.84 o
6 12 0 170.10 169.05 6.39 o
7 12 0 29.35 31.96 3.49 o
1 13 0 326.11 362.88 10.56 o
2 13 0 173.76 180.99 7.52 o
3 13 0 194.61 193.69 7.83 o
4 13 0 292.72 306.25 10.00 o
5 13 0 623.10 632.20 14.77 o
6 13 0 818.98 865.44 15.42 o
7 13 0 363.40 355.23 10.95 o
0 14 0 2786.74 3059.89 64.27 o
1 14 0 43.94 40.38 5.68 o
2 14 0 95.56 86.39 6.23 o
3 14 0 158.42 156.54 8.66 o
4 14 0 619.20 657.81 18.86 o
-13 0 1 692.70 736.79 27.58 o
-11 0 1 1805.28 1873.87 38.40 o
-9 0 1 685.62 670.12 11.24 o
-7 0 1 6552.13 6629.56 51.20 o
-5 0 1 300.96 233.33 4.80 o
-3 0 1 10900.24 11282.53 77.26 o
-1 0 1 12860.53 13174.00 115.15 o
1 0 1 2116.81 2020.84 19.28 o
3 0 1 1092.31 1037.38 10.01 o
5 0 1 310.78 442.53 6.84 o
7 0 1 16.78 22.56 2.21 o
9 0 1 559.99 574.41 13.96 o
11 0 1 4888.16 5424.12 62.41 o
13 0 1 44.55 32.13 7.72 o
-14 1 1 268.78 286.80 12.61 o
-13 1 1 30.18 26.82 4.79 o
-12 1 1 1106.69 1199.33 40.74 o
-11 1 1 3100.60 3276.35 34.72 o
-10 1 1 4027.67 4155.67 44.99 o
-9 1 1 766.33 767.08 8.56 o
-8 1 1 3588.63 3520.61 22.37 o
-7 1 1 1958.18 1902.85 16.11 o
-6 1 1 3318.89 3111.90 18.89 o
-5 1 1 1525.04 1484.79 14.13 o
-4 1 1 395.86 354.90 3.80 o
-3 1 1 3142.34 3251.20 17.46 o
-2 1 1 4022.19 4077.93 20.83 o
-1 1 1 4.68 -1.93 1.93 o
0 1 1 9442.93 9732.02 54.61 o
1 1 1 903.35 967.73 5.89 o
2 1 1 5316.07 5683.54 29.72 o
3 1 1 7860.63 8701.23 43.18 o
4 1 1 2997.67 3206.26 22.48 o
5 1 1 1374.61 1409.95 10.19 o
6 1 1 7494.47 7458.74 39.71 o
7 1 1 608.59 602.93 6.71 o
8 1 1 431.02 442.71 8.10 o
9 1 1 236.93 237.85 6.29 o
10 1 1 1784.20 1808.00 20.19 o
11 1 1 19.28 22.29 2.95 o
12 1 1 607.28 627.54 14.25 o
13 1 1 391.98 387.26 21.25 o
-13 2 1 129.68 153.70 9.13 o
-12 2 1 38.19 40.43 4.30 o
-11 2 1 2145.52 2327.68 27.85 o
-10 2 1 6.17 9.27 2.36 o
-9 2 1 1104.96 1183.16 11.09 o
-8 2 1 1232.94 1244.30 10.90 o
-7 2 1 3461.70 3323.80 20.74 o
-6 2 1 334.23 389.62 4.84 o
-5 2 1 172.36 152.48 3.60 o
-4 2 1 335.66 407.85 4.21 o
-3 2 1 831.46 883.76 6.32 o
-2 2 1 923.15 954.04 6.92 o
-1 2 1 3628.45 3704.33 21.04 o
0 2 1 0.96 1.92 1.09 o
1 2 1 21926.83 22812.01 112.16 o
2 2 1 867.41 900.01 6.41 o
3 2 1 2775.14 2792.70 14.64 o
4 2 1 23.21 18.43 1.11 o
5 2 1 7044.23 7581.87 42.26 o
6 2 1 2362.19 2609.17 16.93 o
7 2 1 6057.42 6403.80 35.73 o
8 2 1 147.70 141.44 4.68 o
9 2 1 563.27 530.27 9.49 o
10 2 1 485.45 473.61 9.45 o
11 2 1 843.57 837.30 16.01 o
12 2 1 620.96 624.94 14.29 o
13 2 1 316.82 373.93 12.99 o
-13 3 1 83.96 73.59 12.02 o
-12 3 1 47.48 53.70 10.75 o
-11 3 1 441.70 469.38 11.13 o
-10 3 1 365.22 358.74 11.55 o
-9 3 1 1475.60 1497.99 14.44 o
-8 3 1 221.23 192.75 4.37 o
-7 3 1 627.06 561.43 6.46 o
-6 3 1 7551.93 7586.76 40.22 o
-5 3 1 27.44 21.39 1.30 o
-4 3 1 201.45 296.93 3.78 o
-3 3 1 0.77 4.12 0.57 o
-2 3 1 19083.64 19683.88 207.25 o
-1 3 1 587.16 649.26 5.65 o
0 3 1 160.60 204.12 6.50 o
1 3 1 216.43 226.77 2.73 o
2 3 1 1040.05 1120.09 7.88 o
3 3 1 258.44 235.45 3.21 o
4 3 1 7.04 11.91 1.00 o
5 3 1 673.99 632.31 6.36 o
6 3 1 21669.80 22830.20 114.29 o
7 3 1 1005.85 1056.61 9.71 o
8 3 1 380.08 354.99 7.33 o
9 3 1 558.76 525.62 9.44 o
10 3 1 454.94 491.89 17.41 o
11 3 1 120.91 119.49 9.05 o
12 3 1 175.97 201.13 8.08 o
13 3 1 0.11 -0.51 3.42 o
-13 4 1 191.05 195.34 16.95 o
-12 4 1 512.93 534.68 16.03 o
-11 4 1 104.05 117.50 7.82 o
-10 4 1 871.05 909.41 19.51 o
-9 4 1 497.98 486.50 7.71 o
-8 4 1 978.92 1010.26 11.05 o
-7 4 1 2171.27 2048.51 14.84 o
-6 4 1 738.90 760.67 9.34 o
-5 4 1 121.66 138.49 3.99 o
-4 4 1 210.81 210.53 4.57 o
-3 4 1 16211.55 16372.83 84.80 o
-2 4 1 16.83 38.00 1.18 o
-1 4 1 2649.48 2682.46 16.88 o
0 4 1 1735.76 1814.39 11.25 o
1 4 1 13.62 23.25 1.13 o
2 4 1 633.75 641.47 6.48 o
3 4 1 2668.55 2685.65 16.32 o
4 4 1 1476.11 1449.20 10.55 o
5 4 1 12192.74 12781.46 59.61 o
6 4 1 2249.42 2454.92 16.74 o
7 4 1 4215.89 4365.75 26.64 o
8 4 1 458.46 463.95 8.43 o
9 4 1 822.12 857.60 14.89 o
10 4 1 388.45 356.40 9.83 o
11 4 1 898.81 964.06 21.97 o
12 4 1 8.65 12.22 3.43 o
13 4 1 46.72 40.86 7.97 o
-13 5 1 244.30 259.47 15.81 o
-12 5 1 804.41 881.05 22.90 o
-11 5 1 205.47 206.88 9.73 o
-10 5 1 415.27 426.57 13.35 o
-9 5 1 42.79 37.63 3.03 o
-8 5 1 386.46 361.31 7.33 o
-7 5 1 250.48 245.11 5.77 o
-6 5 1 7039.08 7277.21 39.51 o
-5 5 1 1.00 2.87 0.79 o
-4 5 1 709.00 783.82 7.02 o
-3 5 1 18.30 25.44 1.24 o
-2 5 1 3225.54 3346.22 20.39 o
-1 5 1 891.96 953.35 7.33 o
0 5 1 2132.97 2114.40 17.43 o
1 5 1 9972.90 11329.20 56.45 o
2 5 1 3912.88 3906.34 25.24 o
3 5 1 2463.57 2650.93 16.66 o
4 5 1 93.69 79.16 2.36 o
5 5 1 326.45 346.07 5.57 o
6 5 1 10174.27 10542.41 55.34 o
7 5 1 786.71 778.72 8.52 o
8 5 1 53.59 55.57 4.43 o
9 5 1 778.66 774.49 18.18 o
10 5 1 220.94 241.79 18.47 o
11 5 1 163.08 139.44 8.95 o
12 5 1 21.45 29.06 5.04 o
-13 6 1 7.38 5.06 3.67 o
-12 6 1 15.00 14.50 4.07 o
-11 6 1 315.12 350.16 13.54 o
-10 6 1 325.02 314.70 18.79 o
-9 6 1 31.33 27.23 2.73 o
-8 6 1 933.57 925.76 18.06 o
-7 6 1 4734.01 4948.54 37.66 o
-6 6 1 331.39 290.53 6.13 o
-5 6 1 1758.88 1779.63 13.64 o
-4 6 1 316.48 329.30 5.31 o
-3 6 1 5211.33 5331.65 39.24 o
-2 6 1 3.43 0.26 0.75 o
-1 6 1 9958.77 11410.12 57.39 o
0 6 1 195.08 163.40 3.09 o
1 6 1 405.26 277.27 7.27 o
2 6 1 368.43 426.59 5.13 o
3 6 1 1846.81 1728.46 12.60 o
4 6 1 775.49 812.90 7.97 o
5 6 1 375.72 346.91 4.78 o
6 6 1 1357.47 1347.78 11.84 o
7 6 1 810.38 816.49 9.98 o
8 6 1 1024.32 1053.97 21.20 o
9 6 1 286.31 289.59 11.21 o
10 6 1 246.49 229.17 20.87 o
11 6 1 35.97 40.84 9.55 o
12 6 1 56.71 54.02 9.24 o
-12 7 1 153.11 142.78 9.58 o
-11 7 1 183.21 163.44 9.39 o
-10 7 1 462.69 475.26 15.29 o
-9 7 1 120.55 111.13 4.74 o
-8 7 1 3432.27 3482.85 34.76 o
-7 7 1 360.05 349.07 10.41 o
-6 7 1 205.25 196.88 5.37 o
-5 7 1 14.52 13.92 1.91 o
-4 7 1 343.36 327.91 5.61 o
-3 7 1 1048.85 1150.01 11.19 o
-2 7 1 15964.60 16468.98 90.00 o
-1 7 1 6.82 13.33 1.16 o
0 7 1 1145.63 1169.08 9.53 o
1 7 1 74.28 77.02 2.47 o
2 7 1 835.30 718.31 7.31 o
3 7 1 204.62 205.22 4.42 o
4 7 1 1963.75 2016.28 18.49 o
5 7 1 136.20 124.18 3.13 o
6 7 1 4159.89 4338.66 27.50 o
7 7 1 705.43 733.94 11.07 o
8 7 1 52.98 54.10 7.15 o
9 7 1 3.39 5.69 2.95 o
10 7 1 715.09 756.86 19.76 o
11 7 1 51.02 49.30 6.17 o
-11 8 1 1280.53 1346.95 40.61 o
-10 8 1 263.85 239.81 11.04 o
-9 8 1 323.10 296.48 10.13 o
-8 8 1 0.75 3.53 1.54 o
-7 8 1 1177.35 1179.75 13.62 o
-6 8 1 74.64 76.66 3.52 o
-5 8 1 84.00 73.56 3.30 o
-4 8 1 70.49 60.10 2.85 o
-3 8 1 2109.54 2100.06 17.39 o
-2 8 1 252.06 257.01 5.05 o
-1 8 1 2457.90 2375.02 18.50 o
0 8 1 443.32 515.11 7.05 o
1 8 1 5809.52 6052.10 37.86 o
2 8 1 426.06 450.68 6.82 o
3 8 1 405.39 405.52 6.61 o
4 8 1 55.73 54.76 3.11 o
5 8 1 601.68 632.78 8.90 o
6 8 1 2399.59 2439.36 20.95 o
7 8 1 727.78 730.76 10.19 o
8 8 1 3854.43 4080.12 51.93 o
9 8 1 352.04 329.06 12.61 o
10 8 1 386.02 376.47 14.00 o
11 8 1 1261.15 1244.22 39.72 o
-11 9 1 38.48 45.36 6.17 o
-10 9 1 1658.87 1689.71 32.16 o
-9 9 1 900.04 894.18 14.36 o
-8 9 1 361.89 347.79 8.44 o
-7 9 1 1322.10 1345.23 15.24 o
-6 9 1 2047.52 2133.10 19.88 o
-5 9 1 752.91 720.65 10.22 o
-4 9 1 0.93 2.89 2.48 o
-3 9 1 5.84 5.08 1.36 o
-2 9 1 1447.35 1424.02 17.70 o
-1 9 1 51.15 55.22 3.28 o
0 9 1 1270.53 1245.23 14.53 o
1 9 1 153.37 113.24 4.25 o
2 9 1 7822.31 8030.61 69.81 o
3 9 1 39.83 39.77 2.62 o
4 9 1 1074.74 1082.64 12.30 o
5 9 1 682.87 675.86 11.00 o
6 9 1 151.06 154.51 5.97 o
7 9 1 222.25 217.67 5.71 o
8 9 1 462.80 450.27 23.34 o
9 9 1 11.01 8.38 4.74 o
10 9 1 751.58 784.36 21.68 o
-10 10 1 24.88 29.33 4.99 o
-9 10 1 29.37 26.80 3.61 o
-8 10 1 1296.47 1338.61 18.23 o
-7 10 1 2900.27 2965.55 25.90 o
-6 10 1 71.49 63.78 3.64 o
-5 10 1 238.57 235.34 6.67 o
-4 10 1 573.62 542.84 12.02 o
-3 10 1 1353.33 1336.21 19.06 o
-2 10 1 939.23 884.60 13.60 o
-1 10 1 786.88 817.14 11.93 o
0 10 1 1082.11 1100.43 14.17 o
1 10 1 1691.43 1643.27 18.13 o
2 10 1 14.39 21.05 2.63 o
3 10 1 468.34 444.58 14.59 o
4 10 1 1.77 3.39 1.88 o
5 10 1 1732.71 1811.86 23.54 o
6 10 1 871.65 878.64 12.16 o
7 10 1 1823.58 1866.70 31.33 o
8 10 1 279.80 290.79 12.09 o
9 10 1 62.48 64.21 6.80 o
10 10 1 395.97 394.20 21.25 o
-10 11 1 304.50 279.33 17.71 o
-9 11 1 77.99 84.70 10.50 o
-8 11 1 149.14 136.26 5.23 o
-7 11 1 237.46 223.33 6.33 o
-6 11 1 852.80 820.20 13.74 o
-5 11 1 39.18 39.32 4.10 o
-4 11 1 875.62 834.78 16.15 o
-3 11 1 4.83 6.00 2.10 o
-2 11 1 3590.23 3639.25 46.09 o
-1 11 1 320.50 331.24 7.77 o
0 11 1 59.98 56.80 3.74 o
1 11 1 1282.11 1104.76 14.93 o
2 11 1 9.16 10.74 2.16 o
3 11 1 503.96 451.82 10.95 o
4 11 1 246.55 237.33 8.03 o
5 11 1 60.14 54.30 4.60 o
6 11 1 2942.28 3177.43 36.05 o
7 11 1 481.55 491.71 14.90 o
8 11 1 7.76 10.12 4.93 o
9 11 1 435.39 468.72 22.65 o
-8 12 1 0.41 0.52 2.09 o
-7 12 1 1536.90 1596.27 23.35 o
-6 12 1 347.93 372.30 9.47 o
-5 12 1 560.41 579.75 13.53 o
-4 12 1 17.07 12.06 2.81 o
-3 12 1 770.87 771.25 15.31 o
-2 12 1 315.67 270.47 8.81 o
-1 12 1 112.35 98.00 5.82 o
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1 2 11 17.70 34.87 12.31 o
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1 1 13 248.62 233.38 7.29 o
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1 2 13 579.17 572.41 11.55 o
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1 3 13 87.68 79.07 4.84 o
2 3 13 801.76 768.23 14.02 o
3 3 13 8.57 9.62 2.37 o
4 3 13 269.68 249.06 11.58 o
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0 1 14 142.59 127.82 5.80 o
1 1 14 559.49 533.22 11.61 o
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1 2 14 66.34 65.28 5.30 o
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1 3 14 2493.91 2509.16 28.18 o
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1 1 15 68.63 66.56 4.94 o
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1 3 15 3.16 2.82 2.78 o
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