#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/89/2018958.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018958_Fobs loop_ _publ_author_name 'Liu, Jian-Jun' 'Liao, Jian-Zhen' 'Li, Zuo-Yin' 'Wang, Yao' 'Huang, Chang-Cang' _publ_section_title ; Di-\m~2~-chlorido-dichloridobis(dimethylformamide)tetrakis[\m~3~-1-(2-oxidobenzoyl)-2-(2-oxo-2-phenylethanethioyl)hydrazine-1,2-diido]octacopper(II) dimethylformamide disolvate ; _journal_coeditor_code FN3135 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 613 _journal_page_last 615 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.526 _cell_angle_gamma 90.000 _cell_length_a 9.5672 _cell_length_b 19.1526 _cell_length_c 23.0064 _exptl_crystal_F_000 2208.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file fn3135Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 665.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 61849.11 61267.85 663.86 o 2 0 0 3607.60 3612.30 219.96 o 3 0 0 39915.24 38480.92 517.24 o 4 0 0 6963.36 6967.71 307.76 o 5 0 0 8648.62 8324.60 272.04 o 6 0 0 1115.10 863.64 187.49 o 7 0 0 8380.03 8713.99 1460.08 o 8 0 0 74.60 342.58 280.68 o 9 0 0 1299.10 984.83 531.12 o 10 0 0 251.94 39.38 353.39 o 11 0 0 43.43 -27.52 481.89 o 1 1 0 11389.08 11515.90 239.74 o 2 1 0 56092.72 55366.86 458.98 o 3 1 0 44847.08 44764.70 412.56 o 4 1 0 12976.86 12539.71 265.74 o 5 1 0 1463.06 1168.63 116.25 o 6 1 0 1182.77 1618.91 342.17 o 7 1 0 7222.47 7638.84 314.39 o 8 1 0 1069.95 895.21 192.35 o 9 1 0 405.73 27.68 223.69 o 10 1 0 22.24 -11.31 272.12 o 11 1 0 2.68 -186.89 329.06 o 0 2 0 50614.08 53452.29 587.38 o 1 2 0 36485.34 37450.49 276.07 o 2 2 0 38289.23 37581.95 336.84 o 3 2 0 8308.58 8327.19 324.01 o 4 2 0 22127.73 22046.43 264.11 o 5 2 0 422.05 544.76 102.61 o 6 2 0 2109.24 2104.03 132.32 o 7 2 0 1656.62 1890.33 171.64 o 8 2 0 315.43 443.38 192.09 o 9 2 0 647.79 583.37 233.74 o 10 2 0 141.32 -16.26 278.42 o 11 2 0 203.40 242.32 332.30 o 1 3 0 9622.14 9324.04 105.24 o 2 3 0 2054.53 2503.20 181.90 o 3 3 0 8140.75 8244.51 137.02 o 4 3 0 12.73 -35.56 76.25 o 5 3 0 712.26 720.40 109.84 o 6 3 0 56.44 -2.64 111.67 o 7 3 0 268.85 279.91 138.78 o 8 3 0 598.48 671.10 234.81 o 9 3 0 1.91 57.69 227.65 o 10 3 0 0.43 113.49 289.64 o 11 3 0 80.47 59.98 354.03 o 0 4 0 1863.88 1859.42 135.25 o 1 4 0 7615.38 7971.47 121.21 o 2 4 0 1517.99 1594.49 67.54 o 3 4 0 14099.89 14422.20 248.68 o 4 4 0 576.93 577.31 101.17 o 5 4 0 381.96 274.58 101.34 o 6 4 0 1428.27 1636.30 200.83 o 7 4 0 175.97 82.88 135.54 o 8 4 0 251.39 299.61 217.28 o 9 4 0 1464.61 1549.71 324.30 o 10 4 0 1.60 131.36 279.34 o 1 5 0 7635.75 6778.90 188.17 o 2 5 0 97.68 132.91 47.67 o 3 5 0 314.28 290.48 72.22 o 4 5 0 3146.66 3261.58 117.87 o 5 5 0 3127.01 2859.31 132.46 o 6 5 0 1851.70 1883.00 189.80 o 7 5 0 337.55 174.18 144.82 o 8 5 0 5930.25 5865.41 367.97 o 9 5 0 362.06 47.36 228.99 o 10 5 0 182.87 182.31 355.15 o 0 6 0 2726.27 2555.58 185.01 o 1 6 0 8584.11 8227.12 163.57 o 2 6 0 430.66 457.48 97.21 o 3 6 0 942.94 774.81 144.34 o 4 6 0 7942.38 7950.44 160.32 o 5 6 0 618.33 508.53 112.09 o 6 6 0 7.52 -135.47 121.04 o 7 6 0 930.10 811.49 158.50 o 8 6 0 1870.84 2057.42 224.63 o 9 6 0 690.42 687.41 295.29 o 10 6 0 380.44 741.51 332.99 o 1 7 0 1514.38 1327.65 77.96 o 2 7 0 13382.83 13158.53 371.64 o 3 7 0 10262.48 9754.44 196.46 o 4 7 0 3425.37 3891.97 182.50 o 5 7 0 1057.59 1029.68 120.76 o 6 7 0 3994.65 3937.81 171.55 o 7 7 0 78.02 208.88 178.64 o 8 7 0 21.80 87.80 201.29 o 9 7 0 852.60 520.51 293.05 o 10 7 0 905.66 840.89 352.19 o 0 8 0 1448.51 1738.94 101.92 o 1 8 0 35.46 78.80 68.75 o 2 8 0 1972.03 2153.34 101.47 o 3 8 0 1936.27 1943.84 137.77 o 4 8 0 5563.70 5366.28 227.78 o 5 8 0 907.45 877.09 124.23 o 6 8 0 4898.01 5784.88 454.32 o 7 8 0 2385.87 2329.88 233.69 o 8 8 0 111.88 182.51 214.56 o 9 8 0 21.88 34.20 292.76 o 10 8 0 254.81 255.19 331.00 o 1 9 0 10131.92 9823.04 164.29 o 2 9 0 782.25 724.89 96.47 o 3 9 0 1990.48 2006.14 138.18 o 4 9 0 10.35 -12.07 121.45 o 5 9 0 19.46 90.86 144.65 o 6 9 0 1188.25 1507.69 315.71 o 7 9 0 14.45 -237.42 190.13 o 8 9 0 101.17 -78.36 214.37 o 9 9 0 120.54 -199.77 290.70 o 10 9 0 2.90 -117.78 345.35 o 0 10 0 234.85 41.84 224.28 o 1 10 0 1962.60 1926.96 109.23 o 2 10 0 747.62 528.81 98.55 o 3 10 0 19705.79 18837.47 588.44 o 4 10 0 14.49 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262.16 o 9 13 0 95.32 -33.37 356.45 o 0 14 0 1559.17 1489.10 226.39 o 1 14 0 4850.96 5086.36 214.18 o 2 14 0 4601.16 4680.11 182.50 o 3 14 0 830.43 657.44 149.78 o 4 14 0 31.01 30.36 155.02 o 5 14 0 1507.25 1117.11 208.84 o 6 14 0 4269.74 3982.32 594.51 o 7 14 0 374.33 523.09 269.61 o 8 14 0 0.08 70.63 281.94 o 1 15 0 333.37 394.75 163.01 o 2 15 0 6227.86 6557.20 247.45 o 3 15 0 4322.76 4582.84 204.20 o 4 15 0 1007.00 1534.52 187.19 o 5 15 0 31.87 131.88 213.61 o 6 15 0 32.94 -34.60 228.90 o 7 15 0 1677.39 1661.46 282.93 o 8 15 0 1.29 38.82 292.04 o 0 16 0 616.78 950.81 268.88 o 1 16 0 79.61 -2.93 175.56 o 2 16 0 1895.31 1760.10 201.61 o 3 16 0 88.29 -29.64 185.96 o 4 16 0 493.32 333.52 184.82 o 5 16 0 619.54 529.06 234.94 o 6 16 0 972.44 982.89 262.52 o 7 16 0 66.05 150.36 279.98 o 1 17 0 1210.48 892.76 261.73 o 2 17 0 57.84 -166.52 185.29 o 3 17 0 8.04 169.97 212.27 o 4 17 0 5.55 42.46 215.79 o 5 17 0 1461.98 1813.52 370.07 o 6 17 0 1407.60 1576.67 285.53 o 7 17 0 575.34 580.94 305.80 o 0 18 0 526.19 280.67 301.70 o 1 18 0 49.18 38.55 206.45 o 2 18 0 473.46 255.77 220.73 o 3 18 0 375.63 27.69 227.08 o 4 18 0 11.19 -198.94 268.59 o 5 18 0 114.93 -43.10 290.00 o 6 18 0 461.69 437.61 328.12 o 1 19 0 1212.89 1445.56 243.60 o 2 19 0 307.57 477.71 241.49 o 3 19 0 25.97 24.36 245.30 o 4 19 0 617.26 900.77 317.72 o 5 19 0 460.26 521.92 326.08 o 6 19 0 891.30 897.90 361.56 o 0 20 0 341.45 332.00 362.18 o 1 20 0 3.78 -191.01 231.53 o 2 20 0 337.31 -86.33 245.87 o 3 20 0 33.98 28.02 264.99 o 4 20 0 58.99 42.35 331.80 o 5 20 0 5.44 -91.50 340.94 o 1 21 0 329.76 361.66 268.09 o 2 21 0 1305.08 1371.76 281.29 o 3 21 0 1.04 86.63 285.63 o 4 21 0 1300.88 1071.99 373.94 o 0 22 0 15.12 -112.75 418.01 o 1 22 0 3.86 112.36 295.16 o 2 22 0 417.57 351.00 303.65 o -11 1 1 13.72 -76.24 331.87 o -10 1 1 200.81 55.90 259.79 o -9 1 1 261.46 248.28 219.84 o -8 1 1 2516.53 2860.91 250.44 o -7 1 1 1335.13 1065.98 174.51 o -6 1 1 7033.55 6547.29 427.13 o -5 1 1 2779.22 2815.40 135.42 o -4 1 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