#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:23:21 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180858 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/89/2018972.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2018972_Fobs loop_ _publ_author_name 'Wang, Bi-Qin' 'Yan, Hai-Biao' 'Huang, Zheng-Qing' 'Zhang, Zhi' _publ_section_title ; Reversible high-temperature phase transition of a manganese(II) formate framework with imidazolium cations ; _journal_coeditor_code LG3108 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 616 _journal_page_last 619 _journal_volume 69 _journal_year 2013 _space_group_IT_number 113 _symmetry_space_group_name_Hall 'P -4 2ab' _symmetry_space_group_name_H-M 'P -4 21 m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.8324 _cell_length_b 8.8324 _cell_length_c 6.4406 _exptl_crystal_F_000 262.00 _reflns_d_resolution_high 0.7736 _cod_data_source_file lg3108I_HTsup3.hkl _cod_data_source_block I_HT #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P-42(1)m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 91.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'y, -x, -z' '-y, x, -z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' '-y+1/2, -x+1/2, z' 'y+1/2, x+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 1922.17 1908.24 45.83 o 0 2 0 4975.91 4653.49 161.28 o 1 2 0 397.12 402.22 7.63 o 2 2 0 5654.01 5706.28 167.74 o 1 3 0 1817.03 1739.22 70.55 o 2 3 0 628.53 575.31 9.71 o 3 3 0 2564.08 2951.21 74.86 o 0 4 0 3031.22 3005.69 102.55 o 1 4 0 89.49 93.19 2.80 o 2 4 0 1952.18 1883.57 49.15 o 3 4 0 20.70 22.83 1.27 o 4 4 0 205.35 218.71 7.32 o 1 5 0 1497.68 1402.15 29.78 o 2 5 0 88.45 85.74 2.36 o 3 5 0 1240.15 1187.03 24.49 o 4 5 0 1.53 0.47 0.71 o 5 5 0 114.03 116.21 5.54 o 0 6 0 119.64 125.30 15.98 o 1 6 0 23.71 23.25 2.40 o 2 6 0 779.51 769.53 14.14 o 3 6 0 24.30 23.48 1.51 o 4 6 0 148.62 138.88 4.36 o 5 6 0 0.28 2.32 1.15 o 6 6 0 270.44 284.89 10.83 o 1 7 0 197.78 198.68 6.62 o 2 7 0 0.02 0.30 0.89 o 3 7 0 268.82 271.39 6.06 o 4 7 0 16.13 14.63 1.61 o 5 7 0 332.56 353.76 9.57 o 6 7 0 2.94 2.25 1.52 o 7 7 0 63.80 58.41 5.37 o 0 8 0 337.92 367.50 18.70 o 1 8 0 9.25 10.79 1.81 o 2 8 0 177.29 157.50 6.42 o 3 8 0 72.73 72.83 3.40 o 4 8 0 146.57 137.94 3.92 o 5 8 0 11.61 14.90 1.72 o 6 8 0 44.50 44.91 3.12 o 7 8 0 0.02 0.39 1.15 o 8 8 0 21.65 16.73 7.97 o 1 9 0 160.47 148.99 10.45 o 2 9 0 0.44 0.68 2.48 o 3 9 0 61.92 63.05 6.95 o 4 9 0 0.60 -0.01 0.58 o 5 9 0 30.69 19.58 5.97 o 6 9 0 0.71 0.38 1.96 o 7 9 0 34.52 30.38 5.12 o 0 10 0 108.06 121.55 13.09 o 1 10 0 0.47 1.14 2.48 o 2 10 0 36.86 35.66 6.44 o 3 10 0 7.36 9.63 4.05 o 4 10 0 57.86 58.98 6.54 o 5 10 0 0.37 0.57 2.96 o 1 11 0 31.06 29.12 6.98 o 2 11 0 0.55 0.18 2.39 o 3 11 0 28.13 26.73 9.23 o 0 0 1 3273.70 2723.99 121.51 o -1 1 1 2938.23 3312.82 109.14 o 0 1 1 13.74 17.56 1.02 o 1 1 1 2942.66 3270.61 95.76 o -2 2 1 333.66 339.74 15.01 o -1 2 1 491.04 497.15 17.46 o 0 2 1 842.86 966.13 18.49 o 1 2 1 491.06 498.41 14.81 o 2 2 1 331.67 314.47 23.90 o -3 3 1 482.00 525.49 26.35 o -2 3 1 454.54 425.35 7.15 o -1 3 1 386.96 355.72 6.41 o 0 3 1 50.60 82.51 2.16 o 1 3 1 385.49 339.73 7.17 o 2 3 1 454.50 425.45 12.27 o 3 3 1 481.90 508.59 40.37 o -4 4 1 283.71 305.25 12.78 o -3 4 1 17.08 16.77 1.65 o -2 4 1 1043.08 1023.47 18.81 o -1 4 1 85.09 115.31 5.26 o 0 4 1 921.94 807.04 15.39 o 1 4 1 85.11 105.22 6.88 o 2 4 1 1044.32 1035.77 28.78 o 3 4 1 17.07 20.79 1.99 o 4 4 1 283.61 301.43 17.88 o -5 5 1 9.55 11.79 2.12 o -4 5 1 1.28 2.75 0.85 o -3 5 1 382.39 340.52 6.41 o -2 5 1 69.92 69.95 1.91 o -1 5 1 550.97 541.28 9.94 o 0 5 1 3.18 2.74 0.88 o 1 5 1 550.86 535.25 11.75 o 2 5 1 69.93 68.70 2.81 o 3 5 1 384.05 318.42 8.47 o 4 5 1 1.28 1.25 1.16 o 5 5 1 7.81 6.10 1.96 o -6 6 1 298.59 334.56 16.68 o -5 6 1 1.07 1.08 0.89 o -4 6 1 186.66 185.01 4.31 o -3 6 1 29.07 29.38 1.41 o -2 6 1 597.82 609.00 11.82 o -1 6 1 28.43 33.59 1.99 o 0 6 1 36.88 59.07 5.99 o 1 6 1 28.43 29.89 1.70 o 2 6 1 595.95 593.80 14.43 o 3 6 1 29.06 24.74 1.72 o 4 6 1 187.66 171.16 5.03 o 5 6 1 1.07 1.20 1.10 o 6 6 1 298.73 294.20 15.45 o -7 7 1 47.92 56.02 3.93 o -6 7 1 4.16 4.30 1.27 o -5 7 1 245.47 263.27 7.51 o -4 7 1 12.28 14.45 1.38 o -3 7 1 198.36 187.69 5.43 o -2 7 1 0.95 1.18 0.58 o -1 7 1 164.33 171.92 6.50 o 0 7 1 1.07 0.58 0.96 o 1 7 1 165.56 157.19 6.72 o 2 7 1 0.95 1.87 0.80 o 3 7 1 197.88 183.23 7.49 o 4 7 1 12.28 12.05 2.02 o 5 7 1 245.04 254.79 8.94 o 6 7 1 4.16 4.50 1.66 o 7 7 1 47.70 53.31 5.60 o -8 8 1 32.60 35.41 3.77 o -7 8 1 0.35 0.23 0.82 o -6 8 1 48.47 54.85 3.28 o -5 8 1 8.00 9.47 1.56 o -4 8 1 119.72 138.55 5.39 o -3 8 1 60.40 67.59 2.49 o -2 8 1 111.53 114.94 5.37 o -1 8 1 14.59 16.21 3.15 o 0 8 1 217.97 207.34 7.46 o 1 8 1 14.58 15.08 2.94 o 2 8 1 111.27 103.33 6.73 o 3 8 1 60.40 61.07 5.09 o 4 8 1 119.47 123.03 8.11 o 5 8 1 8.00 9.49 1.66 o 6 8 1 49.12 48.11 4.57 o 7 8 1 0.35 0.24 1.41 o 8 8 1 32.18 40.16 9.37 o -6 9 1 0.38 1.15 1.65 o -5 9 1 35.12 38.30 3.65 o -4 9 1 0.36 0.78 1.36 o -3 9 1 76.42 81.42 5.60 o -2 9 1 0.09 0.08 1.31 o -1 9 1 176.36 182.73 11.71 o 0 9 1 0.04 -0.32 1.24 o 1 9 1 176.42 196.71 13.54 o 2 9 1 0.09 -0.55 1.62 o 3 9 1 77.21 83.72 5.91 o 4 9 1 0.36 0.05 1.08 o 5 9 1 34.85 29.32 4.33 o 6 9 1 0.38 0.79 1.48 o -5 10 1 0.86 0.07 1.59 o -4 10 1 47.43 55.41 5.19 o -3 10 1 9.64 8.52 2.67 o -2 10 1 33.84 35.70 5.54 o -1 10 1 0.13 0.23 2.11 o 0 10 1 101.37 113.38 9.61 o 1 10 1 0.13 0.44 2.15 o 2 10 1 33.47 33.60 5.14 o 3 10 1 9.64 9.26 4.40 o 4 10 1 47.31 61.83 8.92 o 5 10 1 0.86 0.57 2.06 o -2 11 1 0.08 -0.60 2.75 o -1 11 1 23.80 27.12 5.95 o 0 11 1 0.16 0.29 2.09 o 1 11 1 24.23 30.56 5.67 o 2 11 1 0.08 -0.23 3.13 o 0 0 2 8407.25 8290.89 454.37 o -1 1 2 1454.39 1073.16 52.08 o 0 1 2 12.95 19.82 1.79 o 1 1 2 1459.62 1095.17 67.41 o -2 2 2 814.33 755.80 24.01 o -1 2 2 211.40 247.65 13.10 o 0 2 2 113.42 155.24 3.87 o 1 2 2 211.36 256.71 15.52 o 2 2 2 813.96 757.07 21.00 o -3 3 2 959.59 959.03 27.78 o -2 3 2 300.31 303.95 12.38 o -1 3 2 651.25 590.21 14.40 o 0 3 2 11.04 10.78 1.28 o 1 3 2 647.38 634.54 20.35 o 2 3 2 300.36 295.21 12.96 o 3 3 2 956.95 1014.21 32.24 o -4 4 2 165.86 150.17 6.18 o -3 4 2 14.56 23.77 1.94 o -2 4 2 798.00 688.95 14.20 o -1 4 2 58.61 52.95 4.09 o 0 4 2 894.88 775.69 16.40 o 1 4 2 58.58 66.12 6.12 o 2 4 2 803.13 714.48 16.05 o 3 4 2 14.56 15.69 2.14 o 4 4 2 166.82 162.55 6.13 o -5 5 2 62.65 66.88 6.34 o -4 5 2 1.94 1.83 0.76 o -3 5 2 550.06 550.89 13.39 o -2 5 2 44.25 54.44 2.65 o -1 5 2 702.52 674.15 13.26 o 0 5 2 28.85 31.12 1.75 o 1 5 2 699.73 729.29 27.44 o 2 5 2 44.25 48.63 3.33 o 3 5 2 551.02 595.08 15.39 o 4 5 2 1.94 0.92 1.11 o 5 5 2 62.17 81.58 5.77 o -6 6 2 237.54 248.10 8.03 o -5 6 2 2.26 2.11 1.01 o -4 6 2 146.61 131.20 4.46 o -3 6 2 12.29 16.56 1.33 o -2 6 2 498.18 495.24 9.26 o -1 6 2 17.77 18.31 1.41 o 0 6 2 78.05 80.33 3.06 o 1 6 2 17.76 15.78 1.42 o 2 6 2 498.46 507.73 12.13 o 3 6 2 12.29 11.75 1.66 o 4 6 2 147.42 167.23 7.83 o 5 6 2 2.25 1.81 1.50 o 6 6 2 235.22 262.90 11.71 o -7 7 2 44.50 44.65 3.50 o -6 7 2 1.64 1.50 0.92 o -5 7 2 211.36 208.27 5.33 o -4 7 2 6.73 8.66 1.28 o -3 7 2 186.28 173.94 4.25 o -2 7 2 0.59 0.51 0.59 o -1 7 2 142.97 156.03 5.72 o 0 7 2 0.72 1.72 1.20 o 1 7 2 143.00 135.30 5.16 o 2 7 2 0.59 1.68 0.84 o 3 7 2 184.95 186.98 6.42 o 4 7 2 6.73 5.97 1.69 o 5 7 2 212.97 215.49 8.05 o 6 7 2 1.65 1.34 1.31 o 7 7 2 45.53 44.53 4.64 o -7 8 2 0.35 0.04 0.90 o -6 8 2 51.95 43.08 2.65 o -5 8 2 10.78 10.82 1.44 o -4 8 2 123.95 113.84 3.86 o -3 8 2 39.85 40.96 2.19 o -2 8 2 136.38 147.87 5.41 o -1 8 2 10.71 11.23 1.79 o 0 8 2 249.66 238.44 12.08 o 1 8 2 10.71 7.37 1.42 o 2 8 2 137.84 141.16 5.56 o 3 8 2 39.85 48.67 3.00 o 4 8 2 123.23 122.05 5.09 o 5 8 2 10.78 6.38 1.77 o 6 8 2 52.02 46.26 3.86 o 7 8 2 0.35 0.46 1.07 o -6 9 2 0.44 0.27 1.04 o -5 9 2 27.19 27.64 3.16 o -4 9 2 0.01 0.36 1.17 o -3 9 2 58.04 59.71 3.98 o -2 9 2 0.35 1.26 1.58 o -1 9 2 130.81 127.20 6.57 o 0 9 2 0.27 0.59 1.50 o 1 9 2 129.84 132.70 6.55 o 2 9 2 0.35 0.73 0.83 o 3 9 2 58.49 50.73 5.28 o 4 9 2 0.01 0.00 0.90 o 5 9 2 27.29 18.97 5.17 o 6 9 2 0.44 0.10 1.09 o -4 10 2 47.60 51.71 5.55 o -3 10 2 8.16 5.86 3.06 o -2 10 2 36.30 35.00 4.10 o -1 10 2 0.20 -0.24 1.30 o 0 10 2 86.10 86.59 5.00 o 1 10 2 0.19 0.02 0.99 o 2 10 2 36.79 36.61 5.47 o 3 10 2 8.16 6.35 3.62 o 4 10 2 47.64 42.08 9.28 o -1 11 2 27.62 33.21 7.69 o 0 11 2 0.32 -0.23 2.29 o 1 11 2 27.84 35.29 8.46 o 0 0 3 6868.21 6517.15 349.91 o -1 1 3 1374.93 1268.39 41.32 o 0 1 3 7.51 7.27 1.32 o 1 1 3 1378.64 1280.43 41.29 o -2 2 3 1422.33 1383.11 46.90 o -1 2 3 98.65 81.38 4.77 o 0 2 3 1067.56 1065.20 24.38 o 1 2 3 98.68 81.70 4.01 o 2 2 3 1417.59 1387.85 40.61 o -3 3 3 742.78 708.52 57.42 o -2 3 3 80.00 101.76 5.73 o -1 3 3 671.43 621.81 20.35 o 0 3 3 42.78 42.24 2.18 o 1 3 3 670.03 618.70 21.79 o 2 3 3 79.99 97.23 3.56 o 3 3 3 744.37 547.20 63.34 o -4 4 3 251.23 291.77 23.90 o -3 4 3 7.44 10.52 2.02 o -2 4 3 910.11 940.88 36.32 o -1 4 3 32.65 37.66 6.58 o 0 4 3 1100.99 1108.65 26.41 o 1 4 3 32.67 30.70 7.02 o 2 4 3 908.89 909.66 33.89 o 3 4 3 7.44 7.13 1.73 o 4 4 3 248.35 214.03 32.47 o -5 5 3 89.54 109.14 7.04 o -4 5 3 1.71 1.65 1.21 o -3 5 3 386.96 418.24 18.39 o -2 5 3 25.70 29.64 2.14 o -1 5 3 528.90 491.58 12.75 o 0 5 3 1.90 1.85 1.09 o 1 5 3 528.33 481.32 11.15 o 2 5 3 25.71 26.66 2.21 o 3 5 3 389.48 336.04 22.94 o 4 5 3 1.71 5.04 1.34 o 5 5 3 87.30 80.36 9.93 o -6 6 3 133.10 184.82 12.74 o -5 6 3 1.90 0.48 0.88 o -4 6 3 116.07 132.93 4.80 o -3 6 3 10.12 6.48 1.55 o -2 6 3 390.86 390.33 11.51 o -1 6 3 5.18 2.59 0.82 o 0 6 3 121.09 108.30 4.02 o 1 6 3 5.18 4.80 1.33 o 2 6 3 388.27 367.06 14.14 o 3 6 3 10.12 7.23 1.93 o 4 6 3 116.68 113.01 10.10 o 5 6 3 1.91 0.36 1.23 o 6 6 3 133.08 138.22 21.64 o -7 7 3 49.47 61.60 4.35 o -6 7 3 0.87 1.07 1.07 o -5 7 3 162.96 187.83 9.37 o -4 7 3 4.41 6.58 1.38 o -3 7 3 160.34 178.94 7.60 o -2 7 3 2.15 1.39 1.12 o -1 7 3 137.58 160.67 10.48 o 0 7 3 0.03 0.59 0.89 o 1 7 3 138.60 138.90 8.58 o 2 7 3 2.15 2.60 1.31 o 3 7 3 159.20 157.05 8.84 o 4 7 3 4.41 3.34 1.82 o 5 7 3 162.20 156.77 13.70 o 6 7 3 0.87 0.83 1.75 o 7 7 3 48.51 45.99 8.84 o -7 8 3 0.70 0.07 0.91 o -6 8 3 35.82 37.72 2.56 o -5 8 3 4.27 3.05 1.24 o -4 8 3 77.62 85.40 4.75 o -3 8 3 25.75 24.48 2.00 o -2 8 3 86.28 95.32 3.97 o -1 8 3 3.33 1.93 1.06 o 0 8 3 160.52 147.61 6.38 o 1 8 3 3.33 6.54 1.73 o 2 8 3 86.36 72.58 4.55 o 3 8 3 25.74 18.71 2.44 o 4 8 3 77.31 68.52 8.33 o 5 8 3 4.27 2.57 1.76 o 6 8 3 37.25 21.12 4.53 o 7 8 3 0.70 1.03 2.55 o -5 9 3 28.77 28.79 5.22 o -4 9 3 1.03 0.23 1.05 o -3 9 3 51.27 58.43 3.92 o -2 9 3 0.66 0.82 1.52 o -1 9 3 99.39 97.50 6.43 o 0 9 3 0.59 0.25 1.15 o 1 9 3 99.23 87.84 6.05 o 2 9 3 0.66 1.61 1.32 o 3 9 3 52.16 45.75 4.47 o 4 9 3 1.03 0.10 1.09 o 5 9 3 28.04 14.84 4.28 o -3 10 3 2.86 2.64 2.64 o -2 10 3 29.14 29.49 5.02 o -1 10 3 0.72 0.04 1.60 o 0 10 3 55.32 56.51 5.05 o 1 10 3 0.72 0.45 1.80 o 2 10 3 28.67 29.18 4.36 o 3 10 3 2.86 3.70 3.51 o 0 0 4 885.84 810.32 40.55 o -1 1 4 812.44 766.48 70.49 o 0 1 4 1.10 1.12 1.64 o 1 1 4 815.43 783.94 37.41 o -2 2 4 277.59 244.74 10.64 o -1 2 4 15.59 26.11 2.44 o 0 2 4 121.50 108.26 4.07 o 1 2 4 15.59 23.93 2.26 o 2 2 4 275.56 248.77 10.67 o -3 3 4 371.95 330.61 11.47 o -2 3 4 37.51 51.48 5.12 o -1 3 4 371.59 408.17 10.46 o 0 3 4 3.19 1.78 1.33 o 1 3 4 371.26 418.56 10.62 o 2 3 4 37.52 43.28 4.52 o 3 3 4 372.17 343.55 12.73 o -4 4 4 162.24 158.70 8.02 o -3 4 4 3.14 6.79 2.20 o -2 4 4 339.38 326.45 9.58 o -1 4 4 6.06 9.92 2.09 o 0 4 4 337.25 346.24 9.38 o 1 4 4 6.06 7.56 1.91 o 2 4 4 340.53 331.30 8.82 o 3 4 4 3.14 9.04 2.07 o 4 4 4 162.63 164.00 7.81 o -5 5 4 53.62 50.67 4.53 o -4 5 4 4.04 3.53 1.54 o -3 5 4 193.37 190.35 6.87 o -2 5 4 8.04 7.67 1.87 o -1 5 4 287.74 268.29 10.35 o 0 5 4 0.30 6.80 1.88 o 1 5 4 287.25 292.37 8.68 o 2 5 4 8.05 5.77 1.73 o 3 5 4 194.58 203.24 6.52 o 4 5 4 4.04 1.53 1.53 o 5 5 4 52.91 65.31 5.82 o -6 6 4 118.24 133.62 7.29 o -5 6 4 2.53 1.30 1.30 o -4 6 4 107.21 105.15 3.98 o -3 6 4 4.31 5.87 1.68 o -2 6 4 221.23 236.28 7.22 o -1 6 4 4.05 1.80 1.64 o 0 6 4 82.84 86.43 4.33 o 1 6 4 4.05 1.19 1.46 o 2 6 4 220.65 236.90 7.98 o 3 6 4 4.31 3.44 1.64 o 4 6 4 107.80 116.89 5.15 o 5 6 4 2.53 0.84 1.33 o 6 6 4 116.80 134.68 9.77 o -7 7 4 29.20 33.40 5.15 o -6 7 4 0.47 0.54 1.22 o -5 7 4 85.59 79.89 3.64 o -4 7 4 2.65 1.76 1.12 o -3 7 4 100.96 82.47 3.59 o -2 7 4 2.02 1.59 0.99 o -1 7 4 96.41 103.75 5.25 o 0 7 4 1.60 0.45 1.00 o 1 7 4 96.73 95.54 4.21 o 2 7 4 2.02 2.52 1.64 o 3 7 4 100.23 105.83 5.11 o 4 7 4 2.64 0.68 1.59 o 5 7 4 86.53 71.31 4.16 o 6 7 4 0.48 0.50 1.30 o 7 7 4 29.90 20.96 8.07 o -6 8 4 34.02 26.41 2.88 o -5 8 4 2.73 2.28 1.70 o -4 8 4 64.64 58.70 3.38 o -3 8 4 7.46 5.13 1.68 o -2 8 4 69.16 78.28 4.82 o -1 8 4 3.41 2.44 1.54 o 0 8 4 115.29 112.27 6.50 o 1 8 4 3.41 2.25 1.58 o 2 8 4 69.89 75.10 4.22 o 3 8 4 7.46 8.71 2.20 o 4 8 4 64.07 56.37 4.73 o 5 8 4 2.73 1.24 1.66 o 6 8 4 34.08 33.08 6.08 o -4 9 4 0.15 0.26 1.54 o -3 9 4 39.61 39.55 4.92 o -2 9 4 0.30 -0.01 1.90 o -1 9 4 65.72 64.34 4.70 o 0 9 4 0.58 0.04 1.02 o 1 9 4 65.22 65.32 6.03 o 2 9 4 0.30 1.95 1.99 o 3 9 4 39.99 40.61 3.89 o 4 9 4 0.15 0.34 1.55 o 0 10 4 45.16 11.01 20.47 o 0 0 5 455.11 429.78 23.24 o -1 1 5 104.85 102.44 13.55 o 0 1 5 2.84 0.54 1.30 o 1 1 5 105.34 101.74 9.41 o -2 2 5 156.28 140.85 8.41 o -1 2 5 5.46 6.26 1.88 o 0 2 5 130.44 122.66 5.46 o 1 2 5 5.46 7.99 2.25 o 2 2 5 157.07 136.01 7.54 o -3 3 5 158.27 146.39 9.50 o -2 3 5 8.69 12.54 2.26 o -1 3 5 108.96 121.70 5.18 o 0 3 5 0.27 1.51 1.27 o 1 3 5 107.90 124.46 5.03 o 2 3 5 8.69 9.79 1.98 o 3 3 5 157.73 139.49 14.16 o -4 4 5 73.25 74.70 6.58 o -3 4 5 2.28 3.98 1.83 o -2 4 5 145.71 127.78 4.97 o -1 4 5 3.20 3.68 1.73 o 0 4 5 150.12 168.71 6.39 o 1 4 5 3.20 3.57 1.78 o 2 4 5 147.24 124.98 4.80 o 3 4 5 2.28 3.02 1.88 o 4 4 5 73.83 65.46 5.81 o -5 5 5 58.01 65.88 5.45 o -4 5 5 2.73 2.05 1.90 o -3 5 5 113.73 127.45 5.58 o -2 5 5 4.04 5.02 1.98 o -1 5 5 143.35 136.26 5.91 o 0 5 5 2.70 1.76 1.72 o 1 5 5 142.85 145.77 5.05 o 2 5 5 4.04 3.57 1.70 o 3 5 5 114.49 116.29 5.65 o 4 5 5 2.73 2.78 1.69 o 5 5 5 57.82 65.86 6.05 o -6 6 5 52.45 71.84 8.07 o -5 6 5 0.45 0.06 0.82 o -4 6 5 51.18 55.23 3.63 o -3 6 5 1.07 0.48 1.33 o -2 6 5 102.17 110.15 5.84 o -1 6 5 1.49 0.22 1.46 o 0 6 5 51.20 48.13 3.80 o 1 6 5 1.49 0.68 1.14 o 2 6 5 102.05 112.19 5.32 o 3 6 5 1.07 0.25 1.14 o 4 6 5 51.58 47.91 3.63 o 5 6 5 0.45 -0.01 0.83 o 6 6 5 52.01 44.33 5.76 o -5 7 5 56.67 58.16 4.43 o -4 7 5 0.42 0.70 1.38 o -3 7 5 68.11 67.88 3.92 o -2 7 5 0.13 1.12 1.54 o -1 7 5 66.02 74.63 5.33 o 0 7 5 0.43 0.30 1.21 o 1 7 5 66.24 66.57 4.73 o 2 7 5 0.13 1.47 1.71 o 3 7 5 67.93 63.69 4.69 o 4 7 5 0.42 0.27 1.38 o 5 7 5 57.13 43.22 5.35 o -4 8 5 39.04 35.52 4.36 o -3 8 5 3.22 1.99 1.90 o -2 8 5 40.96 51.56 6.14 o -1 8 5 1.33 0.87 1.52 o 0 8 5 61.45 68.41 4.43 o 1 8 5 1.33 1.73 1.71 o 2 8 5 41.25 44.50 4.22 o 3 8 5 3.22 1.51 2.14 o 4 8 5 38.74 26.31 5.82 o -1 9 5 45.00 35.56 6.50 o 0 9 5 0.01 0.06 1.37 o 1 9 5 44.93 35.57 5.60 o 0 0 6 537.83 542.38 29.38 o -1 1 6 440.68 398.53 28.02 o 0 1 6 2.80 0.87 1.73 o 1 1 6 441.06 398.64 19.49 o -2 2 6 304.22 320.22 15.85 o -1 2 6 3.13 2.09 2.28 o 0 2 6 329.89 361.64 12.10 o 1 2 6 3.13 2.17 2.46 o 2 2 6 303.05 324.20 15.02 o -3 3 6 188.37 166.88 11.69 o -2 3 6 1.69 3.31 2.13 o -1 3 6 248.99 250.62 9.33 o 0 3 6 2.12 2.20 1.91 o 1 3 6 248.85 255.19 8.46 o 2 3 6 1.69 2.68 2.04 o 3 3 6 188.33 163.02 11.00 o -4 4 6 111.52 132.05 8.48 o -3 4 6 0.85 1.49 1.86 o -2 4 6 207.48 215.48 9.07 o -1 4 6 0.87 3.45 2.48 o 0 4 6 238.00 271.98 9.23 o 1 4 6 0.87 1.91 2.30 o 2 4 6 206.77 213.65 7.22 o 3 4 6 0.85 1.81 1.86 o 4 4 6 111.00 119.80 9.18 o -5 5 6 46.46 63.35 7.66 o -4 5 6 0.14 1.32 1.89 o -3 5 6 90.38 101.96 5.42 o -2 5 6 0.28 1.08 1.81 o -1 5 6 129.68 135.00 6.79 o 0 5 6 0.51 1.74 2.29 o 1 5 6 129.53 131.98 5.53 o 2 5 6 0.28 0.89 1.78 o 3 5 6 90.31 96.78 4.90 o 4 5 6 0.14 0.49 1.55 o 5 5 6 45.46 57.25 6.57 o -5 6 6 0.04 0.21 1.28 o -4 6 6 54.55 52.10 4.57 o -3 6 6 0.29 0.72 1.36 o -2 6 6 100.01 99.07 5.79 o -1 6 6 0.21 4.76 2.67 o 0 6 6 83.93 71.32 5.44 o 1 6 6 0.21 0.30 1.74 o 2 6 6 99.51 92.47 5.14 o 3 6 6 0.29 -0.16 1.52 o 4 6 6 54.70 45.32 5.05 o 5 6 6 0.04 0.07 1.36 o -3 7 6 46.24 45.17 4.51 o -2 7 6 0.37 0.53 1.92 o -1 7 6 48.86 58.32 4.62 o 0 7 6 0.59 -0.17 1.56 o 1 7 6 48.85 50.85 4.77 o 2 7 6 0.37 0.38 2.07 o 3 7 6 45.72 41.77 5.89 o 0 0 7 52.99 50.98 16.76 o -1 1 7 54.66 55.42 7.93 o 0 1 7 0.75 0.00 1.75 o 1 1 7 54.76 57.61 7.50 o -2 2 7 34.63 31.57 6.15 o -1 2 7 0.60 2.53 2.45 o 0 2 7 33.93 37.94 3.90 o 1 2 7 0.60 3.15 2.36 o 2 2 7 34.77 31.78 7.48 o -3 3 7 51.40 42.49 7.87 o -2 3 7 0.27 1.66 2.10 o -1 3 7 49.81 57.32 4.73 o 0 3 7 0.03 0.09 1.54 o 1 3 7 49.72 60.52 5.46 o 2 3 7 0.27 1.18 1.96 o 3 3 7 51.42 48.45 4.68 o -4 4 7 26.58 37.94 6.58 o -3 4 7 0.02 0.60 1.66 o -2 4 7 35.09 37.81 5.15 o -1 4 7 0.27 4.44 2.91 o 0 4 7 35.59 44.77 5.18 o 1 4 7 0.27 0.46 2.63 o 2 4 7 35.34 36.53 3.88 o 3 4 7 0.02 1.05 1.83 o 4 4 7 26.65 27.94 5.99 o -3 5 7 35.79 36.44 4.11 o -2 5 7 0.63 2.33 2.35 o -1 5 7 42.83 41.41 4.52 o 0 5 7 0.46 1.45 2.24 o 1 5 7 42.79 41.59 4.38 o 2 5 7 0.63 2.13 2.04 o 3 5 7 36.06 29.49 3.57 o -1 6 7 0.10 2.43 1.95 o 0 6 7 24.73 24.22 3.74 o 1 6 7 0.10 0.06 1.97 o -2 2 8 39.54 39.91 8.26 o -1 2 8 0.02 6.15 6.61 o 0 2 8 41.52 48.74 9.21 o 1 2 8 0.02 12.61 7.34 o 2 2 8 39.61 24.80 11.47 o -1 3 8 28.12 33.85 9.88 o 0 3 8 0.06 0.14 1.53 o 1 3 8 28.20 36.56 8.56 o